avpm guide 1 blister card se… · blister card sealing guidlines interface temperature and...
TRANSCRIPT
1 | A S S O C I A T I O N O F V I S U A L P A C K A G I N G M A N U F A C T U R E R S
B L I S T E R C A R d S E A L I N G G U I d L I N E S
Blister CardBlister Card
SEALINGSEALINGGUIDELINE
SGUIDELINE
S
avpm-online.com ©AVPM 2018 4th Edition 2/18
2 | A S S O C I A T I O N O F V I S U A L P A C K A G I N G M A N U F A C T U R E R S
B L I S T E R C A R d S E A L I N G G U I d L I N E S
A. Background . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3
B. Objective . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4
C. Seal Master Machine SM-500 - . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5 “If you don’t measure it, you can’t control it.”
D. Common Industry Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7
E. Parameters for Heat Sealing . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9
F. Determining Interface Temperature and Pressure . . . . . . . . . . . . . . . . . . . . . . . . . 10
G. Standard Procedure for Determining the Integrity of the Blister Seal on a Visual Carded Package . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .11
1. Purpose . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .11
2. Scope . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .11
3. Referenced Documents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 12
4. Terminology . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 12
5. Discussion . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 13
6. Significance & Use . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 13
7. Apparatus . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 14
8. Sampling . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 15
9. Sample Conditioning . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 15
10. Procedure. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 15
11. Failure Modes . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 18
12. Report. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 19
13. Recommendation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 20
14. Troubleshooting . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 21
Index
3 | A S S O C I A T I O N O F V I S U A L P A C K A G I N G M A N U F A C T U R E R S
B L I S T E R C A R d S E A L I N G G U I d L I N E S
A. Backgound
The Association of Visual Packaging Manufacturers
(AVPM) is a non-profit organization founded in 2003.
Its membership is comprised of manufacturers of skin
and blister cards, thermoformed blisters, blister film,
paperboard, coating, and equipment. The AVPM is
organized exclusively as a business league for the
advancement of the domestic carded packaging industry.
The AVPM membership organized a Blister Sealing
Standards Committee to review, evaluate and recommend
the best practices, guidelines and test procedures for
producing and evaluating quality blister packaging.
4 | A S S O C I A T I O N O F V I S U A L P A C K A G I N G M A N U F A C T U R E R S
B L I S T E R C A R d S E A L I N G G U I d L I N E S
This publication, Blister Card Sealing Guidelines, is
intended to document the mutually agreed upon best
practices for producing and evaluating heat seal blister
packaging for the benefit of AVPM members and their
customers. The following guidelines are not exhaustive
and not intended to cover every blister seal application.
However, these guidelines are designed to cover
a majority of the domestic applications and uses.
B. Objective
5 | A S S O C I A T I O N O F V I S U A L P A C K A G I N G M A N U F A C T U R E R S
B L I S T E R C A R d S E A L I N G G U I d L I N E S
The validation of the quality of a product or process is paramount in the
manufacturing arena. This is especially true in the production of a blister
card.
There are four components of a blister card: 1) board, 2) ink, 3) coating,
and 4) blister. The quality characteristics of each of these materials must
be measured and controlled in order to ensure the product performs
as required. There are tools and instruments that measure the quality
characteristics of each of these components and validate their suitability
for use. Keep in mind: If you do not measure it you cannot control it.
And yet, even with the current technology and monitoring sophistication,
when it comes to checking the quality of sealed blister cards, an old and
outdated method is still used - cut an “X” on the back of the card and
tear each quadrant. Each person that tears a card using this method tears
at a different rate, and at a different angle of tear. No quantifiable data is
generated, thus there is no repeatability. When a sealing problem occurs
in the field there is no hard proof of a successful seal during the quality
checking procedure at the manufacturing facility.
In order to overcome this antiquated validating system, the Seal Master 500
Machine was developed and available for purchase. The SM-500 Machine
measures the actual force it takes to tear a blister from a card and produces
quantifiable data. Also, by producing charts, the SM-500 Machine gives you
a graphic profile of the actual tear. The SM-500 Machine controls the rate of
tear, the angle of tear, and is consistent from card to card. The human factor
is taken out of the equation and repeatability replaces inconsistency.
