Bringing broadband NMR to your benchtop

True X-Nuclei

Tunable broadband preamplifier allows you to select nuclei from 29Si to 31P, whatever your experiment needs.

-20-100102030405060708090100110120130140150160170180190f1 ( ppm)

2

3

4

CH3

CH3

CH3

OH

O-30-25-20-15-10-505101520253035404550556065

f1 (ppm)

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1.0

Si

O

O

SiH

SiH

CH3

CH3

CH3

CH3

CH3

CH3

29Si

No compromises! X-Pulse lets you maximise your signal-to-noise ratio with optional interchangeable X-Pods for specific nuclei.

13C

Reaction Monitoring

Monitor your reactions as they happen.

Observe your reaction at temperatures from 20oC to 70oC and with the variable temperature probe.

2.903.003.103.203.303.403.503.603.703.80

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time

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M)

2.903.003.103.203.303.403.503.603.703.80

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M)

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P-

F

F F

F

F

F K+

-6.0-5.8-5.6-5.4-5.2-5.0-4.8-4.6-4.4-4.2-4.0-3.8-3.6-3.4-3.2-3.0-2.8-2.6-2.4-2.2-2.0-1.8-1.6-1.4-1.2

f1 (ppm)

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Na+

F

B-

F

FF

31P

Learn more at:nmr.oxinst.com/x-pulse

11B

Easy operationQuick experiments turn

complex pulse sequences

into a single click allowing

anyone to access the

power of NMR

Clearer spectraNew shimming

technology allows

spectral resolution of

<0.35Hz/10Hz

as standard

Ultimate stabilityFlow liquid samples at variable temperature (20°C – 70°C) without

spectral artefacts. Run high duty cycle pulse sequences without

destabilising the magnet

Benchtop convenienceNo requirement for special facilities or liquid

cryogens allowing you to use the instrument

wherever is most convenient

Easy to maintain Removable and

easy-to-access probe

for cleaning

Flexible softwareSpinFlow advanced

mode allows you to

define your own

experiments, your way

No need to compromiseInterchangeable X-Pods allow you to optimise

signal-to-noise ratio for specific nuclei

Choose your nucleiMeasure the nuclei you need for your experiment with

the world’s first broadband benchtop NMR spectrometer

Unleash the power of QA/QC in your benchtop NMRQuickly identify compounds, even in mixtures, or low concentration adulterants using chemometric

fingerprinting from your own custom-built database. This allows you to ensure the consistency of your

products and processes while spotting any contaminants.

0.50.60.70.80.91.01.11.21.31.41.51.61.71.81.92.02.12.22.32.42.52.62.72.82.93.03.13.23.33.4

f1 (ppm)

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600Easily analyse your spectraUnique 60MHz magnet design provides high

field homogeneity delivering resolution of

<0.35Hz (FWHM) making it easier to distinguish

overlapping peaks and identify compounds at

lower concentrations.

Compare unknown spectra

against user-defined database

to get top matches.

Generate synthetic

mixtures of combinations

to match the original

unknown spectrum.

Spectrum of ‘unknown’ test sample

2 regions of interest

Synthesised mixture of matches #1 and #6 gives best match to original unknown spectrum.

+

60MHz spectra at 1Hz linewidth (red) and 0.35Hz linewidth (green)

Match #10

Match #9

Match #8

Match #7

Match #6

Match #5

Match #4

Match #3

Match #2

Match #1

Match #1

Match #2

Match #10

Match #9

Match #8

Match #7

Match #6

Match #5

Match #4

Match #3

Match #2

Match #1

Match #1

Match #2

Match #10

Match #9

Match #8

Match #7

Match #6

Match #5

Match #4

Match #3

Match #2

Match #1

Match #1

Match #2

X-Pulse has the tools you

need to understand your

molecules, and determine

their structure.

0.00.51.01.52.02.53.03.54.04.55.05.56.06.57.07.58.08.59.09.5

f1 (ppm)

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O

H2

H2

H2

H2

H2

H2

OHO

CH3

CH3

From spectra to structural elucidation

Shaped RF pulses unlock advanced pulse sequences

and allow you to improve your solvent suppression.

Shaped pulses combined with the improved

linewidth of the X-Pulse make removing

solvent peaks more effective than ever.

Advanced pulse sequences like the selective

1D TOCSY can be used in place of some 2D

experiments, simplifying spectral analysis and

allowing you to obtain your results more quickly.0.00.51.01.52.02.53.03.54.04.55.05.56.06.57.0

f1 ( ppm)

1

2

3

Mixture of trans -3-Hexenoic acid +E thanol

CH31

2

3

4

5

6

OH7

O8

+ CH3E 1

E 2

OHE 3

3, 4

5

21

E2

E1

CH31

2

3

4

5

6

OH7

O8

CH3E 1

E 2

OHE 3

+

CH31

2

3

4

5

6

OH7

O8

CH3E 1

E 2

OHE 3

+

0123456789101112

f2 (ppm)

50

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f1 (

pp

m)

• Simple 1D spectra

• 2D experiments

• Inverse experiments

• Shaped pulses

• Pulsed field gradients

• Powerful MNova software0123456789101112

f2 (ppm)

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f1 (

pp

m)

We’re here to help you!OiService aims to keep your instrumentworking as hard as you do. Our globalnetwork of service hubs provides a fullrange of technical support:

Consumables and accessoriesRange of sample tubes and otheraccessories available.

Extended warrantiesAvoid unplanned costs.

Online diagnosticsIn-depth support over the internet.

Maintenance contractsEnsures your analyser producesthe right result every time.

RepairsFast and efficient turnaround.

Telephone help-desksFor a fast response to your problem.

TrainingUnderstand your analyserand its features.

iService®Petrochemicals Polymers

Pharmaceuticals Chemistry Education

Research Industrial Chemistry

This brochure provides only a glimpse into the technology of X-Pulse and its applications. Find out more at:

nmr.oxinst.com/x-pulse

This publication is the copyright of Oxford Instruments plc and provides outline information only, which (unless agreed by the company in writing) may not be used, applied or reproduced for any purpose or form part of any order or contract or regarded as the representation relating to the products or services concerned. Oxford Instruments’ policy is one of continued improvement. The company reserves the right to alter, without notice the specification, design or conditions of supply of any product or service. Oxford Instruments acknowledges all trademarks and registrations. © Oxford Instruments plc, 2019. All rights reserved. Part no: MR/215/0919

Polymers