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Australian Catholic University

Waste Classification and Waste Recovery Assessment

Proposed Carpark, 25A Barker Road, Strathfield, NSW

15 July 2015

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Coffey Environments Australia Pty Ltd ABN: 65 140 765 902

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Waste Classification and Waste Recovery Assessment

Prepared for Australian Catholic University

Prepared by Coffey Environments Australia Pty Ltd 118 Auburn St Wollongong NSW 2500 Australia t: +61 2 4201 1431 f: +61 2 4201 1401 ABN: 65 140 765 902

Project Director Colee Quayle Senior Associate

Project Manager Alex Williams Environmental Engineer

15 July 2015

ENAUWOLL04223AA-R01

Quality information

Revision history

Revision Description Date Author Reviewer

R01 Final 15/7/2015 Alexander Williams

Manuel Fernandez

Distribution

Report Status No. of copies Format Distributed to Date

Final 1 pdf Australian Catholic University Ltd (David Browning)

15/7/2015


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Table of contents

Abbreviations and Definitions............................................................................................................. iv

1. Introduction .................................................................................................................................. 6

2. Project objectives ........................................................................................................................ 6

3. Scope of work .............................................................................................................................. 6

4. Summary of site details and previous investigation .................................................................... 7

4.1. General .............................................................................................................................. 7

4.2. Site identification and setting ............................................................................................ 8

4.3. Site history ......................................................................................................................... 9

4.4. Site observations ............................................................................................................. 10

4.5. Areas of environmental concern and contaminants of potential concern ....................... 11

5. Sampling and analysis .............................................................................................................. 12

5.1. Quality control plan ......................................................................................................... 12

6. Assessment criteria ................................................................................................................... 13

6.1. Virgin Excavated Natural Material ................................................................................... 13

6.2. Excavated natural material .............................................................................................. 14

6.3. Waste classification ......................................................................................................... 14

7. Fieldwork ................................................................................................................................... 15

8. Data validation assessment ...................................................................................................... 16

8.1. Fieldwork quality control procedures .............................................................................. 16

8.2. Laboratory analysis and quality assurance ..................................................................... 16

8.3. Laboratory data validation ............................................................................................... 16

9. Results ....................................................................................................................................... 17

9.1. Subsurface conditions ..................................................................................................... 17

9.2. Laboratory analytical results ........................................................................................... 19

9.2.1. Virgin Excavated Natural Material ...................................................................... 19

9.2.2. Excavated Natural Material ................................................................................ 19

9.2.3. Waste classification ............................................................................................ 20

10. Conclusions and recommendations .......................................................................................... 21

10.1. General ............................................................................................................................ 21

10.2. Virgin Excavated Natural Material ................................................................................... 22

10.3. ENM Exemption .............................................................................................................. 22

10.4. Waste classification ......................................................................................................... 23

10.5. Suggested approach ....................................................................................................... 24

11. References ................................................................................................................................ 25

12. Limitations ................................................................................................................................. 25

Important information about your Coffey Environmental Report ....................................................... 26


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Tables (in text)

Table 1: Site Identification Details ................................................................................................... 8

Table 2: Topography, drainage, geology and hydrogeology ....................................................... 8

Table 3: Summary of site history .................................................................................................... 9

Table 4: Summary of previously identified AECs and COPCs ................................................... 11

Table 5: Adopted background ranges .......................................................................................... 13

Table 6: Generalised subsurface conditions ............................................................................... 18

Table 7 Summary of waste classification and waste recovery areas ........................................ 21

Tables (end of text)

Table LR1: Summary of Laboratory Results for Soil Samples Representing Natural Soils

Table LR2: Summary of Laboratory Results for Soil Samples for Assessing ENM Exemption

Table LR3: Summary of Laboratory Results for Soil Samples for Waste Classification

Figures

Figure 1: Site layout plan and approximate sampling locations

Appendices

Appendix A – Resource Recovery Exemptions

Appendix B – Data Validation Report

Appendix C – Calibration Certificates

Appendix D – Laboratory Reports


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Abbreviations and Definitions

ACM Asbestos Containing Material

AHD Australian Height Datum

ALS ALS Environmental Pty Ltd

AST Above ground storage tank

bgs below ground surface

BH Borehole

BTEX Benzene, Toluene, Ethylbenzene and Xylenes

C6-C36 Hydrocarbon chainlength fraction

CEC Cation Exchange Capacity

COPC Chemical of Potential Concern

CSM Conceptual Site Model

DLWC Department of Land and Water Conservation (NSW)

DQO Data Quality Objective

DQI Data Quality Indicator

EC Electrical Conductivity

ENM Excavated Natural Material

Eurofins Eurofins Environment Testing Australia Pty Ltd, trading as Eurofins MGT

GSW General Solid Waste

ID Identification

LOR Limit of Reporting

µg/L micrograms per litre

mg/kg milligrams per kilogram

mg/L milligrams per litre

NATA National Association of Testing Authorities

NEHF National Environmental Health Forum

NEPM National Environment Protection (Assessment of Site Contamination) Measure

NSW EPA Environmental Protection Authority of NSW

OCP Organochlorine Pesticide

OPP Organophosphorus Pesticide

PAH Polycyclic Aromatic Hydrocarbon

PCB Polychlorinated Biphenyl

PID Photoionisation Detector


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ppm parts per million

QA /QC Quality Assurance / Quality Control

RPD Relative Percent Difference

SOP Standard Operating Procedures

SWL Standing Water Level

TPH / TRH Total Petroleum Hydrocarbon / Total Recoverable Hydrocarbons

VENM Virgin Excavated Natural Material

VHC Volatile Halogenated Compounds

VOC Volatile Organic Compound

Waste Classification and Waste Recovery Assessment 25A Barker Road, Strathfield, NSW

Coffey ENAUWOLL04223AA-R01 15 July 2015

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1. Introduction

Australian Catholic University (ACU) is redeveloping a portion of the Strathfield Campus located at 12A Barker Road, Strathfield, NSW (the ‘site’). The proposed development comprises a single level basement accessible via driveways located on the northern and southern sides. ACU has estimated 33,700m

3 of soil and rock will be excavated and removed offsite to accommodate the basement.

ACU has indicated there is potential that some excavated material could be reused onsite during the development.

Coffey has previously carried out Phase 1 and Phase 2 contamination assessments and a geotechnical assessment across the broader Strathfield Campus. Relevant information from these investigations has been used as part of this waste classification and resource recovery assessment.

To assist with the development process, ACU commissioned Coffey to carry out a waste classification and resource recovery assessment at the site. This work was carried out in general accordance with our proposal (Ref: ENAUWOLL04223AA-P01, dated 24 April 2015) and agreed variations approving additional laboratory analysis of selected samples. This report includes the findings of this assessment.

2. Project objectives

The project objectives were as follows:

Assess the surplus fill material for compliance with the Resource Recovery Exemption – ENM Order (2014);

Assess if natural undisturbed material, would meet the definition of Virgin Excavated Natural Material (VENM) and if so, provide a report to support offsite use of this type of surplus material; and

Provide a waste classification for material that does not classify as ENM or VENM.

3. Scope of work

To meet the project objectives, the following scope of work was carried out:

Review of three available reports previously prepared by Coffey

A site walkover to visually assess potential new sources of contamination present since the previous investigation

Collection of soil samples from 22 test pit locations and making observations of subsurface conditions. Soil samples were also collected in duplicate and screened for Volatile Organic Compounds (VOC) using a Photoionisation Detector (PID).

Laboratory analysis including;

45 samples for analytes specified in the ENM Order 2014, including total recoverable hydrocarbons (TRH), benzene, toluene, ethylbenzene and xylenes (BTEX), polycyclic aromatic hydrocarbon ( PAH), heavy metals (arsenic, cadmium, chromium, copper, lead, mercury, nickel and zinc), electrical conductivity, pH, foreign materials and asbestos.



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Selected additional samples were analysed for a suite of COPCs including heavy metals, petroleum hydrocarbons, polychlorinated biphenyls (PCBs), organochlorine pesticides (OCP), organophosphorus pesticides (OPP), herbicides and volatile halogenated compounds (VHCs).

Preparation of this report summarising relevant parts of the previous reports, results of fieldwork, presenting and interpreting analytical results and findings, comparing chemical concentrations to applicable assessment criteria and making conclusions and recommendations with respect to the objectives outlined in Section 2.

4. Summary of site details and previous investigation

4.1. General

Coffey completed a geotechnical and contamination assessments previously at this site and in other parts of ACU Strathfield campus. The following previous reports were reviewed as part of this investigation:

Coffey Environments Australia Pty Ltd (2011) Phase 1 Environmental Site Assessment (report ref: GEOTLCOV24279AA-AG, dated 13 December 2011)

Coffey Environments Australia Pty Ltd (2012) Phase 2 Contamination Assessment (report ref: GEOTLCOV24279AB-AD, dated 29 February 2012)

Coffey Geotechnics Pty Ltd (2012) Geotechnical Investigation (report ref: GEOTLCOV24279AB-AC , dated 5 March 2012)

The objective of the Phase 1 (2011) assessment was to assess the potential for contamination to be present on the site from previous site activities with respect to its proposed land use. The assessment was required as part of a proposed development within the ACU owned property and included other areas outside the site. These other areas have not been summarised in this assessment. The scope of work developed to meet this objective included a review of available site history information, review of published information, and a site walkover. Within the current site, three areas of environmental concern (AECs) and associated chemicals of potential concern (COPCs) were identified (See Section 4.5) and recommendations were made to carry out further assessment.

A subsequent Phase 2 (2012) assessment was carried out to further assess the nature and extent of petroleum contamination around underground storage tanks (USTs), and further assess the identified AECs for potential contamination. A geotechnical investigation was also carried out at this time. Several boreholes were drilled through the current site, and selected soil samples were tested for COPCs.

The following sections summarise the relevant sections of the previous Phase 1 and Phase Contamination Assessments (2011 and 2012a) and geotechnical investigation (2012b).



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4.2. Site identification and setting

General information pertaining to the site is summarised in Table 1. The topography, drainage, geology and hydrogeology associated with the site is summarised in Table 2. The site layout is shown on Figure 1. Table 1: Site Identification Details

Site name: ACU Strathfield Campus

Site address: 12A Barker Road, Strathfield, NSW

Title identification details:

Part Lot 11 DP869042

Site ownership: Australian Catholic University Ltd

Site area: 1.1ha

Local government area:

Strathfield

Zoning: Special Uses (ecclesiastical – Mount St Mary College)

under the Strathfield Planning Scheme Ordinance as amended by LEP

89 gazetted 16/07/1999.

Adjoining land uses: North: Educational (St Patricks College), Edgar Street and then Residential properties

East: Sports playing fields (within ACU property)

South: Southwest carpark (within ACU property), Barker Road and then residential properties

West: Residential properties

Site coordinates: 321922E; 6250044N (north-eastern corner of the site)

Table 2: Topography, drainage, geology and hydrogeology

Elevation: Approximately 20m above Australian Height Datum (AHD)

General slope direction:

Level playing fields.

Based on recent observations, the surrounding topography slopes down to the north-east, and south-west suggesting the playing fields are on a localised crest or ridge.

Soil landscape: Blacktown soil landscape group

Geology: Overlapping Bringelly Shale, Minchinbury Sandstone and Ashfield shale

Groundwater bore search:

No registered bores within 500m of the site.

Expected groundwater flow direction:

South towards Cooks River

Expected depth to groundwater:

Between 1m and 4m bgs

Closest surface water body:

Cooks River

Drainage: Surface water that is not absorbed into the ground is likely to follow the topography, flowing into urban drainage pits to the north and south of the site.



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4.3. Site history

Site history information was obtained during the Phase 1 assessment (2011) from several online services maintained by the NSW EPA and WorkCover, aerial photographs, historical titles and Council records. Relevant information from the site history study is summarised in Table 3.

Table 3: Summary of site history

Historical land uses: The site forms part of a larger property owned by various religious and educational institutions since 1823. The site is currently used as a sporting field.

The site has remained largely undeveloped based on aerial photography since 1930. In 1986 aerial photography, widespread disturbance of site soils appears to have occurred. This is likely during recontouring to level the playing fields.

A carpark was developed in the area immediately south of the site between 1986 and 1997. A stockpile of unknown quality and origin appeared in the south-eastern corner of the site at this time. The stockpile may have originated from this part of the site.

Chemical usage: Glyphosate (herbicides) were listed in the Phase 1 as a potential contaminant of concern on vegetated and grassed areas.

Council records and Section 149 Planning Certificate:

No notifications under the Contaminated Land Management Act 1997.

Stored Chemical Information Database (SCID) maintained by WorkCover:

Two listings were noted on the Workcover database indicating USTs were present between 1971 and 1992. Based on available drawings, there were two potential USTs noted and labelled as ‘existing 1000 gallon tank’ and ‘proposed 2600 gallon tank’. This location is approximately 70m further south of the site within the ACU Strathfield campus. Only one UST was located during the Phase 2, suggesting that the second UST was either not installed or may have been removed.

The presence of these USTs is not considered to affect the site as they are well outside the site boundary.

NSW EPA Contaminated Land Register:

No listing.

Protection of the Environment Operations Act 1997 public register:

No listing.



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4.4. Site observations

Site observations were made during fieldwork undertaken between 22 and 23 December 2014. The site features previously observed during previous assessments were relatively unchanged. The main site features included:

The site was level vacant grassed playing fields (Photo 1).

A stockpile was located in the south-eastern corner of the site (Photo 2).

Evidence of filling had occurred in the playing field based on surrounding local topography. The areas surrounding the site to the north-east, west and south-west (Photo 3) were distinctly lower in elevation to the levelled playing fields.

A single ACM fragment was observed during test pitting

No other visible evidence of potentially contaminating activities or indications of contamination (such as oil staining, etc) were observed.

Photo 1 Panoramic photo from northern site boundary looking east and south across the site

Photo 2 Stockpile in south-eastern corner

Photo 3 Evidence of filling in south-western portion of the site



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4.5. Areas of environmental concern and contaminants of potential concern

Three previously identified areas of environmental concern (AECs) and associated Contaminants of Potential Concern (COPCs) are considered to be applicable to the current investigation site and have been summarised in Table 4. These were identified based on site history information and site observations made during the Phase 1 (2011). We note that other AECs identified applied to other parts of the ACU property away from the site and are considered not applicable to this assessment. Further AECs were not identified based on the more recent observations made during this investigation (refer to section 4.4).

Table 4: Summary of previously identified AECs and COPCs

AEC #

Description Area Potentially Impacted during this investigation

Likelihood of contamination*

COPCs

1 Stockpile of unknown source and composition situated at the western end of the site (northeastern corner of the southwest car park) (potentially containing ACM fragments, SMF, construction waste)

Soils beneath the stockpile will be excavated as part of the proposed carpark. At the request of ACU, the stockpiled material was excluded from this waste classification and waste recovery assessment.

The Phase 2 assessment identified contamination within several samples collected within this stockpile, including heavy metals, benzo(a)pyrene and other PAHs.

Low to moderate TRH, BTEX, PAH, OCP, OPP, PCB, metals**, asbestos

2 Vegetated and grassed areas

The application of herbicides was suspected to have occurred. No soil samples were tested for herbicides during the Phase 2 assessment. Given the grassed areas are used as a playing field, there is a potential that herbicides may have been used at the surface to control weed growth. Impact (if any) would be generally limited to the ground surface.

Low Glyphosate (herbicides)

3 Areas of fill potentially under the playing fields

During previous geotechnical investigations (2012b), widespread fill was encountered at several borehole locations within the site to depths ranging between 0.3m and 2.4m. The origin and quality of the fill was unknown, however soil descriptions suggested they may have comprised reworked natural soils. Selected soil samples in the upper 0.2m were tested for COPCs at three locations (BH102, BH115 and BH117). Reported concentrations did not indicate contamination at these locations.

Low to moderate TPH, PAHs, VHCs, heavy metals, asbestos

Table 4 notes:

* It is important to note that this is not an assessment of financial risk associated with the AEC in the event contamination is detected, but a qualitative assessment of the probability of contamination being detected at the potential AEC, based on the site history study and field observations.

** Metals includes arsenic, cadmium, chromium, copper, lead, nickel, mercury, zinc



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5. Sampling and analysis

The resource recovery exemption (The ENM Order 2014) requires a minimum of 22 sampling locations for an area of about 1.1ha. We collected soil samples from 22 test pit locations spread out in an approximate grid across the site. These locations were also considered to target the previously identified AECs and COPCs which applied broadly to the ‘playing fields’.

Vertically, samples were collected in accordance with Table 3, page 4 of the “Excavated Natural Material (ENM) Order 2014”. We collected between one and four samples down the vertical profile at each location, based on fill thicknesses ranging from 0.2m to 2.6m respectively. Test pits were used to facilitate sampling and extended at least 0.4m past the base of fill into natural soils. A copy of the resource recovery exemptions for “ENM Order 2014” is included in Appendix A.

Laboratory analysis included;

45 samples for analytes specified in the ENM Order 2014, including total recoverable hydrocarbons (TRH), benzene, toluene, ethylbenzene and xylenes (BTEX), polycyclic aromatic hydrocarbon ( PAH), heavy metals (arsenic, cadmium, chromium, copper, lead, mercury, nickel and zinc), electrical conductivity, pH, foreign materials and asbestos.

Selected additional samples were analysed for a suite of COPCs including heavy metals, petroleum hydrocarbons, polychlorinated biphenyls (PCBs), organochlorine pesticides (OCP), organophosphorus pesticides (OPP), herbicides and volatile halogenated compounds (VHCs).

We consider the sampling frequency is also acceptable for assessment of VENM and waste classification.

It was not considered necessary to analyse samples for PCBs and VHCs in natural soil because this was not a primary COPC.

5.1. Quality control plan

A quality assurance/quality control plan was designed to achieve the predetermined data quality objectives (DQOs) and to demonstrate accuracy, precision, comparability, representativeness and completeness of the data generated and the procedures for assessing the DQOs are met. The Data Quality Indicators (DQIs) adopted to assess DQOs are outlined in the data validation report presented in Appendix B.



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6. Assessment criteria

6.1. Virgin Excavated Natural Material

To classify natural soils as Virgin Excavated Natural Material (VENM) they must meet the following definition:

“Virgin excavated natural material means natural material (such as clay, gravel, sand, soil or rock fines):

that has been excavated or quarried from areas that are not contaminated with manufactured chemicals, or with process residues, as a result of industrial, commercial, mining or agricultural activities

that does not contain sulfidic ores or soils, or any other waste, and includes excavated natural material that meets such criteria for virgin excavated natural material as may be approved from time to time by a notice published in the NSW Government Gazette.”

By definition, VENM cannot be ‘made’ from processed soils. Excavated material that has been stored

or processed in any way cannot be classified as VENM.

For this site, a combination of chemical characterisation, site history and observations were used to

support a VENM classification.

Consideration of background concentrations are required as part of assessing if soils meet the definition of VENM. The background concentrations published by South Australian Health Commission (1995) for new suburbs and low traffic areas were used to provide a general reference for heavy metals expected in natural soils. For anthropogenic based organic contaminants, such as petroleum hydrocarbons, concentrations must be below laboratory reporting limits. Laboratory results were compared to adopted background concentrations which are listed in Table 5 below.

Table 5: Adopted background ranges

Contaminant of Concern Published background range (mg/kg)

Arsenic 5 to 111

Cadmium 0.251

Chromium 6 to 211

Copper 6 to 321

Lead 13 to 441

Nickel 5 to 501

Mercury 0.051

Zinc 17 to 771

Petroleum hydrocarbons (TRH, BTEX, PAH) < LOR

Pesticides (OCP / OPP) < LOR

PCB < LOR

Asbestos < LOR / Not present

Table 5 notes:

1. NSW soils for new suburbs in low traffic areas listed on page 17 (South Australian Health Commission (1995)). Only adopted for imported materials as a general reference. Depending on source of material, other reference data may be adopted.

LOR = Laboratory reporting limit



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6.2. Excavated natural material

Fill derived from natural soil and rock (including roadbase beneath existing carpark) and reworked natural soils were assessed in accordance with the “ENM Order 2014” and laboratory results compared to criteria listed in Table 4, page 5 of the Order. Criteria are also listed in Table LR2.

In addition to listed criteria, fill material must be excavated natural material, which is defined as:

“...naturally occurring rock and soil (including but not limited to materials such as sandstone, shale, clay and soil) that has:

a. been excavated from the ground, and

b. contains at least 98% (by weight) natural material, and

c. does not meet the definition of Virgin Excavated Natural Material in the Act.

Excavated natural material does not include material located in a hotspot; that has been processed; or that contains asbestos, Acid Sulfate Soils (ASS), Potential Acid Sulfate soils (PASS) or sulfidic ores.”

6.3. Waste classification

The waste classification of site soils was undertaken in general accordance with the six step procedure for classifying waste as detailed in the Waste Classification Guidelines - Part 1: Classifying Waste (NSW EPA (2014)).

Laboratory results were compared to waste classification criteria which are listed in Table LR3.



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7. Fieldwork

Field investigations were carried out between 22 and 23 June 2015 by a Coffey environmental engineer.

A 3.5 tonne rubber tracked excavator fitted with a 300mm bucket was used to collect soil samples at each sampling location. Samples were collected from within soils that had not come in contact with the excavator bucket. All soil samples were collected with a new pair of nitrile gloves.

Soil samples were generally collected at the surface, in the fill at a rate of 1 sample every 1m, as per the requirements of the ENM Order 2014. Additional soil samples were collected where evidence of odours or staining was noted (if observed). Clean 250mL glass jars were filled with soil to the brim and immediately sealed with Teflon lined caps to lower the potential for loss of volatile contaminants. Samples were then labelled and placed directly into ice filled cooler boxes. Soil required for asbestos testing was placed in a plastic zip-lock bag. Material fragment samples were placed directly into a zip-lock bag.

A bulk sample of approximately 10kg was collected at selected locations for the purposes of foreign materials testing. The bag was labelled and secured with a rubber band.

Soil samples for analysis were collected in duplicate into tightly sealed plastic bags. The headspace above each sample was measured using a Mini Rae Lite PID fitted with a 10.6eV lamp and calibrated with isobutylene gas at a concentration of 100ppm. This instrument allows rapid, semi quantitative analysis of ionisable volatile organic compounds in the soil.

The sampling locations were measured with a GPS device and relative positions confirmed with existing site features. Sampling locations are shown in Figure 1. Subsurface conditions were recorded on field logs including depth of fill, groundwater inflows and results of soil headspace screening.



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8. Data validation assessment

8.1. Fieldwork quality control procedures

The field quality control was generally in accordance with the DQOs and DQIs and consisted of:

Sampling was performed by a qualified Coffey environmental professionals generally in accordance with the procedures outlined in Coffey’s Standard Operating Procedures (SOPs) which are based on industry accepted protocols for environmental sampling and are consistent with Schedule B(2) of the National Environment Protection (Assessment of Site Contamination) Measure (NEPM) 1999, amended 2013. Sampling activities were carried out by Coffey staff who had completed Coffey’s training for Coffey SOPs including supervised field training;

Calibration of field instruments in accordance with manufacturer’s instructions. The calibration certificates are included in Appendix C;

Collection and analysis of four blind coded duplicates and two triplicate samples. Relevant laboratory results and calculated Relative Percent Differences (RPDs) are presented in Table QAQC1 in Appendix B. Duplicate and triplicate results are also presented in the results Tables LR1 to LR3;

Hand tools were not required during soil sampling and therefore no rinsate samples were collected.

One laboratory prepared trip spike and trip blank samples were carried into the field and despatched to the laboratory for analysis of volatile contaminants to check the potential for cross contamination or loss of volatile contaminants during transport and sample preparation at the laboratory. Results are presented in Table QAQC2 in Appendix B; and

Samples (as designated on the chain of custody form) were transported in ice-cooled chests to Eurofins | MGT Pty Ltd (Eurofins) and ALS Environmental Pty Ltd (ALS) for analysis. A copy of the chain of custody record is included in Appendix D.

8.2. Laboratory analysis and quality assurance

Laboratory analysis of the primary and duplicate samples was undertaken by Eurofins in Sydney. The triplicate sample was analysed at ALS Environmental in Sydney. Foreign materials testing was carried out by Coffey at Fyshwick, ACT. The laboratories were NATA accredited for the tests performed.

Samples were selected for analysis as per the sampling and analysis plan (refer to Section 5).

Laboratory results are discussed in Section 9.2 and laboratory reports (NATA certified) are presented in Appendix D. Laboratory test methods and holding times applicable for the chemicals analysed are listed in laboratory reports.

8.3. Laboratory data validation

Coffey assessed the laboratory data against predetermined DQOs and DQIs for laboratory procedures and results. This assessment is presented in a data validation report included in Appendix B. Coffey concluded that the analytical results are representative of the characteristics of materials sampled and suitable for the purposes of the contamination and resource recovery assessment.



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9. Results

9.1. Subsurface conditions

The subsurface conditions encountered were similar to those reported by Coffey in 1991 and 2012 geotechnical investigations with fill overlying natural soils. Natural soils comprised residual clays overlying weathered rock.

Fill was encountered across most of the site comprising topsoil and reworked natural soils. Topsoils appeared to have been placed in a uniform thickness (between 0.2m and 0.3m) across the site and were likely to have been imported to site for the grassed playing field. Reworked natural soil was encountered at most locations and was typically thicker in the northern portion of the site. Based on the depths of fill observed and surrounding topography, the playing fields were likely to have been levelled by ‘cutting’ in the south-east and ‘filling’ in the north. Filling also appears to have occurred in the south-west near the paved carpark. A former topsoil layer, buried beneath reworked natural soil, was also encountered as some locations near the western site boundary.

Foreign materials were observed at several locations across the site including;

A layer of fill comprising some demolition debris (bricks, asphalt and concrete blocks up to 0.8m in length) was noted at locations CTP14, CTP18 and CTP19 to depths ranging from 0.4m and 1.3m.

Some ceramic plate and glass fragments, glass bottle, brick, metal rod, electrical wire and plastic were noted at location CTP01, CTP03 and CTP11, to depths ranging from 0.5m to 1.6m.

Traces of bricks and terracotta fragment were also noted in CTP16, CTP21 and CTP22.

A single fibre cement fragment suspected to contain ACM was encountered within reworked natural soil at CTP22 a depth between 0.8m and 1.2m. Apart from this, no other fragments of suspected ACM were observed during this investigation.

A single golf tee was observed in topsoil at CTP10.

During sampling at location CTP06, a thin layer of unusual ‘red’ staining (less than 5cm) was noted at the topsoil/reworked natural interface. Apart from this, no unusual odours or staining/discolouration were observed at sampling locations. Soil samples screened recorded negligible PID readings of less than 2.2ppm, indicating that volatile ionisable compounds were not present. PID results were consistent with laboratory results.

Shallow groundwater inflows were encountered at CTP01 to CTP03, CTP06, CTP15, CTP17, and CTP19 to CTP21 between 0.8m and 1.9m. Except at location CTP01, water inflows were at or near the base of the fill unit. Standing water levels of were measured where rapid inflows occurred; CTP01 (1.6m), CTP17 (1.0m) and CTP20 (2.5m). At CTP17, water inflows were associated with a buried subsurface drainage pipe which was encountered at 0.6m.

