characterization report and delta western warehouse drainage … · 2017. 5. 24. ·...

Characterization Report and Soil Work Plan Addendum for

Delta Western Warehouse Drainage Improvements 1617 East Point Rd Unalaska, AK 99685

Section 3, T. 73S, R118 W SM Latitude 53°53'32", Longitude W 166°32'13"

Prepared for:

Delta Western Inc. PO Box 920688

Dutch Harbor, AK 99692

May 23, 2017

Prepared By

TZ Engineering Tyler Zimmerman, P.E.

Table of Contents LIST OF ACRONYMS ........................................................................................................................... 3

1.0 Introduction ................................................................................................................................. 4

2.0 Work Plan Field Screening Narrative ........................................................................................... 5

3.0 Field Screening Results ................................................................................................................ 6

4.0 Work Plan Addendum .................................................................................................................. 9

5.0 Conclusions & Recommendations ............................................................................................. 12

6.0 Limitations ................................................................................................................................. 13

LIST OF ACRONYMS

SDS Safety Data Sheet PCB Polychlorinated Biphenyl

revisions to draft work plan based on the ADEC review are noted with grey highlightingAAC Alaska Administrative CodeACLs alternative cleanu levelsADEC Alaska Department of Environmental Conservationbgs below ground surfaceBTEX benzene, toluene, ethylbenzene, and total xylenesCFR code of federal regulationsCoC chain of custody COC constituents of concernCOPC contaminants of potential concernCULs cleanup levelsDRO diesel range organicsFUDS formerly used defense sitesGRO gasoline range organicsGPS RTK global positionings system with real time kinematic satellite navigationLCS/LCSD lab control sample and lab control sample duplicateMLLW mean lower low water (tide level, considered 0.00 feet elevation in NGVD 29 elevation

system; approximately '-3.17 feet orthometric height in GEOID 99 based on GPS RTK survey of NOAA benchmark 2620 M 1982)

MS/MSD matrix spike and matrix spike duplicateNAD83 North America Datum 1983NGVD 29 national geodetic vertical datum 1929 No. numberNOAA national oceanic and atmospheric administration PAHs polynuclear aromatic hydrocarbonsPE professional engineerPID photo-ionization detectorPPE personal protective equipmentppmv parts per million by volumeQC quality controlRPMA Rocky Point Management AreaRRO residual range organicsSCM site conceptual modelUSACE United States Army Corps of EngineersUSGS United States Geological SurveyVOCs volatile organic compoundsWWII World War 2; era from 1930's through 1940's when US military maintained

a garrison in Dutch Harbor and Unalaska

1.0 Introduction TZ Engineering (TZE) has prepared this Characterization Report and Work Plan Addendum on behalf of Delta Western (DW) to document the November 2016 characterization of soils along the path of proposed storm drain improvements at the Delta Western Warehouse Drainage Project (the Project) in Dutch Harbor, Alaska. The purpose of the characterization was to delineate if any potential contamination existed in the top 5-feet (below ground surface) bgs of soil along the storm drain improvement route. Previously, TZE submitted a Work Plan to the Alaska Department of Environmental Conservation (ADEC) for the Project entitled “Soil Work Plan for Delta Western Warehouse Drainage Improvements” dated October 26, 2016. ADEC approved the Work Plan on November 3, 2016 and field work sampling took place on November 4th and 5th. TZ Engineering requests ADECs written review and approval or review and approval with comments of this report and work plan addendum.

2.0 Work Plan Field Screening Narrative On November 1, 2016 TZE marked out the proposed test pit locations along the storm drain route using GPS-RTK surveying equipment. On November 2, 2016 the City of Unalaska and TelAlaska were onsite locating and marking subsurface utilities at the Project site. Utility locations were surveyed using GPS-RTK equipment and the paint marks were pinned with PK nails and utility appropriate colored wiskers. On November 3, 2016 TZE and Northern Alaska Contractors (NAC) mobilized to the site and advanced seven test pits to 5-feet bgs. A field screen was collected at 2.5-feet and 5-feet bgs from each test pit. Confirmation samples were collected from each test pit at the location with the highest PID reading. Soil samples were identified by the pit ID and approximate depth of collection; i.e. TP1-2 is the soil sample from test pit 1 and was collected at approximately 2 feet bgs. No groundwater or free product was encountered during the excavation. Test pits were backfilled with the excavator bucket immediately following sampling. Confirmation samples were stored in a refrigerator at the TZE office. Weather was generally acceptable during excavation activities with intermittent light rain. Work was stopped when the weather deteriorated and heavy rain began. The following test pits were excavated and sampled; TP2, TP3, TP4, TP5, TP6, TP7 and TP8. On November 4, 2016 TZE and NAC returned to the site and excavated the remaining three test pits to 5-feet bgs. A field screen was collected at 2.5-feet and 5-feet bgs from each test pit. Confirmation samples were collected from each test pit at the location with the highest PID reading. No groundwater or free product was encountered during the excavation. Test pits were backfilled with the excavator bucket immediately following sampling. Weather was generally acceptable during excavation activities with intermittent light rain. Confirmation samples were packaged and delivered to PenAir Cargo for shipment to SGS labs in Anchorage. Field notes and a photolog are included in Attachment B.

3.0 Field Screening Results Confirmation soil samples were analyzed for gasoline range organics (GRO) by method AK101, BTEX by US Environmental Protection Agency (EPA) method 8021, polynuclear aromatic hydrocarbons (PAHs) by EPA method 8270D, diesel range organics (DRO) by method AK102, and residential range organics (RRO) by method AK103 and polychlorinated biphenyls (PCB’s) by EPA Method 8082(a) by SGS Labs in Anchorage, Alaska. The laboratory analytical results, chain of custody (CoC) documentation and sample map are presented in Attachment A. The Rocky Point Management Area (RPMA) has the following cleanup levels: 8250 milligrams per kilograms (mg/kg) for DRO, 8300 mg/kg for RRO, 1400 mg/kg for GRO, 0.2 mg/kg for benzene, 48 mg/kg for toluene, 50 mg/kg for ethylbenzene, 81 for mg/kg xylene, and for PCB’s 1 mg/kg Field duplicates were collected simultaneously from the same sampling locations. One laboratory prepared trip blank was submitted to the laboratory.

