chemical science and technology laboratory overview process analytical technologies subcommittee...
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Chemical Science and Technology Chemical Science and Technology Laboratory OverviewLaboratory Overview
Process Analytical Technologies Process Analytical Technologies Subcommittee MeetingSubcommittee Meeting
June 12 – 13, 2002June 12 – 13, 2002Rockville, MDRockville, MD
Chemical Science and Technology Laboratory
James Whetstone, ChiefProcess Measurements Division
Chemical Science and Technology Laboratory
NIST Vision …NIST Vision … is to be the global leader in measurement and enabling technology, delivering outstanding value to the nation.
NIST Mission … NIST Mission … is to develop and promote measurement, standards, and technology to enhance productivity, facilitate trade, and improve the quality of life.
Core Values:Core Values:• People … we respect, value and support each other in all our activities.• Integrity … we are objective, ethical, and honest.• Customer focus …we anticipate the needs of our customers and are
committed to meeting or exceeding their expectations.• Excellence … we expect world-class performance and continuous
improvement in all we do.
NIST … enabling a better futureNIST … enabling a better future
Chemical Science and Technology Laboratory
Improving the Economy:Refrigerants Automobiles
…working with U.S. Industry
Electric Power
Information & SemiconductorTechnology Cell Phones
Improving the Quality of Life:
Medical Tests
Mammography
Cancer Treatment
Smoke Detectors
Body Armor
Dentistry
Chemical Science and Technology Laboratory
National Institute of Standards and TechnologyNational Institute of Standards and Technology
Electronics andElectrical
EngineeringLaboratory
Electronics andElectrical
EngineeringLaboratory
Wm. Anderson Wm. Anderson
Chemical Scienceand Technology
Laboratory
Chemical Scienceand Technology
Laboratory
Hratch SemerjianHratch Semerjian
Materials Scienceand Engineering
Laboratory
Materials Scienceand Engineering
Laboratory
Leslie SmithLeslie Smith
InformationTechnologyLaboratory
InformationTechnologyLaboratory
Susan Zevin (Act.)Susan Zevin (Act.)
ManufacturingEngineeringLaboratory
ManufacturingEngineeringLaboratory
Dale Hall Dale Hall
PhysicsLaboratory
PhysicsLaboratory
Katharine GebbieKatharine Gebbie
Building and FireResearch
Laboratory
Building and FireResearch
Laboratory
Jack SnellJack Snell
Boulder LaboratoriesBoulder Laboratories
VacantVacant
DirectorDirectorArden BementArden Bement
DirectorDirectorArden BementArden Bement
Deputy DirectorDeputy DirectorKaren BrownKaren Brown
Deputy DirectorDeputy DirectorKaren BrownKaren Brown
National QualityProgram
National QualityProgram
Harry HertzHarry Hertz
TechnologyServices
TechnologyServices
Richard KayserRichard Kayser
AdvancedTechnology
Program
AdvancedTechnology
Program
Marc Stanley (Act.)Marc Stanley (Act.)
ManufacturingExtension
Partnership
ManufacturingExtension
Partnership
Kevin CarrKevin Carr
Jorge UrrutiaJorge Urrutia
Director forAdministration
Chemical Science and Technology Laboratory
National Institute of Standards and TechnologyNational Institute of Standards and Technology
Electronics andElectrical
EngineeringLaboratory
Electronics andElectrical
EngineeringLaboratory
Wm. Anderson Wm. Anderson
Chemical Scienceand Technology
Laboratory
Chemical Scienceand Technology
Laboratory
Hratch SemerjianHratch Semerjian
Materials Scienceand Engineering
Laboratory
Materials Scienceand Engineering
Laboratory
Leslie SmithLeslie Smith
InformationTechnologyLaboratory
InformationTechnologyLaboratory
Susan Zevin (Act.)Susan Zevin (Act.)
ManufacturingEngineeringLaboratory
ManufacturingEngineeringLaboratory
Dale Hall Dale Hall
PhysicsLaboratory
PhysicsLaboratory
Katharine GebbieKatharine Gebbie
Building and FireResearch
Laboratory
Building and FireResearch
Laboratory
Jack SnellJack Snell
Boulder LaboratoriesBoulder Laboratories
VacantVacant
DirectorDirectorArden BementArden Bement
DirectorDirectorArden BementArden Bement
Deputy DirectorDeputy DirectorKaren BrownKaren Brown
Deputy DirectorDeputy DirectorKaren BrownKaren Brown
National QualityProgram
National QualityProgram
Harry HertzHarry Hertz
TechnologyServices
TechnologyServices
Richard KayserRichard Kayser
AdvancedTechnology
Program
AdvancedTechnology
Program
Marc Stanley (Act.)Marc Stanley (Act.)
ManufacturingExtension
Partnership
ManufacturingExtension
Partnership
Kevin CarrKevin Carr
Jorge UrrutiaJorge Urrutia
Director forAdministration
Chemical Science and Technology Laboratory
CSTL MissionCSTL MissionAs the Nation’s Reference Laboratory, CSTL’s Mission is to provide the chemical measurement infrastructure to:
• enhance U.S. industry's productivity and competitiveness;
• assure equity in trade; and
• improve public health, safety, and environmental quality.