The subsurface conditions encountered were generally similar to those reported in previous geotechnical investigations (Coffey 2012). We note the following exceptions where subsurface conditions differed:

Roadbase material was previously encountered to a depth of 0.5m in borehole (BH115) drilled through the asphalt paved carpark. Roadbase materials were not encountered during this investigation. We note that test pits were positioned outside of the asphalt paved carpark at the request of ACU and roadbase material is likely to be limited to the carpark area.



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Fill material was previously logged to a maximum depth of 2.4m in borehole BH101, with standing water level at 2m. During this investigation, a nearby test pit CTP18 encountered shallower fill to a depth of 1.6m (approximately 0.8m higher) and no water inflows were observed. The remainder of test pit locations were generally consistent with depth of fill previously encountered.

The generalised subsurface conditions encountered in previous and current investigations are summarised in Table 6. Natural materials encountered were generally consistent with published

geological information.

Table 6: Generalised subsurface conditions

Soil or Rock Unit

Description Depth range to top of unit below

ground surface (m)

Fill Topsoil Clayey sand, sandy clay and silty clay: dark brown, low to medium

plasticity clay, sands fine to medium grained, that varied in consistency from loose to medium dense (sand) and firm to friable (clay), with some silt. Encountered at each sampling location to depths of 0.2m to 0.35m.

Surface

Fill (reworked natural soil)

Clay: medium to high plasticity, various colours (pale brown, grey,

yellow and red), with some gravel, cobbles and boulders comprising sandstone. Encountered at each location (except CTP02, CTP04, CTP05, CTP08 and CTP09), to depths of 0.4m and 2.5m, respectively.

0.2 to 0.35

Fill (Former topsoil)

Sandy Clay; low to medium plasticity, dark grey, fine to coarse

grained sands, with some organics (roots) and traces of glass and brick encountered at CTP03 and CTP06 to depths of 1.1m and 0.55m respectively.

0.45 to 0.8

Natural Soil (Residual)

Clay: high plasticity, grey/yellow/red mottled. The clay consistency

generally varied between stiff and very stiff. Encountered at each sampling location during this investigation.

Sand; fine to medium grained, brown yellow with some clay.

Encountered during previous investigation at BH101 to depths of 2.6m

0.2 to 2.5

Natural Soil / Rock (Residual/XW Sandstone)

Sandy clay: medium to high plasticity, red/yellow/grey/white mottled

fine to medium grained sand, with some gravel and cobbles comprising sandstone. Encountered at CTP14 and CTP19 to depths greater than 1.7 and 2.6m respectively.

1.3 to 1.9

Natural Rock (XW / HW Sandstone or shale)

Sandstone or shale: XW to HW sandstone or shale was encountered

in previous boreholes BH1-91, BH101 and BH116 to depths greater than 3.0m. XW sandstone was previously encountered described as clayey silt, high plasticity, mottled light red-brown and grey (BH1-91). XW to HW sandstone or shale was described as fine grained, yellow brown or grey/pale grey, very low strength (BH101 and BH116)

1.00 to 2.9

Notes: XW = Extremely Weathered



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9.2. Laboratory analytical results

The laboratory analytical results for soil are summarised in Tables LR1 to LR3. Laboratory reports are included in Appendix D.

9.2.1. Virgin Excavated Natural Material

The laboratory analytical results for soil are summarised in Table LR1. The following comments are made with respect to natural materials encountered onsite:

Soil samples representing residual clay at locations CTP01, CTP04, CTP13, CTP19 and CTP22 have reported one or more heavy metals outside the adopted background range. Elevated heavy metal concentrations were reported in soil sample collected near the top of residual clay (that is, collected between 0.1m and 0.2m deeper than the base of fill). An exception to this was for concentrations of arsenic and lead reported in samples CTP13/0.7-0.8 and CTP19/2.4-2.6, respectively, collected deeper within residual clay (that is, between 0.3m and 0.7m deeper than the base of fill).

The source of the elevated metals within residual clays is unknown. Mercury and zinc detected in residual clays appeared to be associated with elevated concentrations within overlying fill material. The remaining elevated metals (arsenic, chromium, copper and lead) appeared to be higher in concentration within residual clays compared to overlying fill material. Elevated metals were observed to decrease with depth at locations CTP01 and CTP13. This could suggest some influence from overlying fill materials.

Remaining COPCs were below laboratory limits of reporting (LOR).

9.2.2. Excavated Natural Material

The laboratory analytical results for soil are summarised in Table LR2. The following comments are made with respect to the ENM assessment criteria for both natural and fill materials:

Several locations (CTP01, CTP02A, CTP03, CTP04, CTP06, CTP08, CTP10, CTP14, CTP18 and CTP22) recorded one or more heavy metals and/or PAHs above the absolute maximum concentrations within the fill material at various depths. Asbestos was detected in two soil samples (CTP14/1.0-1.2, CTP18/0.0-0.2) and fibre cement fragment sample (CTP22/0.8-1.2 ACM). Based on this criteria, these locations were excluded from the ENM assessment on this basis and classified in accordance with waste classification guidelines.

Concentrations of arsenic and copper exceed the absolute maximum concentration of 40mg/kg and 200mg/kg, at locations CTP13 and CTP01, respectively. These samples represented residual clay soils approximately 0.2m deeper than the base of fill. These locations were excluded from the ENM assessment on this basis and classified in accordance with waste classification guidelines. Deeper samples collected at these locations within residual clay (up to 0.4m deeper than base of fill) did not exceed these thresholds.

The absolute maximum concentrations for TRH (C10-C36) was initially exceeded at locations CTP05, CTP11 and CTP15 within topsoil samples. A subsequent test of TPH (C10-C36) after silica gel cleanup indicated these exceedences were associated with natural hydrocarbons, likely from the organic sources in the topsoil. These exceedences of the absolute maximum concentrations for TRH have therefore been disregarded.



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9.2.3. Waste classification

The remainder of fill soils and residual soils which did not meet the ENM assessment criteria and therefore was asessed for waste classification in accordance with Waste Classification Guidelines - Part 1: Classifying Waste (NSW EPA (2014). The waste classification procedure followed is described below:

Step 1 - Is the waste special waste?: Asbestos in the form of ACM fragments and fibre bundles were encountered at the site at three locations (CTP14, CTP18 and CTP22) within fill soils. At locations CTP18, asbestos fibre bundles were detected in the soil samples collected between 0 to 0.2m (representing topsoil fill). At locations CTP14 and CTP22, fibre cement fragments (containing asbestos) were detected at depths between 0.8 and 1.2m in fill soils where builders rubble was present. The asbestos identified included chrysotile, amosite and/or crocidolite.

The current assessment does not provide sufficient information to delineate the extent of the asbestos but distribution of asbestos suggest it may be associated with builders rubble in this portion of the site. At a preliminary level, we consider that fill soils in the north-western corner of the site designated Area 3 contain asbestos fibres and/or ACM and therefore will classify as Special Waste (Asbestos). These soils will need to be managed accordingly. No asbestos was detected in soils samples collected at the remaining locations onsite.

Step 2 - Is the waste liquid waste?: The material is not a liquid waste in its current form. The material comprised soil and was capable of being picked up by a spade or shovel.

Step 3 - Is the waste pre-classified?: The material is not pre-classified.

Step 4 - Does the waste possess hazardous characteristics?: The material does not possess hazardous characteristics based on the site history, observations and chemical testing as defined under the Australian Code for the Transport of Dangerous Goods by Road and Rail;

Step 5 - Determining a waste’s classification using chemical assessment: The waste has been assessed using chemical analysis. The laboratory analytical results for soil are summarised in Table LR3. The following comments are made with respect to the waste classification criteria for both fill and natural materials:

Specific contaminant concentrations were generally below the CT1 criteria, with the exception of arsenic, lead and PAHs at several locations. These concentrations were below the SCC1 criteria. Further assessment using the toxicity characteristic leachability procedure (TCLP) confirmed that leachable concentrations were below the TCLP1 criteria.

Asbestos in the form of ACM fragments and fibre bundles were encountered at the site at three locations (CTP14, CTP18 and CTP22) within fill soils.

Remaining COPCs did not exceed CT1 criteria.

Step 6 - Is the waste putrescible or non-putrescible: The material consisted predominantly of soil and thus is deemed to be non-putrescible. NSW EPA (2014) notes that materials that are generally not classified as putrescible include soils, timber, garden trimmings, agricultural, forestry and crop materials, and natural fibrous organic and vegetative materials. Based on observations by Coffey, the material is considered to be non-putrescible.

Based on the above some soils classify as General Solid Waste (non putrescible) (to be managed as asbestos) and some soils classify as General Solid Waste (non putrescible). The specific areas to where these classifications apply are discussed in the next section.



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10. Conclusions and recommendations

10.1. General

Based on discussions with ACU, we consider there is opportunity to divide the site into separate areas pertaining to waste classification and waste recovery of excavated soils. We consider that there are four separate areas where soils can be managed according to separate waste as shown on Figure 1. We have assessed the current waste classification and/or waste recovery opportunity in sections 10.210.4 to 10.4. A summary of waste classifications is included in the Table 7 below.

Table 7 Summary of waste classification and waste recovery areas

Soil or Rock Unit

Depth to top of layer (m)

Waste Classification and Waste Recovery Management Area

Area 1 Area 2 Area 3 Area 4

Fill Soil Surface ENM GSW GSW (to be managed as

asbestos waste)

GSW (around CTP01)

ENM (around CTP13)

Natural Soil (Residual Clay / Extremely weathered sandstone)

0.2 to 2.5 ENM ENM ENM GSW

(Depth and lateral extents

subject to validation sampling)

Following excavation a further 0.5m to 0.7m deeper than current level.

Potential VENM (Subject to further assessment)

Natural Rock 1.0 to 2.9 Potential VENM (Subject to further assessment)

ENM = Excavated Natural Material

GSW = General Solid Waste (non-putrescible)

As requested by ACU, this assessment excluded the soil stockpile in the south-eastern corner of the site and our discussion does not apply to this stockpile in any way.



22

10.2. Virgin Excavated Natural Material

Natural materials comprising residual clay and extremely weathered material (sandy clays) were encountered at the site. Residual soils reported elevated heavy metal concentrations outside the published background ranges. With increasing depth, the concentrations of heavy metals appeared to decrease, suggesting the residual soil may have been exposed to human activities. Site history suggested widespread disturbance of site soils as part of recontouring to level the playing fields. This may have resulted in slightly higher concentrations of metals. Therefore, the residual clay is not considered to meet the definition of VENM.

We consider that the upper portion of residual clay could be excavated to approximately 0.5m to 0.7m deeper than the current elevation. The majority of these soils have been assessed and do meet the requirements of ENM, with the exception of two locations within management Area 4 (Refer to Section 10.3). Following excavation of this upper portion, we recommend further assessment of deeper residual soils and underlying weathered rock to confirm whether this soil/rock meets the definition of VENM. This will need verification by an environmental consultant and will require issue of a VENM certificate.

10.3. ENM Exemption

Laboratory results indicate fill soils located in Area 1 satisfy the requirements of the “ENM Order 2014”. This area is shown on Figure 1.

We note that the ENM Order and Exemption provide conditions such as:

The excavated natural material can only be applied to land as engineering fill or for use in earthworks. In the exemption, ‘apply to land’ means applying to land by: spraying, spreading or depositing on the land; or ploughing, injecting or mixing into the land; or filling, raising, reclaiming or contouring the land.

Record keeping requirements are also provided in the Order and Exemption along with responsibilities of the generator and recipient which must be followed. Copies of the ENM Order and Exemption are included in Appendix A and must be read in conjunction with this classification to ensure compliance with the Protection of the Environment Operations (Waste) Regulation 2014.

Fill within Areas 2 and Area 3, do not meet requirements of the “ENM Order 2014” due to heavy metals exceeding the absolute maximum concentration and/or presence of asbestos. In addition, the upper 0.2m of residual clay in Area 4 do not meet the requirements. Therefore, it is recommended that material from these areas is disposed offsite as per the relevant waste classification described in Section 10.4.



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10.4. Waste classification

The remainder of fill soils and residual soils were assessed for waste classification in accordance with Waste Classification Guidelines - Part 1: Classifying Waste (NSW EPA (2014).

Within Area 2, fill soil will classify as General Solid Waste (non-putrescible) because COPCs were

below CT1/SCC1 criteria.

Within Area 3, there were three locations (CTP14, 18, 22) where we found asbestos (2 fibro fragments, 1 fibre bundles), which the laboratory assessed as non respirable. The asbestos identified included chrysotile, amosite and/or crocidolite. The asbestos seems to be in an area where builders rubble was present however the location with fibre bundles were (CTP18), at the surface in topsoil (0.0-0.2m), but still within this same area. The fill soils in Area 3 will classify as General Solid Waste (non-putrescible) (to be managed as asbestos waste). The individual ACM fragments will classify as Special Waste (Asbestos waste). Any excavated material containing asbestos or ACM removed from site from will classify as General Solid Waste (non-putrescible) (to be managed as asbestos waste).

We understand that ACU are considering the potential to reuse some excavated material in other parts of the site during construction. If ACU wish to reuse any of this material from Area 3, we can assess the degree and extent of asbestos contamination in Area 3 with respect to future landuse as a paved carpark. In the meantime, we can prepare an interim site management plan which applies to soils in this area.

Within Area 4, there remains elevated copper (sample CTP01/1.7-1.8) and arsenic (sample CTP13/0.4-0.5) within residual clay above the absolute maximum concentrations of 40mg/kg and 200mg/kg. Deeper samples at these locations reported concentrations below the ENM exemption threshold, suggesting these exceedences were associated with overlying fill. Therefore, the upper 0.2m of residual clay in Area 4 classifies as General Solid Waste (non-putrescible).

We recommend that a specific exemption is requested from the NSW EPA as these contaminants reported only marginal exceedences in a relative minority of samples tested. This may or may not achieve a specific exemption being granted. We also recommend that deeper residual clay in these areas (that is, at least 0.3m deeper than the base of fill) may be assessed further for potential ENM exemption.

The Protection of the Environment Operations (Waste) Regulation 2014 (the Waste Regulation) makes it an offence to transport waste generated in NSW by motor vehicle for disposal more than 150 kilometres from the place of generation, unless the waste is transported to one of the two nearest lawful disposal facilities to the place of generation (even if that facility is located more than 150 kilometres from its place of generation). From 1 July 2015 asbestos loads greater than 100 kg, or more than 10 square metres of asbestos sheeting will require special monitoring requirements. Further advice should be sought from EPA regarding these requirements and if they would apply to soils with asbestos.



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10.5. Suggested approach

Based on the results of this assessment and proposed development, Coffey recommends the following approach to manage identified asbestos contamination and waste segregation:

1. Planning phase:

Preparation of a Site Management Plan for asbestos contamination within Area 3. The recommendations of this plan should be followed, until further assessment confirms whether soils are suitability for onsite reuse. If ACU wish to reuse any of this material from Area 3, we can assess these soils for onsite reuse suitability with respect to future landuse as a basement carpark.

Apply for specific exemption from the NSW EPA for residual clay soils in Area 4 which currently do not meet the requirements of ‘The ENM Order 2014’ due to marginal exceedences of arsenic and copper. Current data may be suitable to obtain a specific exemption, but we note that the process requires a separate submission and can take several weeks for approval.

Preparation of a Remediation and Waste Disposal Work Plan, including an Unexpected Finds Procedure. These planning documents will outline key steps in preventing cross contamination, inadvertent mixing of wastes and what to do if ground conditions differ from those discussed in this report. This can be scaled back or omitted if full time guidance is provided as discussed below.

2. Bulk earthworks and waste segregation:

An environmental consultant guides segregation of material ensuring soils from differed waste management areas are not mixed and that over excavation of underlying ENM (or potential VENM) does not occur. Additional soil sampling may be required to validate the effective removal of layers with different classifications in selected areas.

Once the required depth of residual clay is exposed, deeper residual soils and underlying weathered rock will be assessed to confirm whether this soil/rock meets the definition of VENM. A VENM certificate will be issued for underlying material.



25

11. References

1. Coffey Environments Australia Pty Ltd (2011) Phase 1 Environmental Site Assessment (report ref: GEOTLCOV24279AA-AG , dated 13 December 2011)

2. Coffey Environments Australia Pty Ltd (2012a) Phase 2 Contamination Assessment (report ref: GEOTLCOV24279AB-AD, dated 29 February 2012)

3. Coffey Geotechnics Pty Ltd (2012b) Geotechnical Investigation (report ref: GEOTLCOV24279AB-AC , dated 5 March 2012)

3. NEPC (2013) National Environmental Protection (Assessment of Site Contamination) Measure 1999, as amended in 2013, National Environment Protection Council.

4. NSW DEC (2006) Guidelines for the NSW Auditor Scheme, 2nd

Ed.

5. NSW OEH (2000) Guidelines for Reporting on Contaminated Sites.

6. NSW EPA (2014) Waste Classification Guidelines: Part 1 Classify Waste.

7. Resource Recovery Order under Part 9, Clause 93 of the Protection of the Environment Operations (Waste) Regulation 2014 - The excavated natural material order 2014.

12. Limitations

Limited information is available on the early history of the site and therefore, some site activities may not have been identified. In addition, aerial photographs are up to 25 years apart and other site history information available prior to 1971 is limited. We cannot preclude that potentially contaminating activities took place during these periods. Allowances for uncertainties and potential unexpected finds should be made during planning and development phases.

It is the nature of contaminated site investigations that the degree of variability in site conditions cannot be known completely and no sampling and analysis program can eliminate all uncertainty concerning the condition of the site. Professional judgement must be exercised in the collection and interpretation of the data.

In preparing this report, current guidelines for assessment and management of waste soils were followed. This work has been conducted in good faith in accordance with Coffey understanding of the client’s brief and general accepted practice for environmental consulting.

This report was prepared for Australian Catholic University Ltd based on the objective and scope of work list in Sections 2 and 3. No warranty, expressed or implied, is made as to the information and professional advice included in this report. Anyone using this document does so at their own risk and should satisfy themselves concerning its applicability and, where necessary, should seek expert advice in relation to the particular situation.

In preparing this report, Coffey has relied on information in previous Coffey reports prepared by other persons. Coffey has assumed that these consultants performed the scope of works in general accordance with standard industry procedures and guidance materials at the time and that the information is suitable.

We draw your attention to the attached sheets titled "Important Information about your Coffey Environmental Report" which should be read in conjunction with this report. These information sheets are located at the end of this section.



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Important information about your Coffey Environmental Report

1. Introduction

This report has been prepared by Coffey for you, as Coffey’s client, in accordance with our agreed purpose, scope, schedule and budget. The report has been prepared using accepted procedures and practices of the consulting profession at the time it was prepared, and the opinions, recommendations and conclusions set out in the report are made in accordance with generally accepted principles and practices of that profession. The report is based on information gained from environmental conditions (including assessment of some or all of soil, groundwater, vapour and surface water) and supplemented by reported data of the local area and professional experience. Assessment has been scoped with consideration to industry standards, regulations, guidelines and your specific requirements, including budget and timing. The characterisation of site conditions is an interpretation of information collected during assessment, in accordance with industry practice, This interpretation is not a complete description of all material on or in the vicinity of the site, due to the inherent variation in spatial and temporal patterns of contaminant presence and impact in the natural environment. Coffey may have also relied on data and other information provided by you and other qualified individuals in preparing this report. Coffey has not verified the accuracy or completeness of such data or information except as otherwise stated in the report. For these reasons the report must be regarded as interpretative, in accordance with industry standards and practice, rather than being a definitive record. 2. Your report has been written for a specific

purpose

Your report has been developed for a specific purpose as agreed by us and applies only to the site or area investigated. Unless otherwise stated in the report, this report cannot be applied to an adjacent site or area, nor can it be used when the nature of the specific purpose changes from that which we agreed. For each purpose, a tailored approach to the assessment of potential soil and groundwater contamination is required. In most cases, a key objective is to identify, and if possible quantify, risks that both recognised and potential contamination posed in the context of the agreed purpose. Such risks may be financial (for example, clean up costs or constraints on site use) and/or physical (for example, potential health risks to users of the site or the general public). 3. Limitations of the Report

The work was conducted, and the report has been

prepared, in response to an agreed purpose and scope, within time and budgetary constraints, and in reliance on certain data and information made available to Coffey. The analyses, evaluations, opinions and conclusions presented in this report are based on that purpose and scope, requirements, data or information, and they could change if such requirements or data are inaccurate or incomplete. This report is valid as of the date of preparation. The condition of the site (including subsurface conditions) and extent or nature of contamination or other environmental hazards can change over time, as a result of either natural processes or human influence. Coffey should be kept appraised of any such events and should be consulted for further investigations if any changes are noted, particularly during construction activities where excavations often reveal subsurface conditions. In addition, advancements in professional practice regarding contaminated land and changes in applicable statues and/or guidelines may affect the validity of this report. Consequently, the currency of conclusions and recommendations in this report should be verified if you propose to use this report more than 6 months after its date of issue. The report does not include the evaluation or assessment of potential geotechnical engineering constraints of the site. 4. Interpretation of factual data

Environmental site assessments identify actual conditions only at those points where samples are taken and on the date collected. Data derived from indirect field measurements, and sometimes other reports on the site, are interpreted by geologists, engineers or scientists to provide an opinion about overall site conditions, their likely impact with respect to the report purpose and recommended actions. Variations in soil and groundwater conditions may occur between test or sample locations and actual conditions may differ from those inferred to exist. No environmental assessment program, no matter how comprehensive, can reveal all subsurface details and anomalies. Similarly, no professional, no matter how well qualified, can reveal what is hidden by earth, rock or changed through time. The actual interface between different materials may be far more gradual or abrupt than assumed based on the facts obtained. Nothing can be done to change the actual site conditions which exist, but steps can be taken to reduce the impact of unexpected conditions. For this reason, parties involved with land acquisition, management and/or redevelopment should retain the services of a suitably qualified and experienced environmental consultant through the development and



27

use of the site to identify variances, conduct additional tests if required, and recommend solutions to unexpected conditions or other unrecognised features encountered on site. Coffey would be pleased to assist with any investigation or advice in such circumstances. 5. Recommendations in this report

This report assumes, in accordance with industry practice, that the site conditions recognised through discrete sampling are representative of actual conditions throughout the investigation area. Recommendations are based on the resulting interpretation. Should further data be obtained that differs from the data on which the report recommendations are based (such as through excavation or other additional assessment), then the recommendations would need to be reviewed and may need to be revised. 6. Report for benefit of client

Unless otherwise agreed between us, the report has been prepared for your benefit and no other party. Other parties should not rely upon the report or the accuracy or completeness of any recommendation and should make their own enquiries and obtain independent advice in relation to such matters. Coffey assumes no responsibility and will not be liable to any other person or organisation for, or in relation to, any matter dealt with or conclusions expressed in the report, or for any loss or damage suffered by any other person or organisation arising from matters dealt with or conclusions expressed in the report. To avoid misuse of the information presented in your report, we recommend that Coffey be consulted before the report is provided to another party who may not be familiar with the background and the purpose of the report. In particular, an environmental disclosure report for a property vendor may not be suitable for satisfying the needs of that property’s purchaser. This report should not be applied for any purpose other than that stated in the report.

7. Interpretation by other professionals

Costly problems can occur when other professionals develop their plans based on misinterpretations of a report. To help avoid misinterpretations, a suitably qualified and experienced environmental consultant should be retained to explain the implications of the report to other professionals referring to the report and then review plans and specifications produced to see how other professionals have incorporated the report findings. Given Coffey prepared the report and has familiarity with the site, Coffey is well placed to provide such assistance. If another party is engaged to interpret the recommendations of the report, there is a risk that the contents of the report may be misinterpreted and Coffey disowns any responsibility for such misinterpretation. 8. Data should not be separated from the report

The report as a whole presents the findings of the site assessment and the report should not be copied in part or altered in any way. Logs, figures, laboratory data, drawings, etc. are customarily included in our reports and are developed by scientists or engineers based on their interpretation of field logs, field testing and laboratory evaluation of samples. This information should not under any circumstances be redrawn for inclusion in other documents or separated from the report in any way. This report should be reproduced in full. No responsibility is accepted for use of any part of this report in any other context or for any other purpose or by third parties. 9. Responsibility

Environmental reporting relies on interpretation of factual information using professional judgement and opinion and has a level of uncertainty attached to it, which is much less exact than other design disciplines. This has often resulted in claims being lodged against consultants, which are unfounded. As noted earlier, the recommendations and findings set out in this report should only be regarded as interpretive and should not be taken as accurate and complete information about all environmental media at all depths and locations across the site.