Test

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TP1 2.5 0.070 111 606 ND ND ND ND ND TP2 5 0.142 ND 248 ND ND ND ND ND TP3 5 0.069 ND ND ND ND ND ND ND TP4 5 0.340 243 1320 ND ND ND ND ND TP5 2.5 0.256 ND ND ND ND ND ND ND TP6 5 0.387 306 1740 ND ND ND ND ND TP7 5 1.520 500 2580 ND ND ND ND ND TP8 2.5 ND 39.4 145 ND ND ND ND 0.35 TP9 2.5 ND 27.7 133 ND ND ND ND ND TP10 5 0.072 34.5 155 ND ND ND ND ND TP11 2.5 1.240 108 484 ND ND ND ND ND Bold indicates and exceedance of cleanup levels. All Units mg/kg unless noted.

The City owns the public rights of way including East Point Loop Road and has also established public utility easements through privately owned land adjacent to these rights of way. The path of the storm drain improvements are within these public rights of way and in other areas designated as utility easements. These areas are contiguous to the Rocky Point Management Area (the RPMA) and the World War Two Tank Farm FUDS Site No. F10AK084103 on Amaknak Island (the FUDS Site). The RPMA and the FUDS Site have been used as bulk petroleum storage and distribution facilities for the fueling of marine vessels and loading of tanker trucks for over 70 years. The Department of Defense initially operated fueling facilities through the conclusion of World War II. Standard Oil of California, a corporate predecessor to Chevron, subsequently leased portions of the facilities until 1986. Since 1986, DW has leased and operated portions of the facility for fueling operations. Surface rights to most of the land on Amaknak Island, including the RPMA and the FUDS Site, were transferred to Ounalashka Corporation in response to the Alaska Native Claims Act of 1971. The storm drain will run through or in a right of way which adjoins land zoned Marine Related/Industrial. These zoning descriptions are per City of Unalaska Code of Ordinances 8.12.060. With the exception East Point Road right of way, all of these properties are owned by the Ounalashka Corporation. Various reports written by the responsible parties for area wide soil and groundwater total petroleum hydrocarbon contamination attribute it to fueling operations which have historical extent from the 1920’s to ongoing operations in the present day. This area-wide contamination is not the result of any activities conducted by DW, and they have not contributed to the contamination that will be encountered during project implementation. Due to the wide-spread nature of the soil and groundwater contamination in the project vicinity and anecdotal evidence, DW has assumed that soil impacts could be present in any location excavated along the drain’s route. The results of the field screening demonstrated that this was indeed the case. This work plan focuses on proper management of wastes derived from the project (which will be minimized) and not on remediation of historic contamination for which DW is not responsible. Nonetheless, any soils removed from the excavation that are anticipated to exceed the cleanup

criteria for the RPMA will be stockpiled to determine whether they should be hauled off site as waste and disposed of at a licensed landfill. Sampling of the potential waste stockpiles will be performed in accord with ADEC guidance. One additional consideration is the water building in the work area that presents a risk to workers when ice forms and saturated soils damage the roadbed leading to failures in the driving surface. This project will reduce that risk by draining water away and providing a safer work environment, while not altering the environmental risk posed by contamination soils. These safety benefits should be considered as an element of project implementation.

4.0 Work Plan Addendum The work has been planned in general accordance with ADEC’s March 2014 Technical Memorandum entitled Managing Petroleum-Contaminated Soil, Water, or Free Product during Public Utility and Right-of-Way Construction and Maintenance Projects. The area has been developed over the years and many feet of aggregate and silty fill material must be assumed to have replaced and/or overlaid native bedrock or soils (USACE 2009 estimates 4 to 6-feet within in the FUDS Site). During test pit excavation it was confirmed that a minimum of the top 2.5’ of soil along the length of the proposed storm drain route consisted of imported crushed rock surfacing material. As previously discussed with ADEC, the top 2.0’ of soil may be excavated, and beneficially reused as clean fill on or offsite (figure 2). Excavated soils located within 25’ of TP7 and TP11 exhibited higher levels of PCB contamination during field screening (Section 3.0). These soils will be excavated and reused in the trench from 2-5’ bgs from CB2 to CB3 as space allows (figure 1). Geotextile fabric for soil separation will be placed in the trench prior to backfilling to act a delineator during future work on the trench (if needed) and ensure that soils which have been field screened are not mixed with contaminated soils. The top 2’ of trench backfill will consist of the previously removed clean material, and surfacing material will consist of imported crushed rock from an established quarry. The material excavated outside of the TP7 and TP11 area and deeper than 2’ bgs will be reused as backfill in the proposed storm drain trench. If there is a greater volume of excavated material then will fit back into the trench it will be temporarily stockpiled within the RPMA on DW property. The stockpile will be screened per ADEC guidance and disposed of in an approved manner. Bentonite/sand seals will be installed along the storm drain system. The bentonite/sand seals will be installed downstream of catch basin two (CB-2) and catch basin one (CB-1). The final bentonite/sand seals will be a minimum of 1-foot hydrated thickness and will extend for a minimum of the width of the trench, and from the base of the trench to at least 6-inches above the top of pipe. Following ADEC approval of this work plan all storm drain improvements will begin to be installed per the Plans and this document. Following completion of this project, the record keeping documents and any results of soil characterization will be submitted to ADEC along with the follow-up reporting that was required in the Work Plan.