The SM-500 Machine is a valuable tool to use in the everyday quality control
procedures in the manufacturing of a blister card. By producing a graphic
profile of a particular card along with quantifiable data you now have
predictability as to the performance of that card in the future. The SM-500
Machine is also a valuable tool to be used in the resolution of sealing
C. Seal Master Machine SM-500
6 | A S S O C I A T I O N O F V I S U A L P A C K A G I N G M A N U F A C T U R E R S
B L I S T E R C A R d S E A L I N G G U I d L I N E S
problems in the field. The quantifiable data can be used in a statistical
format producing quality curves and a statistical history of that particular
card.
In a nutshell, The Seal Master SM-500 will:
• Consistently measure and record seal strength to improve your overall
process
• Improve overall productivity and profitability with standardized and quanti-
tative methods that provide a historical record
• Minimize customer complaints, downtime and re-work
Bottom line, would you rather “Pull it and guess” or “Measure it and know”?
For more information regarding the
Seal Master SM-500, please contact:
Cheminstruments, Inc.
510 Comercial Drive
Fairfield, OH 45014
Phone: 513.869.1598
7 | A S S O C I A T I O N O F V I S U A L P A C K A G I N G M A N U F A C T U R E R S
B L I S T E R C A R d S E A L I N G G U I d L I N E S
Adhesive Failure
A failure between bonded layers of materials; specifically paper-board
pigment coating to ink interface, ink to blister coating interface, blister coating to blister interface.
Aqueous Coating
A blister card industry term used to describe a water-soluble, heat seal blister adhesive.
Blister
A thermoformed part made of PVC or other polymer that has been formed through the application of heat, pressure and/or vacuum to create a product cavity.
Blister Card
A pigment coated (typically clay) paperboard card, usually printed, heat seal coated and die cut, designed to seal to a blister for the purpose of display-ing a product.
Blister Flange
The engineered flat sealing area of a thermoformed blister.
Blister Package
A finished package formed by heat sealing a thermoformed blister to a pigment coated paperboard card.
Cold Forming (also known as Stress or Soft Forming)
Caused by forming a blister outside its optimum temperature range.
Durometer Gauge
An instrument used to measure the hardness of rubber compounds.
Dwell (Seal) Time
The amount of time that heat and pressure are applied to the blister card and blister flange area to achieve proper seal.
Face Pressure
The pressure applied to the card and blister flange by the heat seal platen during the heat sealing process.
D. Common Industry Definitions
8 | A S S O C I A T I O N O F V I S U A L P A C K A G I N G M A N U F A C T U R E R S
B L I S T E R C A R d S E A L I N G G U I d L I N E S
Fiber Tear
The result of a successfully sealed blister to a paperboard card that can visually be confirmed by the attachment of paper fiber to the blister flange upon separation.
Grain Direction
The orientation of paperboard fibers in a blister card relative to the machine direction of the paperboard manufacturing process.
Heat Tape
A thermally sensitive tape designed to indicate a maximum achieved
temperature at the blister flange/blister card interface within a specific range for a single event.
Interface Temperature
The temperature achieved between the blister flange and the blister card during sealing.
Mayer Rod
A device used to apply a specific thickness of coating to a substrate.
Seal Strength
The degree of bond between the blister card and the blister flange created by the heat sealing process.
Slip Agent
A silicone coating or internal additive applied to the blister film to prevent the blisters from adhering to each other while nested.
Solvent Coating
A blister card industry term used to describe a solvent soluble, heat seal
blister adhesive.
Tear Direction
Fiber tear inline with the board grain (machine direction, MD) or across the board grain (cross direction, CD).