28

Figures

321820 321840 321860 321880 321900 321920 321940 321960 321980 322000 322020 322040 322060

6249880

6249900

6249920

6249940

6249960

6249980

6250000

6250020

6250040

6250060

6250080

0 25 50

Site Locality Plan

Not to ScaleRef: Google Maps accessed 19/5/2015

Ref: AERIAL IMAGE SOURCE: GOOGLE EARTH PRO 7.1.2.2041AERIAL IMAGE ©: SINCLAIR KNIGHT MERZ 2009

Legend

Site Boundary and Investigation Area

Approximate Location of Test Pit (current Coffey assessment)

Existing Stockpile (does not form part of this investigation)

Approximate Location of Borehole (Coffey, 1991 & 2012)

SITE

CTP01

CTP02A

CTP03 CTP04

CTP06

CTP05CTP07

CTP09

CTP08CTP10

CTP11

CTP12

CTP13

CTP14

CTP15

CTP17

CTP18

CTP19

CTP20

CTP21CTP22

CTP16

BH103BH104

BH102

BH117

BH116

BH1-91

BH115

BH101

Summary of site soil classification

Area 1: Fill soils comply with Resource Recovery Order - ENM

Area 2: Fill soil classifies as General Solid Waste (GSW)

Area 3: Fill soil classifies as General Solid Waste managed as Asbestos Waste

Area 4: Natural soils found to have elevated arsenic or copper & classifies as GSW

JMF

CTP02

Scale (m)

Australian Catholic University (ACU)

Waste Classification and Waste Recovery AssessmentProposed Carpark, 25A Barker Road, Strathfield, NSW

Site Layout Plan and Approximate Sampling Locations

ENAUWOLL04223AA-R01 1

CCQ

15/7/2015

1:1,000

A3



29

Laboratory Summary Tables

TABLE LR1:

SUMMARY OF LABORATORY RESULTS FOR SOIL SAMPLES REPRESENTING NATURAL SOILSHeavy Metals, TRH, BTEX, PAH, OCP, OPP and field observations(All results in mg/kg, unless otherwise stated)

Sample ID CTP01 CTP01 CTP02 CTP03 CTP04 CTP06 CTP08 CTP10 CTP13 CTP13 CTP14 CTP18 CTP19 CTP21 CTP22

Date of Sampling 22-Jun-15 22-Jun-15 22-Jun-15 22-Jun-15 22-Jun-15 22-Jun-15 22-Jun-15 23-Jun-15 22-Jun-15 22-Jun-15 23-Jun-15 23-Jun-15 23-Jun-15 23-Jun-15 23-Jun-15

Soil Layer Description (Texture) Residual Clay

Residual Clay

Residual Clay

Residual Clay

Residual Clay

Residual Clay

Residual Clay

Residual Clay

Residual Clay

Residual Clay

Residual Clay / XW Material

Residual Clay


Residual Clay

Residual Clay

Depth (m) 1.7-1.8 2.0-2.1 1.35-1.45 1.2-1.3 0.3-0.4 0.75-0.85 0.35-0.45 0.7-0.8 0.4-0.5 0.7-0.8 1.6-1.7 1.7-1.9 2.4-2.6 2.0-2.2 2.2-2.3

HEAVY METALS (TOTAL)Arsenic 5 to 11 11.0 6.0 8.2 - 16 - 10 5.0 50 35 3.3 - 4.4 12 35 16 50Cadmium 0.25 < 0.4 < 0.4 < 0.4 - < 0.4 - < 0.4 < 0.4 < 0.4 < 0.4 < 0.4 - < 0.4 < 0.4 < 0.4 < 0.4 < 0.4Chromium 6 to 21 11 10 8.5 - 21 - 10 15 24 11 8.1 - 6.7 16 12 13 24Copper 6 to 32 210 21 25 - 20 - 16 23 18 26 22 - 14 10 21 36 210Lead 13 to 44 11 10 23 17 15 14 10 13 20 13 9.1 13 58 13 11 17 58Mercury 0.05 0.08 < 0.05 < 0.05 - < 0.05 - < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 - < 0.05 < 0.05 < 0.05 0.08 0.08Nickel 5 to 50 < 5 < 5 < 5 - < 5 - < 5 < 5 < 5 < 5 < 5 - 5.2 6.5 8.2 7 8Zinc 17 to 77 24 14 28 13 100 55 22 33 43 14 37 25 30 19 40 33 100

TOTAL PETROLEUM HYDROCARBONSF1 (C6-C10) < LOR < 20 - < 20 - - - < 20 - - - - - < 20 < 20 - < 20 < 20F1 (C6-C10 less BTEX) < LOR < 20 - < 20 - - - < 20 - - - - - < 20 < 20 - < 20 < 20F2 (>C10-C16) < LOR < 50 - < 50 - - - < 50 - - - - - < 50 < 50 - < 50 < 50F2 (>C10-C16 less naphthalene) < LOR < 50 - < 50 - - - < 50 - - - - - < 50 < 50 - < 50 < 50F3 (>C16-C34) < LOR < 100 - < 100 - - - < 100 - - - - - < 100 < 100 - < 100 < 100F4 (>C34-C40) < LOR < 100 - < 100 - - - < 100 - - - - - < 100 < 100 - < 100 < 100

BTEXBenzene < LOR < 0.1 - < 0.1 - - - < 0.1 - - - - - < 0.1 < 0.1 - < 0.1 < 0.1Toluene < LOR < 0.1 - < 0.1 - - - < 0.1 - - - - - < 0.1 < 0.1 - < 0.1 < 0.1Ethylbenzene < LOR < 0.1 - < 0.1 - - - < 0.1 - - - - - < 0.1 < 0.1 - < 0.1 < 0.1Total Xylene < LOR < 0.3 - < 0.3 - - - < 0.3 - - - - - < 0.3 < 0.3 - < 0.3 < 0.3

POLYCYCLIC AROMATIC HYDROCARBONSNaphthalene < LOR < 0.5 - < 0.5 < 0.5 - - < 0.5 < 0.5 - - < 0.5 - < 0.5 < 0.5 - < 0.5 < 0.5Carcenogenic PAHs (as BaP TEQ) < LOR 1.2 - 1.2 1.2 - - 1.2 1.2 - - 1.2 - 1.2 1.2 - 1.2 1.2Benzo(a)pyrene < LOR < 0.5 - < 0.5 < 0.5 - - < 0.5 < 0.5 - - < 0.5 - < 0.5 < 0.5 - < 0.5 < 0.5Total PAH < LOR < 0.5 - < 0.5 < 0.5 - - < 0.5 < 0.5 - - < 0.5 - < 0.5 < 0.5 - < 0.5 < 0.5

ORGANOCHLORINE PESTICIDES < LOR < LOR - < LOR - - < LOR - - < LOR - - - < LOR - - < LOR < LOR

ORGANOPHOSPHORUS PESTICIDES < LOR < LOR - < LOR - - < LOR - - < LOR - - - < LOR - - < LOR < LOR

FIELD OBSERVATIONSHeadspace Screening (ppm) - 0.5 0.2 0.6 0.6 0.7 0.7 0.7 0.5 0.8 0.8 1.1 0.9 0.8 1.0 0.6 N/A N/AOdour Description - NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO N/A N/AStaining / Foreigns - NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO N/A N/A

Fibre cement fragments observed? NO NO NO NO NO NO NO NO NO NO NO NO NO NO NO N/A N/A

NOTES:Bold Concentration is outside the published background range

1 NSW soils for new suburbs in low traffic areas listed on page 17 (South Australian Health Commission (1995)). - No result or guideline

ND Not detectedNO Not observedNL Not limiting

LOR Limit of reporting

Published Background Range1

THRESHOLD CONCENTRATIONS

Ave

rage

Max

imum

TABLE LR2: SUMMARY OF LABORATORY RESULTS FOR SOIL SAMPLES FOR ASSESSING ENM EXEMPTION (Page 1 of 2)Heavy Metals, TRH, TPH after silica gel cleanup, BTEX, PAH, soil properties, asbestos, foreign materials, additional analytes and field observations(All results in mg/kg, unless otherwise stated)

Sample ID CTP01 CTP04 CTP05 BH102 CTP09 CTP11 CTP11 CTP12 CTP12 CTP13

QC3 (Intra-laboratory

duplicate of CTP13/0.0-

0.2)

CTP13 CTP15 CTP15 CTP16 CTP16 CTP16 CTP17 BH115 BH117 CTP17

Date of Sampling 22-Jun-15 22-Jun-15 22-Jun-15 23-Jan-12 22-Jun-15 23-Jun-15 23-Jun-15 23-Jun-15 23-Jun-15 22-Jun-15 22-Jun-15 22-Jun-15 23-Jun-15 23-Jun-15 23-Jun-15 23-Jun-15 23-Jun-15 23-Jun-15 01-Feb-12 01-Feb-12 23-Jun-15

Soil Layer Description Residual Clay

Residual Clay Fill (Topsoil) Topsoil

(Sandy Clay) Fill (Topsoil) Fill (Topsoil)Fill /

Reworked Residual

Fill (Topsoil)Fill /

Reworked Residual

Fill (Topsoil) Fill (Topsoil) Residual Clay Fill (Topsoil)

Fill / Reworked Residual


Reworked Residual


Fill (Topsoil) Fill (Topsoil) Fill (Topsoil)Fill /

Reworked Residual

Depth (m) 2.0-2.1 0.3-0.4 0.0-0.2 0.0-0.2 0.0-0.2 0.0-0.2 0.3-0.5 0.0-0.2 0.25-0.45 0.0-0.2 0.0-0.2 0.7-0.8 0.0-0.2 1.0-1.1 0.0-0.2 1.2-1.4 1.5-1.7 0.0-0.2 0.0-02 0.0-02 0.9-1.1

HEAVY METALS (TOTAL)Arsenic 20 40 6 16 < 2 <3 2.1 3.5 8.9 6.7 21 3.8 2.4 35 4.2 13 2.3 7.1 7.7 < 2 <3 <3 13Cadmium 0.5 1 < 0.4 < 0.4 < 0.4 <0.3 < 0.4 < 0.4 < 0.4 < 0.4 < 0.4 < 0.4 < 0.4 < 0.4 < 0.4 < 0.4 < 0.4 < 0.4 < 0.4 < 0.4 0.3 <0.3 < 0.4Chromium 75 150 10 21 5.3 6.3 6.8 7 12 32 17 7.3 6.2 11 8.6 11 6.5 12 11 < 5 20 7 15Copper 100 200 21 20 6.5 11 13 12 26 25 31 7.8 7.7 26 12 15 6.1 13 15 5.5 55 9.9 12Lead 50 100 10 15 19 27 95 34 41 15 48 19 17 13 47 16 18 24 13 11 2 22 15Mercury 0.5 1 < 0.05 < 0.05 < 0.05 <0.05 0.06 0.05 < 0.05 0.06 < 0.05 0.06 < 0.05 < 0.05 0.06 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 <0.05 0.08 < 0.05Nickel 30 60 < 5 < 5 < 5 3.5 < 5 < 5 7 21 < 5 < 5 < 5 < 5 < 5 < 5 < 5 7.5 7.9 < 5 46 4.1 6.4Zinc 150 300 14 100 200 120 200 180 240 60 51 120 110 14 230 32 100 30 32 48 34 110 41

TOTAL PETROLEUM HYDROCARBONSTRH C6-C9 - - < 20 < 20 < 20 < 20 < 20 < 20 < 20 < 20 - - < 20 < 20 < 20 < 20 < 20 < 20 < 20 < 20 < 20TRH C10-C14 - - < 20 < 20 < 20 32 < 20 < 20 < 20 < 20 - - < 20 < 20 < 20 < 20 < 20 < 20 < 20 < 20 < 20TRH C15-C28 - - 210 < 50 < 50 540 < 50 < 50 < 50 < 50 - - 170 < 50 < 50 < 50 < 50 < 50 < 50 < 50 < 50TRH C29-C36 - - 1,200 77 110 930 < 50 < 50 < 50 < 50 - - 420 < 50 110 < 50 < 50 < 50 < 50 < 50 < 50TRH C10-36 (Total) 250 500 - - 1400 77 110 1500 < 50 < 50 < 50 < 50 - - 590 < 50 110 < 50 < 50 < 50 < LOR < LOR < 50

TOTAL PETROLEUM HYDROCARBONS (after Silica Gel Cleanup)TRH C6-C9 - - - - - - - - - - - - - - - - - - - - -TRH C10-C14 - - < 50 - - < 50 - - - - - - < 50 - - - - - - - -TRH C15-C28 - - < 100 - - < 100 - - - - - - < 100 - - - - - - - -TRH C29-C36 - - < 100 - - < 100 - - - - - - < 100 - - - - - - - -TRH C10-36 (Total) 250 500 - - < LOR - - < LOR - - - - - - < LOR - - - - - - - -

BTEXBenzene 0.5 1 - - < 0.1 - < 0.1 < 0.1 < 0.1 < 0.1 < 0.1 < 0.1 - - < 0.1 < 0.1 < 0.1 < 0.1 < 0.1 < 0.1 < 0.1 < 0.1 < 0.1Toluene NA 0.5 - - < 0.1 - < 0.1 < 0.1 < 0.1 < 0.1 < 0.1 < 0.1 - - < 0.1 < 0.1 < 0.1 < 0.1 < 0.1 < 0.1 < 0.1 < 0.1 < 0.1Ethylbenzene NA 65 - - < 0.1 - < 0.1 < 0.1 < 0.1 < 0.1 < 0.1 < 0.1 - - < 0.1 < 0.1 < 0.1 < 0.1 < 0.1 < 0.1 < 0.1 < 0.1 < 0.1Total Xylene NA 25 - - < 0.3 - < 0.3 < 0.3 < 0.3 < 0.3 < 0.3 < 0.3 - - < 0.3 < 0.3 < 0.3 < 0.3 < 0.3 < 0.3 < 0.3 < 0.3 < 0.3

POLYCYCLIC AROMATIC HYDROCARBONSBenzo(a)pyrene 0.5 1 - - < 0.5 0.2 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 - - < 0.5 < 0.5 < 0.5 0.7 < 0.5 < 0.5 <0.1 - < 0.5Total PAH 20 40 - - < 0.5 2 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 - - < 0.5 < 0.5 < 0.5 3 < 0.5 < 0.5 <0.8 - < 0.5

SOIL PROPERTIESConductivity (uS/cm) - - 32 - 36 40 30 30 27 27 - - 33 52 37 120 110 59 - - 35Conductivity (dS/m) 1.5 3 - - 0.032 - 0.036 0.04 0.03 0.03 0.027 0.027 - - 0.033 0.052 0.037 0.12 0.11 0.059 - - 0.035pH (units)(1:5 soil:CaCl2 extract) 5 to 9 4.5 to 10 - - 6.5 - 6.5 6.3 5.8 6.2 5.9 6.1 - - 6 5.1 6.2 6.3 6.1 6.4 - - 6.6

ASBESTOS ND ND - - ND ND ND ND ND ND ND ND - - ND ND ND ND ND ND ND - ND

FOREIGN MATERIALSType III - Rubber, plastic, bitumen, paper, cloth, paint and wood* (%) 0.05% 0.10% - - < 0.05 - < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 - - < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 - - < 0.05

ADDITIONAL ANALYTESOrganochlorine pesticides (OCPs) - - <LOR <LOR <LOR 0.18 - <LOR - <LOR - - <LOR - <LOR - - <LOR <LOR - -Organophosphate pesticides (OPPs) - - <LOR - <LOR <LOR - <LOR - <LOR - - <LOR - <LOR - - <LOR - - -Volatile Halogenated Compounds (VHCs) - - - - - - - - - <LOR <LOR - - - - - - - <LOR - -Polychlorinated biphenyls (PCBs) - - - <1 - - - - - < 0.1 < 0.1 - - - - - - - <1 - -Acid Herbicides - - - - - - - - - <LOR - - - - - - - - - - -

FIELD OBSERVATIONSHeadspace Screening (ppm) - - 0.2 0.7 0.6 1.0 1.0 1.0 0.5 0.5 0.5 0.7 - 0.8 0.5 0.6 0.6 0.8 0.7 0.6 1.0 0.4 0.6Odour Description - - NO NO NO NO NO NO NO NO NO NO - NO NO NO NO NO NO NO NO NO NO

Staining / Foreigns - - NO NO NO NO NO NOConcrete, metal, wire and plastic

NO NO NO - NO NO NO NO Brick NO NO NO NO

Plastic drainage pipe and

gravel

Fibre cement fragments observed? NO NO NO NO NO NO NO NO NO NO - NO NO NO NO NO NO NO NO NO NO

NOTES:Bold Concentration exceeds the Absolute MaximumBold Concentration exceeds Maximum Average

1 Based on the Resource Recovery Order under Part 9, Clause 93 of the Protection of the Environment Operations (Waste) Regulation 2014 - The excavated natural material order 2014.- No result or guideline

ND Not detectedNO Not observed

LOR Limit of reporting* Excludes 'other vegetable matter'

Maximum average

concentration for characterisation

(mg/kg ‘dry weight’ unless

otherwise specified)

Absolute maximum

concentration(mg/kg ‘dry

weight’ unless otherwise specified)


Sample ID

Date of Sampling

Soil Layer Description

Depth (m)

HEAVY METALS (TOTAL)Arsenic 20 40Cadmium 0.5 1Chromium 75 150Copper 100 200Lead 50 100Mercury 0.5 1Nickel 30 60Zinc 150 300

TOTAL PETROLEUM HYDROCARBONSTRH C6-C9TRH C10-C14TRH C15-C28TRH C29-C36TRH C10-36 (Total) 250 500

TOTAL PETROLEUM HYDROCARBONS (after Silica Gel Cleanup)TRH C6-C9TRH C10-C14TRH C15-C28TRH C29-C36TRH C10-36 (Total) 250 500

BTEXBenzene 0.5 1Toluene NA 0.5Ethylbenzene NA 65Total Xylene NA 25

POLYCYCLIC AROMATIC HYDROCARBONSBenzo(a)pyrene 0.5 1Total PAH 20 40

SOIL PROPERTIESConductivity (uS/cm)Conductivity (dS/m) 1.5 3pH (units)(1:5 soil:CaCl2 extract) 5 to 9 4.5 to 10

ASBESTOS ND ND

FOREIGN MATERIALSType III - Rubber, plastic, bitumen, paper, cloth, paint and wood* (%) 0.05% 0.10%

ADDITIONAL ANALYTESOrganochlorine pesticides (OCPs)Organophosphate pesticides (OPPs)Volatile Halogenated Compounds (VHCs)Polychlorinated biphenyls (PCBs)Acid Herbicides

FIELD OBSERVATIONSHeadspace Screening (ppm) - -Odour Description - -

Staining / Foreigns - -

Fibre cement fragments observed?

NOTES:BoldBold

1-

NDNO

LOR*

Maximum average

concentration for characterisation

(mg/kg ‘dry weight’ unless

otherwise specified)

Absolute maximum

concentration(mg/kg ‘dry

weight’ unless otherwise specified)


TABLE LR2: SUMMARY OF LABORATORY RESULTS FOR SOIL SAMPLES FOR ASSESSING ENM EXEMPTION (Page 2 of 2)Heavy Metals, TRH, TPH after silica gel cleanup, BTEX, PAH, soil properties, asbestos, foreign materials, additional analytes and field observations(All results in mg/kg, unless otherwise stated)

CTP19 CTP19



1.2)

CTP19 CTP19 CTP20 CTP20 CTP20 CTP20 CTP21 CTP21 CTP21 CTP22

Aver

age

Max

imum

23-Jun-15 23-Jun-15 23-Jun-15 23-Jun-15 23-Jun-15 23-Jun-15 23-Jun-15 23-Jun-15 23-Jun-15 23-Jun-15 23-Jun-15 23-Jun-15 23-Jun-15


Reworked Residual





Reworked Residual




Reworked Residual


Residual Clay

0.0-0.2 1.0-1.2 1.0-1.2 1.8-1.9 2.4-2.6 0.0-0.2 1.0-1.1 1.9-2.1 2.3-2.5 0.0-0.2 0.9-1.0 1.8-2.0 2.2-2.3

4.2 17 13 11 4.4 2.2 11 24 11 < 2 14 10 35 11 35< 0.4 < 0.4 < 0.4 < 0.4 < 0.4 < 0.4 < 0.4 < 0.4 < 0.4 < 0.4 < 0.4 < 0.4 < 0.4 <0.4 <0.47.5 16 12 10 6.7 6.4 10 11 10 < 5 16 13 12 12 3212 15 10 11 14 9.3 13 130 93 17 28 20 21 23 13043 26 20 19 58 24 20 20 17 78 57 24 11 28 95

< 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 0.19 0.06 < 0.05 < 0.05 0.08 0.19< 5 < 5 < 5 < 5 5.2 < 5 < 5 < 5 < 5 < 5 8.9 13 8.2 12 46200 22 14 16 30 130 18 17 15 59 67 60 40 82 240

< 20 < 20 < 20 < 20 < 20 < 20 < 20 < 20 < 20 < 20 < 20 < 20 - < 20 < 20< 20 < 20 < 20 < 20 < 20 < 20 < 20 < 20 < 20 < 20 < 20 < 20 - < 20 < 2077 < 50 < 50 < 50 < 50 < 50 < 50 < 50 < 50 < 50 < 50 < 50 - 77 77

250 < 50 < 50 < 50 < 50 97 < 50 < 50 < 50 < 50 < 50 < 50 - 134 250330 < 50 < 50 < 50 < 50 97 < 50 < 50 < 50 < 50 < 50 < 50 - 154 330

- - - - - - - - - - - - - - -- - - - - - - - - - - - - < 50 < 50- - - - - - - - - - - - - < 100 < 100- - - - - - - - - - - - - < 100 < 100- - - - - - - - - - - - - < LOR < LOR

< 0.1 < 0.1 < 0.1 < 0.1 < 0.1 < 0.1 < 0.1 < 0.1 < 0.1 < 0.1 < 0.1 < 0.1 - < 0.1 < 0.1< 0.1 < 0.1 < 0.1 < 0.1 < 0.1 < 0.1 < 0.1 < 0.1 < 0.1 < 0.1 < 0.1 < 0.1 - < 0.1 < 0.1< 0.1 < 0.1 < 0.1 < 0.1 < 0.1 < 0.1 < 0.1 < 0.1 < 0.1 < 0.1 < 0.1 < 0.1 - < 0.1 < 0.1< 0.3 < 0.3 < 0.3 < 0.3 < 0.3 < 0.3 < 0.3 < 0.3 < 0.3 < 0.3 < 0.3 < 0.3 - < 0.3 < 0.3

< 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 0.8 1 < 0.5 < 0.5 - 0.3 1< 0.5 2 2 < 0.5 < 0.5 < 0.5 < 0.5 < 0.5 10 9 < 0.5 < 0.5 - 5 9.5

33 34 30 25 - 34 81 130 95 30 45 44 - 51 1300.033 0.034 0.03 0.025 - 0.034 0.081 0.13 0.095 0.03 0.045 0.044 - 0.05 0.13

6.2 5.3 5.2 5.5 - 6.2 5.3 5.4 5.6 6.7 6.4 6 - 6 7

ND ND - ND - ND ND ND ND ND ND ND - N/A N/A

< 0.05 < 0.05 - < 0.05 - < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 - < 0.05 < 0.05

<LOR - - - < LOR <LOR - - - <LOR - - - N/A N/A<LOR - - - < LOR <LOR - - - <LOR - - - N/A N/A

- - - - - - - - - - <LOR - - N/A N/A- - - - - - - - - - < 0.1 - - N/A N/A- - - - - <LOR - - - - - - - N/A N/A

0.7 0.8 - 0.7 0.8 0.8 0.7 0.5 0.7 1.0 1.0 1.1 0.6 N/A N/ANO NO - NO NO NO NO NO NO NO NO NO NO N/A N/A

NO Brick and concrete - NO NO NO NO NO NO NO Brick Terracotta

fragment NO

N/A N/A

NO NO - NO NO NO NO NO NO NO NO NO NON/A N/A

Concentration exceeds the Absolute MaximumConcentration exceeds Maximum AverageBased on the Resource Recovery Order under Part 9, Clause 93 of the Protection of the Environment Operations (Waste) Regulation 2014 - The excavated natural material order 2014.No result or guidelineNot detectedNot observedLimit of reportingExcludes 'other vegetable matter'

TABLE LR3:

SUMMARY OF LABORATORY RESULTS FOR SOIL SAMPLES FOR WASTE CLASSIFICATIONHeavy Metals (including TCLP), TRH, BTEX, PAH (including TCLP), OCP, OPP, VHC, PCB, herbicides, asbestos and field observations(All results in mg/kg, unless otherwise stated)

Sample ID CTP01



0.2)

CTP01 CTP01 CTP01 CTP02A CTP03 CTP03 CTP04



0.2)

QC2A (Inter-laboratory


0.2)

CTP06 CTP06 CTP06 CTP07 CTP08 CTP10



0.2)

QC4A (Inter-laboratory


0.2)

CTP10 CTP13 CTP14 CTP14 CTP18 CTP18 CTP18 CTP22 CTP22 CTP22

Date of Sampling 22-Jun-15 22-Jun-15 22-Jun-15 22-Jun-15 22-Jun-15 22-Jun-15 22-Jun-15 22-Jun-15 22-Jun-15 22-Jun-15 22-Jun-15 22-Jun-15 22-Jun-15 22-Jun-15 22-Jun-15 22-Jun-15 23-Jun-15 23-Jun-15 23-Jun-15 23-Jun-15 22-Jun-15 23-Jun-15 23-Jun-15 23-Jun-15 23-Jun-15 23-Jun-15 23-Jun-15 23-Jun-15 23-Jun-15

Soil Layer Description (Texture) Fill (Topsoil) Fill (Topsoil)Fill

(Reworked residual)

Fill Residual Clay Fill (Topsoil) Fill (Topsoil) Fill (Former

Topsoil) Fill (Topsoil) Fill (Topsoil) Fill (Topsoil) Fill (Topsoil) Fill (Topsoil) Fill (Former Topsoil) Fill (Topsoil) Fill (Topsoil) Fill (Topsoil) Fill (Topsoil) Fill (Topsoil)


Residual Clay Fill (Topsoil)

Fill (Cobbly Gravelly

Clay)Fill (Topsoil)

Fill (Cobbly Gravelly

Clay)



Reworked Residual


Depth (m) 0.0-0.2 0.0-0.2 1.0-1.2 1.4-1.6 1.7-1.8 0.0-0.2 0.0-0.2 0.8-1.0 0.0-0.2 0.0-0.2 0.0-0.2 0.0-0.2 0.2-0.25 0.35-0.55 0.0-0.2 0.0-0.2 0.0-0.2 0.0-0.2 0.0-0.2 0.45-0.65 0.4-0.5 0.0-0.2 1.0-1.2 0.0-0.2 0.8-0.9 1.4-1.6 0.0-0.2 0.8-1.2 1.9-2.1

HEAVY METALS (TOTAL)Arsenic 100 / 500 3,1 400 / 2,000 6,4 18 15 14 9.4 11 290 2.7 10 8.8 8.8 10 4.7 6.7 16 2.3 5.9 < 2 2.6 <5 19 50 3.1 17 6.8 12 15 4.1 11 12Cadmium 20 3 80 6 < 0.4 < 0.4 < 0.4 < 0.4 < 0.4 < 0.4 < 0.4 0.6 < 0.4 < 0.4 <1 < 0.4 < 0.4 0.7 < 0.4 < 0.4 < 0.4 < 0.4 <1 < 0.4 < 0.4 < 0.4 < 0.4 < 0.4 < 0.4 < 0.4 < 0.4 < 0.4 < 0.4Chromium 100 400 19 20 17 14 11 18 5 24 13 14 15 16 21 24 9 11 < 5 7.2 7 15 24 7.6 9.4 10 10 14 12 12 17Copper N/A N/A 27 33 24 37 210 22 7 91 27 65 25 15 22 62 8 9 8 9 9 21 18 10 17 19 22 16 12 22 12Lead 100 / 1,500 3,1 400 / 6,000 6,4 110 150 40 320 11 77 18 860 270 280 236 50 70 420 26 160 55 54 55 36 20 52 49 120 63 20 17 51 12Mercury 4 3 16 6 0.08 0.11 < 0.05 0.25 0.08 0.05 < 0.05 0.46 0.11 0.12 0.1 0.06 0.08 0.19 0.05 0.07 < 0.05 0.09 <0.1 < 0.05 < 0.05 < 0.05 1.3 < 0.05 0.06 < 0.05 < 0.05 < 0.05 < 0.05Nickel 40 3 160 6 8.3 11 < 5 5.5 < 5 9.7 < 5 10 5.6 6.5 6 6.5 9.1 7.4 < 5 5.2 < 5 < 5 4 6.9 < 5 < 5 5.1 < 5 10 < 5 9.7 < 5 < 5Zinc N/A N/A 610 340 42 150 24 510 78 440 1,400 830 382 450 500 670 93 500 150 190 188 110 43 200 82 220 110 24 44 73 22

HEAVY METALS (TCLP, mg/L)Arsenic 5 2 20 5 - - - - - < 0.01 - - - - - - - - - - - - - - - - - - - - - - -Lead 5 2 20 5 - - - 0.09 - - - 0.16 - - - - - - - < 0.01 - - - - - - - 0.02 - - - - -

TOTAL PETROLEUM HYDROCARBONSTRH C6-C9 650 1 2,600 4 < 20 - < 20 < 20 < 20 < 20 < 20 < 20 < 20 < 20 <10 < 20 - < 20 < 20 < 20 < 20 < 20 <10 < 20 - < 20 < 20 < 20 < 20 < 20 < 20 < 20 < 20TRH C10-C14 < 20 - < 20 < 20 < 20 < 20 22 < 20 < 20 < 20 <50 < 20 - < 20 < 20 < 20 < 20 < 20 <50 < 20 - < 20 < 20 < 20 < 20 < 20 < 20 < 20 < 20TRH C15-C28 68 - < 50 < 50 < 50 270 < 50 < 50 < 50 210 <100 200 - < 50 67 550 140 330 <100 280 - 130 560 480 430 < 50 130 110 < 50TRH C29-C36 260 - < 50 < 50 < 50 960 < 50 < 50 < 50 180 <100 910 - < 50 270 3,200 490 1,300 <100 200 - 300 710 1,400 540 < 50 < 50 < 50 < 50TRH C10-36 (Total) 10,000 1 40,000 4 330 - < 50 < 50 < 50 1,200 < 50 < 50 < 50 390 <50 1,100 - < 50 340 3,800 630 1,600 <50 480 - 430 1,300 1,900 970 < 50 130 110 < 50