CSTL VisionCSTL Vision
A world class research laboratory recognized by the Nation as the primary resource for chemical, biomolecular, and chemical engineering measurements, data, models, and reference standards required to enhance U.S. industrial competitiveness in the world market.
Chemical Science and Technology Laboratory
CSTL GoalsCSTL Goals
Measurement Standards Establish CSTL as the pinnacle of the national traceability and international comparability structure for measurements in chemistry, chemical engineering and biotechnology, and provide the fundamental basis of the nation’s measurement system
Chemical and Process InformationAssure that U.S. industry has access to accurate and reliable data and predictive models to determine the chemical and physical properties of materials and processes
Measurement ScienceAnticipate and address next generation measurement needs of the nation, by performing cutting-edge research
Chemical Science and Technology Laboratory
CHEMICAL SCIENCE AND TECHNOLOGY LABORATORY
CHEMICAL SCIENCE AND TECHNOLOGY LABORATORY
Hratch G. Semerjian, DirectorWilliam F. Koch, Deputy Director
• Atmospheric Chemistry
• Microanalysis Research
• Surface & Interface Research
• Analytical Microscopy
Surface & Microanalysis
ScienceR. Cavanagh, Chief
Surface & Microanalysis
ScienceR. Cavanagh, Chief
• Experimental Kinetics & Thermodynamics
• Chemical Reference Data & Modeling
• Computational Chemistry
• Experimental Properties of Fluids
• Theory & Modeling of Fluids
• Cryogenic Tech.
Physical & Chemical Properties
M. Haynes, Chief
Physical & Chemical Properties
M. Haynes, Chief
• Spectrochemical Methods
• Organic Analytical Methods
• Gas Metrology & Classical Methods
• Molecular Spectroscopy & Microfluidic Methods
• Nuclear Methods
Analytical Chemistry
W. May, Chief
Analytical Chemistry
W. May, Chief
• Fluid Flow• Fluid Science• Process Sensing• Thermometry• Pressure and Vacuum• Thermal and Reactive Processes
Process Measurements
J. Whetstone, Chief
Process Measurements
J. Whetstone, Chief
Biotechnology
V. Vilker, Act. Chief
Biotechnology
V. Vilker, Act. Chief
• DNA Technologies• Bioprocess Engineering
• Structural Biology• Biomolecular Materials
Organized by Discipline …
Chemical Science and Technology Laboratory
CSTL ProgramsCSTL ProgramsTransportation
Energy Systems
Biotechnology
Nanotechnology
Healthcare
Environmental Technologies
Microelectronics
Data and Informatics
Biomaterials
Forensics
International Measurement Standards
Chemical and Allied Products
Industrial and Analytical Instrument Services
Ener gy System s
Food and Nutrition
… Focused by Customer-Driven Programs
Chemical Science and Technology Laboratory
CSTL FacilitiesCSTL Facilities
CARBCARB
ACSLACSL
NIST BoulderNIST Boulder
NIST CharlestonNIST Charleston
Chemical Science and Technology Laboratory
CSTL Activities Impacting Process CSTL Activities Impacting Process Analytical & Process MeasurementsAnalytical & Process Measurements
• Standard Reference Materials Raman Spectroscopy – Intensity Standards Spectrophotometry – Optical Absorbance Standards
• Reference Data NIR Spectral Data Directly Tied to U.S. National Gas
Concentration Standards Mass Spectrometric Database and Spectral Diagnostic
Tools Protein Data Bank – Biomolecular Structures
• Instrument Calibration Services Temperature, Pressure, Vacuum, Humidity, Flowrate,
and Liquid Volume and Density
Chemical Science and Technology Laboratory
Intensity Standards for Raman SpectroscopyIntensity Standards for Raman Spectroscopy
Objective: : Provide (first-ever) standard for intensity and frequency shift of Raman signals
Customers: Instrument mfrs., chemical processing, DoD, DoE, pharmaceutical Industry
Form: Uranyl Silicate Glass standard cuvette geometry
Status:• Evaluated prototype standard
with ASTM Committee• First SRM (785 nm) by 9/2002
Next Steps: Develop additional SRMs (488, 514.5, 533, 633, 1064 nm)
nm
500 525 550 575 600 625Broadband fluorescence from uranyl silicate glass
Impacts: These standards will transform Raman from qualitative lab diagnostic into process instrumentation, allowing quantitative comparison of instrument response in differing locations and installations
Chemical Science and Technology Laboratory
NIST Mission … NIST Mission … is to develop and promote measurement, standards, and technology to enhance productivity, facilitate trade, and improve the quality of life.
– Assist Industry and Other Government Agencies to improve measurements, measurement standards, technologies, and practices.
IFPAC 2003 – January 2003
An opportunity to interact with Process Analytical Specialists in a Range of Industrial Applications