9 | A S S O C I A T I O N O F V I S U A L P A C K A G I N G M A N U F A C T U R E R S
B L I S T E R C A R d S E A L I N G G U I d L I N E S
Blisters
a) Gauge - 0.0075” min to 0.0300” max thickness before thermoforming1
b) Flange Width 0.312” recommended minimum flange width
c) Chemical Composition PVC2
d) Sheet or Formed Blister Formed blister1
Coating
a) Application Thickness 0.50 lb/MSF min to 0.75 lb/ MSF max (aqueous); 0.85 lb/MSF min to 1.20 lb/ MSF max (solvent)
b) Coating Type Solvent or aqueous
c) Application Method In-line press coating or off-line coating; Mayer rod for lab testing aqueous coating; Mayer rod for lab testing solvent coating
Board Board formulated for blister application
Ink Ink formulated for blister application
Drying Hot air for aqueous and solvent coatings
Forming Seals
a) Apparatus Commercially available heat seal machine in good operating condition with the rubber on the seal tray surface having a hardness ranging from 50 to 90 durometer
b) Pressure Minimum face pressure of 80 psi on seal area
c) Interface Temperature 200˚F to 220˚F for aqueous coating; 200˚F to 220˚F for aqueous coating
d) Seal Time (Dwell) Optimized to achieve proper interface temperature
E. Parameters for Heat Sealing
1 Flange should be no less than 40% of original thickness after thermoforming. Blisters should be well formed with a tight cavity radius
2 Other Materials such as PET, PETG, and Polystyrene could require different coatings and may have different performance results.
1 0 | A S S O C I A T I O N O F V I S U A L P A C K A G I N G M A N U F A C T U R E R S
B L I S T E R C A R d S E A L I N G G U I d L I N E S
Interface temperature and pressure are considered critical metrics in the
heat sealing process. The ultimate objective is to ensure intimate contact
between the components for the purpose of transferring sufficient energy
to effect a good heat seal by activation of the blister card adhesive.
Achieving a proper seal is dependent on multiple factors such as coating
type, blister card thickness, blister flange thickness, heat seal surface
material composition, face pressure, and seal (dwell) time. Heat and
pressure sensing materials are available.
To measure interface temperature: 1) place thermal sensitive heat tape
between the blister flange and blister card and 2) apply heat and pressure.
The heat tape will indicate the maximum temperature reached.
To measure interface pressure: 1) place pressure sensing materials
between the blister flange and the blister card without heat and
2) apply pressure. The pressure sensing material will indicate the
maximum pressure achieved. This is shown by color; follow the
manufacturer’s supplied documentation.
In the absence of pressure sensing materials, the face pressure can be
calculated by dividing the pressure at the sealing face by the area of the
sealing face.
F. Determining Interface Temperature and Pressure
1 1 | A S S O C I A T I O N O F V I S U A L P A C K A G I N G M A N U F A C T U R E R S
B L I S T E R C A R d S E A L I N G G U I d L I N E S
1. Purpose
1.1. The purpose of this procedure is to establish a method to determine
the integrity of a sealed, thermoformed blister to a blister card by both
a Manual Method and a Machine Method. This will provide a real world
test that can be accepted and used by material suppliers, machine
suppliers, package assemblers, and their quality departments to agree
on acceptance or rejection of a blister package.
2. Scope
2.1. This test method measures the strength of the seal at the pigment
coated paperboard and blister flange juncture.
2.2. This test method covers low-density, solid bleached sulfate board and
recycled board.
2.3. This test method includes Rigid PVC, PETG, Polystyrene, and PET films.
2.4. The Manual Method visually establishes the integrity of a seal by
evaluating the degree of fiber tear achieved.
2.5. The Machine Methods measure the maximum force required to tear a
coated blister card from a thermoformed blister.
2.6. This test method identifies the various modes of system failure.
2.7. This guideline does not cover materials such as foil, plastic, or other
types of impervious stock.
2.8. This standard does not purport to address the cause of the failure.
G. Standard Procedure for Determining the Integrity of the Blister Seal on a Visual Carded Package
1 2 | A S S O C I A T I O N O F V I S U A L P A C K A G I N G M A N U F A C T U R E R S
B L I S T E R C A R d S E A L I N G G U I d L I N E S
3. Referenced Documents
3.1. TAPPI Standard: T 402
Standard Conditioning and Testing Atmospheres for Paper, Board, Pulp
Handsheets, and Related Products.