BTEXBenzene 10 3 40 6 < 0.1 - < 0.1 < 0.1 < 0.1 < 0.1 < 0.1 < 0.1 < 0.1 < 0.1 <0.2 < 0.1 - < 0.1 < 0.1 < 0.1 < 0.1 < 0.1 <0.2 < 0.1 - < 0.1 < 0.1 < 0.1 < 0.1 < 0.1 < 0.1 < 0.1 < 0.1Toluene 288 3 1152 6 < 0.1 - < 0.1 < 0.1 < 0.1 < 0.1 < 0.1 < 0.1 < 0.1 < 0.1 <0.5 < 0.1 - < 0.1 < 0.1 < 0.1 < 0.1 < 0.1 <0.5 < 0.1 - < 0.1 < 0.1 < 0.1 < 0.1 < 0.1 < 0.1 < 0.1 < 0.1Ethylbenzene 600 3 2400 6 < 0.1 - < 0.1 < 0.1 < 0.1 < 0.1 < 0.1 < 0.1 < 0.1 < 0.1 <0.5 < 0.1 - < 0.1 < 0.1 < 0.1 < 0.1 < 0.1 <0.5 < 0.1 - < 0.1 < 0.1 < 0.1 < 0.1 < 0.1 < 0.1 < 0.1 < 0.1Total Xylene 1000 3 4000 6 < 0.3 - < 0.3 < 0.3 < 0.3 < 0.3 < 0.3 < 0.3 < 0.3 < 0.3 <0.5 < 0.3 - < 0.3 < 0.3 < 0.3 < 0.3 < 0.3 <0.5 < 0.3 - < 0.3 < 0.3 < 0.3 < 0.3 < 0.3 < 0.3 < 0.3 < 0.3

POLYCYCLIC AROMATIC HYDROCARBONSBenzo(a)pyrene 0.8 / 10 3,1 3.2 / 23 6,4 < 0.5 - 0.9 1.3 < 0.5 < 0.5 < 0.5 7.5 0.7 3.6 0.5 < 0.5 - < 0.5 < 0.5 < 0.5 0.8 < 0.5 <0.5 6.8 - < 0.5 7.7 < 0.5 7.1 < 0.5 < 0.5 < 0.5 < 0.5Total PAH 200 1 800 4 2 - 7 12 < 0.5 < 0.5 < 0.5 110 3 39 5 < 0.5 - 2 < 0.5 1 8 5 <0.5 100 - < 0.5 70 5 65 < 0.5 < 0.5 < 0.5 < 0.5

POLYCYCLIC AROMATIC HYDROCARBONS (TCLP)Benzo(a)pyrene 0.04 2 0.16 5 - - - < 0.001 - - - < 0.001 < 0.001 < 0.001 - - - - - - - - - < 0.001 - - < 0.001 - < 0.001 - - - -

ORGANOCHLORINE PESTICIDES7 <50 1 <50 4 - - - - < LOR <LOR <LOR - <LOR <LOR - - - <LOR <LOR 0.39 <LOR <LOR - - < LOR <LOR - <LOR - - - - -

ORGANOPHOSPHORUS PESTICIDES8 250 1 1,000 4 - - - - < LOR <LOR <LOR - <LOR <LOR - - - <LOR <LOR <LOR <LOR <LOR - - < LOR <LOR - <LOR - - - - -

VOLATILE HALOGENATED COMPOUNDSVinyle chloride 4 3 16 6 - < 0.5 - < 0.5 - - - - - - - - - < 0.5 - - - - - - - - - - < 0.5 - - - -Other VHCs - <LOR - <LOR - - - - - - - - - <LOR - - - - - - - - - - <LOR - - - -

POLYCHLORINATED BIPHENYLS <50 1 <50 4 - < 0.1 - < 0.1 - - - - - - - - - < 0.1 - - - - - - - - - - < 0.1 - - - -

ACID HERBICIDES2.4.5-T <50 1 <50 4 < 0.5 < 0.5 - - - - - - - - - - - - < 0.5 - - - - - - < 0.5 - - - - - - -2.4-D 200 1 800 4 < 0.5 < 0.5 - - - - - - - - - - - - < 0.5 - - - - - - < 0.5 - - - - - - -Other Herbicides <LOR <LOR - - - - - - - - - - - - <LOR - - - - - - <LOR - - - - - - -

ASBESTOS ND ND ND - ND ND - ND ND ND ND - ND - ND ND ND ND - - ND - ND

Chrysotile, amosite and crocidolite detected

Chrysotileand amosite

detectedND ND ND Yes - Fibre

cement fragment

ND

FIELD OBSERVATIONSHeadspace Screening (ppm) 2.2 - 1.1 0.6 0.5 1.1 0.5 0.6 0.7 - - 0.7 - 0.7 0.7 0.6 0.9 - - 0.8 0.8 0.5 0.8 0.7 0.9 0.7 0.6 0.7 0.6Odour Description NO - NO NO NO NO NO NO NO - - NO NO NO NO NO NO - - NO NO NO NO NO NO NO NO NO NO

Staining / Foreigns Ceramic Brick

Ceramic and glass

(including bottles)

NO NO NOGlass and

brick fragments

NO NO Red stained layer NO NO NO Golf tee NO NO NO

Brick, concrete,

asphalt and metal

NOBrick,

concrete and asphalt

NO NO Bricks NO

Fibre cement fragments observed? NO - NO NO NO NO NO NO NO - - NO NO NO NO NO NO - - NO NO NO NO NO NO NO NO Yes (1 piece) NO

NOTES:Bold Concentration exceed the respective General Solid Waste CriteriaBold Concentration exceed the respective Restricted Solid Waste CriteriaBold Contains asbestos

Based on NSW EPA (2014) Waste Classification Guidelines Part 1: Classifying Waste1 Specific Contaminant Concentration (SCC1) for General Solid Waste2 Leachable Concentration (TCLP1) for General Solid Waste3 Contamination Threshold Value (CT1) for General Solid Waste4 Specific Contaminant Concentration (SCC2) for Restricted Solid Waste5 Leachable Concentration (TCLP2) for Restricted Solid Waste6 Contamination Threshold Value (CT2) for Restricted Solid Waste7 Some OC Pesticides are listed as scheduled chemicals8 Some OP Peticides are listed as 'moderately harmful pesticides' in the guidelines and the relevant SCC1 and SCC2 values have been used

ND Not DetectedNO Not observed

See original laboratory reports for detection limits

General Solid Waste

Restricted Solid Waste


Appendix A – Resource Recovery Exemptions

www.epa.nsw.gov.au 1

Resource Recovery Exemption under Part 9, Clauses 91 and 92 of the Protection of the Environment Operations (Waste) Regulation 2014

The excavated natural material exemption 2014

Introduction This exemption:

• is issued by the Environment Protection Authority (EPA) under clauses 91 and 92 of the Protection of the Environment Operations (Waste) Regulation 2014 (Waste Regulation); and

• exempts a consumer of excavated natural material from certain requirements under the Protection of the Environment Operations Act 1997 (POEO Act) and the Waste Regulation in relation to the application of that waste to land, provided the consumer complies with the conditions of this exemption.

This exemption should be read in conjunction with ‘the excavated natural material order 2014’.

1. Waste to which this exemption applies 1.1. This exemption applies to excavated natural material that is, or is intended to

be, applied to land as engineering fill or for use in earthworks. 1.2. Excavated natural material is naturally occurring rock and soil (including but

not limited to materials such as sandstone, shale, clay and soil) that has: a) been excavated from the ground, and b) contains at least 98% (by weight) natural material, and c) does not meet the definition of Virgin Excavated Natural Material in

the Act. Excavated natural material does not include material located in a hotspot; that has been processed; or that contains asbestos, Acid Sulfate Soils (ASS), Potential Acid Sulfate soils (PASS) or sulfidic ores.

2. Persons to whom this exemption applies 2.1. This exemption applies to any person who applies or intends to apply

excavated natural material to land as set out in 1.1.

2 www.epa.nsw.gov.au

3. Duration 3.1. This exemption commences on 24 November 2014 and is valid until revoked

by the EPA by notice published in the Government Gazette.

4. Premises to which this exemption applies 4.1. This exemption applies to the premises at which the consumer’s actual or

intended application of excavated natural material is carried out.

5. Revocation 5.1. ‘The excavated natural material exemption 2012’ which commenced 19

October 2012 is revoked from 24 November 2014.

6. Exemption 6.1. Subject to the conditions of this exemption, the EPA exempts each consumer

from the following provisions of the POEO Act and the Waste Regulation in relation to the consumer’s actual or intended application of excavated natural material to land as engineering fill or for use in earthworks at the premises: • section 48 of the POEO Act in respect of the scheduled activities

described in clauses 39 of Schedule 1 of the POEO Act; • Part 4 of the Waste Regulation; • section 88 of the POEO Act; and • clause 109 and 110 of the Waste Regulation.

6.2. The exemption does not apply in circumstances where excavated natural material is received at the premises for which the consumer holds a licence under the POEO Act that authorises the carrying out of the scheduled activities on the premises under clause 39 ‘waste disposal (application to land) or clause 40 ‘waste disposal’ (thermal treatment) of Schedule 1 of the POEO Act.

7. Conditions of exemption The exemption is subject to the following conditions: 7.1. At the time the excavated natural material is received at the premises, the

material must meet all chemical and other material requirements for excavated natural material which are required on or before the supply of excavated natural material under ‘the excavated natural material order 2014’.

7.2. The excavated natural material can only be applied to land as engineering fill or for use in earthworks.

7.3. The consumer must keep a written record of the following for a period of six years: • the quantity of any excavated natural material received; and • the name and address of the supplier of the excavated natural material

received. 7.4. The consumer must make any records required to be kept under this

exemption available to authorised officers of the EPA on request. 7.5. The consumer must ensure that any application of excavated natural material

to land must occur within a reasonable period of time after its receipt.


8. Definitions In this exemption: application or apply to land means applying to land by:

• spraying, spreading or depositing on the land; or • ploughing, injecting or mixing into the land; or • filling, raising, reclaiming or contouring the land. consumer means a person who applies, or intends to apply excavated natural material to land. Manager Waste Strategy and Innovation Environment Protection Authority (by delegation)


Notes The EPA may amend or revoke this exemption at any time. It is the responsibility of the consumer to ensure they comply with all relevant requirements of the most current exemption The current version of this exemption will be available on www.epa.nsw.gov.au In gazetting or otherwise issuing this exemption, the EPA is not in any way endorsing the use of this substance or guaranteeing that the substance will confer benefit. The conditions set out in this exemption are designed to minimise the risk of potential harm to the environment, human health or agriculture, although neither this exemption nor the accompanying order guarantee that the environment, human health or agriculture will not be harmed. The consumer should assess whether or not the excavated natural material is fit for the purpose the material is proposed to be used for, and whether this use will cause harm. The consumer may need to seek expert engineering or technical advice. Regardless of any exemption provided by the EPA, the person who causes or permits the application of the substance to land must ensure that the action is lawful and consistent with any other legislative requirements including, if applicable, any development consent(s) for managing operations on the site(s). The receipt of excavated natural material remains subject to other relevant environmental regulations in the POEO Act and the Waste Regulation. For example, a person who pollutes land (s. 142A) or water (s. 120), or causes air pollution through the emission of odours (s. 126), or does not meet the special requirements for asbestos waste (Part 7 of the Waste Regulation), regardless of having an exemption, is guilty of an offence and subject to prosecution. This exemption does not alter the requirements of any other relevant legislation that must be met in utilising this material, including for example, the need to prepare a Safety Data Sheet (SDS). Failure to comply with the conditions of this exemption constitutes an offence under clause 91 of the Waste Regulation.


Resource Recovery Order under Part 9, Clause 93 of the Protection of the Environment Operations (Waste) Regulation 2014

The excavated natural material order 2014 Introduction This order, issued by the Environment Protection Authority (EPA) under clause 93 of the Protection of the Environment Operations (Waste) Regulation 2014 (Waste Regulation), imposes the requirements that must be met by suppliers of excavated natural material to which ‘the excavated natural material exemption 2014’ applies. The requirements in this order apply in relation to the supply of excavated natural material for application to land as engineering fill or for use in earthworks.

1. Waste to which this order applies 1.1. This order applies to excavated natural material. In this order, excavated

natural material means naturally occurring rock and soil (including but not limited to materials such as sandstone, shale, clay and soil) that has:

a) been excavated from the ground, and b) contains at least 98% (by weight) natural material, and c) does not meet the definition of Virgin Excavated Natural Material in

the Act. Excavated natural material does not include material located in a hotspot; that has been processed; or that contains asbestos, Acid Sulfate Soils (ASS), Potential Acid Sulfate soils (PASS) or sulfidic ores.

2. Persons to whom this order applies 2.1. The requirements in this order apply, as relevant, to any person who supplies

excavated natural material, that has been generated, processed or recovered by the person.

2.2. This order does not apply to the supply of excavated natural material to a consumer for land application at a premises for which the consumer holds a licence under the POEO Act that authorises the carrying out of the scheduled activities on the premises under clause 39 ‘waste disposal (application to land)’ or clause 40 ‘waste disposal (thermal treatment)’ of Schedule 1 of the POEO Act.

3. Duration 3.1. This order commences on 24 November 2014 and is valid until revoked by

the EPA by notice published in the Government Gazette.


4. Generator requirements The EPA imposes the following requirements on any generator who supplies excavated natural material.

Sampling requirements 4.1. On or before supplying excavated natural material, the generator must:

4.1.1. Prepare a written sampling plan which includes a description of sample preparation and storage procedures for the excavated natural material.

4.1.2. Undertake sampling and testing of the excavated natural material as required under clauses 4.2, 4.3, and 4.4 below. The sampling must be carried out in accordance with the written sampling plan.

4.2. The generator must undertake sampling and analysis of the material for ASS and PASS, in accordance with the NSW Acid Sulfate Soil Manual, Acid Sulfate Soils Management Advisory Council, 1998 and the updated Laboratory Methods Guidelines version 2.1 – June 2004 where: 4.2.1. the pH measured in the material is below 5, and/or 4.2.2. the review of the applicable Acid Sulfate Soil Risk Maps (published by

the former Department of Land and Water Conservation and available at http://www.environment.nsw.gov.au/acidsulfatesoil/riskmaps.htm) indicates the potential presence of ASS.

4.3. For stockpiled material, the generator must: 4.3.1. undertake sampling in accordance with Australian Standard 1141.3.1-

2012 Methods for sampling and testing aggregates – Sampling – Aggregates (or equivalent);

4.3.2. undertake characterisation sampling by collecting the number of samples listed in Column 2 of Table 1 with respect to the quantity of the waste listed in Column 1 of Table 1 and testing each sample for the chemicals and other attributes listed in Column 1 of Table 4. For the purposes of characterisation sampling the generator must collect:

4.3.2.1. composite samples for attributes 1 to 10 and 18 in Column 1 of Table 4.

4.3.2.2. discrete samples for attributes 11 to 17 in Column 1 of Table 4.

4.3.2.3. The generator must carry out sampling in a way that ensures that the samples taken are representative of the material from the entire stockpile. All parts of the stockpile must be equally accessible for sampling.

4.3.2.4. for stockpiles greater than 4,000 tonnes the number of samples described in Table 1 must be repeated.

4.3.3. store the excavated natural material appropriately until the characterisation test results are validated as compliant with the maximum average concentration or other value listed in Column 2 of Table 4 and the absolute maximum concentration or other value listed in Column 3 of Table 4.


Table 1 Sampling of Stockpiled Material

Column 1 Column 2 Column 3

Quantity (tonnes) Number of samples Validation

<500 3

Required

500 – 1,000 4

1,000 – 2,000 5

2,000 – 3,000 7

3,000 – 4,000 10

4.4. For in situ material, the generator must:

4.4.1. undertake sampling by collecting discrete samples. Compositing of samples is not permitted for in-situ materials.

4.4.2. undertake characterisation sampling for the range of chemicals and other attributes listed in Column 1 of Table 4 according to the requirements listed in Columns 1, 2 and 3 of Table 2. When the ground surface is not comprised of soil (e.g. concrete slab), samples must be taken at the depth at which the soil commences.

4.4.3. undertake sampling at depth according to Column 1 of Table 3. 4.4.4. collect additional soil samples (and analyse them for the range of

chemicals and other attributes listed in Column 1 of Table 4), at any depth exhibiting discolouration, staining, odour or other indicators of contamination inconsistent with soil samples collected at the depth intervals indicated in Table 3.

4.4.5. segregate and exclude hotspots identified in accordance with Table 2, from material excavated for reuse.

4.4.6. subdivide sites larger than 50,000 m² into smaller areas and sample each area as per Table 2.

4.4.7. store the excavated natural material appropriately until the characterisation test results are validated as compliant with the maximum average concentration or other value listed in Column 2 of Table 4 and the absolute maximum concentration or other value listed in Column 3 of Table 4.


Table 2 In Situ Sampling at surface

Column 1 Column 2 Column 3 Column 4 Column 5

Size of in situ area (m2)

Number of systematic

sampling points recommended

Distance between two sampling

points (m)

Diameter of the hot spot that can be

detected with 95% confidence (m)

Validation

500 5 10.0 11.8

Required

1000 6 12.9 15.2

2000 7 16.9 19.9

3000 9 18.2 21.5

4000 11 19.1 22.5

5000 13 19.6 23.1

6000 15 20.0 23.6

7000 17 20.3 23.9

8000 19 20.5 24.2

9000 20 21.2 25.0

10,000 21 21.8 25.7

15,000 25 25.0 28.9

20,000 30 25.8 30.5

25,000 35 26.7 31.5

30,000 40 27.5 32.4

35,000 45 27.9 32.9

40,000 50 28.3 33.4

45,000 52 29.3 34.6

50,000 55 30.2 35.6

Table 2 has been taken from NSW EPA 1995, Contaminated Sites Sampling Design Guidelines, NSW Environment Protection Authority.

Table 3 In Situ Sampling at Depth

Column 1 Column 2

Sampling Requirements * Validation

1 soil sample at 1.0 m bgl from each surface sampling point followed by 1 soil sample for every metre thereafter. From 1.0 m bgl, sample at the next metre interval until the proposed depth of excavation of the material is reached. If the proposed depth of excavation is between 0.5 to 0.9 m after the last metre interval, sample at the base of the proposed depth of excavation.

Required if the depth of excavation is equal to or greater than 1.0 m bgl

* Refer to Notes for examples


Chemical and other material requirements 4.5. The generator must not supply excavated natural material waste to any

person if, in relation to any of the chemical and other attributes of the excavated natural material:

4.5.1. The chemical concentration or other attribute of any sample collected and tested as part of the characterisation of the excavated natural material exceeds the absolute maximum concentration or other value listed in Column 3 of Table 4:

4.5.2. The average concentration or other value of that attribute from the characterisation of the excavated natural material (based on the arithmetic mean) exceeds the maximum average concentration or other value listed in Column 2 of Table 4.

4.6. The absolute maximum concentration or other value of that attribute in any excavated natural material supplied under this order must not exceed the absolute maximum concentration or other value listed in Column 3 of Table 4.

Table 4 Column 1 Column 2 Column 3

Chemicals and other attributes

Maximum average concentration for characterisation

(mg/kg ‘dry weight’ unless otherwise specified)

Absolute maximum concentration

(mg/kg ‘dry weight’ unless otherwise specified)

1. Mercury 0.5 1

2. Cadmium 0.5 1

3. Lead 50 100

4. Arsenic 20 40

5. Chromium (total) 75 150

6. Copper 100 200

7. Nickel 30 60

8. Zinc 150 300

9. Electrical Conductivity 1.5 dS/m 3 dS/m

10. pH * 5 to 9 4.5 to 10

11. Total Polycyclic Aromatic Hydrocarbons (PAHs) 20 40

12. Benzo(a)pyrene 0.5 1

13. Benzene NA 0.5

14. Toluene NA 65

15. Ethyl-benzene NA 25

16. Xylene NA 15

17. Total Petroleum Hydrocarbons C10-C36

250 500

18. Rubber, plastic, bitumen, paper, cloth, paint and wood 0.05% 0.10%

* The ranges given for pH are for the minimum and maximum acceptable pH values in the excavated natural material.


Test methods 4.7. The generator must ensure that any testing of samples required by this order

is undertaken by analytical laboratories accredited by the National Association of Testing Authorities (NATA), or equivalent.

4.8. The generator must ensure that the chemicals and other attributes (listed in Column 1 of Table 4) in the excavated natural material it supplies are tested in accordance with the test methods specified below or other equivalent analytical methods. Where an equivalent analytical method is used the detection limit must be equal to or less than that nominated for the given method below. 4.8.1. Test methods for measuring the mercury concentration.

4.8.1.1. Analysis using USEPA SW-846 Method 7471B Mercury in solid or semisolid waste (manual cold vapour technique), or an equivalent analytical method with a detection limit < 20% of the stated absolute maximum concentration in Column 3 of Table 2 (i.e. < 0.20 mg/kg dry weight).

4.8.1.2. Report as mg/kg dry weight. 4.8.2. Test methods for measuring chemicals 2 to 8.

4.8.2.1. Sample preparation by digesting using USEPA SW-846 Method 3051A Microwave assisted acid digestion of sediments, sludges, soils, and oils (or an equivalent analytical method).

4.8.2.2. Analysis using USEPA SW-846 Method 6010C Inductively coupled plasma - atomic emission spectrometry, or an equivalent analytical method with a detection limit < 10% of the stated absolute maximum concentration in Column 3 of Table 2, (e.g. 10 mg/kg dry weight for lead).

4.8.2.3. Report as mg/kg dry weight. 4.8.3. Test methods for measuring electrical conductivity and pH.

4.8.3.1. Sample preparation by mixing 1 part excavated natural material with 5 parts distilled water.

4.8.3.2. Analysis using Method 103 (pH) and 104 (Electrical Conductivity) in Schedule B (3): Guideline on Laboratory Analysis of Potentially Contaminated Soils, National Environment Protection (Assessment of Site Contamination) Measure 1999 (or an equivalent analytical method).

4.8.3.3. Report electrical conductivity in deciSiemens per metre (dS/m).

4.8.4. Test method for measuring Polynuclear Aromatic Hydrocarbons (PAHs) and benzo(a)pyrene.

4.8.4.1. Analysis using USEPA SW-846 Method 8100 Polynuclear Aromatic Hydrocarbons (or an equivalent analytical method).

4.8.4.2. Calculate the sum of all 16 PAHs for total PAHs. 4.8.4.3. Report total PAHs as mg/kg dry weight. 4.8.4.4. Report benzo(a)pyrene as mg/kg.


4.8.5. Test method for measuring benzene, toluene, ethylbenzene and xylenes (BTEX).

4.8.5.1. Method 501 (Volatile Alkanes and Monocyclic Aromatic Hydrocarbons) in Schedule B (3): Guideline on Laboratory Analysis of Potentially Contaminated Soils, National Environment Protection (Assessment of Site Contamination) Measure 1999 (or an equivalent analytical method).

4.8.5.2. Report BTEX as mg/kg.

4.8.6. Test method for measuring Total Petroleum Hydrocarbons (TPH). 4.8.6.1. Method 506 (Petroleum Hydrocarbons) in Schedule B (3):

Guideline on Laboratory Analysis of Potentially Contaminated Soils, National Environment Protection (Assessment of Site Contamination) Measure 1999 (or an equivalent analytical method).

4.8.6.2. Report as mg/kg dry weight.

4.8.7. Test method for measuring rubber, plastic, bitumen, paper, cloth, paint and wood.

4.8.7.1. NSW Roads & Traffic Authority Test Method T276 Foreign Materials Content of Recycled Crushed Concrete (or an equivalent method).

4.8.7.2. Report as percent.

Notification 4.9. On or before each transaction, the generator must provide the following to

each person to whom the generator supplies the excavated natural material: • a written statement of compliance certifying that all the requirements set

out in this order have been met; • a copy of the excavated natural material exemption, or a link to the EPA

website where the excavated natural material exemption can be found; and

• a copy of the excavated natural material order, or a link to the EPA website where the excavated natural material order can be found.

Record keeping and reporting 4.10. The generator must keep a written record of the following for a period of six

years: • the sampling plan required to be prepared under clause 4.1.1; • all characterisation sampling results in relation to the excavated natural

material supplied; • the volume of detected hotspot material and the location; • the quantity of the excavated natural material supplied; and • the name and address of each person to whom the generator supplied the

excavated natural material. 4.11. The generator must provide, on request, the characterisation and sampling

results for that excavated natural material supplied to the consumer of the excavated natural material.


5. Definitions In this order: application or apply to land means applying to land by:

• spraying, spreading or depositing on the land; or • ploughing, injecting or mixing into the land; or • filling, raising, reclaiming or contouring the land.

Bgl means below ground level, referring to soil at depth beneath the ground surface. composite sample means a sample that combines five discrete sub-samples of equal size into a single sample for the purpose of analysis. consumer means a person who applies, or intends to apply excavated natural material to land. discrete sample means a sample collected and analysed individually that will not be composited. generator means a person who generates excavated natural material for supply to a consumer. hotspot means a cylindrical volume which extends through the soil profile from the ground surface to the proposed depth of excavation, where the level of any contaminant listed in Column 1 of Table 2 is greater than the absolute maximum concentration in Column 3 of Table 2. in situ material means material that exists on or below the ground level. It does not include stockpiled material. in situ sampling means sampling undertaken on in situ material. N/A means not applicable. stockpiled material means material that has been excavated from the ground and temporarily stored on the ground prior to use. systematic sampling means sampling at points that are selected at even intervals and are statistically unbiased. transaction means:

• in the case of a one-off supply, the supply of a batch, truckload or stockpile of excavated natural material that is not repeated.

• in the case where the supplier has an arrangement with the recipient for more than one supply of excavated natural material, the first supply of excavated natural material as required under the arrangement.

Manager Waste Strategy and Innovation Environment Protection Authority (by delegation)


Notes The EPA may amend or revoke this order at any time. It is the responsibility of each of the generator and processor to ensure it complies with all relevant requirements of the most current order. The current version of this order will be available on ’ www.epa.nsw.gov.au In gazetting or otherwise issuing this order, the EPA is not in any way endorsing the supply or use of this substance or guaranteeing that the substance will confer benefit. The conditions set out in this order are designed to minimise the risk of potential harm to the environment, human health or agriculture, although neither this order nor the accompanying exemption guarantee that the environment, human health or agriculture will not be harmed. Any person or entity which supplies excavated natural material should assess whether the material is fit for the purpose the material is proposed to be used for, and whether this use may cause harm. The supplier may need to seek expert engineering or technical advice. Regardless of any exemption or order provided by the EPA, the person who causes or permits the application of the substance to land must ensure that the action is lawful and consistent with any other legislative requirements including, if applicable, any development consent(s) for managing operations on the site(s). The supply of excavated natural material remains subject to other relevant environmental regulations in the POEO Act and Waste Regulation. For example, a person who pollutes land (s. 142A) or water (s. 120), or causes air pollution through the emission of odours (s. 126), or does not meet the special requirements for asbestos waste (Part 7 of the Waste Regulation), regardless of this order, is guilty of an offence and subject to prosecution. This order does not alter the requirements of any other relevant legislation that must be met in supplying this material, including for example, the need to prepare a Safety Data Sheet. Failure to comply with the conditions of this order constitutes an offence under clause 93 of the Waste Regulation.