Figure 1-Soil 2’ – 5’ bgs in these areas to be relocated between CB-2 and CB-3

Figure 2 – Area 0’-2’ bgs Designated for Beneficial Reuse

Figure 3 – Standard Trench Section for areas that soils from around TP7 and TP11 are used as backfill.

5.0 Conclusions & Recommendations The original work plan desired to beneficially reuse all soil offsite or within the excavated trench. As noted in Sections 3.0 and 4.0 of this plan, soils from the vicinity of TP11, TP7 and TP6 will remain in the trench and covered with landscape cloth. Other soils will be stockpiled and characterized for either on site reuse of disposal offsite as waste. Review of the laboratory data indicated that matrix interference did not cause any of the sample results to exceed the applicable RPMA cleanup criteria. Hence, even though the detection limits varied, in no case did the detection limit of a non-detect compound result in a false negative result. In all cases, detection limits were two orders of magnitude less than the applicable RPMA cleanup criteria. Variances in the matrix spike and matrix spike duplicate results noted by the laboratory do not indicate problems in the sample data. This data set is considered usable for this work. Delta Western requests ADEC’s consideration, review and approval of this characterization report and work plan addendum. Attachment C includes agency review documentation.

6.0 Limitations This characterization report and work plan addendum was prepared in accordance with 18 AAC 75 and with generally accepted professional engineering and environmental management practices existing at the time this report was prepared and which are applicable to the location of the Site. It was prepared for the exclusive use of ADEC and DW for the express purpose stated above. Any re-use of this report for a different purpose or by others not identified above shall be at the user’s sole risk without liability to TZE. To the extent that this work plan is based on information provided to TZE by third parties, TZE may have made efforts to verify this third party information, but TZE cannot guarantee the completeness or accuracy of this information. The opinions expressed and data collected are based on the conditions of the Site existing at the time of the proposed field investigation. No other warranties, expressed or implied are made by TZE. All information, conclusions, and recommendations provided by TZE in this document regarding the Site have been prepared under the supervision of and reviewed by the qualified person whose signature appears below: Approved by: Tyler Zimmerman, P.E.

[email protected] Cell: (907) 359-3596

mailto:[email protected]

ATTACHMENT A

Tyler ZimmermanOval

Tyler ZimmermanOval

Tyler ZimmermanOval

Tyler ZimmermanOval

Tyler ZimmermanOval

Tyler ZimmermanOval

Tyler ZimmermanOval

Tyler ZimmermanOval

Tyler ZimmermanOval

Tyler ZimmermanRectangle



Tyler ZimmermanOval

Tyler ZimmermanText BoxSAMPLE LOCATIONS

Tyler ZimmermanText BoxPCB SAMPLE

Tyler ZimmermanText BoxALL COPC

Tyler ZimmermanText BoxTP1Aroclro-1260 70 ug/kgRRO 606 mg/kgDRO 111 mg/kg

Tyler ZimmermanText BoxTP2Aroclro-1260 142 ug/kgRRO 248 mg/kg

Tyler ZimmermanLine

Tyler ZimmermanLine

Tyler ZimmermanText BoxTP3Aroclro-1260 69.2 ug/kg

Tyler ZimmermanLine


Tyler ZimmermanLine

Tyler ZimmermanText BoxTP5Aroclro-1260 256 ug/kg


Tyler ZimmermanPolygonal Line



Tyler ZimmermanText BoxTP8RRO 145 mg/kgDRO 39.4 mg/kg


Tyler ZimmermanText BoxTP9RRO 133 mg/kgDRO 27.7 mg/kg


Tyler ZimmermanText BoxTP10Aroclro-1260 72.8 ug/kgRRO 155 mg/kgDRO 34.5 mg/kg





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11/11/2016

Report Number: 1166791

Client Project: Warehouse Stormdrain

Laboratory Report of Analysis

Dear Tyler Zimmerman,

Enclosed are the results of the analytical services performed under the referenced project for the received

samples and associated QC as applicable. The samples are certified to meet the requirements of the National

Environmental Laboratory Accreditation Conference Standards. Copies of this report and supporting data will be

retained in our files for a period of ten years in the event they are required for future reference. All results are

intended to be used in their entirety and SGS is not responsible for use of less than the complete report. Any

samples submitted to our laboratory will be retained for a maximum of fourteen (14) days from the date of this

report unless other archiving requirements were included in the quote.

If there are any questions about the report or services performed during this project, please call Forest at (907)

562-2343. We will be happy to answer any questions or concerns which you may have.

Thank you for using SGS North America Inc. for your analytical services. We look forward to working with you

again on any additional analytical needs.

Sincerely,

SGS North America Inc.

__________________________________________________________________

Forest Taylor Date

Project [email protected]

To: Delta Western-Anchorage

,

(907)359-3596

Print Date: 12/01/2016 9:36:05AM

Member of SGS Group

SGS North America Inc. 200 West Potter Drive, Anchorage, AK 99518

t 907.562.2343 f 907.561.5301 www.us.sgs.com

1 of 98

Case Narrative

SGS Client: Delta Western-Anchorage

SGS Project: 1166791

Project Name/Site: Warehouse Stormdrain

Project Contact: Tyler Zimmerman

Refer to sample receipt form for information on sample condition.

1166791011MS (1365522) MS

8270D SIM - PAH MS recovery for several analytes do not meet QC criteria. Refer to the LCS for accuracy requirements.

1166791011MSD (1365523) MSD

8270D SIM - PAH MSD recovery for several analytes do not meet QC criteria. Refer to the LCS for accuracy

requirements.

1166791012(1365698MSD) (1365700) MSD

6020A - Metals MSD recoveries for do not meet QC criteria. The post digestion spike was successful.

1166791006MSD (1365894) MSD

8082A - PCB Aroclor 1260 MSD recovery (47.6%) does not meet QC criteria. Refer to the LCS for accuracy

requirements.

*QC comments may be associated with the field samples found in this report. When applicable, comments will be applied to

associated field samples.