3.2. ASTM Standard: E 691
Practice for Conducting an Interlaboratory Study to Determine the
Precision of a Test Method.
4. Terminology
4.1. Definition of terms specific to this standard
4.1.1. Blister Package - a finished package formed by heat sealing
a thermoformed blister to a pigment coated paperboard card.
4.1.2. Fiber Tear - the result of a successfully sealed blister to a pa-
perboard card that can visually be confirmed by the attachment
of paper fiber to the blister flange upon separation.
4.1.3. Maximum Seal Strength - the maximum force required to
separate the bond between the blister card and the blister
flange created by the heat sealing process.
4.1.4. Tear Direction - fiber tear inline with the board grain (machine
direction, MD) or across the board grain (cross direction, CD).
1 3 | A S S O C I A T I O N O F V I S U A L P A C K A G I N G M A N U F A C T U R E R S
B L I S T E R C A R d S E A L I N G G U I d L I N E S
5. Discussion
5.1. In both the manual and machine methods, the criteria for a successful
fiber tear is for fiber separation to be present in 85% of the flange seal
area.
5.2. All test samples should be cooled to ambient conditions before manual
or machine tear tests are performed.
5.3. The manual test method provides a qualitative (accept/reject) visual
inspection method. Constraints associated with this method are the
rate of tear, the tear direction, and the repeatability.
5.4. The machine test method provides a quantitative (numerical)
inspection method. In this method, the maximum tear force is
calculated by the testing machine from the digitized plot of force
versus grip travel distance.
6. Significance & Use
6.1. Maximum seal strength is a quantitative measure for use in process
validation, process control, and capability. Seal strength is not only
relevant to opening force and package integrity, but to measuring the
packaging process’ ability to produce consistent seals. Seal strength
at some minimum level is a necessary package requirement. At times
it is desirable to limit the strength of the seal to facilitate opening.
6.2. The test sample will fail at the weakest point. This point may not
necessarily be the seal. Other modes of failure constitute constraints
that can prevent the method from indicating the true strength of the
seal. This methodology is not intended to include the myriad of causes
for the failure modes.
1 4 | A S S O C I A T I O N O F V I S U A L P A C K A G I N G M A N U F A C T U R E R S
B L I S T E R C A R d S E A L I N G G U I d L I N E S
6.3. The intent of this test is to determine the seal strength by measuring
the force required to initiate a separation at the board pigment coating/
substrate interface. Essentially, this is the goal of package design.
This is accomplished by pulling on the ends of a strip of material
containing the seal. However, the pulling process may or may not result
in the desired mode of strip failure. Extension of the sample ends can
cause one or more failure modes within the sample.
6.4. When a seal fails at the pigment coated/substrate interface (fiber tear),
the value of the bond strength measured is recorded. A failure at this
interface is considered to be a successful seal. (See “Fiber Tear” section 4.1.2, Terminology)
6.5. Other failure modes do exist and represent a limiting factor in the
strength of the package. These failure modes should also be recorded.
The value obtained for seal strength can be affected by properties of
the sample other than seal strength. (These failure modes are discussed in section 11, Failure Modes)
7. Apparatus
7.1. Testing Machine
7.1.1. A tensile testing machine of the constant rate-of-grip-separation
type is to be used. The grips must move a sufficient distance
to strip the blister flange area. The rate of separation of the
grips shall be uniform and capable of adjustment from approxi-
mately 50 to 300 mm/min (2 to 12 in/min). The gripping system
shall be capable of minimizing sample slippage and applying an
even stress distribution to the sample.
7.1.2. The calculation of maximum seal strength is required. The
testing machine system shall have the capability to calculate its
value over a specified range of grip travel, programmable by the
operator. Preferably, the machine shall have the capability also
to plot the curve of force versus grip travel distance.
1 5 | A S S O C I A T I O N O F V I S U A L P A C K A G I N G M A N U F A C T U R E R S
B L I S T E R C A R d S E A L I N G G U I d L I N E S
8. Sampling
8.1. The number of test specimens shall be randomly chosen to permit
adequate determination of representative performance. Sealed test
samples should be examined for any defects. Noted defects can provide
an insight into malfunctions in the sealing process. Defective samples
should be excluded from testing.