Examples In situ sampling at depth Example 1. If the proposed depth of ENM excavation is between 1 m bgl and 1.4 m bgl, then:

• 1 sample on surface (as per the requirements of Table 2). • 1 sample at 1 m bgl. • No further depth sampling after 1 m bgl, unless required under section 4.4.4.

Example 2. If the proposed depth of ENM excavation is at 1.75 m bgl, then:

• 1 sample on surface (as per the requirements of Table 2). • 1 sample at 1 m bgl. • 1 sample at 1.75 m bgl. • No further depth sampling after 1.75 m bgl, unless required under section

4.4.4.


Example 3. If the proposed depth of ENM excavation is at 2.25 m bgl, then:

• 1 sample on surface (as per the requirements of Table 2). • 1 sample at 1 m bgl. • 1 sample at 2 m bgl. • No further depth sampling after 2 m bgl, unless required under section 4.4.4.

Appendix B – Data Validation Report

QA/QC DATA VALIDATION REPORT Job No: ENAUWOLL04223AA

Batches:

Eurofins MGT: 462743, 463922

ALS: ES1524748

Coffey Testing: FYSH15W00725 to FYSH15W00728

page 1 of 7

I. SAMPLE HANDLING

Yes No

(Comment

below)

1. Were the sample holding times* met?

2. Were the samples in proper custody between the field and

reaching the laboratory?

See note

3. Were the samples properly and adequately preserved?

This includes keeping the samples chilled, where applicable.

See note

4. Were the samples received by the laboratory in good condition?

* Refer to laboratory reports for specific holding times.

COMMENTS:

In batch 463743, the recommended sample holding times were exceeded by 2 days for analysis of

pH and EC. The laboratory has previously indicated that samples are analysed for pH and EC

immediately after addition of water, as per standard laboratory practice. Coffey considers that the

exceeded holding times are unlikely to affect the usability of this data.

Sample temperatures upon receipt ranged between 1.8C and 6.5C. Slightly elevated sample

temperatures are not considered to affect usability of the data because all samples were packed with

sufficient ice during fieldwork and again prior to transport. This is consistent with the NEPM and

industry standards. It is considered unlikely that data is affected through potential loss of volatiles at

these elevated sample temperatures because:

o Samples are considered representative of the material and laboratory results generally

reflect field observations.

o Samples were received by the laboratory within several hours of despatch, and ice chests

containing samples were immediately placed in a fridge. Therefore the opportunity for

degradation of contaminants of potential concern (COPCs) within the sample is considered

low; and o Trip spike and blank results during soil sampling did not indicate volatile loss.

Sample Handling was: Satisfactory Unsatisfactory

Partially Satisfactory


Batches:

Eurofins MGT: 462743, 463922

ALS: ES1524748


page 2 of 7

II PRECISION/ACCURACY ASSESSMENT

Yes No

(Comment below)

1. Was a NATA registered laboratory used?

2. Did the laboratory perform the requested tests?

3. Were the laboratory methods adopted NATA endorsed?*

4. Were the appropriate test procedures followed? See note

5. Were the reporting limits satisfactory?

6. Was the NATA Seal on the reports?

7. Were the reports signed by an authorised person?

* The test methods adopted are listed in relevant laboratory reports.

COMMENTS:

The Coffey Testing laboratory was requested to exclude the ‘other vegetable matter’ component which is normally reported in the NSW RMS Test method T276 - Foreign materials type III test. The laboratory reports indicated that reported concentrations of foreign materials “Type III does not include "other vegetable matter" (natural organic matter) as per Client Specification.” For the purposes of assessing soils with respect to The ENM Order 2014, we consider that reported concentrations of Foreign Materials (including rubber, plastic, bitumen, paper, cloth, paint and wood) do meet the testing requirements of ENM.

In Eurofins MGT batch 462743, sample CTP22/0.8-1.2 recorded 0.84% of ‘Wood and other

vegetable matter’ (from Foreign Materials Type III test) is above the absolute maximum threshold

concentration of 0.10%. This is not considered significant as soils at this location did not meet other

requirements of the ENM exemption.

In ALS batch ES1524748, the certificate of analysis indicated that sample QC4A was confirmed by

re-extraction and re-analysis.

Precision/Accuracy of the Laboratory Report Satisfactory Unsatisfactory



Batches:

Eurofins MGT: 462743, 463922

ALS: ES1524748


page 3 of 7

III. FIELD QA/QC

1. Number of Primary Samples Analysed:

Analyte No of samples analysed (percentage):

Primary Duplicates Triplicate

Heavy Metals 61 5 (8%) 2 (3%)

TRH / BTEX 50 3 (6%) 2 (4%)

PAH 53 3 (6%) 2 (4%)

OCP / OPP 25 2 (8%) 1 (4%)

PCB, VHCs 6 1 (17%) -

Herbicides 5 1 (20%) -

TRH Silica Gel cleanup 3 - -

TCLP Metals 5 - -

TCLP Benzo(a)pyrene 6 1 (17%) -

Foreign Materials 45 N/A N/A

Asbestos 46 N/A N/A

pH / EC 45 3 (7%) 2 (4%)

2. Number of Days of Sampling: 2 days (soil)

3. Number and Type of QA/QC Samples Collected:

SOIL WATER

Field Duplicates (at least 1 in 10

samples)

5 intra-laboratory duplicate +

2 inter-laboratory

N/A

Trip Spikes 1 N/A

Trip Blanks (at least 1/day or sampling

event)

1 N/A

Wash Blanks / Equipment Rinsate

(at least 1/day/matrix/equipment)

N/A N/A

Other (Field Blanks, etc.) 0 N/A

4. FIELD DUPLICATES

Yes No

(Comment below)

A. Were an Adequate Number of field duplicates

analysed for each chemical (min. 10%)?

See note

B. Were RPDs within Control Limits?

a. Organics

b. Metals/Inorganics

* - Result < 10 times LOR then No Limit

- Result > 10 times LOR then control limit of 30%

COMMENTS:


Batches:

Eurofins MGT: 462743, 463922

ALS: ES1524748


page 4 of 7

Results of quality control soil samples are presented in Table QAQC1.

Duplicates were not analysed for TRH Silica Gel Cleanup and TCLP metals as these were not

considered primary contaminants of concern. An insufficient number of inter-laboratory soil

duplicates were analysed for several analytes. This is not considered significant as sufficient

duplicates were analysed as a whole.

RPDs of 31% to 175%, above the control limit of 30%, were recorded for heavy metals (lead, copper

and zinc) and PAHs between several duplicate pairs. Some variability may be expected for these

analytes. The variability is likely to be attributed to the heterogeneity of the contaminant distribution in

the topsoil matrix. This should be considered in the context of this assessment, especially where

sample concentrations were slightly above or below the adopted thresholds.

5. TRIP BLANKS

Yes No

(Comment below)

A. Were an adequate number of trip blanks collected? See below

B. Were the trip blanks free of contaminants?

(If no, comment whether the contaminants present are also

detected in the samples and whether they are common

laboratory chemicals.)

6. TRIP SPIKES

Yes No

(Comment below)

A. Were an adequate number of trip spikes collected?

B. Were the spike recoveries within control limits (60% to

110%)?

7. WASH BLANKS

Yes No

(Comment below)

A. Were an adequate number of Wash Blanks collected? N/A

B. Were the Wash Blanks free of contaminants?

(If no, comment whether the contaminants present are also

detected in the samples and whether they are common

laboratory chemicals.)

N/A

COMMENTS:

Results of quality control soil samples are presented in Table QAQC2.

A laboratory-prepared trip spike and trip blank sample was carried into the field and transported with

samples collected in this project. Trip spike and blanks were not carried into the field during all days of

sampling. We consider that volatile contamination, although possible, was not a primary contaminant of


Batches:

Eurofins MGT: 462743, 463922

ALS: ES1524748


page 5 of 7

concern for this project. The results of the trip spike and trip blank indicate that a loss or gain of

volatiles is unlikely to have occurred during transport.

Soil samples were collected directly from the testpit from soils which had not come in contact with

excavation equipment. A rinsate blank was therefore not required on all days of sampling.

Field QA/QC was: Satisfactory Unsatisfactory



Batches:

Eurofins MGT: 462743, 463922

ALS: ES1524748


page 6 of 7

IV LABORATORY INTERNAL QUALITY CONTROL PROCEDURES

1. Type of QA/QC Samples

TR

H

TP

H (

with S

ilica

Gel C

leanup)

BT

EX

PA

H

OC

P/O

PP

PC

B

VH

C

Herb

icid

es

Meta

ls

pH

EC

Laboratory Blanks/Reagent Blanks (at least 1 per batch)

NA

Laboratory Duplicates (at least 1 per batch or 1 per 10 samples whichever is the smaller)

Matrix Spikes/Matrix Spike Duplicates (1 for each soil type)

NA NA

Laboratory Control Spike NA NA Surrogate (where appropriate)* NA NA 1 2 2/1 2 1 1 NA NA NA *Number of surrogate spikes carried out on each sample

Yes No

(Comment below)

2 Were the laboratory blanks/reagent blanks free of contamination?

3. Were the spike recoveries within laboratory control limits?*

a. Organics

b. Metals/Inorganic

4. Were the RPDs of the laboratory duplicates within control limits?#

See note

5. Were the surrogate recoveries within control limits?

Eurofins Laboratory control limits:

* - General: MS & LCS (70 to 130%) & surrogates (50 to

150%)

- Phenols: MS & LCS (30 to 130%) & surrogates (20 to

130%) # - Result < 10 times LOR then No Limit

- Result between 10 and 20 times LOR then control limit

of 0 to 50%

- Result > 20 times LOR then control limit of 0 to 30%

ALS control limits:

* - Inorganics: LCS & surrogates (various)

- Organics: LCS & surrogates (various)

- Matrix spikes: (70 to 130%) # - Result < 10 times LOR: No Limit

- Result between 10 and 20 times LOR: 0% - 50%

- Result > 20 times LOR: 0% - 20%

COMMENTS:

In batch 462743, laboratory duplicates recorded RPDs between 33% and 65% above the control

limit of 30% for nickel. The laboratory indicated that these RPDs pass the Eurofins MGT

acceptance criteria and therefore are not significant.

5. The laboratory internal QA/QC was: Satisfactory Unsatisfactory



Batches:

Eurofins MGT: 462743, 463922

ALS: ES1524748


page 7 of 7

V. DATA USABILITY

1. Data Directly Usable

2. Data Usable with the following corrections/modifications (see comment below)

3. Data Not Usable.

COMMENTS:

Higher RPDs were recorded between soil duplicate pairs for lead, zinc and PAHs. Some variability may

be expected for these analytes. The significance of this variability was considered for samples which

reported lead or zinc concentrations marginally below or marginally above the adopted threshold

concentrations. In the context of this assessment, the variability was not considered to affect the overall

conclusions of this assessment.

QA/QC Report Prepared by _________________________

QA/QC Report Reviewed by: _________________________

(Reviewer)

Alexander Williams

Manuel Fernandez

Table QAQC1: Relative Percentage Difference for Soil Samples

Primary

Sample Conc.

(mg/kg)

Intra-

laboratory

duplicate

Sample Conc.

(mg/Kg)

RPD (%)

Primary

Sample Conc.

(mg/kg)

Intra-

laboratory

duplicate

Sample Conc.

(mg/Kg)

RPD (%)

Primary

Sample Conc.

(mg/kg)

Inter-

laboratory

duplicate

Sample Conc.

(mg/Kg)

RPD (%)

Primary

Sample Conc.

(mg/kg)

Intra-

laboratory

duplicate

Sample Conc.

(mg/Kg)

RPD (%)

Primary

Sample Conc.

(mg/kg)

Intra-

laboratory

duplicate

Sample Conc.

(mg/Kg)

RPD (%)

Primary

Sample Conc.

(mg/kg)

Inter-

laboratory

duplicate

Sample Conc.

(mg/Kg)

RPD (%)

Primary

Sample Conc.

(mg/kg)

Intra-

laboratory

duplicate

Sample Conc.

(mg/Kg)

RPD (%)

Sample No. CTP01 QC1 CTP04 QC2 CTP04 QC2A CTP-13 QC3 CTP-10 QC4 CTP-10 QC4A CBH-8 QC5

Depth (m) Eurofins ALS 0.0-0.2 0.0-0.2 0.0-0.2 0.0-0.2 0.0-0.2 0.0-0.2 0.0-0.1 0.0-0.1 0.0-0.1 0.0-0.1 0.0-0.1 0.0-0.1 0.0-0.1 0.0-0.1

HEAVY METALS

Arsenic 2 5 18 15.0 18 8.8 8.8 0 8.8 10.0 13 3.8 2.4 45 < 2 2.6 NC < 2 <5 ND 17 13.0 27

Cadmium 0.4 1 < 0.4 < 0.4 ND < 0.4 < 0.4 ND < 0.4 <1 ND < 0.4 < 0.4 ND < 0.4 < 0.4 ND < 0.4 <1 ND < 0.4 < 0.4 ND

Chromium 5 2 19 20 5 13 14 7 13 15 14 7.3 6.2 16 < 5 7.2 NC < 5 7 NC 16 12 29Copper 5 5 27 33 20 27 65 83 27 25 8 7.8 7.7 1 8.4 8.6 2 8.4 9 7 15 10 40

Lead 5 5 110 150 31 270 280 4 270 236 13 19 17 11 55 54 2 55 55 0 26 20 26

Mercury 0.05 0.1 0.08 0.11 32 0.11 0.12 9 0.11 0.1 10 0.06 < 0.05 NC < 0.05 0.09 NC < 0.05 <0.1 ND < 0.05 < 0.05 ND

Nickel 5 2 8.3 11.0 28 5.6 6.5 15 5.6 6.0 7 < 5 < 5 ND < 5 < 5 ND < 5 4.0 NC < 5 < 5 NDZinc 5 5 610 340 57 1400 830 51 1400 382 114 120 110 9 150 190 24 150 188 22 22 14 44

TOTAL PETROLEUM HYDROCARBONS

TRH C6-C9 20 10 < 20 - - < 20 < 20 ND < 20 <10 ND < 20 - - < 20 < 20 ND < 20 <10 ND < 20 < 20 ND

TRH C10-C14 20 50 < 20 - - < 20 < 20 ND < 20 <50 ND < 20 - - < 20 < 20 ND < 20 <50 ND < 20 < 20 ND

TRH C15-C28 50 100 68 - - < 50 210 NC < 50 <100 ND < 50 - - 140 330 81 140 <100 NC < 50 < 50 ND

TRH C29-C36 50 100 260 - - < 50 180 NC < 50 <100 ND < 50 - - 490 1300 91 490 <100 NC < 50 < 50 NDTRH C10-36 (Total) 50 50 330 - - < 50 390 NC < 50 <50 ND < 50 - - 630 1600 87 630 <50 171 < 50 < 50 ND

BTEX

Benzene 0.1 0.2 < 0.1 - - < 0.1 < 0.1 ND < 0.1 <0.2 ND < 0.1 - - < 0.1 < 0.1 ND < 0.1 <0.2 ND < 0.1 < 0.1 ND

Toluene 0.1 0.5 < 0.1 - - < 0.1 < 0.1 ND < 0.1 <0.5 ND < 0.1 - - < 0.1 < 0.1 ND < 0.1 <0.5 ND < 0.1 < 0.1 ND

Ethylbenzene 0.1 0.5 < 0.1 - - < 0.1 < 0.1 ND < 0.1 <0.5 ND < 0.1 - - < 0.1 < 0.1 ND < 0.1 <0.5 ND < 0.1 < 0.1 ND

Total Xylene 0.3 0.5 < 0.3 - - < 0.3 < 0.3 ND < 0.3 <0.5 ND < 0.3 - - < 0.3 < 0.3 ND < 0.3 <0.5 ND < 0.3 < 0.3 ND

POLYCYCLIC AROMATIC HYDROCARBONS

Benzo(a)pyrene 0.5 0.5 < 0.5 - - 0.7 3.6 135 0.7 0.5 33 < 0.5 - - 0.8 < 0.5 NC 0.8 <0.5 NC < 0.5 < 0.5 ND

Total PAH 0.5 0.5 2.2 - - 2.8 39.0 173 2.8 4.9 55 < 0.5 - - 7.6 5.4 34 7.6 <0.5 175 1.9 2.2 15

POLYCYCLIC AROMATIC HYDROCARBONS (TCLP)

Benzo(a)pyrene (mg/L) <0.001 <0.001 - - - <0.001 <0.001 ND <0.001 - - - - - - - - - - - - - -

ORGANOPHOSPHORUS PESTICIDES

Organochlorine pesticides (OCPs) various N/A - - - <LOR <LOR ND <LOR - - <LOR - - <LOR <LOR ND <LOR - - - - -

Organophosphate pesticides (OPPs) various N/A - - - <LOR <LOR ND <LOR - - <LOR - - <LOR <LOR ND <LOR - - - - -

Volatile Halogenated Compounds (VHCs) various N/A - <LOR - - - - - - - <LOR <LOR ND - - - - - - - - -

Polychlorinated biphenyls (PCBs) 0.1 N/A - < 0.1 - - - - - - - < 0.1 < 0.1 ND - - - - - - - - -

Acid Herbicides 0.5 N/A <LOR <LOR ND - - - - - - <LOR - - - - - - - - - - -

SOIL PROPERTIES

Conductivity (uS/cm) 5 - 35 - - 32 26 21 32 28 13 27 - - 26 37 35 26 22 17 34 30 13

Conductivity (dS/m) 0.005 - 0.035 - - 0.032 0.026 21 0.032 0.028 13 0.027 - - 0.026 0.037 35 0.026 0.022 17 0.034 0.030 13pH (units)(1:5 soil:CaCl2 extract) 0.1 - 6 - - 6 6.1 2 6 6.3 2 6 - - 6 6 2 6 6.5 6 5 5.2 2

Notes:

Bold RPD exceeds control limit of 30% for soil if:

- Result < 10 times LOR then No Limit

- Result > 10 times LOR then control limit of 30%

RPD Relative Percentage Difference

NA Not Applicable

ND Not Detected

NC Contaminant is not detected in primary sample but is detected in duplicate sample, or vice versa

LOR Limit of Reporting

- No result or guideline

Laboratory Reporting

Limits (mg/kg)

Batch 462743 462743462743 462743462743 / ES1524748 462743 / ES1524748462743 / 463922

TABLE QAQC2

SUMMARY OF FIELD CONTROL SAMPLES LABORATORY RESULTS

Sample ID Trip Blank Trip Spike

Date of Sampling 18-Jun-15 18-Jun-15

QAQC Type Trip Blank Trip Spike

Batch 462743 462743

Unit mg/kg %

Matrix Soil Soil

TOTAL PETROLEUM HYDROCARBONS

F1 (C6-C10) <20 -

F1 (C6-C10 less BTEX) <20 -

F2 (>C10-C16) - -

F2 (>C10-C16 less naphthalene) - -

F3 (>C16-C34) - -

F4 (>C34-C40) - -

BTEX

Benzene < 0.1 93%

Toluene < 0.1 94%

Ethylbenzene < 0.1 94%

Total Xylene < 0.3 95%

Notes:

Bold Concentration exceeds control limit

- Not Analysed

ND Not Detected

QAQC Control Ordinates

Trip Spike Recorvery concentrations to between 60% and 110%

Trip Blank Recovery concentrations to be ND

Appendix C – Calibration Certificates

Appendix D – Laboratory Reports

Certificate of Analysis

Coffey Environments Pty Ltd Wollongong

118 Auburn Street

Wollongong

NSW 2500

Attention: Alexander Williams

Report 462743-S

Project name ENAUWOLL04223AA

Received Date Jun 24, 2015

Client Sample ID CTP01/0.0-0.2 CTP01/1.0-1.2 CTP01/1.4-1.6 CTP01/1.7-1.8

Sample Matrix Soil Soil Soil Soil

Eurofins | mgt Sample No. S15-Jn20258 S15-Jn20259 S15-Jn20260 S15-Jn20261

Date Sampled Jun 22, 2015 Jun 22, 2015 Jun 22, 2015 Jun 22, 2015

Test/Reference LOR Unit

Total Recoverable Hydrocarbons - 1999 NEPM Fractions

TRH C6-C9 20 mg/kg < 20 < 20 < 20 < 20

TRH C10-C14 20 mg/kg < 20 < 20 < 20 < 20

TRH C15-C28 50 mg/kg 68 < 50 < 50 < 50

TRH C29-C36 50 mg/kg 260 < 50 < 50 < 50

TRH C10-36 (Total) 50 mg/kg 330 < 50 < 50 < 50

BTEX

Benzene 0.1 mg/kg < 0.1 < 0.1 < 0.1 < 0.1

Toluene 0.1 mg/kg < 0.1 < 0.1 < 0.1 < 0.1

Ethylbenzene 0.1 mg/kg < 0.1 < 0.1 < 0.1 < 0.1

m&p-Xylenes 0.2 mg/kg < 0.2 < 0.2 < 0.2 < 0.2

o-Xylene 0.1 mg/kg < 0.1 < 0.1 < 0.1 < 0.1

Xylenes - Total 0.3 mg/kg < 0.3 < 0.3 < 0.3 < 0.3

4-Bromofluorobenzene (surr.) 1 % 73 74 73 71


NaphthaleneN02 0.5 mg/kg < 0.5 < 0.5 < 0.5 < 0.5

TRH C6-C10 20 mg/kg < 20 < 20 < 20 < 20

TRH C6-C10 less BTEX (F1)N04 20 mg/kg < 20 < 20 < 20 < 20

TRH >C10-C16 50 mg/kg < 50 < 50 < 50 < 50

TRH >C10-C16 less Naphthalene (F2)N01 50 mg/kg < 50 < 50 < 50 < 50

TRH >C16-C34 100 mg/kg 310 < 100 < 100 < 100

TRH >C34-C40 100 mg/kg 200 < 100 < 100 < 100

Halogenated Volatile Organics

1.1-Dichloroethane 0.5 mg/kg - - < 0.5 -

1.1-Dichloroethene 0.5 mg/kg - - < 0.5 -

1.1.1-Trichloroethane 0.5 mg/kg - - < 0.5 -

1.1.1.2-Tetrachloroethane 0.5 mg/kg - - < 0.5 -



1.2-Dibromoethane 0.5 mg/kg - - < 0.5 -

1.2-Dichlorobenzene 0.5 mg/kg - - < 0.5 -


1.2-Dichloropropane 0.5 mg/kg - - < 0.5 -

1.2.3-Trichloropropane 0.5 mg/kg - - < 0.5 -




Date Reported: Jul 01, 2015

Eurofins | mgt Unit F3, Building F, 16 Mars Road, Lane Cove West, NSW, Australia, 2066

ABN : 50 005 085 521 Telephone: +61 2 9900 8400 Facsimile: +61 2 9420 2977

Page 1 of 72

Report Number: 462743-S

NATA AccreditedAccreditation Number 1261Site Number 1254

Accredited for compliance with ISO/IEC 17025.The results of the tests, calibrations and/ormeasurements included in this document are traceableto Australian/national standards.