Print Date: 12/01/2016 9:36:07AM

Member of SGS Group

SGS North America Inc.

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Laboratory ID Client Sample ID Analytical Batch Analyte Reason

Report of Manual Integrations

8270D SIM (PAH)

TP1-2 XMS9761 Benzo[k]fluoranthene RP1166791001



TP4-4 XMS9761 Dibenzo[a,h]anthracene RP1166791004

TP6-4 XMS9761 Benzo[g,h,i]perylene RP1166791006



TP6-4 XMS9761 Indeno[1,2,3-c,d] pyrene RP1166791006

TP7-4 XMS9761 Benzo[g,h,i]perylene RP1166791007



TP7-4 XMS9761 Indeno[1,2,3-c,d] pyrene RP1166791007



DUP10-4 XMS9761 Benzo[k]fluoranthene RP1166791011


DUP11-2 XMS9762 Benzo[k]fluoranthene RP1166791013

Manual Integration Reason Code Descriptions

Code Description

O Original Chromatogram

M Modified Chromatogram

SS Skimmed surrogate

BLG Closed baseline gap

RP Reassign peak name

PIR Pattern integration required

IT Included tail

SP Split peak

RSP Removed split peak

FPS Forced peak start/stop

BLC Baseline correction

PNF Peak not found by software

All DRO/RRO analysis are integrated per SOP.

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Laboratory Qualifiers

Enclosed are the analytical results associated with the above work order. All results are intended to be used in their

entirety and SGS is not responsible for use of less than the complete report. This document is issued by the Company

under its General Conditions of Service accessible at .

Attention is drawn to the limitation of liability, indenmification and jurisdiction issues defined therein.

Any holder of this document is advised that information contained hereon reflects the Company's findings at the time of

its intervention only and within the limits of Client's instructions, if any. The Company's sole responsibility is to its Client

and this document does not exonerate parties to a transaction from exercising all their rights and obligations under the

transaction documents. Any unauthorized alteration, forgery or falsification of the context or appearance of this

document is unlawful and offenders may be prosecuted to the fullest extent of the law.

SGS maintains a formal Quality Assurance/Quality Control (QA/QC) program. A copy of our Quality Assurance Plan

(QAP), which outlines this program, is available at your request. The laboratory certification numbers are AK00971

(DW Chemistry & Microbiology) & UST-005 (CS) for ADEC and 2944.01 for DOD ELAP/ISO17025 (RCRA methods:

1020B, 1311, 3010A, 3050B, 3520C, 3550C, 5030B, 5035A, 6020A, 7470A, 7471B, 8021B, 8082A, 8260B, 8270D,

8270D-SIM, 9040C, 9045D, 9056A, 9060A, AK101 and AK102/103). Except as specifically noted, all statements and

data in this report are in conformance to the provisions set forth by the SGS QAP and, when applicable, other regulatory

authorities.

The following descriptors or qualifiers may be found in your report:

* The analyte has exceeded allowable regulatory or control limits.

! Surrogate out of control limits.

B Indicates the analyte is found in a blank associated with the sample.

CCV/CVA/CVB Continuing Calibration Verification

CCCV/CVC/CVCA/CVCB Closing Continuing Calibration Verification

CL Control Limit

D The analyte concentration is the result of a dilution.

DF Dilution Factor

DL Detection Limit (i.e., maximum method detection limit)

E The analyte result is above the calibrated range.

F Indicates value that is greater than or equal to the DL

GT Greater Than

IB Instrument Blank

ICV Initial Calibration Verification

J The quantitation is an estimation.

JL The analyte was positively identified, but the quantitation is a low estimation.

LCS(D) Laboratory Control Spike (Duplicate)

LOD Limit of Detection (i.e., 1/2 of the LOQ)

LOQ Limit of Quantitation (i.e., reporting or practical quantitation limit)

LT Less Than

M A matrix effect was present.

MB Method Blank

MS(D) Matrix Spike (Duplicate)

ND Indicates the analyte is not detected.

Q QC parameter out of acceptance range.

R Rejected

RPD Relative Percent Difference

U Indicates the analyte was analyzed for but not detected.

Note: Sample summaries which include a result for "Total Solids" have already been adjusted for moisture content.

All DRO/RRO analyses are integrated per SOP.

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http://www.sgs.com/terms_and_conditions.htmhttp://www.sgs.com/terms_and_conditions.htm

Sample Summary

Client Sample ID Lab Sample ID Collected Received Matrix

TP1-2 1166791001 11/04/2016 11/11/2016 Soil/Solid (dry weight)










DUP10-4 1166791011 11/04/2016 11/11/2016 Soil/Solid (dry weight)


DUP11-2 1166791013 11/04/2016 11/11/2016 Soil/Solid (dry weight)

Trip Blank 1166791014 11/03/2016 11/11/2016 Soil/Solid (dry weight)