9. Sample Conditioning
9.1. Before samples are tested they should be conditioned to 50 +/-2% R.H.
at 23.0 +/-1˚C (73.4 +/-1.8˚F), reference TAPPI T 402.
10. Procedure
10.1. Manual Method
10.1.1. This test should be performed on 3 to 5 samples.
10.1.2. To prepare a sample for testing, the blister package should
be cut with a utility knife in a cross cut pattern. These cuts
are to be made through the back of the card into the blister
cavity. They should extend across the blister flange to the
outer edges of the card. (See Figure #1)
10.1.3. At the intersection of the cut lines, the corner of each
quadrant should be folded back slightly to afford an area
to grip that particular quadrant. (See Figure #2)
FIGURE 1
FIGURE 2
FIGURE 3
1 6 | A S S O C I A T I O N O F V I S U A L P A C K A G I N G M A N U F A C T U R E R S
B L I S T E R C A R d S E A L I N G G U I d L I N E S
10.1.4. Each quadrant of the cut card is then torn from the blister
by hand in a direction toward the corner at an approximate
angle of 45˚. (See Figure #3)
10.1.5. Each quadrant should be torn at a moderate rate to ensure
consistency in the test. Care should be taken since fluctuations
in tear rate can result in deviation of fiber tear results.
10.1.6. The entire perimeter of the flange/paperboard interface
should be visually examined to determine the extent of
acceptable fiber tear (AFT). The percentage of acceptable fiber
tear should be caculated around the total flange. For example,
if the total flange circumference (TFC) is 12 inches and the
acceptable fiber tear circumference (AFTC) is 8 inches, then
the percentage of acceptable fiber tear (%FT) equals 67%
(%FT = AFTC/TFC).
10.2. Machine Method – Sample Preparation
This method is suggested for field testing of production runs.
10.2.1. This test should be performed on 3 to 5 samples.
10.2.2. This test method can be used in the field (a production
environment) or in a laboratory environment.
10.2.3. This test method can be used on packaging of various card
and blister sizes.
10.2.4. The one constraint in this test method is that the blister profile
(height) must be tall enough to cut the top off the blister and
still leave an upright blister tab of at least a minimum of
0.5 inch (one half inch) long. This 0.5 inch long blister tab
is required by the upper grip to pull at a 90-degree angle.
FIGURE 1
FIGURE 2
FIGURE 3
1 7 | A S S O C I A T I O N O F V I S U A L P A C K A G I N G M A N U F A C T U R E R S
B L I S T E R C A R d S E A L I N G G U I d L I N E S
10.2.5 To prepare the sample for testing, make a cut in the blister
profile approximately 0.5 inch long. The initial cut can be
made with a razor blade. (See Photo #1) Then insert a scissor
into the cut and proceed to cut around the entire blister cavity.
(See Photo #2)
10.2.6. Cut a 1 inch cross section from sample card. This cut should
extend to the outer perimeter of the card. (See Photo #3)
10.2.7 This method provides a system for checking the tear
direction with the board grain (machine direction MD) or
across the board grain (cross direction CD)
10.3 The Test Procedure
10.3.1 Calibrate the machine according to the manufacturer’s
specifications.
10.3.2 Place the sample horizontally in the lower fixture of the
machine with the blister tab perpendicular to this fixture and
held in position by the upper grip. The card is held to the
lower fixture by a clamp. Allow sufficient slack so that the seal
is not stressed prior to initiation of the test. (See Photo #4)
10.3.4 The seal shall be tested at a grip separation rate of 10mm/mm.
(4in/mib) With this test method, the one inch test strip can be
cut in both the x and Y orientation.
10.3.5 For each tab, record the maximum force encountered as the
seal is stressed to failure and identify the mode of failure.