Bromodichloromethane 0.5 mg/kg - - < 0.5 -

Bromoform 0.5 mg/kg - - < 0.5 -

Bromomethane 0.5 mg/kg - - < 0.5 -

Carbon Tetrachloride 0.5 mg/kg - - < 0.5 -

Chlorobenzene 0.5 mg/kg - - < 0.5 -

Chloroform 0.5 mg/kg - - < 0.5 -

Chloromethane 0.5 mg/kg - - < 0.5 -

cis-1.2-Dichloroethene 0.5 mg/kg - - < 0.5 -

cis-1.3-Dichloropropene 0.5 mg/kg - - < 0.5 -

Dibromochloromethane 0.5 mg/kg - - < 0.5 -

Dibromomethane 0.5 mg/kg - - < 0.5 -

Iodomethane 0.5 mg/kg - - < 0.5 -

Methylene Chloride 0.5 mg/kg - - < 0.5 -

Tetrachloroethene 0.5 mg/kg - - < 0.5 -

trans-1.2-Dichloroethene 0.5 mg/kg - - < 0.5 -

trans-1.3-Dichloropropene 0.5 mg/kg - - < 0.5 -

Trichloroethene 0.5 mg/kg - - < 0.5 -

Trichlorofluoromethane 0.5 mg/kg - - < 0.5 -

Vinyl chloride 0.5 mg/kg - - < 0.5 -

Fluorobenzene (surr.) 1 % - - 99 -

Polycyclic Aromatic Hydrocarbons

Benzo(a)pyrene TEQ (lower bound) * 0.5 mg/kg < 0.5 1.2 1.6 < 0.5

Benzo(a)pyrene TEQ (medium bound) * 0.5 mg/kg 0.6 1.5 1.9 0.6

Benzo(a)pyrene TEQ (upper bound) * 0.5 mg/kg 1.2 1.7 2.2 1.2

Acenaphthene 0.5 mg/kg < 0.5 < 0.5 < 0.5 < 0.5

Acenaphthylene 0.5 mg/kg < 0.5 < 0.5 < 0.5 < 0.5

Anthracene 0.5 mg/kg < 0.5 < 0.5 < 0.5 < 0.5

Benz(a)anthracene 0.5 mg/kg < 0.5 0.9 1.2 < 0.5

Benzo(a)pyrene 0.5 mg/kg < 0.5 0.9 1.3 < 0.5

Benzo(b&j)fluorantheneN07 0.5 mg/kg < 0.5 1.0 0.8 < 0.5

Benzo(g.h.i)perylene 0.5 mg/kg < 0.5 < 0.5 < 0.5 < 0.5

Benzo(k)fluoranthene 0.5 mg/kg < 0.5 0.8 1.0 < 0.5

Chrysene 0.5 mg/kg < 0.5 0.8 1.1 < 0.5

Dibenz(a.h)anthracene 0.5 mg/kg < 0.5 < 0.5 < 0.5 < 0.5

Fluoranthene 0.5 mg/kg 1.1 1.3 2.8 < 0.5

Fluorene 0.5 mg/kg < 0.5 < 0.5 < 0.5 < 0.5

Indeno(1.2.3-cd)pyrene 0.5 mg/kg < 0.5 < 0.5 < 0.5 < 0.5

Naphthalene 0.5 mg/kg < 0.5 < 0.5 < 0.5 < 0.5

Phenanthrene 0.5 mg/kg < 0.5 < 0.5 1.7 < 0.5

Pyrene 0.5 mg/kg 1.1 1.5 2.5 < 0.5

Total PAH* 0.5 mg/kg 2.2 7.2 12 < 0.5

2-Fluorobiphenyl (surr.) 1 % 120 116 125 114

p-Terphenyl-d14 (surr.) 1 % 121 121 114 112

Organochlorine Pesticides

Chlordanes - Total 0.1 mg/kg - - - < 0.1

4.4'-DDD 0.05 mg/kg - - - < 0.05

4.4'-DDE 0.05 mg/kg - - - < 0.05

4.4'-DDT 0.05 mg/kg - - - < 0.05

a-BHC 0.05 mg/kg - - - < 0.05




Page 2 of 72








Aldrin 0.05 mg/kg - - - < 0.05

b-BHC 0.05 mg/kg - - - < 0.05

d-BHC 0.05 mg/kg - - - < 0.05

Dieldrin 0.05 mg/kg - - - < 0.05

Endosulfan I 0.05 mg/kg - - - < 0.05

Endosulfan II 0.05 mg/kg - - - < 0.05

Endosulfan sulphate 0.05 mg/kg - - - < 0.05

Endrin 0.05 mg/kg - - - < 0.05

Endrin aldehyde 0.05 mg/kg - - - < 0.05

Endrin ketone 0.05 mg/kg - - - < 0.05

g-BHC (Lindane) 0.05 mg/kg - - - < 0.05

Heptachlor 0.05 mg/kg - - - < 0.05

Heptachlor epoxide 0.05 mg/kg - - - < 0.05

Hexachlorobenzene 0.05 mg/kg - - - < 0.05

Methoxychlor 0.2 mg/kg - - - < 0.2

Toxaphene 1 mg/kg - - - < 1

Dibutylchlorendate (surr.) 1 % - - - 81

Tetrachloro-m-xylene (surr.) 1 % - - - 92

Polychlorinated Biphenyls

Aroclor-1016 0.5 mg/kg - - < 0.5 -

Aroclor-1221 0.1 mg/kg - - < 0.1 -

Aroclor-1232 0.5 mg/kg - - < 0.5 -

Aroclor-1242 0.5 mg/kg - - < 0.5 -

Aroclor-1248 0.5 mg/kg - - < 0.5 -

Aroclor-1254 0.5 mg/kg - - < 0.5 -

Aroclor-1260 0.5 mg/kg - - < 0.5 -

Total PCB* 0.1 mg/kg - - < 0.1 -

Dibutylchlorendate (surr.) 1 % - - 77 -

Acid Herbicides

2.4-D 0.5 mg/kg < 0.5 - - -

2.4-DB 0.5 mg/kg < 0.5 - - -

2.4.5-T 0.5 mg/kg < 0.5 - - -

2.4.5-TP 0.5 mg/kg < 0.5 - - -

Actril (loxynil) 0.5 mg/kg < 0.5 - - -

Dicamba 0.5 mg/kg < 0.5 - - -

Dichlorprop 0.5 mg/kg < 0.5 - - -

Dinitro-o-cresol 0.5 mg/kg < 0.5 - - -

Dinoseb 0.5 mg/kg < 0.5 - - -

MCPA 0.5 mg/kg < 0.5 - - -

MCPB 0.5 mg/kg < 0.5 - - -

Mecoprop 0.5 mg/kg < 0.5 - - -

Warfarin (surr.) 1 % 83 - - -

Organophosphorus Pesticides (OP)