Method DescriptionMethod

8270 PAH SIM Semi-Volatiles GC/MS8270D SIM (PAH)

AK101/8021 Combo. (S)AK101

AK101/8021 Combo. (S)SW8021B

Diesel/Residual Range OrganicsAK102

Diesel/Residual Range OrganicsAK103

Metals by ICP-MS (S)SW6020A

Percent Solids SM2540GSM21 2540G

SW8082 PCB'sSW8082A

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Detectable Results Summary

Client Sample ID: TP1-2

Lab Sample ID: 1166791001 UnitsParameter ResultLead mg/Kg20.0Metals by ICP/MS

Aroclor-1260 ug/Kg70.5Polychlorinated Biphenyls

Acenaphthene ug/Kg65.0Polynuclear Aromatics GC/MS

Anthracene ug/Kg87.5

Benzo(a)Anthracene ug/Kg111

Benzo[a]pyrene ug/Kg104

Benzo[b]Fluoranthene ug/Kg105

Benzo[g,h,i]perylene ug/Kg60.5

Benzo[k]fluoranthene ug/Kg32.1

Chrysene ug/Kg133

Fluoranthene ug/Kg226

Fluorene ug/Kg42.3

Indeno[1,2,3-c,d] pyrene ug/Kg37.1

Phenanthrene ug/Kg346

Pyrene ug/Kg319

Diesel Range Organics mg/Kg111Semivolatile Organic Fuels

Residual Range Organics mg/Kg606



Aroclor-1260 ug/Kg142Polychlorinated Biphenyls

Benzo(a)Anthracene ug/Kg74.2Polynuclear Aromatics GC/MS

Benzo[a]pyrene ug/Kg71.1

Benzo[b]Fluoranthene ug/Kg90.0



Chrysene ug/Kg82.2



Phenanthrene ug/Kg55.0

Pyrene ug/Kg132

Residual Range Organics mg/Kg248Semivolatile Organic Fuels


Lab Sample ID: 1166791003 UnitsParameter ResultAroclor-1260 ug/Kg69.2Polychlorinated Biphenyls

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1-Methylnaphthalene ug/Kg83.6Polynuclear Aromatics GC/MS

2-Methylnaphthalene ug/Kg49.0

Acenaphthene ug/Kg437

Acenaphthylene ug/Kg36.5

Anthracene ug/Kg779




Benzo[g,h,i]perylene ug/Kg382

Benzo[k]fluoranthene ug/Kg292

Chrysene ug/Kg1550

Dibenzo[a,h]anthracene ug/Kg104


Fluorene ug/Kg286

Indeno[1,2,3-c,d] pyrene ug/Kg290


Pyrene ug/Kg3410




Lab Sample ID: 1166791005 UnitsParameter ResultAroclor-1260 ug/Kg256Polychlorinated Biphenyls





Anthracene ug/Kg155






Chrysene ug/Kg308




Pyrene ug/Kg663



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Anthracene ug/Kg196






Chrysene ug/Kg399


Fluorene ug/Kg73.3



Pyrene ug/Kg826





Benzo[b]Fluoranthene ug/Kg6.91Polynuclear Aromatics GC/MS

Fluoranthene ug/Kg8.82

Pyrene ug/Kg7.92

Diesel Range Organics mg/Kg39.4Semivolatile Organic Fuels


o-Xylene ug/Kg35.3Volatile Fuels





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Acenaphthylene ug/Kg7.90Polynuclear Aromatics GC/MS


Benzo(a)Anthracene ug/Kg27.2





Chrysene ug/Kg39.0

Dibenzo[a,h]anthracene ug/Kg5.95




Pyrene ug/Kg53.0



Client Sample ID: DUP10-4





Benzo(a)Anthracene ug/Kg30.9





Chrysene ug/Kg42.4





Pyrene ug/Kg62.3



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Chrysene ug/Kg269





Pyrene ug/Kg355



Client Sample ID: DUP11-2




Acenaphthylene ug/Kg58.1

Anthracene ug/Kg138






Chrysene ug/Kg815

Dibenzo[a,h]anthracene ug/Kg223


Fluorene ug/Kg36.9



Pyrene ug/Kg847

Residual Range Organics mg/Kg430Semivolatile Organic Fuels

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Client Project ID: Warehouse Stormdrain

Lab Sample ID: 1166791001

Lab Project ID: 1166791

Collection Date: 11/04/16 13:45

Received Date: 11/11/16 16:05

Matrix: Soil/Solid (dry weight)

Solids (%):90.9

Results by Metals by ICP/MS

Results of TP1-2

Location:

Date AnalyzedParameter DFUnitsResult LOQ/CL DLAllowable

LimitsQual

Lead 20.0 mg/Kg 500.984 0.305 11/21/16 15:38

Batch Information

Prep Batch: MXX30365

Prep Method: SW3050B

Prep Date/Time: 11/18/16 11:29

Prep Initial Wt./Vol.: 1.118 g

Prep Extract Vol: 50 mL

Analytical Batch: MMS9625

Analytical Method: SW6020A

Analyst: VDL

Analytical Date/Time: 11/21/16 15:38

Container ID: 1166791001-A

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Solids (%):90.9

Results by Polychlorinated Biphenyls

Results of TP1-2

Location:


LimitsQual

Aroclor-1016 54.7 ug/Kg 154.7 16.4 11/22/16 17:35U

Aroclor-1221 219 ug/Kg 1219 67.9 11/22/16 17:35U

Aroclor-1232 54.7 ug/Kg 154.7 16.4 11/22/16 17:35U

Aroclor-1242 54.7 ug/Kg 154.7 16.4 11/22/16 17:35U

Aroclor-1248 54.7 ug/Kg 154.7 16.4 11/22/16 17:35U

Aroclor-1254 54.7 ug/Kg 154.7 16.4 11/22/16 17:35U

Aroclor-1260 70.5 ug/Kg 154.7 16.4 11/22/16 17:35

Surrogates

Decachlorobiphenyl (surr) 61 % 160-125 11/22/16 17:35

Batch Information

Prep Batch: XXX36714

Prep Method: SW3550C




Analytical Batch: XGC9601


Analyst: AEE



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Solids (%):90.9

Results by Polynuclear Aromatics GC/MS

Results of TP1-2

Location:


LimitsQual

1-Methylnaphthalene 21.7 ug/Kg 421.7 6.51 11/22/16 21:21U


Acenaphthene 65.0 ug/Kg 421.7 6.51 11/22/16 21:21

Acenaphthylene 21.7 ug/Kg 421.7 6.51 11/22/16 21:21U

Anthracene 87.5 ug/Kg 421.7 6.51 11/22/16 21:21

Benzo(a)Anthracene 111 ug/Kg 421.7 6.51 11/22/16 21:21

Benzo[a]pyrene 104 ug/Kg 421.7 6.51 11/22/16 21:21

Benzo[b]Fluoranthene 105 ug/Kg 421.7 6.51 11/22/16 21:21

Benzo[g,h,i]perylene 60.5 ug/Kg 421.7 6.51 11/22/16 21:21

Benzo[k]fluoranthene 32.1 ug/Kg 421.7 6.51 11/22/16 21:21

Chrysene 133 ug/Kg 421.7 6.51 11/22/16 21:21

Dibenzo[a,h]anthracene 21.7 ug/Kg 421.7 6.51 11/22/16 21:21U

Fluoranthene 226 ug/Kg 421.7 6.51 11/22/16 21:21

Fluorene 42.3 ug/Kg 421.7 6.51 11/22/16 21:21

Indeno[1,2,3-c,d] pyrene 37.1 ug/Kg 421.7 6.51 11/22/16 21:21

Naphthalene 21.7 ug/Kg 421.7 6.51 11/22/16 21:21U

Phenanthrene 346 ug/Kg 421.7 6.51 11/22/16 21:21

Pyrene 319 ug/Kg 421.7 6.51 11/22/16 21:21

Surrogates

2-Fluorobiphenyl (surr) 86.7 % 446-115 11/22/16 21:21

Terphenyl-d14 (surr) 89.9 % 458-133 11/22/16 21:21

Batch Information






Analytical Batch: XMS9761

Analytical Method: 8270D SIM (PAH)

Analyst: S.G



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Solids (%):90.9

Results by Semivolatile Organic Fuels

Results of TP1-2

Location:


LimitsQual

Diesel Range Organics 111 mg/Kg 487.0 27.0 11/21/16 19:46

Surrogates

5a Androstane (surr) 112 % 450-150 11/21/16 19:46

Batch Information






Analytical Batch: XFC13073

Analytical Method: AK102

Analyst: S.G




LimitsQual

Residual Range Organics 606 mg/Kg 487.0 27.0 11/21/16 19:46

Surrogates

n-Triacontane-d62 (surr) 99.7 % 450-150 11/21/16 19:46

Batch Information








Analyst: S.G



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Solids (%):90.9

Results by Volatile Fuels

Results of TP1-2

Location:


LimitsQual

Gasoline Range Organics 1.41 mg/Kg 11.41 0.424 11/12/16 04:09U

Surrogates

4-Bromofluorobenzene (surr) 102 % 150-150 11/12/16 04:09

Batch Information

Prep Batch: VXX29966

Prep Method: SW5035A



Prep Extract Vol: 38.6767 mL

Analytical Batch: VFC13470


Analyst: NRO


Container ID: 1166791001-B


LimitsQual

Benzene 7.07 ug/Kg 17.07 2.26 11/12/16 04:09U

Ethylbenzene 14.1 ug/Kg 114.1 4.41 11/12/16 04:09U

o-Xylene 14.1 ug/Kg 114.1 4.41 11/12/16 04:09U

P & M -Xylene 28.3 ug/Kg 128.3 8.48 11/12/16 04:09U

Toluene 14.1 ug/Kg 114.1 4.41 11/12/16 04:09U

Surrogates

1,4-Difluorobenzene (surr) 84.4 % 172-119 11/12/16 04:09

Batch Information







Analytical Method: SW8021B

Analyst: NRO



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Solids (%):87.9


Results of TP2-4

Location:


LimitsQual

Lead 15.0 mg/Kg 501.03 0.319 11/21/16 15:42

Batch Information








Analyst: VDL



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Solids (%):87.9


Results of TP2-4

Location:


LimitsQual

Aroclor-1016 57.1 ug/Kg 157.1 17.1 11/22/16 17:45U

Aroclor-1221 228 ug/Kg 1228 70.8 11/22/16 17:45U

Aroclor-1232 57.1 ug/Kg 157.1 17.1 11/22/16 17:45U

Aroclor-1242 57.1 ug/Kg 157.1 17.1 11/22/16 17:45U

Aroclor-1248 57.1 ug/Kg 157.1 17.1 11/22/16 17:45U

Aroclor-1254 57.1 ug/Kg 157.1 17.1 11/22/16 17:45U

Aroclor-1260 142 ug/Kg 157.1 17.1 11/22/16 17:45

Surrogates


Batch Information








Analyst: AEE



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Solids (%):87.9


Results of TP2-4

Location:


LimitsQual



Acenaphthene 23.0 ug/Kg 423.0 6.91 11/22/16 19:18U


Anthracene 23.0 ug/Kg 423.0 6.91 11/22/16 19:18U

Benzo(a)Anthracene 74.2 ug/Kg 423.0 6.91 11/22/16 19:18

Benzo[a]pyrene 71.1 ug/Kg 423.0 6.91 11/22/16 19:18

Benzo[b]Fluoranthene 90.0 ug/Kg 423.0 6.91 11/22/16 19:18

Benzo[g,h,i]perylene 48.7 ug/Kg 423.0 6.91 11/22/16 19:18


Chrysene 82.2 ug/Kg 423.0 6.91 11/22/16 19:18



Fluorene 23.0 ug/Kg 423.0 6.91 11/22/16 19:18U



Phenanthrene 55.0 ug/Kg 423.0 6.91 11/22/16 19:18

Pyrene 132 ug/Kg 423.0 6.91 11/22/16 19:18

Surrogates


Terphenyl-d14 (surr) 84.4 % 458-133 11/22/16 19:18

Batch Information








Analyst: S.G



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Solids (%):87.9


Results of TP2-4

Location:


LimitsQual

Diesel Range Organics 88.2 mg/Kg 488.2 27.4 11/21/16 20:07U

Surrogates


Batch Information








Analyst: S.G




LimitsQual


Surrogates

n-Triacontane-d62 (surr) 107 % 450-150 11/21/16 20:07

Batch Information








Analyst: S.G



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Solids (%):87.9


Results of TP2-4

Location:


LimitsQual


Surrogates


Batch Information








Analyst: NRO




LimitsQual

Benzene 8.82 ug/Kg 18.82 2.82 11/12/16 04:28U


o-Xylene 17.6 ug/Kg 117.6 5.50 11/12/16 04:28U

P & M -Xylene 35.3 ug/Kg 135.3 10.6 11/12/16 04:28U

Toluene 17.6 ug/Kg 117.6 5.50 11/12/16 04:28U

Surrogates


Batch Information








Analyst: NRO



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Solids (%):85.4


Results of TP3-4

Location:


LimitsQual

Aroclor-1016 57.5 ug/Kg 157.5 17.2 11/22/16 18:05U

Aroclor-1221 230 ug/Kg 1230 71.2 11/22/16 18:05U

Aroclor-1232 57.5 ug/Kg 157.5 17.2 11/22/16 18:05U

Aroclor-1242 57.5 ug/Kg 157.5 17.2 11/22/16 18:05U

Aroclor-1248 57.5 ug/Kg 157.5 17.2 11/22/16 18:05U

Aroclor-1254 57.5 ug/Kg 157.5 17.2 11/22/16 18:05U

Aroclor-1260 69.2 ug/Kg 157.5 17.2 11/22/16 18:05

Surrogates


Batch Information








Analyst: AEE



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Solids (%):84.3


Results of TP4-4

Location:


LimitsQual

Lead 72.0 mg/Kg 501.10 0.340 11/21/16 15:47

Batch Information








Analyst: VDL



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Solids (%):84.3


Results of TP4-4

Location:


LimitsQual

Aroclor-1016 58.9 ug/Kg 158.9 17.7 11/22/16 16:33U

Aroclor-1221 236 ug/Kg 1236 73.1 11/22/16 16:33U

Aroclor-1232 58.9 ug/Kg 158.9 17.7 11/22/16 16:33U

Aroclor-1242 58.9 ug/Kg 158.9 17.7 11/22/16 16:33U

Aroclor-1248 58.9 ug/Kg 158.9 17.7 11/22/16 16:33U

Aroclor-1254 58.9 ug/Kg 158.9 17.7 11/22/16 16:33U

Aroclor-1260 340 ug/Kg 158.9 17.7 11/22/16 16:33

Surrogates


Batch Information








Analyst: AEE



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Solids (%):84.3


Results of TP4-4

Location:


LimitsQual

1-Methylnaphthalene 83.6 ug/Kg 423.9 7.16 11/22/16 21:41

2-Methylnaphthalene 49.0 ug/Kg 423.9 7.16 11/22/16 21:41

Acenaphthene 437 ug/Kg 423.9 7.16 11/22/16 21:41

Acenaphthylene 36.5 ug/Kg 423.9 7.16 11/22/16 21:41

Anthracene 779 ug/Kg 40239 71.6 11/23/16 13:58

Benzo(a)Anthracene 1380 ug/Kg 40239 71.6 11/23/16 13:58

Benzo[a]pyrene 1310 ug/Kg 40239 71.6 11/23/16 13:58

Benzo[b]Fluoranthene 1310 ug/Kg 40239 71.6 11/23/16 13:58

Benzo[g,h,i]perylene 382 ug/Kg 423.9 7.16 11/22/16 21:41

Benzo[k]fluoranthene 292 ug/Kg 423.9 7.16 11/22/16 21:41

Chrysene 1550 ug/Kg 40239 71.6 11/23/16 13:58

Dibenzo[a,h]anthracene 104 ug/Kg 423.9 7.16 11/22/16 21:41

Fluoranthene 2550 ug/Kg 40239 71.6 11/23/16 13:58

Fluorene 286 ug/Kg 423.9 7.16 11/22/16 21:41

Indeno[1,2,3-c,d] pyrene 290 ug/Kg 423.9 7.16 11/22/16 21:41


Phenanthrene 3110 ug/Kg 40239 71.6 11/23/16 13:58

Pyrene 3410 ug/Kg 40239 71.6 11/23/16 13:58

Surrogates


Terphenyl-d14 (surr) 106 % 458-133 11/22/16 21:41

Batch Information








Analyst: S.G










Analyst: S.G



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Solids (%):84.3


Results of TP4-4

Location:


LimitsQual


Surrogates


Batch Information








Analyst: S.G




LimitsQual


Surrogates

n-Triacontane-d62 (surr) 109 % 450-150 11/21/16 20:28

Batch Information








Analyst: S.G



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Solids (%):84.3


Results of TP4-4

Location:


LimitsQual


Surrogates


Batch Information








Analyst: NRO




LimitsQual

Benzene 10.4 ug/Kg 110.4 3.34 11/12/16 04:47U


o-Xylene 20.9 ug/Kg 120.9 6.51 11/12/16 04:47U

P & M -Xylene 41.7 ug/Kg 141.7 12.5 11/12/16 04:47U

Toluene 20.9 ug/Kg 120.9 6.51 11/12/16 04:47U

Surrogates


Batch Information








Analyst: NRO



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Solids (%):86.7


Results of TP5-2

Location:


LimitsQual

Aroclor-1016 56.9 ug/Kg 156.9 17.1 11/22/16 18:16U

Aroclor-1221 227 ug/Kg 1227 70.5 11/22/16 18:16U

Aroclor-1232 56.9 ug/Kg 156.9 17.1 11/22/16 18:16U

Aroclor-1242 56.9 ug/Kg 156.9 17.1 11/22/16 18:16U

Aroclor-1248 56.9 ug/Kg 156.9 17.1 11/22/16 18:16U

Aroclor-1254 56.9 ug/Kg 156.9 17.1 11/22/16 18:16U

Aroclor-1260 256 ug/Kg 156.9 17.1 11/22/16 18:16

Surrogates


Batch Information








Analyst: AEE



Print Date: 12/01/2016 9:36:15AM

Member of SGS Group


t 907.562.2343 f 907.561.5301 www.us.sgs.com

27 of 98








Solids (%):82.6


Results of TP6-4

Location:


LimitsQual

Lead 45.2 mg/Kg 501.14 0.354 11/21/16 15:51

Batch Information








Analyst: VDL



Print Date: 12/01/2016 9:36:15AM

Member of SGS Group


t 907.562.2343 f 907.561.5301 www.us.sgs.com

28 of 98








Solids (%):82.6


Results of TP6-4

Location:


LimitsQual

Aroclor-1016 60.5 ug/Kg 160.5 18.2 11/22/16 16:44U

Aroclor-1221 242 ug/Kg 1242 75.1 11/22/16 16:44U

Aroclor-1232 60.5 ug/Kg 160.5 18.2 11/22/16 16:44U

Aroclor-1242 60.5 ug/Kg 160.5 18.2 11/22/16 16:44U

Aroclor-1248 60.5 ug/Kg 160.5 18.2 11/22/16 16:44U

Aroclor-1254 60.5 ug/Kg 160.5 18.2 11/22/16 16:44U

Aroclor-1260 387 ug/Kg 160.5 18.2 11/22/16 16:44

Surrogates


Batch Information








Analyst: AEE



Print Date: 12/01/2016 9:36:15AM

Member of SGS Group


t 907.562.2343 f 907.561.5301 www.us.sgs.com

29 of 98








Solids (%):82.6


Results of TP6-4

Location:


LimitsQual





Anthracene 155 ug/Kg 1059.7 17.9 11/22/16 22:02






Chrysene 308 ug/Kg 1059.7 17.9 11/22/16 22:02



Fluorene 59.7 ug/Kg 1059.7 17.9 11/22/16 22:02U




Pyrene 663 ug/Kg 1059.7 17.9 11/22/16 22:02

Surrogates


Terphenyl-d14 (surr) 87.7 % 1058-133 11/22/16 22:02

Batch Information








Analyst: S.G



Print Date: 12/01/2016 9:36:15AM

Member of SGS Group


t 907.562.2343 f 907.561.5301 www.us.sgs.com

30 of 98








Solids (%):82.6


Results of TP6-4

Location:


LimitsQual


Surrogates


Batch Information








Analyst: S.G




LimitsQual


Surrogates

n-Triacontane-d62 (surr) 93.2 % 450-150 11/21/16 21:09

Batch Information








Analyst: S.G



Print Date: 12/01/2016 9:36:15AM

Member of SGS Group


t 907.562.2343 f 907.561.5301 www.us.sgs.com

31 of 98








Solids (%):82.6


Results of TP6-4

Location:


LimitsQual


Surrogates

4-Bromofluorobenzene (surr) 67.9 % 150-150 11/12/16 05:06

Batch Information








Analyst: NRO




LimitsQual

Benzene 11.1 ug/Kg 111.1 3.57 11/12/16 05:06U


o-Xylene 22.3 ug/Kg 122.3 6.95 11/12/16 05:06U

P & M -Xylene 44.6 ug/Kg 144.6 13.4 11/12/16 05:06U

Toluene 22.3 ug/Kg 122.3 6.95 11/12/16 05:06U

Surrogates


Batch Information








Analyst: NRO



Print Date: 12/01/2016 9:36:15AM

Member of SGS Group


t 907.562.2343 f 907.561.5301 www.us.sgs.com

32 of 98








Solids (%):81.2


Results of TP7-4

Location:


LimitsQual

Lead 34.9 mg/Kg 501.18 0.365 11/21/16 15:56

Batch Information








Analyst: VDL



Print Date: 12/01/2016 9:36:15AM

Member of SGS Group


t 907.562.2343 f 907.561.5301 www.us.sgs.com

33 of 98








Solids (%):81.2


Results of TP7-4

Location:


LimitsQual

Aroclor-1016 61.3 ug/Kg 161.3 18.4 11/23/16 16:36U

Aroclor-1221 245 ug/Kg 1245 76.0 11/23/16 16:36U

Aroclor-1232 61.3 ug/Kg 161.3 18.4 11/23/16 16:36U

Aroclor-1242 61.3 ug/Kg 161.3 18.4 11/23/16 16:36U

Aroclor-1248 61.3 ug/Kg 161.3 18.4 11/23/16 16:36U

Aroclor-1254 61.3 ug/Kg 161.3 18.4 11/23/16 16:36U

Aroclor-1260 1520 ug/Kg 161.3 18.4 11/23/16 16:36

Surrogates


Batch Information








Analyst: AEE



Print Date: 12/01/2016 9:36:15AM

Member of SGS Group


t 907.562.2343 f 907.561.5301 www.us.sgs.com

34 of 98








Solids (%):81.2


Results of TP7-4

Location:


LimitsQual





Anthracene 196 ug/Kg 1060.6 18.2 11/22/16 22:22





Benzo[k]fluoranthene 122 ug/Kg 1060.6 18.2 11/22/16 22:22

Chrysene 399 ug/Kg 1060.6 18.2 11/22/16 22:22



Fluorene 73.3 ug/Kg 1060.6 18.2 11/22/16 22:22

Indeno[1,2,3-c,d] pyrene 118 ug/Kg 1060.6 18.2 11/22/16 22:22



Pyrene 826 ug/Kg 1060.6 18.2 11/22/16 22:22

Surrogates


Terphenyl-d14 (surr) 93 % 1058-133 11/22/16 22:22

Batch Information








Analyst: S.G



Print Date: 12/01/2016 9:36:15AM

Member of SGS Group


t 907.562.2343 f 907.561.5301 www.us.sgs.com

35 of 98








Solids (%):81.2


Results of TP7-4

Location:

characterization report and delta western warehouse drainage … · 2017. 5. 24. ·...

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