Photo 1
Photo 2
Photo 3
Photo 4
1 8 | A S S O C I A T I O N O F V I S U A L P A C K A G I N G M A N U F A C T U R E R S
B L I S T E R C A R d S E A L I N G G U I d L I N E S
11. Failure Modes
FT (Fiber Tear) Fiber tear at the board pigment coating/
substrate interface.
PCS Cohesive failure of the board pigment coating
(Pigment Coating Split) (typically clay).
ACIS Fracture or bond failure between the blister
(Adhesive Coating/Ink Split) adhesive coating and the printed ink film.
BAF (Blister/ Fracture or bond failure between the thermo
Adhesive Coating Split) formed blister and the heat reactive, blister
adhesive coating.
BLIS
TER
ADH
ESIV
E C
OAT
ING
FAILURE
BLIS
TER
ADH
ESIV
E C
OAT
ING
INK
FILM
FAILURE
BLIS
TER
ADH
ESIV
E C
OAT
ING
INK
FILM
PIG
MEN
T C
OAT
ING
FAILURE
BLIS
TER
ADH
ESIV
E C
OAT
ING
INK
FILM
PIG
MEN
T C
OAT
ING
SUBS
TRAT
E
FAILURE
1 9 | A S S O C I A T I O N O F V I S U A L P A C K A G I N G M A N U F A C T U R E R S
B L I S T E R C A R d S E A L I N G G U I d L I N E S
INTER
B B B B B NO O O O O Base A
Blister N Blister N Ink N Second N First N Sheet LD Coating D 4 - Color D Clay D Clay D Paperboard
Coating Coating No Coating PE D C B A L
YBOND
Internal Plybond of Paperboard Bond C = Bond of Ink to Second Clay CoatingBond A = First Clay Coating Bond to Paperboard Bond D = Bond of Blister Coating to Ink and Second Clay CoatiBond B = Second Clay Coating Bond to First Clay Coating Bond E = Bond of Blister to Blister Coating
Heat Seal Diagram
BOND E > BOND D > BOND C > BOND B > BOND A > INTERNAL PLYBOND
15
Heat Seal Diagam
12. Report
12.1. Complete identification of material being tested.
12.2. Conditions and equipment used to form seals.
12.3. Blister flange width.
12.4. Grain direction of board in relation to direction of pull.
12.5. Equipment used to test the seals.
12.6. Grip separation rate.
12.7. Report the number of samples tested.
12.8. Report the maximum seal strength for each tab in Newtons
per centimeter of width to three significant places or other
acceptable units to the same degree of accuracy.
12.9. Report the mode of failure for each tab. More than one mode
of failure can occur during testing.
Heat Tapes can be ordered from:
Paper Thermometer Co., Inc.
603.547.2034
web: paperthermometer.com
email: [email protected]
Pressure Film can be ordered from:
Sensor Products, Inc.
973.884.1755
sensorprod.com
2 0 | A S S O C I A T I O N O F V I S U A L P A C K A G I N G M A N U F A C T U R E R S
B L I S T E R C A R d S E A L I N G G U I d L I N E S
Recommendation
The association recommends using the machine method wherever possible.
The use of this method provides a system for monitoring and measuring
the sealing process though the collection of meaningful data. This collection
of historical data can provide confidence and predictability in the future
performance of the process. It is also suggested that statistical process
control tools be used to convert the historical data to sealing process
tolerances and capability.
For more information regarding
the Seal Master Machine SM-500,
please contact:
Cheminstruments, Inc.
510 Comercial Drive
Fairfield, OH 45014
Phone: 513.869.1598
2 1 | A S S O C I A T I O N O F V I S U A L P A C K A G I N G M A N U F A C T U R E R S
B L I S T E R C A R d S E A L I N G G U I d L I N E S
Troubleshooting
The purpose of this procedure is to assist you in the resolution of a
customer-sealing problem.
Determine which blister coating is being used and the type of blister
material - PVC or RPET. If the customer is using a blister coating and either
of these blister types, you can be pretty sure that the problem is the sealing
process. Most sealing compounds are very forgiving and will seal on most
plastics if proper sealing protocols are followed. In most cases, you will find
that the problem is not card related.