Chlorpyrifos 0.5 mg/kg - - - < 0.5

Coumaphos 0.5 mg/kg - - - < 0.5

Demeton (total) 1 mg/kg - - - < 1

Diazinon 0.5 mg/kg - - - < 0.5

Dichlorvos 0.5 mg/kg - - - < 0.5

Dimethoate 0.5 mg/kg - - - < 0.5




Page 3 of 72








Disulfoton 0.5 mg/kg - - - < 0.5

Ethoprop 0.5 mg/kg - - - < 0.5

Fenitrothion 0.5 mg/kg - - - < 0.5

Fensulfothion 0.5 mg/kg - - - < 0.5

Fenthion 0.5 mg/kg - - - < 0.5

Methyl azinphos 0.5 mg/kg - - - < 0.5

Malathion 0.5 mg/kg - - - < 0.5

Methyl parathion 0.5 mg/kg - - - < 0.5

Mevinphos 0.5 mg/kg - - - < 0.5

Monocrotophos 10 mg/kg - - - < 10

Parathion 0.5 mg/kg - - - < 0.5

Phorate 0.5 mg/kg - - - < 0.5

Profenofos 0.5 mg/kg - - - < 0.5

Prothiofos 0.5 mg/kg - - - < 0.5

Ronnel 0.5 mg/kg - - - < 0.5

Stirophos 0.5 mg/kg - - - < 0.5

Trichloronate 0.5 mg/kg - - - < 0.5

Triphenylphosphate (surr.) 1 % - - - 112

Conductivity (1:5 aqueous extract at 25°C) 5 uS/cm 35 58 31 -

pH (1:5 Aqueous extract) 0.1 pH Units 6.4 5.8 6.5 -

% Moisture 0.1 % 27 21 26 23

Heavy Metals

Arsenic 2 mg/kg 18 14 9.4 11

Cadmium 0.4 mg/kg < 0.4 < 0.4 < 0.4 < 0.4

Chromium 5 mg/kg 19 17 14 11

Copper 5 mg/kg 27 24 37 210

Lead 5 mg/kg 110 40 320 11

Mercury 0.05 mg/kg 0.08 < 0.05 0.25 0.08

Nickel 5 mg/kg 8.3 < 5 5.5 < 5

Zinc 5 mg/kg 610 42 150 24

Client Sample ID CTP02/1.35-1.45 CTP02A/0.0-0.2 CTP03/0.0-0.2 CTP03/0.8-1.0






TRH C6-C9 20 mg/kg < 20 < 20 < 20 < 20

TRH C10-C14 20 mg/kg < 20 < 20 22 < 20

TRH C15-C28 50 mg/kg < 50 270 < 50 < 50

TRH C29-C36 50 mg/kg < 50 960 < 50 < 50

TRH C10-36 (Total) 50 mg/kg < 50 1200 < 50 < 50




Page 4 of 72







BTEX

Benzene 0.1 mg/kg < 0.1 < 0.1 < 0.1 < 0.1

Toluene 0.1 mg/kg < 0.1 < 0.1 < 0.1 < 0.1


m&p-Xylenes 0.2 mg/kg < 0.2 < 0.2 < 0.2 < 0.2

o-Xylene 0.1 mg/kg < 0.1 < 0.1 < 0.1 < 0.1





TRH C6-C10 20 mg/kg < 20 < 20 < 20 < 20


TRH >C10-C16 50 mg/kg < 50 < 50 < 50 < 50


TRH >C16-C34 100 mg/kg < 100 830 < 100 < 100

TRH >C34-C40 100 mg/kg < 100 500 < 100 < 100


Benzo(a)pyrene TEQ (lower bound) * 0.5 mg/kg < 0.5 < 0.5 < 0.5 11

Benzo(a)pyrene TEQ (medium bound) * 0.5 mg/kg 0.6 0.6 0.6 11

Benzo(a)pyrene TEQ (upper bound) * 0.5 mg/kg 1.2 1.2 1.2 11


Acenaphthylene 0.5 mg/kg < 0.5 < 0.5 < 0.5 3.3

Anthracene 0.5 mg/kg < 0.5 < 0.5 < 0.5 4.3

Benz(a)anthracene 0.5 mg/kg < 0.5 < 0.5 < 0.5 7.7

Benzo(a)pyrene 0.5 mg/kg < 0.5 < 0.5 < 0.5 7.5

Benzo(b&j)fluorantheneN07 0.5 mg/kg < 0.5 < 0.5 < 0.5 6.0

Benzo(g.h.i)perylene 0.5 mg/kg < 0.5 < 0.5 < 0.5 3.9

Benzo(k)fluoranthene 0.5 mg/kg < 0.5 < 0.5 < 0.5 7.5

Chrysene 0.5 mg/kg < 0.5 < 0.5 < 0.5 7.1

Dibenz(a.h)anthracene 0.5 mg/kg < 0.5 < 0.5 < 0.5 0.8

Fluoranthene 0.5 mg/kg < 0.5 < 0.5 < 0.5 19

Fluorene 0.5 mg/kg < 0.5 < 0.5 < 0.5 2.2

Indeno(1.2.3-cd)pyrene 0.5 mg/kg < 0.5 < 0.5 < 0.5 3.5


Phenanthrene 0.5 mg/kg < 0.5 < 0.5 < 0.5 18

Pyrene 0.5 mg/kg < 0.5 < 0.5 < 0.5 16

Total PAH* 0.5 mg/kg < 0.5 < 0.5 < 0.5 110




Chlordanes - Total 0.1 mg/kg < 0.1 < 0.1 < 0.1 -

4.4'-DDD 0.05 mg/kg < 0.05 < 0.05 < 0.05 -

4.4'-DDE 0.05 mg/kg < 0.05 < 0.05 < 0.05 -

4.4'-DDT 0.05 mg/kg < 0.05 < 0.05 < 0.05 -

a-BHC 0.05 mg/kg < 0.05 < 0.05 < 0.05 -

Aldrin 0.05 mg/kg < 0.05 < 0.05 < 0.05 -

b-BHC 0.05 mg/kg < 0.05 < 0.05 < 0.05 -

d-BHC 0.05 mg/kg < 0.05 < 0.05 < 0.05 -

Dieldrin 0.05 mg/kg < 0.05 < 0.05 < 0.05 -

Endosulfan I 0.05 mg/kg < 0.05 < 0.05 < 0.05 -




Page 5 of 72








Endosulfan II 0.05 mg/kg < 0.05 < 0.05 < 0.05 -

Endosulfan sulphate 0.05 mg/kg < 0.05 < 0.05 < 0.05 -

Endrin 0.05 mg/kg < 0.05 < 0.05 < 0.05 -

Endrin aldehyde 0.05 mg/kg < 0.05 < 0.05 < 0.05 -

Endrin ketone 0.05 mg/kg < 0.05 < 0.05 < 0.05 -

g-BHC (Lindane) 0.05 mg/kg < 0.05 < 0.05 < 0.05 -

Heptachlor 0.05 mg/kg < 0.05 < 0.05 < 0.05 -

Heptachlor epoxide 0.05 mg/kg < 0.05 < 0.05 < 0.05 -

Hexachlorobenzene 0.05 mg/kg < 0.05 < 0.05 < 0.05 -

Methoxychlor 0.2 mg/kg < 0.2 < 0.2 < 0.2 -

Toxaphene 1 mg/kg < 1 < 1 < 1 -

Dibutylchlorendate (surr.) 1 % 89 93 107 -

Tetrachloro-m-xylene (surr.) 1 % 84 109 105 -


Chlorpyrifos 0.5 mg/kg < 0.5 < 0.5 < 0.5 -

Coumaphos 0.5 mg/kg < 0.5 < 0.5 < 0.5 -

Demeton (total) 1 mg/kg < 1 < 1 < 1 -

Diazinon 0.5 mg/kg < 0.5 < 0.5 < 0.5 -

Dichlorvos 0.5 mg/kg < 0.5 < 0.5 < 0.5 -

Dimethoate 0.5 mg/kg < 0.5 < 0.5 < 0.5 -

Disulfoton 0.5 mg/kg < 0.5 < 0.5 < 0.5 -

Ethoprop 0.5 mg/kg < 0.5 < 0.5 < 0.5 -

Fenitrothion 0.5 mg/kg < 0.5 < 0.5 < 0.5 -

Fensulfothion 0.5 mg/kg < 0.5 < 0.5 < 0.5 -

Fenthion 0.5 mg/kg < 0.5 < 0.5 < 0.5 -

Methyl azinphos 0.5 mg/kg < 0.5 < 0.5 < 0.5 -

Malathion 0.5 mg/kg < 0.5 < 0.5 < 0.5 -

Methyl parathion 0.5 mg/kg < 0.5 < 0.5 < 0.5 -

Mevinphos 0.5 mg/kg < 0.5 < 0.5 < 0.5 -

Monocrotophos 10 mg/kg < 10 < 10 < 10 -

Parathion 0.5 mg/kg < 0.5 < 0.5 < 0.5 -

Phorate 0.5 mg/kg < 0.5 < 0.5 < 0.5 -

Profenofos 0.5 mg/kg < 0.5 < 0.5 < 0.5 -

Prothiofos 0.5 mg/kg < 0.5 < 0.5 < 0.5 -

Ronnel 0.5 mg/kg < 0.5 < 0.5 < 0.5 -

Stirophos 0.5 mg/kg < 0.5 < 0.5 < 0.5 -

Trichloronate 0.5 mg/kg < 0.5 < 0.5 < 0.5 -

Triphenylphosphate (surr.) 1 % 104 104 107 -

Conductivity (1:5 aqueous extract at 25°C) 5 uS/cm - 120 33 52

pH (1:5 Aqueous extract) 0.1 pH Units - 7.2 6.3 6.9

% Moisture 0.1 % 17 30 16 30

Heavy Metals

Arsenic 2 mg/kg 8.2 290 2.7 10

Cadmium 0.4 mg/kg < 0.4 < 0.4 < 0.4 0.6

Chromium 5 mg/kg 8.5 18 5.0 24

Copper 5 mg/kg 25 22 7.1 91

Lead 5 mg/kg 23 77 18 860

Mercury 0.05 mg/kg < 0.05 0.05 < 0.05 0.46




Page 6 of 72







Heavy Metals

Nickel 5 mg/kg < 5 9.7 < 5 10

Zinc 5 mg/kg 28 510 78 440

Client Sample ID CTP04/0.0-0.2 CTP04/0.3-0.4 CTP05/0.0-0.2 QC2






TRH C6-C9 20 mg/kg < 20 - < 20 < 20

TRH C10-C14 20 mg/kg < 20 - < 20 < 20

TRH C15-C28 50 mg/kg < 50 - 210 210

TRH C29-C36 50 mg/kg < 50 - 1200 180

TRH C10-36 (Total) 50 mg/kg < 50 - 1400 390

BTEX

Benzene 0.1 mg/kg < 0.1 - < 0.1 < 0.1

Toluene 0.1 mg/kg < 0.1 - < 0.1 < 0.1

Ethylbenzene 0.1 mg/kg < 0.1 - < 0.1 < 0.1

m&p-Xylenes 0.2 mg/kg < 0.2 - < 0.2 < 0.2

o-Xylene 0.1 mg/kg < 0.1 - < 0.1 < 0.1

Xylenes - Total 0.3 mg/kg < 0.3 - < 0.3 < 0.3

4-Bromofluorobenzene (surr.) 1 % 71 - 71 72


NaphthaleneN02 0.5 mg/kg < 0.5 - < 0.5 < 0.5

TRH C6-C10 20 mg/kg < 20 - < 20 < 20

TRH C6-C10 less BTEX (F1)N04 20 mg/kg < 20 - < 20 < 20

TRH >C10-C16 50 mg/kg < 50 - < 50 < 50

TRH >C10-C16 less Naphthalene (F2)N01 50 mg/kg < 50 - < 50 < 50

TRH >C16-C34 100 mg/kg < 100 - 910 290

TRH >C34-C40 100 mg/kg < 100 - 520 < 100


Benzo(a)pyrene TEQ (lower bound) * 0.5 mg/kg 0.7 - < 0.5 5.5

Benzo(a)pyrene TEQ (medium bound) * 0.5 mg/kg 1.1 - 0.6 5.5

Benzo(a)pyrene TEQ (upper bound) * 0.5 mg/kg 1.4 - 1.2 5.5

Acenaphthene 0.5 mg/kg < 0.5 - < 0.5 < 0.5

Acenaphthylene 0.5 mg/kg < 0.5 - < 0.5 < 0.5

Anthracene 0.5 mg/kg < 0.5 - < 0.5 1.0

Benz(a)anthracene 0.5 mg/kg < 0.5 - < 0.5 3.6

Benzo(a)pyrene 0.5 mg/kg 0.7 - < 0.5 3.6

Benzo(b&j)fluorantheneN07 0.5 mg/kg < 0.5 - < 0.5 2.3

Benzo(g.h.i)perylene 0.5 mg/kg < 0.5 - < 0.5 2.1

Benzo(k)fluoranthene 0.5 mg/kg < 0.5 - < 0.5 2.5

Chrysene 0.5 mg/kg < 0.5 - < 0.5 3.4

Dibenz(a.h)anthracene 0.5 mg/kg < 0.5 - < 0.5 0.8

Fluoranthene 0.5 mg/kg 1.0 - < 0.5 7.1

Fluorene 0.5 mg/kg < 0.5 - < 0.5 < 0.5

Indeno(1.2.3-cd)pyrene 0.5 mg/kg < 0.5 - < 0.5 1.8




Page 7 of 72








Naphthalene 0.5 mg/kg < 0.5 - < 0.5 < 0.5

Phenanthrene 0.5 mg/kg < 0.5 - < 0.5 3.3

Pyrene 0.5 mg/kg 1.1 - < 0.5 7.3

Total PAH* 0.5 mg/kg 2.8 - < 0.5 39

2-Fluorobiphenyl (surr.) 1 % 117 - 117 117

p-Terphenyl-d14 (surr.) 1 % 116 - 119 114


Chlordanes - Total 0.1 mg/kg < 0.1 - < 0.1 < 0.1

4.4'-DDD 0.05 mg/kg < 0.05 - < 0.05 < 0.05

4.4'-DDE 0.05 mg/kg < 0.05 - < 0.05 < 0.05

4.4'-DDT 0.05 mg/kg < 0.05 - < 0.05 < 0.05

a-BHC 0.05 mg/kg < 0.05 - < 0.05 < 0.05

Aldrin 0.05 mg/kg < 0.05 - < 0.05 < 0.05

b-BHC 0.05 mg/kg < 0.05 - < 0.05 < 0.05

d-BHC 0.05 mg/kg < 0.05 - < 0.05 < 0.05

Dieldrin 0.05 mg/kg < 0.05 - < 0.05 < 0.05

Endosulfan I 0.05 mg/kg < 0.05 - < 0.05 < 0.05

Endosulfan II 0.05 mg/kg < 0.05 - < 0.05 < 0.05

Endosulfan sulphate 0.05 mg/kg < 0.05 - < 0.05 < 0.05

Endrin 0.05 mg/kg < 0.05 - < 0.05 < 0.05

Endrin aldehyde 0.05 mg/kg < 0.05 - < 0.05 < 0.05

Endrin ketone 0.05 mg/kg < 0.05 - < 0.05 < 0.05

g-BHC (Lindane) 0.05 mg/kg < 0.05 - < 0.05 < 0.05

Heptachlor 0.05 mg/kg < 0.05 - < 0.05 < 0.05

Heptachlor epoxide 0.05 mg/kg < 0.05 - < 0.05 < 0.05

Hexachlorobenzene 0.05 mg/kg < 0.05 - < 0.05 < 0.05

Methoxychlor 0.2 mg/kg < 0.2 - < 0.2 < 0.2

Toxaphene 1 mg/kg < 1 - < 1 < 1

Dibutylchlorendate (surr.) 1 % 116 - 97 114

Tetrachloro-m-xylene (surr.) 1 % 95 - 108 119


Chlorpyrifos 0.5 mg/kg < 0.5 - < 0.5 < 0.5

Coumaphos 0.5 mg/kg < 0.5 - < 0.5 < 0.5

Demeton (total) 1 mg/kg < 1 - < 1 < 1

Diazinon 0.5 mg/kg < 0.5 - < 0.5 < 0.5

Dichlorvos 0.5 mg/kg < 0.5 - < 0.5 < 0.5

Dimethoate 0.5 mg/kg < 0.5 - < 0.5 < 0.5

Disulfoton 0.5 mg/kg < 0.5 - < 0.5 < 0.5

Ethoprop 0.5 mg/kg < 0.5 - < 0.5 < 0.5

Fenitrothion 0.5 mg/kg < 0.5 - < 0.5 < 0.5

Fensulfothion 0.5 mg/kg < 0.5 - < 0.5 < 0.5

Fenthion 0.5 mg/kg < 0.5 - < 0.5 < 0.5

Methyl azinphos 0.5 mg/kg < 0.5 - < 0.5 < 0.5

Malathion 0.5 mg/kg < 0.5 - < 0.5 < 0.5

Methyl parathion 0.5 mg/kg < 0.5 - < 0.5 < 0.5

Mevinphos 0.5 mg/kg < 0.5 - < 0.5 < 0.5

Monocrotophos 10 mg/kg < 10 - < 10 < 10

Parathion 0.5 mg/kg < 0.5 - < 0.5 < 0.5

Phorate 0.5 mg/kg < 0.5 - < 0.5 < 0.5




Page 8 of 72








Profenofos 0.5 mg/kg < 0.5 - < 0.5 < 0.5

Prothiofos 0.5 mg/kg < 0.5 - < 0.5 < 0.5

Ronnel 0.5 mg/kg < 0.5 - < 0.5 < 0.5

Stirophos 0.5 mg/kg < 0.5 - < 0.5 < 0.5

Trichloronate 0.5 mg/kg < 0.5 - < 0.5 < 0.5

Triphenylphosphate (surr.) 1 % 101 - 102 92

Conductivity (1:5 aqueous extract at 25°C) 5 uS/cm 32 - 32 26

pH (1:5 Aqueous extract) 0.1 pH Units 6.2 - 6.5 6.1

% Moisture 0.1 % 21 24 18 21

Heavy Metals

Arsenic 2 mg/kg 8.8 16 < 2 8.8

Cadmium 0.4 mg/kg < 0.4 < 0.4 < 0.4 < 0.4

Chromium 5 mg/kg 13 21 5.3 14

Copper 5 mg/kg 27 20 6.5 65

Lead 5 mg/kg 270 15 19 280

Mercury 0.05 mg/kg 0.11 < 0.05 < 0.05 0.12

Nickel 5 mg/kg 5.6 < 5 < 5 6.5

Zinc 5 mg/kg 1400 100 200 830

Client Sample ID QC1 CTP06/0.0-0.2 CTP06/0.2-0.25CTP06/0.35-0.55






TRH C6-C9 20 mg/kg - < 20 - < 20

TRH C10-C14 20 mg/kg - < 20 - < 20

TRH C15-C28 50 mg/kg - 200 - < 50

TRH C29-C36 50 mg/kg - 910 - < 50

TRH C10-36 (Total) 50 mg/kg - 1100 - < 50

BTEX

Benzene 0.1 mg/kg - < 0.1 - < 0.1

Toluene 0.1 mg/kg - < 0.1 - < 0.1

Ethylbenzene 0.1 mg/kg - < 0.1 - < 0.1

m&p-Xylenes 0.2 mg/kg - < 0.2 - < 0.2

o-Xylene 0.1 mg/kg - < 0.1 - < 0.1

Xylenes - Total 0.3 mg/kg - < 0.3 - < 0.3

4-Bromofluorobenzene (surr.) 1 % - 75 - 71


NaphthaleneN02 0.5 mg/kg - < 0.5 - < 0.5

TRH C6-C10 20 mg/kg - < 20 - < 20

TRH C6-C10 less BTEX (F1)N04 20 mg/kg - < 20 - < 20

TRH >C10-C16 50 mg/kg - < 50 - < 50

TRH >C10-C16 less Naphthalene (F2)N01 50 mg/kg - < 50 - < 50

TRH >C16-C34 100 mg/kg - 750 - < 100

TRH >C34-C40 100 mg/kg - 520 - < 100




Page 9 of 72








1.1-Dichloroethane 0.5 mg/kg < 0.5 - - < 0.5

1.1-Dichloroethene 0.5 mg/kg < 0.5 - - < 0.5

1.1.1-Trichloroethane 0.5 mg/kg < 0.5 - - < 0.5

1.1.1.2-Tetrachloroethane 0.5 mg/kg < 0.5 - - < 0.5

1.1.2-Trichloroethane 0.5 mg/kg < 0.5 - - < 0.5

1.1.2.2-Tetrachloroethane 0.5 mg/kg < 0.5 - - < 0.5

1.2-Dibromoethane 0.5 mg/kg < 0.5 - - < 0.5

1.2-Dichlorobenzene 0.5 mg/kg < 0.5 - - < 0.5

1.2-Dichloroethane 0.5 mg/kg < 0.5 - - < 0.5

1.2-Dichloropropane 0.5 mg/kg < 0.5 - - < 0.5

1.2.3-Trichloropropane 0.5 mg/kg < 0.5 - - < 0.5


1.3-Dichloropropane 0.5 mg/kg < 0.5 - - < 0.5


Bromodichloromethane 0.5 mg/kg < 0.5 - - < 0.5

Bromoform 0.5 mg/kg < 0.5 - - < 0.5

Bromomethane 0.5 mg/kg < 0.5 - - < 0.5

Carbon Tetrachloride 0.5 mg/kg < 0.5 - - < 0.5

Chlorobenzene 0.5 mg/kg < 0.5 - - < 0.5

Chloroform 0.5 mg/kg < 0.5 - - < 0.5

Chloromethane 0.5 mg/kg < 0.5 - - < 0.5

cis-1.2-Dichloroethene 0.5 mg/kg < 0.5 - - < 0.5

cis-1.3-Dichloropropene 0.5 mg/kg < 0.5 - - < 0.5

Dibromochloromethane 0.5 mg/kg < 0.5 - - < 0.5

Dibromomethane 0.5 mg/kg < 0.5 - - < 0.5

Iodomethane 0.5 mg/kg < 0.5 - - < 0.5

Methylene Chloride 0.5 mg/kg < 0.5 - - < 0.5

Tetrachloroethene 0.5 mg/kg < 0.5 - - < 0.5

trans-1.2-Dichloroethene 0.5 mg/kg < 0.5 - - < 0.5

trans-1.3-Dichloropropene 0.5 mg/kg < 0.5 - - < 0.5

Trichloroethene 0.5 mg/kg < 0.5 - - < 0.5

Trichlorofluoromethane 0.5 mg/kg < 0.5 - - < 0.5

Vinyl chloride 0.5 mg/kg < 0.5 - - < 0.5

Fluorobenzene (surr.) 1 % 99 - - 99


Benzo(a)pyrene TEQ (lower bound) * 0.5 mg/kg - < 0.5 - < 0.5

Benzo(a)pyrene TEQ (medium bound) * 0.5 mg/kg - 0.6 - 0.6

Benzo(a)pyrene TEQ (upper bound) * 0.5 mg/kg - 1.2 - 1.2

Acenaphthene 0.5 mg/kg - < 0.5 - < 0.5

Acenaphthylene 0.5 mg/kg - < 0.5 - < 0.5

Anthracene 0.5 mg/kg - < 0.5 - < 0.5

Benz(a)anthracene 0.5 mg/kg - < 0.5 - < 0.5

Benzo(a)pyrene 0.5 mg/kg - < 0.5 - < 0.5

Benzo(b&j)fluorantheneN07 0.5 mg/kg - < 0.5 - < 0.5

Benzo(g.h.i)perylene 0.5 mg/kg - < 0.5 - < 0.5

Benzo(k)fluoranthene 0.5 mg/kg - < 0.5 - < 0.5

Chrysene 0.5 mg/kg - < 0.5 - < 0.5

Dibenz(a.h)anthracene 0.5 mg/kg - < 0.5 - < 0.5

Fluoranthene 0.5 mg/kg - < 0.5 - 0.9




Page 10 of 72








Fluorene 0.5 mg/kg - < 0.5 - < 0.5

Indeno(1.2.3-cd)pyrene 0.5 mg/kg - < 0.5 - < 0.5

Naphthalene 0.5 mg/kg - < 0.5 - < 0.5

Phenanthrene 0.5 mg/kg - < 0.5 - < 0.5

Pyrene 0.5 mg/kg - < 0.5 - 0.8

Total PAH* 0.5 mg/kg - < 0.5 - 1.7

2-Fluorobiphenyl (surr.) 1 % - 126 - 116

p-Terphenyl-d14 (surr.) 1 % - 129 - 113


Chlordanes - Total 0.1 mg/kg - - - < 0.1

4.4'-DDD 0.05 mg/kg - - - < 0.05

4.4'-DDE 0.05 mg/kg - - - < 0.05

4.4'-DDT 0.05 mg/kg - - - < 0.05

a-BHC 0.05 mg/kg - - - < 0.05

Aldrin 0.05 mg/kg - - - < 0.05

b-BHC 0.05 mg/kg - - - < 0.05

d-BHC 0.05 mg/kg - - - < 0.05

Dieldrin 0.05 mg/kg - - - < 0.05

Endosulfan I 0.05 mg/kg - - - < 0.05

Endosulfan II 0.05 mg/kg - - - < 0.05

Endosulfan sulphate 0.05 mg/kg - - - < 0.05

Endrin 0.05 mg/kg - - - < 0.05

Endrin aldehyde 0.05 mg/kg - - - < 0.05

Endrin ketone 0.05 mg/kg - - - < 0.05

g-BHC (Lindane) 0.05 mg/kg - - - < 0.05

Heptachlor 0.05 mg/kg - - - < 0.05

Heptachlor epoxide 0.05 mg/kg - - - < 0.05

Hexachlorobenzene 0.05 mg/kg - - - < 0.05

Methoxychlor 0.2 mg/kg - - - < 0.2

Toxaphene 1 mg/kg - - - < 1

Dibutylchlorendate (surr.) 1 % - - - 98

Tetrachloro-m-xylene (surr.) 1 % - - - 89


Aroclor-1016 0.5 mg/kg < 0.5 - - < 0.5

Aroclor-1221 0.1 mg/kg < 0.1 - - < 0.1

Aroclor-1232 0.5 mg/kg < 0.5 - - < 0.5

Aroclor-1242 0.5 mg/kg < 0.5 - - < 0.5

Aroclor-1248 0.5 mg/kg < 0.5 - - < 0.5

Aroclor-1254 0.5 mg/kg < 0.5 - - < 0.5

Aroclor-1260 0.5 mg/kg < 0.5 - - < 0.5

Total PCB* 0.1 mg/kg < 0.1 - - < 0.1

Dibutylchlorendate (surr.) 1 % 90 - - 98

Tetrachloro-m-xylene (surr.) 1 % 94 - - 89

Acid Herbicides

2.4-D 0.5 mg/kg < 0.5 - - -

2.4-DB 0.5 mg/kg < 0.5 - - -

2.4.5-T 0.5 mg/kg < 0.5 - - -

2.4.5-TP 0.5 mg/kg < 0.5 - - -





Page 11 of 72







Acid Herbicides

Dicamba 0.5 mg/kg < 0.5 - - -



Dinoseb 0.5 mg/kg < 0.5 - - -

MCPA 0.5 mg/kg < 0.5 - - -

MCPB 0.5 mg/kg < 0.5 - - -




Chlorpyrifos 0.5 mg/kg - - - < 0.5

Coumaphos 0.5 mg/kg - - - < 0.5

Demeton (total) 1 mg/kg - - - < 1

Diazinon 0.5 mg/kg - - - < 0.5

Dichlorvos 0.5 mg/kg - - - < 0.5

Dimethoate 0.5 mg/kg - - - < 0.5

Disulfoton 0.5 mg/kg - - - < 0.5

Ethoprop 0.5 mg/kg - - - < 0.5

Fenitrothion 0.5 mg/kg - - - < 0.5

Fensulfothion 0.5 mg/kg - - - < 0.5

Fenthion 0.5 mg/kg - - - < 0.5

Methyl azinphos 0.5 mg/kg - - - < 0.5

Malathion 0.5 mg/kg - - - < 0.5

Methyl parathion 0.5 mg/kg - - - < 0.5

Mevinphos 0.5 mg/kg - - - < 0.5

Monocrotophos 10 mg/kg - - - < 10

Parathion 0.5 mg/kg - - - < 0.5

Phorate 0.5 mg/kg - - - < 0.5

Profenofos 0.5 mg/kg - - - < 0.5

Prothiofos 0.5 mg/kg - - - < 0.5

Ronnel 0.5 mg/kg - - - < 0.5

Stirophos 0.5 mg/kg - - - < 0.5

Trichloronate 0.5 mg/kg - - - < 0.5

Triphenylphosphate (surr.) 1 % - - - 103

Conductivity (1:5 aqueous extract at 25°C) 5 uS/cm - 46 - 22

pH (1:5 Aqueous extract) 0.1 pH Units - 6.4 - 5.9

% Moisture 0.1 % 23 27 34 26

Heavy Metals

Arsenic 2 mg/kg 15 4.7 6.7 16

Cadmium 0.4 mg/kg < 0.4 < 0.4 < 0.4 0.7


Copper 5 mg/kg 33 15 22 62

Lead 5 mg/kg 150 50 70 420

Mercury 0.05 mg/kg 0.11 0.06 0.08 0.19

Nickel 5 mg/kg 11 6.5 9.1 7.4

Zinc 5 mg/kg 340 450 500 670




Page 12 of 72


Client Sample ID CTP06/0.75-0.85 CTP07/0.0-0.2 CTP08/0.0-0.2

CTP08/0.35-0.45






TRH C6-C9 20 mg/kg - < 20 < 20 < 20

TRH C10-C14 20 mg/kg - < 20 < 20 < 20

TRH C15-C28 50 mg/kg - 67 550 < 50

TRH C29-C36 50 mg/kg - 270 3200 < 50

TRH C10-36 (Total) 50 mg/kg - 340 3800 < 50

BTEX

Benzene 0.1 mg/kg - < 0.1 < 0.1 < 0.1

Toluene 0.1 mg/kg - < 0.1 < 0.1 < 0.1

Ethylbenzene 0.1 mg/kg - < 0.1 < 0.1 < 0.1

m&p-Xylenes 0.2 mg/kg - < 0.2 < 0.2 < 0.2

o-Xylene 0.1 mg/kg - < 0.1 < 0.1 < 0.1

Xylenes - Total 0.3 mg/kg - < 0.3 < 0.3 < 0.3

4-Bromofluorobenzene (surr.) 1 % - 74 73 75


NaphthaleneN02 0.5 mg/kg - < 0.5 < 0.5 < 0.5

TRH C6-C10 20 mg/kg - < 20 < 20 < 20

TRH C6-C10 less BTEX (F1)N04 20 mg/kg - < 20 < 20 < 20

TRH >C10-C16 50 mg/kg - < 50 < 50 < 50

TRH >C10-C16 less Naphthalene (F2)N01 50 mg/kg - < 50 < 50 < 50

TRH >C16-C34 100 mg/kg - 220 2500 < 100

TRH >C34-C40 100 mg/kg - 150 1700 < 100


Benzo(a)pyrene TEQ (lower bound) * 0.5 mg/kg - < 0.5 < 0.5 < 0.5

Benzo(a)pyrene TEQ (medium bound) * 0.5 mg/kg - 0.6 0.6 0.6

Benzo(a)pyrene TEQ (upper bound) * 0.5 mg/kg - 1.2 1.2 1.2

Acenaphthene 0.5 mg/kg - < 0.5 < 0.5 < 0.5

Acenaphthylene 0.5 mg/kg - < 0.5 < 0.5 < 0.5

Anthracene 0.5 mg/kg - < 0.5 < 0.5 < 0.5

Benz(a)anthracene 0.5 mg/kg - < 0.5 < 0.5 < 0.5

Benzo(a)pyrene 0.5 mg/kg - < 0.5 < 0.5 < 0.5

Benzo(b&j)fluorantheneN07 0.5 mg/kg - < 0.5 < 0.5 < 0.5

Benzo(g.h.i)perylene 0.5 mg/kg - < 0.5 < 0.5 < 0.5

Benzo(k)fluoranthene 0.5 mg/kg - < 0.5 < 0.5 < 0.5

Chrysene 0.5 mg/kg - < 0.5 < 0.5 < 0.5

Dibenz(a.h)anthracene 0.5 mg/kg - < 0.5 < 0.5 < 0.5

Fluoranthene 0.5 mg/kg - < 0.5 0.6 < 0.5

Fluorene 0.5 mg/kg - < 0.5 < 0.5 < 0.5

Indeno(1.2.3-cd)pyrene 0.5 mg/kg - < 0.5 < 0.5 < 0.5

Naphthalene 0.5 mg/kg - < 0.5 < 0.5 < 0.5

Phenanthrene 0.5 mg/kg - < 0.5 < 0.5 < 0.5

Pyrene 0.5 mg/kg - < 0.5 0.7 < 0.5

Total PAH* 0.5 mg/kg - < 0.5 1.3 < 0.5

2-Fluorobiphenyl (surr.) 1 % - 114 118 117

p-Terphenyl-d14 (surr.) 1 % - 115 115 119




Page 13 of 72



CTP08/0.35-0.45







4.4'-DDD 0.05 mg/kg < 0.05 < 0.05 < 0.05 -

4.4'-DDE 0.05 mg/kg < 0.05 < 0.05 < 0.05 -

4.4'-DDT 0.05 mg/kg < 0.05 < 0.05 < 0.05 -

a-BHC 0.05 mg/kg < 0.05 < 0.05 < 0.05 -

Aldrin 0.05 mg/kg < 0.05 < 0.05 < 0.05 -

b-BHC 0.05 mg/kg < 0.05 < 0.05 < 0.05 -

d-BHC 0.05 mg/kg < 0.05 < 0.05 0.39 -

Dieldrin 0.05 mg/kg < 0.05 < 0.05 < 0.05 -




Endrin 0.05 mg/kg < 0.05 < 0.05 < 0.05 -




Heptachlor 0.05 mg/kg < 0.05 < 0.05 < 0.05 -







Acid Herbicides

2.4-D 0.5 mg/kg - < 0.5 - -

2.4-DB 0.5 mg/kg - < 0.5 - -

2.4.5-T 0.5 mg/kg - < 0.5 - -

2.4.5-TP 0.5 mg/kg - < 0.5 - -

Actril (loxynil) 0.5 mg/kg - < 0.5 - -

Dicamba 0.5 mg/kg - < 0.5 - -

Dichlorprop 0.5 mg/kg - < 0.5 - -

Dinitro-o-cresol 0.5 mg/kg - < 0.5 - -

Dinoseb 0.5 mg/kg - < 0.5 - -

MCPA 0.5 mg/kg - < 0.5 - -

MCPB 0.5 mg/kg - < 0.5 - -

Mecoprop 0.5 mg/kg - < 0.5 - -

Warfarin (surr.) 1 % - 79 - -



Coumaphos 0.5 mg/kg < 0.5 < 0.5 < 0.5 -


Diazinon 0.5 mg/kg < 0.5 < 0.5 < 0.5 -

Dichlorvos 0.5 mg/kg < 0.5 < 0.5 < 0.5 -

Dimethoate 0.5 mg/kg < 0.5 < 0.5 < 0.5 -

Disulfoton 0.5 mg/kg < 0.5 < 0.5 < 0.5 -

Ethoprop 0.5 mg/kg < 0.5 < 0.5 < 0.5 -



Fenthion 0.5 mg/kg < 0.5 < 0.5 < 0.5 -




Page 14 of 72



CTP08/0.35-0.45







Malathion 0.5 mg/kg < 0.5 < 0.5 < 0.5 -


Mevinphos 0.5 mg/kg < 0.5 < 0.5 < 0.5 -


Parathion 0.5 mg/kg < 0.5 < 0.5 < 0.5 -

Phorate 0.5 mg/kg < 0.5 < 0.5 < 0.5 -

Profenofos 0.5 mg/kg < 0.5 < 0.5 < 0.5 -

Prothiofos 0.5 mg/kg < 0.5 < 0.5 < 0.5 -

Ronnel 0.5 mg/kg < 0.5 < 0.5 < 0.5 -

Stirophos 0.5 mg/kg < 0.5 < 0.5 < 0.5 -



Conductivity (1:5 aqueous extract at 25°C) 5 uS/cm - 36 36 -

pH (1:5 Aqueous extract) 0.1 pH Units - 6.2 6.0 -

% Moisture 0.1 % 24 18 20 19

Heavy Metals

Arsenic 2 mg/kg - 2.3 5.9 10

Cadmium 0.4 mg/kg - < 0.4 < 0.4 < 0.4

Chromium 5 mg/kg - 9.0 11 10

Copper 5 mg/kg - 7.9 8.6 16

Lead 5 mg/kg - 26 160 10

Mercury 0.05 mg/kg - 0.05 0.07 < 0.05

Nickel 5 mg/kg - < 5 5.2 < 5

Zinc 5 mg/kg - 93 500 22

Client Sample ID CTP09/0.0-0.2 CTP10/0.0-0.2CTP10/0.45-065 CTP11/0.0-0.2






TRH C6-C9 20 mg/kg < 20 < 20 < 20 < 20

TRH C10-C14 20 mg/kg < 20 < 20 < 20 32

TRH C15-C28 50 mg/kg < 50 140 280 540

TRH C29-C36 50 mg/kg 110 490 200 930

TRH C10-36 (Total) 50 mg/kg 110 630 480 1500

BTEX

Benzene 0.1 mg/kg < 0.1 < 0.1 < 0.1 < 0.1

Toluene 0.1 mg/kg < 0.1 < 0.1 < 0.1 < 0.1


m&p-Xylenes 0.2 mg/kg < 0.2 < 0.2 < 0.2 < 0.2

o-Xylene 0.1 mg/kg < 0.1 < 0.1 < 0.1 < 0.1






Page 15 of 72









TRH C6-C10 20 mg/kg < 20 < 20 < 20 < 20


TRH >C10-C16 50 mg/kg < 50 < 50 < 50 < 50


TRH >C16-C34 100 mg/kg < 100 420 360 690

TRH >C34-C40 100 mg/kg < 100 270 < 100 750


Benzo(a)pyrene TEQ (lower bound) * 0.5 mg/kg < 0.5 1.0 10 < 0.5

Benzo(a)pyrene TEQ (medium bound) * 0.5 mg/kg 0.6 1.3 10 0.6

Benzo(a)pyrene TEQ (upper bound) * 0.5 mg/kg 1.2 1.6 10 1.2


Acenaphthylene 0.5 mg/kg < 0.5 < 0.5 2.8 < 0.5

Anthracene 0.5 mg/kg < 0.5 < 0.5 3.6 < 0.5


Benzo(a)pyrene 0.5 mg/kg < 0.5 0.8 6.8 < 0.5


Benzo(g.h.i)perylene 0.5 mg/kg < 0.5 < 0.5 3.1 < 0.5

Benzo(k)fluoranthene 0.5 mg/kg < 0.5 0.8 5.9 < 0.5

Chrysene 0.5 mg/kg < 0.5 0.8 6.8 < 0.5

Dibenz(a.h)anthracene 0.5 mg/kg < 0.5 < 0.5 1.1 < 0.5

Fluoranthene 0.5 mg/kg < 0.5 1.4 20 < 0.5

Fluorene 0.5 mg/kg < 0.5 < 0.5 1.1 < 0.5