You can determine if the blister is PVC or PET/RPET material by several
simple tests as follows: 1) crease a PVC blister and it will turn white at the
crease, or 2) burn it and it will smoke and char (blacken) badly. The PET
or RPET material will not char and will turn white in the heated area. It will
also drip. Blister gauge should be at 0.0075’’ min to 0.0300” max thickness
before thermoforming. Flange width should be 0.312” minimum.
If there is a question regarding the type of coating, you can conduct a simple
test. Put a few drops of ammonia on the blister coating and let it remain
there five or ten minutes, and then wipe it off. If it “eats” into the coating,
the coating is an aqueous coating. If it does not destroy the coating, the
coating is a solvent coating.
Your investigation should begin with the sealing process trilogy: 1) time,
2) temperature, and 3) pressure. The one element that must be maintained
in the sealing of a blister card is the interface temperature. Blister coatings
are designed to be reactivated at very specific temperatures. The blister
coating will reactive at 180-190 °F and the AquaSeal will reactive at
190-205°F.
This reactivation of the coating creates a hot sticky mass known as “hot
tack” wherein this hot mass sticks to the plastic blister and as the coating
cools the bonding of the blister and card takes place.
2 2 | A S S O C I A T I O N O F V I S U A L P A C K A G I N G M A N U F A C T U R E R S
B L I S T E R C A R d S E A L I N G G U I d L I N E S
If too much heat is applied, or the dwell time is excessive, the blister coating
viscosity will be reduced and the coating will penetrate into the card leaving
insufficient coating on the card surface to adhere to the blister. Of course
the dwell time must be long enough to reactivate the coating.
Heat tapes are used to determine the interface temperature. See the
photographs on left:
The card is then turned over and placed in the tray face down. The
sealing process commences. The last square on the tape that turns black
determines the interface temperature. Occasionally, the placement of the
tapes will not be in line with the flange area. The result is that you will not
get a reading. The tape must have pressure on it to work.
The next step is to take your pyrometer and check the heat platen. Usually,
the temperature on the machine-reading indicator varies from the true
reading of the heat platen. Also, check the platen in different areas. The
platen could have a burned element that causes a fluctuation in sealing
around the flange area. If the situation allows, the heat platen can be taken
off the sealing machine, laid on a flat surface, and checked for warping with
a straight edge placed diagonally on the platen.
Look at the unsealed area of the blister flange that is not sealing. If it’s
“glossy” like the unsealed areas of the entire card, you can assume that
there is no pressure or heat being applied in the flange area. If the configu-
ration of the blister allows it, turn a new blister around in the tray and see if
it fails in the same area. If the failure moves to a different area, it could be a
blister problem. Also, note how many cavities are being sealed at one time.
Now is the time to check the platen pressure with your pressure film.
2 3 | A S S O C I A T I O N O F V I S U A L P A C K A G I N G M A N U F A C T U R E R S
B L I S T E R C A R d S E A L I N G G U I d L I N E S
The photographs to the left demonstrate the process of measuring heat
platen pressure using pressure film. The process flows top to bottom.
The first two photographs show two pieces of pressure film. Both have a
glossy and dull side; one piece is opaque, the other is translucent.
The second two photographs show the two pieces put together: 1) film put
together dull side to dull side and 2) film put into the tray on top of a blister
with opaque piece on the bottom, dull side facing up with translucent piece
on top and dull side facing down. To register a reading, the film must be
placed dull side to dull side.
The last two photographs show the card placed face down over the two
pieces of pressure film. The sealing machine is put in motion and the results
are shown in the last photograph on the right. The translucent top piece of
pressure film usually sticks to the face of the card and resulting pressure
shows up on the bottom opaque piece. A minimum face pressure of 80psi
is required in the face area.
Any light colored areas on the opaque piece indicate a lack of heat platen
pressure on that area of the card. Incidentally, wooden trays are noted
for this problem because they warp badly with the fluctuation of relative
humidity in the atmosphere. If the problem is on a carousel sealing machine,
check the rails and tray fixtures for the degree of vertical fluctuation.
Heat platens can either be milled tooling or flat head platens. The milled
tooling does not put as much heat into the blister card as a flat head platen.
Flat head platens without a Teflon cover can easily burn the back of a blister
card. The rubber or cork used on trays should be checked for damage and
compression caused by too much platen pressure. The rubber on the seal
tray surface should range from 50 to 90 durometer.
Keep in mind that the thickness of the blister card can have a bearing on
the heat transmission through the back of the card. Old blister cards have
a tendency to dry out, therefore temperatures and dwell times will have to
be increased to attain a successful seal.
2 4 | A S S O C I A T I O N O F V I S U A L P A C K A G I N G M A N U F A C T U R E R S
B L I S T E R C A R d S E A L I N G G U I d L I N E S
The board generally used is known as “low density board”, which means it
has a “fluffy” surface so the blister coating can easily bind with the surface
layer of clay coating. Carton board has a hard smooth finish.
See the diagram below and note the various interfaces of a sealed blister
card.
The weakest interface, and the one that should fail, is Bond A to the base
sheet. The fracture at this juncture results in fiber tear (a successful seal).
A failure at any other juncture would be considered a failed seal. If the
bond between Bond A and the base sheet is too strong, it would be a board
problem. The split between Bond B and Bond A (clay split) is often a result of
this situation. With clay spit you will have white coating on the blister flange,
but there will be no board fiber attached.
This is why conducting various lab tests is recommended on all incoming
board before the board goes into production.
One of the most prevalent sealing problems today is the sealing of RPET
blisters (oriented). The plastics used, and the quantities used in the film,
varies greatly. As a result, film properties change from batch to batch. In
addition to this situation, the heat history of the film that the thermoformer
receives has a significant bearing on the thermoforming process used.
INTER
B B B B B NO O O O O Base A
Blister N Blister N Ink N Second N First N Sheet LD Coating D 4 - Color D Clay D Clay D Paperboard
Coating Coating No Coating PE D C B A L
YBOND
Internal Plybond of Paperboard Bond C = Bond of Ink to Second Clay CoatingBond A = First Clay Coating Bond to Paperboard Bond D = Bond of Blister Coating to Ink and Second Clay CoatiBond B = Second Clay Coating Bond to First Clay Coating Bond E = Bond of Blister to Blister Coating
Heat Seal Diagram
BOND E > BOND D > BOND C > BOND B > BOND A > INTERNAL PLYBOND
15
2 5 | A S S O C I A T I O N O F V I S U A L P A C K A G I N G M A N U F A C T U R E R S
B L I S T E R C A R d S E A L I N G G U I d L I N E S
When the thermoformer processes PVC film, a temperature can be used that
is high enough to reach the Glass Transition point. Once past this point, the
film reaches the “Optimum Forming Temperature,” which allows the film to
be stretched and formed without creating orientation or stress.
When processing RPET film, the thermoformer cannot achieve the
“Optimum Forming Temperature” because the film surface will become
crystallized and will not seal. Therefore, the film is processed at a lower
temperature. The result is a formed blister that contains stress, a Cold
Formed blister. Memory remains in the film: during the sealing process,
when heat is applied, the blister flange softens and the stressed film tries
to return to its original shape.
As a result of this stress, the blister flange will 1) ripple and pull away
the card, 2) it will pick off ink from the inside of the blister wall, and
3) the flange will curl back up towards the vertical blister wall.
When dealing with RPET blisters and a sealing problem, you can save time
and effort if you have two pieces of Polarized Film. By placing the blister
between the two pieces of film, one piece at held at 45° angle, you will
immediately see the stress areas in the blister. The stress will show up as
colored rings or areas. The more purple rings that show, the more stress is
present in the blister. Check the flange area in particular. This method, in
many cases, will direct you to the source of the problem immediately. It also
gives you something definite you can show a customer. The technical term
for the purple rings is Birefringence.
Several other points to consider in trouble shooting a sealing problem:
1) the number of cavities on a sealing tray, 2) the shape of the blister (long
narrow flanges can create sealing problems), and 3) thin and narrow flanges
will ripple if too much heat is applied.
avpm-online.com