Indeno(1.2.3-cd)pyrene 0.5 mg/kg < 0.5 < 0.5 3.0 < 0.5


Phenanthrene 0.5 mg/kg < 0.5 0.7 18 < 0.5

Pyrene 0.5 mg/kg < 0.5 1.6 16 < 0.5

Total PAH* 0.5 mg/kg < 0.5 7.6 100 < 0.5




Chlordanes - Total 0.1 mg/kg < 0.1 < 0.1 - < 0.1

4.4'-DDD 0.05 mg/kg < 0.05 < 0.05 - < 0.05

4.4'-DDE 0.05 mg/kg < 0.05 < 0.05 - < 0.05

4.4'-DDT 0.05 mg/kg < 0.05 < 0.05 - < 0.05

a-BHC 0.05 mg/kg < 0.05 < 0.05 - < 0.05

Aldrin 0.05 mg/kg < 0.05 < 0.05 - < 0.05

b-BHC 0.05 mg/kg < 0.05 < 0.05 - < 0.05

d-BHC 0.05 mg/kg < 0.05 < 0.05 - < 0.05

Dieldrin 0.05 mg/kg < 0.05 < 0.05 - 0.18

Endosulfan I 0.05 mg/kg < 0.05 < 0.05 - < 0.05

Endosulfan II 0.05 mg/kg < 0.05 < 0.05 - < 0.05

Endosulfan sulphate 0.05 mg/kg < 0.05 < 0.05 - < 0.05

Endrin 0.05 mg/kg < 0.05 < 0.05 - < 0.05

Endrin aldehyde 0.05 mg/kg < 0.05 < 0.05 - < 0.05

Endrin ketone 0.05 mg/kg < 0.05 < 0.05 - < 0.05

g-BHC (Lindane) 0.05 mg/kg < 0.05 < 0.05 - < 0.05

Heptachlor 0.05 mg/kg < 0.05 < 0.05 - < 0.05

Heptachlor epoxide 0.05 mg/kg < 0.05 < 0.05 - < 0.05




Page 16 of 72








Hexachlorobenzene 0.05 mg/kg < 0.05 < 0.05 - < 0.05

Methoxychlor 0.2 mg/kg < 0.2 < 0.2 - < 0.2

Toxaphene 1 mg/kg < 1 < 1 - < 1

Dibutylchlorendate (surr.) 1 % 89 93 - 109

Tetrachloro-m-xylene (surr.) 1 % 98 114 - 108


Chlorpyrifos 0.5 mg/kg < 0.5 < 0.5 - < 0.5

Coumaphos 0.5 mg/kg < 0.5 < 0.5 - < 0.5

Demeton (total) 1 mg/kg < 1 < 1 - < 1

Diazinon 0.5 mg/kg < 0.5 < 0.5 - < 0.5

Dichlorvos 0.5 mg/kg < 0.5 < 0.5 - < 0.5

Dimethoate 0.5 mg/kg < 0.5 < 0.5 - < 0.5

Disulfoton 0.5 mg/kg < 0.5 < 0.5 - < 0.5

Ethoprop 0.5 mg/kg < 0.5 < 0.5 - < 0.5

Fenitrothion 0.5 mg/kg < 0.5 < 0.5 - < 0.5

Fensulfothion 0.5 mg/kg < 0.5 < 0.5 - < 0.5

Fenthion 0.5 mg/kg < 0.5 < 0.5 - < 0.5

Methyl azinphos 0.5 mg/kg < 0.5 < 0.5 - < 0.5

Malathion 0.5 mg/kg < 0.5 < 0.5 - < 0.5

Methyl parathion 0.5 mg/kg < 0.5 < 0.5 - < 0.5

Mevinphos 0.5 mg/kg < 0.5 < 0.5 - < 0.5

Monocrotophos 10 mg/kg < 10 < 10 - < 10

Parathion 0.5 mg/kg < 0.5 < 0.5 - < 0.5

Phorate 0.5 mg/kg < 0.5 < 0.5 - < 0.5

Profenofos 0.5 mg/kg < 0.5 < 0.5 - < 0.5

Prothiofos 0.5 mg/kg < 0.5 < 0.5 - < 0.5

Ronnel 0.5 mg/kg < 0.5 < 0.5 - < 0.5

Stirophos 0.5 mg/kg < 0.5 < 0.5 - < 0.5

Trichloronate 0.5 mg/kg < 0.5 < 0.5 - < 0.5

Triphenylphosphate (surr.) 1 % 99 101 - 103

Conductivity (1:5 aqueous extract at 25°C) 5 uS/cm 36 26 47 40

pH (1:5 Aqueous extract) 0.1 pH Units 6.5 6.1 5.6 6.3

% Moisture 0.1 % 23 24 21 22

Heavy Metals

Arsenic 2 mg/kg 2.1 < 2 19 3.5

Cadmium 0.4 mg/kg < 0.4 < 0.4 < 0.4 < 0.4

Chromium 5 mg/kg 6.8 < 5 15 7.0

Copper 5 mg/kg 13 8.4 21 12

Lead 5 mg/kg 95 55 36 34

Mercury 0.05 mg/kg 0.06 < 0.05 < 0.05 0.05

Nickel 5 mg/kg < 5 < 5 6.9 < 5

Zinc 5 mg/kg 200 150 110 180




Page 17 of 72


Client Sample ID CTP11/0.3-0.5 QC4 CTP12/0.0-0.2CTP12/0.25-0.45






TRH C6-C9 20 mg/kg < 20 < 20 < 20 < 20

TRH C10-C14 20 mg/kg < 20 < 20 < 20 < 20

TRH C15-C28 50 mg/kg < 50 330 < 50 < 50

TRH C29-C36 50 mg/kg < 50 1300 < 50 < 50

TRH C10-36 (Total) 50 mg/kg < 50 1600 < 50 < 50

BTEX

Benzene 0.1 mg/kg < 0.1 < 0.1 < 0.1 < 0.1

Toluene 0.1 mg/kg < 0.1 < 0.1 < 0.1 < 0.1


m&p-Xylenes 0.2 mg/kg < 0.2 < 0.2 < 0.2 < 0.2

o-Xylene 0.1 mg/kg < 0.1 < 0.1 < 0.1 < 0.1





TRH C6-C10 20 mg/kg < 20 < 20 < 20 < 20


TRH >C10-C16 50 mg/kg < 50 < 50 < 50 < 50


TRH >C16-C34 100 mg/kg < 100 1100 < 100 < 100

TRH >C34-C40 100 mg/kg < 100 660 < 100 < 100


Benzo(a)pyrene TEQ (lower bound) * 0.5 mg/kg < 0.5 < 0.5 < 0.5 < 0.5





Anthracene 0.5 mg/kg < 0.5 < 0.5 < 0.5 < 0.5

Benz(a)anthracene 0.5 mg/kg < 0.5 0.8 < 0.5 < 0.5

Benzo(a)pyrene 0.5 mg/kg < 0.5 < 0.5 < 0.5 < 0.5

Benzo(b&j)fluorantheneN07 0.5 mg/kg < 0.5 < 0.5 < 0.5 < 0.5


Benzo(k)fluoranthene 0.5 mg/kg < 0.5 < 0.5 < 0.5 < 0.5

Chrysene 0.5 mg/kg < 0.5 0.8 < 0.5 < 0.5


Fluoranthene 0.5 mg/kg < 0.5 1.5 < 0.5 < 0.5

Fluorene 0.5 mg/kg < 0.5 < 0.5 < 0.5 < 0.5



Phenanthrene 0.5 mg/kg < 0.5 0.8 < 0.5 < 0.5

Pyrene 0.5 mg/kg < 0.5 1.5 < 0.5 < 0.5

Total PAH* 0.5 mg/kg < 0.5 5.4 < 0.5 < 0.5






Page 18 of 72








Chlordanes - Total 0.1 mg/kg - < 0.1 < 0.1 -

4.4'-DDD 0.05 mg/kg - < 0.05 < 0.05 -

4.4'-DDE 0.05 mg/kg - < 0.05 < 0.05 -

4.4'-DDT 0.05 mg/kg - < 0.05 < 0.05 -

a-BHC 0.05 mg/kg - < 0.05 < 0.05 -

Aldrin 0.05 mg/kg - < 0.05 < 0.05 -

b-BHC 0.05 mg/kg - < 0.05 < 0.05 -

d-BHC 0.05 mg/kg - < 0.05 < 0.05 -

Dieldrin 0.05 mg/kg - < 0.05 < 0.05 -

Endosulfan I 0.05 mg/kg - < 0.05 < 0.05 -

Endosulfan II 0.05 mg/kg - < 0.05 < 0.05 -

Endosulfan sulphate 0.05 mg/kg - < 0.05 < 0.05 -

Endrin 0.05 mg/kg - < 0.05 < 0.05 -

Endrin aldehyde 0.05 mg/kg - < 0.05 < 0.05 -

Endrin ketone 0.05 mg/kg - < 0.05 < 0.05 -

g-BHC (Lindane) 0.05 mg/kg - < 0.05 < 0.05 -

Heptachlor 0.05 mg/kg - < 0.05 < 0.05 -

Heptachlor epoxide 0.05 mg/kg - < 0.05 < 0.05 -

Hexachlorobenzene 0.05 mg/kg - < 0.05 < 0.05 -

Methoxychlor 0.2 mg/kg - < 0.2 < 0.2 -

Toxaphene 1 mg/kg - < 1 < 1 -

Dibutylchlorendate (surr.) 1 % - 101 96 -

Tetrachloro-m-xylene (surr.) 1 % - 106 103 -


Chlorpyrifos 0.5 mg/kg - < 0.5 < 0.5 -

Coumaphos 0.5 mg/kg - < 0.5 < 0.5 -

Demeton (total) 1 mg/kg - < 1 < 1 -

Diazinon 0.5 mg/kg - < 0.5 < 0.5 -

Dichlorvos 0.5 mg/kg - < 0.5 < 0.5 -

Dimethoate 0.5 mg/kg - < 0.5 < 0.5 -

Disulfoton 0.5 mg/kg - < 0.5 < 0.5 -

Ethoprop 0.5 mg/kg - < 0.5 < 0.5 -

Fenitrothion 0.5 mg/kg - < 0.5 < 0.5 -

Fensulfothion 0.5 mg/kg - < 0.5 < 0.5 -

Fenthion 0.5 mg/kg - < 0.5 < 0.5 -

Methyl azinphos 0.5 mg/kg - < 0.5 < 0.5 -

Malathion 0.5 mg/kg - < 0.5 < 0.5 -

Methyl parathion 0.5 mg/kg - < 0.5 < 0.5 -

Mevinphos 0.5 mg/kg - < 0.5 < 0.5 -

Monocrotophos 10 mg/kg - < 10 < 10 -

Parathion 0.5 mg/kg - < 0.5 < 0.5 -

Phorate 0.5 mg/kg - < 0.5 < 0.5 -

Profenofos 0.5 mg/kg - < 0.5 < 0.5 -

Prothiofos 0.5 mg/kg - < 0.5 < 0.5 -

Ronnel 0.5 mg/kg - < 0.5 < 0.5 -

Stirophos 0.5 mg/kg - < 0.5 < 0.5 -

Trichloronate 0.5 mg/kg - < 0.5 < 0.5 -

Triphenylphosphate (surr.) 1 % - 98 107 -




Page 19 of 72









% Moisture 0.1 % 20 25 23 22

Heavy Metals

Arsenic 2 mg/kg 8.9 2.6 6.7 21

Cadmium 0.4 mg/kg < 0.4 < 0.4 < 0.4 < 0.4

Chromium 5 mg/kg 12 7.2 32 17

Copper 5 mg/kg 26 8.6 25 31

Lead 5 mg/kg 41 54 15 48

Mercury 0.05 mg/kg < 0.05 0.09 0.06 < 0.05

Nickel 5 mg/kg 7.0 < 5 21 < 5

Zinc 5 mg/kg 240 190 60 51







TRH C6-C9 20 mg/kg < 20 - < 20 < 20

TRH C10-C14 20 mg/kg < 20 - < 20 < 20

TRH C15-C28 50 mg/kg < 50 - 130 560

TRH C29-C36 50 mg/kg < 50 - 300 710

TRH C10-36 (Total) 50 mg/kg < 50 - 430 1300

BTEX

Benzene 0.1 mg/kg < 0.1 - < 0.1 < 0.1

Toluene 0.1 mg/kg < 0.1 - < 0.1 < 0.1

Ethylbenzene 0.1 mg/kg < 0.1 - < 0.1 < 0.1

m&p-Xylenes 0.2 mg/kg < 0.2 - < 0.2 < 0.2

o-Xylene 0.1 mg/kg < 0.1 - < 0.1 < 0.1

Xylenes - Total 0.3 mg/kg < 0.3 - < 0.3 < 0.3

4-Bromofluorobenzene (surr.) 1 % 76 - 75 77


NaphthaleneN02 0.5 mg/kg < 0.5 - < 0.5 < 0.5

TRH C6-C10 20 mg/kg < 20 - < 20 < 20

TRH C6-C10 less BTEX (F1)N04 20 mg/kg < 20 - < 20 < 20

TRH >C10-C16 50 mg/kg < 50 - < 50 < 50

TRH >C10-C16 less Naphthalene (F2)N01 50 mg/kg < 50 - < 50 < 50

TRH >C16-C34 100 mg/kg < 100 - 290 1200

TRH >C34-C40 100 mg/kg < 100 - 260 420


1.1-Dichloroethane 0.5 mg/kg < 0.5 - - -

1.1-Dichloroethene 0.5 mg/kg < 0.5 - - -

1.1.1-Trichloroethane 0.5 mg/kg < 0.5 - - -

1.1.1.2-Tetrachloroethane 0.5 mg/kg < 0.5 - - -






Page 20 of 72








1.2-Dibromoethane 0.5 mg/kg < 0.5 - - -

1.2-Dichlorobenzene 0.5 mg/kg < 0.5 - - -


1.2-Dichloropropane 0.5 mg/kg < 0.5 - - -

1.2.3-Trichloropropane 0.5 mg/kg < 0.5 - - -




Bromodichloromethane 0.5 mg/kg < 0.5 - - -

Bromoform 0.5 mg/kg < 0.5 - - -

Bromomethane 0.5 mg/kg < 0.5 - - -

Carbon Tetrachloride 0.5 mg/kg < 0.5 - - -

Chlorobenzene 0.5 mg/kg < 0.5 - - -

Chloroform 0.5 mg/kg < 0.5 - - -

Chloromethane 0.5 mg/kg < 0.5 - - -

cis-1.2-Dichloroethene 0.5 mg/kg < 0.5 - - -

cis-1.3-Dichloropropene 0.5 mg/kg < 0.5 - - -

Dibromochloromethane 0.5 mg/kg < 0.5 - - -

Dibromomethane 0.5 mg/kg < 0.5 - - -

Iodomethane 0.5 mg/kg < 0.5 - - -

Methylene Chloride 0.5 mg/kg < 0.5 - - -

Tetrachloroethene 0.5 mg/kg < 0.5 - - -

trans-1.2-Dichloroethene 0.5 mg/kg < 0.5 - - -

trans-1.3-Dichloropropene 0.5 mg/kg < 0.5 - - -

Trichloroethene 0.5 mg/kg < 0.5 - - -

Trichlorofluoromethane 0.5 mg/kg < 0.5 - - -

Vinyl chloride 0.5 mg/kg < 0.5 - - -

Fluorobenzene (surr.) 1 % 98 - - -


Benzo(a)pyrene TEQ (lower bound) * 0.5 mg/kg < 0.5 - < 0.5 12

Benzo(a)pyrene TEQ (medium bound) * 0.5 mg/kg 0.6 - 0.6 12

Benzo(a)pyrene TEQ (upper bound) * 0.5 mg/kg 1.2 - 1.2 12

Acenaphthene 0.5 mg/kg < 0.5 - < 0.5 < 0.5

Acenaphthylene 0.5 mg/kg < 0.5 - < 0.5 < 0.5

Anthracene 0.5 mg/kg < 0.5 - < 0.5 1.6

Benz(a)anthracene 0.5 mg/kg < 0.5 - < 0.5 6.7

Benzo(a)pyrene 0.5 mg/kg < 0.5 - < 0.5 7.7

Benzo(b&j)fluorantheneN07 0.5 mg/kg < 0.5 - < 0.5 9.4

Benzo(g.h.i)perylene 0.5 mg/kg < 0.5 - < 0.5 5.0

Benzo(k)fluoranthene 0.5 mg/kg < 0.5 - < 0.5 6.2

Chrysene 0.5 mg/kg < 0.5 - < 0.5 4.1

Dibenz(a.h)anthracene 0.5 mg/kg < 0.5 - < 0.5 1.7

Fluoranthene 0.5 mg/kg < 0.5 - < 0.5 10

Fluorene 0.5 mg/kg < 0.5 - < 0.5 < 0.5

Indeno(1.2.3-cd)pyrene 0.5 mg/kg < 0.5 - < 0.5 4.0

Naphthalene 0.5 mg/kg < 0.5 - < 0.5 < 0.5

Phenanthrene 0.5 mg/kg < 0.5 - < 0.5 3.6

Pyrene 0.5 mg/kg < 0.5 - < 0.5 10

Total PAH* 0.5 mg/kg < 0.5 - < 0.5 70




Page 21 of 72








2-Fluorobiphenyl (surr.) 1 % 128 - 110 114

p-Terphenyl-d14 (surr.) 1 % 113 - 105 112



4.4'-DDD 0.05 mg/kg < 0.05 < 0.05 < 0.05 -

4.4'-DDE 0.05 mg/kg < 0.05 < 0.05 < 0.05 -

4.4'-DDT 0.05 mg/kg < 0.05 < 0.05 < 0.05 -

a-BHC 0.05 mg/kg < 0.05 < 0.05 < 0.05 -

Aldrin 0.05 mg/kg < 0.05 < 0.05 < 0.05 -

b-BHC 0.05 mg/kg < 0.05 < 0.05 < 0.05 -

d-BHC 0.05 mg/kg < 0.05 < 0.05 < 0.05 -

Dieldrin 0.05 mg/kg < 0.05 < 0.05 < 0.05 -




Endrin 0.05 mg/kg < 0.05 < 0.05 < 0.05 -




Heptachlor 0.05 mg/kg < 0.05 < 0.05 < 0.05 -








Aroclor-1016 0.5 mg/kg < 0.5 - - -

Aroclor-1221 0.1 mg/kg < 0.1 - - -

Aroclor-1232 0.5 mg/kg < 0.5 - - -

Aroclor-1242 0.5 mg/kg < 0.5 - - -

Aroclor-1248 0.5 mg/kg < 0.5 - - -

Aroclor-1254 0.5 mg/kg < 0.5 - - -

Aroclor-1260 0.5 mg/kg < 0.5 - - -

Total PCB* 0.1 mg/kg < 0.1 - - -

Dibutylchlorendate (surr.) 1 % 120 - - -

Tetrachloro-m-xylene (surr.) 1 % 100 - - -

Acid Herbicides

2.4-D 0.5 mg/kg < 0.5 - < 0.5 -

2.4-DB 0.5 mg/kg < 0.5 - < 0.5 -

2.4.5-T 0.5 mg/kg < 0.5 - < 0.5 -

2.4.5-TP 0.5 mg/kg < 0.5 - < 0.5 -

Actril (loxynil) 0.5 mg/kg < 0.5 - < 0.5 -

Dicamba 0.5 mg/kg < 0.5 - < 0.5 -

Dichlorprop 0.5 mg/kg < 0.5 - < 0.5 -

Dinitro-o-cresol 0.5 mg/kg < 0.5 - < 0.5 -

Dinoseb 0.5 mg/kg < 0.5 - < 0.5 -

MCPA 0.5 mg/kg < 0.5 - < 0.5 -

MCPB 0.5 mg/kg < 0.5 - < 0.5 -




Page 22 of 72







Acid Herbicides

Mecoprop 0.5 mg/kg < 0.5 - < 0.5 -

Warfarin (surr.) 1 % 80 - 83 -



Coumaphos 0.5 mg/kg < 0.5 < 0.5 < 0.5 -


Diazinon 0.5 mg/kg < 0.5 < 0.5 < 0.5 -

Dichlorvos 0.5 mg/kg < 0.5 < 0.5 < 0.5 -

Dimethoate 0.5 mg/kg < 0.5 < 0.5 < 0.5 -

Disulfoton 0.5 mg/kg < 0.5 < 0.5 < 0.5 -

Ethoprop 0.5 mg/kg < 0.5 < 0.5 < 0.5 -



Fenthion 0.5 mg/kg < 0.5 < 0.5 < 0.5 -


Malathion 0.5 mg/kg < 0.5 < 0.5 < 0.5 -


Mevinphos 0.5 mg/kg < 0.5 < 0.5 < 0.5 -


Parathion 0.5 mg/kg < 0.5 < 0.5 < 0.5 -

Phorate 0.5 mg/kg < 0.5 < 0.5 < 0.5 -

Profenofos 0.5 mg/kg < 0.5 < 0.5 < 0.5 -

Prothiofos 0.5 mg/kg < 0.5 < 0.5 < 0.5 -

Ronnel 0.5 mg/kg < 0.5 < 0.5 < 0.5 -

Stirophos 0.5 mg/kg < 0.5 < 0.5 < 0.5 -



Conductivity (1:5 aqueous extract at 25°C) 5 uS/cm 27 - 41 110

pH (1:5 Aqueous extract) 0.1 pH Units 6.1 - 6.5 7.2

% Moisture 0.1 % 20 20 20 16

Heavy Metals

Arsenic 2 mg/kg 3.8 50 3.1 17

Cadmium 0.4 mg/kg < 0.4 < 0.4 < 0.4 < 0.4

Chromium 5 mg/kg 7.3 24 7.6 9.4

Copper 5 mg/kg 7.8 18 10 17

Lead 5 mg/kg 19 20 52 49

Mercury 0.05 mg/kg 0.06 < 0.05 < 0.05 1.3

Nickel 5 mg/kg < 5 < 5 < 5 5.1

Zinc 5 mg/kg 120 43 200 82




Page 23 of 72








TRH C6-C9 20 mg/kg - < 20 < 20 < 20

TRH C10-C14 20 mg/kg - < 20 < 20 < 20

TRH C15-C28 50 mg/kg - 170 < 50 < 50

TRH C29-C36 50 mg/kg - 420 < 50 110

TRH C10-36 (Total) 50 mg/kg - 590 < 50 110

BTEX

Benzene 0.1 mg/kg - < 0.1 < 0.1 < 0.1

Toluene 0.1 mg/kg - < 0.1 < 0.1 < 0.1

Ethylbenzene 0.1 mg/kg - < 0.1 < 0.1 < 0.1

m&p-Xylenes 0.2 mg/kg - < 0.2 < 0.2 < 0.2

o-Xylene 0.1 mg/kg - < 0.1 < 0.1 < 0.1

Xylenes - Total 0.3 mg/kg - < 0.3 < 0.3 < 0.3

4-Bromofluorobenzene (surr.) 1 % - 78 77 79


NaphthaleneN02 0.5 mg/kg - < 0.5 < 0.5 < 0.5

TRH C6-C10 20 mg/kg - < 20 < 20 < 20

TRH C6-C10 less BTEX (F1)N04 20 mg/kg - < 20 < 20 < 20

TRH >C10-C16 50 mg/kg - < 50 < 50 < 50

TRH >C10-C16 less Naphthalene (F2)N01 50 mg/kg - < 50 < 50 < 50

TRH >C16-C34 100 mg/kg - 460 < 100 130

TRH >C34-C40 100 mg/kg - 350 < 100 < 100


Benzo(a)pyrene TEQ (lower bound) * 0.5 mg/kg - < 0.5 < 0.5 < 0.5

Benzo(a)pyrene TEQ (medium bound) * 0.5 mg/kg - 0.6 0.6 0.6

Benzo(a)pyrene TEQ (upper bound) * 0.5 mg/kg - 1.2 1.2 1.2

Acenaphthene 0.5 mg/kg - < 0.5 < 0.5 < 0.5

Acenaphthylene 0.5 mg/kg - < 0.5 < 0.5 < 0.5

Anthracene 0.5 mg/kg - < 0.5 < 0.5 < 0.5

Benz(a)anthracene 0.5 mg/kg - < 0.5 < 0.5 < 0.5

Benzo(a)pyrene 0.5 mg/kg - < 0.5 < 0.5 < 0.5

Benzo(b&j)fluorantheneN07 0.5 mg/kg - < 0.5 < 0.5 < 0.5

Benzo(g.h.i)perylene 0.5 mg/kg - < 0.5 < 0.5 < 0.5

Benzo(k)fluoranthene 0.5 mg/kg - < 0.5 < 0.5 < 0.5

Chrysene 0.5 mg/kg - < 0.5 < 0.5 < 0.5

Dibenz(a.h)anthracene 0.5 mg/kg - < 0.5 < 0.5 < 0.5

Fluoranthene 0.5 mg/kg - < 0.5 < 0.5 < 0.5

Fluorene 0.5 mg/kg - < 0.5 < 0.5 < 0.5

Indeno(1.2.3-cd)pyrene 0.5 mg/kg - < 0.5 < 0.5 < 0.5

Naphthalene 0.5 mg/kg - < 0.5 < 0.5 < 0.5

Phenanthrene 0.5 mg/kg - < 0.5 < 0.5 < 0.5

Pyrene 0.5 mg/kg - < 0.5 < 0.5 < 0.5

Total PAH* 0.5 mg/kg - < 0.5 < 0.5 < 0.5




Chlordanes - Total 0.1 mg/kg - < 0.1 - < 0.1

4.4'-DDD 0.05 mg/kg - < 0.05 - < 0.05

4.4'-DDE 0.05 mg/kg - < 0.05 - < 0.05

4.4'-DDT 0.05 mg/kg - < 0.05 - < 0.05




Page 24 of 72








a-BHC 0.05 mg/kg - < 0.05 - < 0.05

Aldrin 0.05 mg/kg - < 0.05 - < 0.05

b-BHC 0.05 mg/kg - < 0.05 - < 0.05

d-BHC 0.05 mg/kg - < 0.05 - < 0.05

Dieldrin 0.05 mg/kg - < 0.05 - < 0.05

Endosulfan I 0.05 mg/kg - < 0.05 - < 0.05

Endosulfan II 0.05 mg/kg - < 0.05 - < 0.05

Endosulfan sulphate 0.05 mg/kg - < 0.05 - < 0.05

Endrin 0.05 mg/kg - < 0.05 - < 0.05

Endrin aldehyde 0.05 mg/kg - < 0.05 - < 0.05

Endrin ketone 0.05 mg/kg - < 0.05 - < 0.05

g-BHC (Lindane) 0.05 mg/kg - < 0.05 - < 0.05

Heptachlor 0.05 mg/kg - < 0.05 - < 0.05

Heptachlor epoxide 0.05 mg/kg - < 0.05 - < 0.05

Hexachlorobenzene 0.05 mg/kg - < 0.05 - < 0.05

Methoxychlor 0.2 mg/kg - < 0.2 - < 0.2

Toxaphene 1 mg/kg - < 1 - < 1

Dibutylchlorendate (surr.) 1 % - 96 - 91

Tetrachloro-m-xylene (surr.) 1 % - 112 - 103


Chlorpyrifos 0.5 mg/kg - < 0.5 - < 0.5

Coumaphos 0.5 mg/kg - < 0.5 - < 0.5

Demeton (total) 1 mg/kg - < 1 - < 1

Diazinon 0.5 mg/kg - < 0.5 - < 0.5

Dichlorvos 0.5 mg/kg - < 0.5 - < 0.5

Dimethoate 0.5 mg/kg - < 0.5 - < 0.5

Disulfoton 0.5 mg/kg - < 0.5 - < 0.5

Ethoprop 0.5 mg/kg - < 0.5 - < 0.5

Fenitrothion 0.5 mg/kg - < 0.5 - < 0.5

Fensulfothion 0.5 mg/kg - < 0.5 - < 0.5

Fenthion 0.5 mg/kg - < 0.5 - < 0.5

Methyl azinphos 0.5 mg/kg - < 0.5 - < 0.5

Malathion 0.5 mg/kg - < 0.5 - < 0.5

Methyl parathion 0.5 mg/kg - < 0.5 - < 0.5

Mevinphos 0.5 mg/kg - < 0.5 - < 0.5

Monocrotophos 10 mg/kg - < 10 - < 10

Parathion 0.5 mg/kg - < 0.5 - < 0.5

Phorate 0.5 mg/kg - < 0.5 - < 0.5

Profenofos 0.5 mg/kg - < 0.5 - < 0.5

Prothiofos 0.5 mg/kg - < 0.5 - < 0.5

Ronnel 0.5 mg/kg - < 0.5 - < 0.5

Stirophos 0.5 mg/kg - < 0.5 - < 0.5

Trichloronate 0.5 mg/kg - < 0.5 - < 0.5

Triphenylphosphate (surr.) 1 % - 113 - 103

Conductivity (1:5 aqueous extract at 25°C) 5 uS/cm - 33 52 37

pH (1:5 Aqueous extract) 0.1 pH Units - 6.0 5.1 6.2

% Moisture 0.1 % 19 23 21 20




Page 25 of 72







Heavy Metals

Arsenic 2 mg/kg 3.3 4.2 13 2.3

Cadmium 0.4 mg/kg < 0.4 < 0.4 < 0.4 < 0.4

Chromium 5 mg/kg 8.1 8.6 11 6.5

Copper 5 mg/kg 22 12 15 6.1

Lead 5 mg/kg 9.1 47 16 18

Mercury 0.05 mg/kg < 0.05 0.06 < 0.05 < 0.05

Nickel 5 mg/kg < 5 < 5 < 5 < 5

Zinc 5 mg/kg 37 230 32 100







TRH C6-C9 20 mg/kg < 20 < 20 < 20 < 20

TRH C10-C14 20 mg/kg < 20 < 20 < 20 < 20

TRH C15-C28 50 mg/kg < 50 < 50 < 50 < 50

TRH C29-C36 50 mg/kg < 50 < 50 < 50 < 50

TRH C10-36 (Total) 50 mg/kg < 50 < 50 < 50 < 50

BTEX

Benzene 0.1 mg/kg < 0.1 < 0.1 < 0.1 < 0.1

Toluene 0.1 mg/kg < 0.1 < 0.1 < 0.1 < 0.1


m&p-Xylenes 0.2 mg/kg < 0.2 < 0.2 < 0.2 < 0.2

o-Xylene 0.1 mg/kg < 0.1 < 0.1 < 0.1 < 0.1





TRH C6-C10 20 mg/kg < 20 < 20 < 20 < 20


TRH >C10-C16 50 mg/kg < 50 < 50 < 50 < 50


TRH >C16-C34 100 mg/kg < 100 < 100 < 100 < 100

TRH >C34-C40 100 mg/kg < 100 < 100 < 100 < 100


Benzo(a)pyrene TEQ (lower bound) * 0.5 mg/kg 0.8 < 0.5 < 0.5 < 0.5





Anthracene 0.5 mg/kg < 0.5 < 0.5 < 0.5 < 0.5

Benz(a)anthracene 0.5 mg/kg < 0.5 < 0.5 < 0.5 < 0.5

Benzo(a)pyrene 0.5 mg/kg 0.7 < 0.5 < 0.5 < 0.5

Benzo(b&j)fluorantheneN07 0.5 mg/kg 0.9 < 0.5 < 0.5 < 0.5






Page 26 of 72








Chrysene 0.5 mg/kg < 0.5 < 0.5 < 0.5 < 0.5


Fluoranthene 0.5 mg/kg 0.8 < 0.5 < 0.5 < 0.5

Fluorene 0.5 mg/kg < 0.5 < 0.5 < 0.5 < 0.5



Phenanthrene 0.5 mg/kg < 0.5 < 0.5 < 0.5 < 0.5

Pyrene 0.5 mg/kg 0.8 < 0.5 < 0.5 < 0.5

Total PAH* 0.5 mg/kg 3.2 < 0.5 < 0.5 < 0.5




Chlordanes - Total 0.1 mg/kg - - < 0.1 -

4.4'-DDD 0.05 mg/kg - - < 0.05 -

4.4'-DDE 0.05 mg/kg - - < 0.05 -

4.4'-DDT 0.05 mg/kg - - < 0.05 -

a-BHC 0.05 mg/kg - - < 0.05 -

Aldrin 0.05 mg/kg - - < 0.05 -

b-BHC 0.05 mg/kg - - < 0.05 -

d-BHC 0.05 mg/kg - - < 0.05 -

Dieldrin 0.05 mg/kg - - < 0.05 -

Endosulfan I 0.05 mg/kg - - < 0.05 -

Endosulfan II 0.05 mg/kg - - < 0.05 -

Endosulfan sulphate 0.05 mg/kg - - < 0.05 -

Endrin 0.05 mg/kg - - < 0.05 -

Endrin aldehyde 0.05 mg/kg - - < 0.05 -

Endrin ketone 0.05 mg/kg - - < 0.05 -

g-BHC (Lindane) 0.05 mg/kg - - < 0.05 -

Heptachlor 0.05 mg/kg - - < 0.05 -

Heptachlor epoxide 0.05 mg/kg - - < 0.05 -

Hexachlorobenzene 0.05 mg/kg - - < 0.05 -

Methoxychlor 0.2 mg/kg - - < 0.2 -

Toxaphene 1 mg/kg - - < 1 -


Tetrachloro-m-xylene (surr.) 1 % - - 98 -


Chlorpyrifos 0.5 mg/kg - - < 0.5 -

Coumaphos 0.5 mg/kg - - < 0.5 -

Demeton (total) 1 mg/kg - - < 1 -

Diazinon 0.5 mg/kg - - < 0.5 -

Dichlorvos 0.5 mg/kg - - < 0.5 -

Dimethoate 0.5 mg/kg - - < 0.5 -

Disulfoton 0.5 mg/kg - - < 0.5 -

Ethoprop 0.5 mg/kg - - < 0.5 -

Fenitrothion 0.5 mg/kg - - < 0.5 -

Fensulfothion 0.5 mg/kg - - < 0.5 -

Fenthion 0.5 mg/kg - - < 0.5 -

Methyl azinphos 0.5 mg/kg - - < 0.5 -

Malathion 0.5 mg/kg - - < 0.5 -




Page 27 of 72








Methyl parathion 0.5 mg/kg - - < 0.5 -

Mevinphos 0.5 mg/kg - - < 0.5 -

Monocrotophos 10 mg/kg - - < 10 -

Parathion 0.5 mg/kg - - < 0.5 -

Phorate 0.5 mg/kg - - < 0.5 -

Profenofos 0.5 mg/kg - - < 0.5 -

Prothiofos 0.5 mg/kg - - < 0.5 -

Ronnel 0.5 mg/kg - - < 0.5 -

Stirophos 0.5 mg/kg - - < 0.5 -

Trichloronate 0.5 mg/kg - - < 0.5 -

Triphenylphosphate (surr.) 1 % - - 105 -



% Moisture 0.1 % 23 24 19 22

Heavy Metals

Arsenic 2 mg/kg 7.1 7.7 < 2 13

Cadmium 0.4 mg/kg < 0.4 < 0.4 < 0.4 < 0.4

Chromium 5 mg/kg 12 11 < 5 15

Copper 5 mg/kg 13 15 5.5 12

Lead 5 mg/kg 24 13 11 15

Mercury 0.05 mg/kg < 0.05 < 0.05 < 0.05 < 0.05

Nickel 5 mg/kg 7.5 7.9 < 5 6.4

Zinc 5 mg/kg 30 32 48 41

Client Sample ID QC5 CTP18/0.0-0.2 CTP18/0.8-0.9 CTP18/1.4-1.6






TRH C6-C9 20 mg/kg < 20 < 20 < 20 < 20

TRH C10-C14 20 mg/kg < 20 < 20 < 20 < 20

TRH C15-C28 50 mg/kg < 50 480 430 < 50

TRH C29-C36 50 mg/kg < 50 1400 540 < 50

TRH C10-36 (Total) 50 mg/kg < 50 1900 970 < 50

BTEX

Benzene 0.1 mg/kg < 0.1 < 0.1 < 0.1 < 0.1

Toluene 0.1 mg/kg < 0.1 < 0.1 < 0.1 < 0.1


m&p-Xylenes 0.2 mg/kg < 0.2 < 0.2 < 0.2 < 0.2

o-Xylene 0.1 mg/kg < 0.1 < 0.1 < 0.1 < 0.1






Page 28 of 72









TRH C6-C10 20 mg/kg < 20 < 20 < 20 < 20


TRH >C10-C16 50 mg/kg < 50 < 50 < 50 < 50


TRH >C16-C34 100 mg/kg < 100 1700 890 < 100

TRH >C34-C40 100 mg/kg < 100 850 300 < 100



1.1-Dichloroethene 0.5 mg/kg - - < 0.5 -





1.2-Dibromoethane 0.5 mg/kg - - < 0.5 -




1.2.3-Trichloropropane 0.5 mg/kg - - < 0.5 -




Bromodichloromethane 0.5 mg/kg - - < 0.5 -

Bromoform 0.5 mg/kg - - < 0.5 -

Bromomethane 0.5 mg/kg - - < 0.5 -

Carbon Tetrachloride 0.5 mg/kg - - < 0.5 -

Chlorobenzene 0.5 mg/kg - - < 0.5 -

Chloroform 0.5 mg/kg - - < 0.5 -

Chloromethane 0.5 mg/kg - - < 0.5 -

cis-1.2-Dichloroethene 0.5 mg/kg - - < 0.5 -

cis-1.3-Dichloropropene 0.5 mg/kg - - < 0.5 -

Dibromochloromethane 0.5 mg/kg - - < 0.5 -

Dibromomethane 0.5 mg/kg - - < 0.5 -

Iodomethane 0.5 mg/kg - - < 0.5 -

Methylene Chloride 0.5 mg/kg - - < 0.5 -

Tetrachloroethene 0.5 mg/kg - - < 0.5 -

trans-1.2-Dichloroethene 0.5 mg/kg - - < 0.5 -

trans-1.3-Dichloropropene 0.5 mg/kg - - < 0.5 -

Trichloroethene 0.5 mg/kg - - < 0.5 -

Trichlorofluoromethane 0.5 mg/kg - - < 0.5 -

Vinyl chloride 0.5 mg/kg - - < 0.5 -

Fluorobenzene (surr.) 1 % - - 97 -


Benzo(a)pyrene TEQ (lower bound) * 0.5 mg/kg < 0.5 < 0.5 9.7 < 0.5


Benzo(a)pyrene TEQ (upper bound) * 0.5 mg/kg 1.2 1.3 10 1.2



Anthracene 0.5 mg/kg < 0.5 < 0.5 1.5 < 0.5




Page 29 of 72









Benzo(a)pyrene 0.5 mg/kg < 0.5 < 0.5 7.1 < 0.5


Benzo(g.h.i)perylene 0.5 mg/kg < 0.5 < 0.5 4.8 < 0.5

Benzo(k)fluoranthene 0.5 mg/kg < 0.5 < 0.5 6.8 < 0.5

Chrysene 0.5 mg/kg < 0.5 0.7 4.2 < 0.5


Fluoranthene 0.5 mg/kg 1.1 1.2 9.7 < 0.5

Fluorene 0.5 mg/kg < 0.5 < 0.5 < 0.5 < 0.5

Indeno(1.2.3-cd)pyrene 0.5 mg/kg < 0.5 < 0.5 3.8 < 0.5


Phenanthrene 0.5 mg/kg < 0.5 < 0.5 2.9 < 0.5

Pyrene 0.5 mg/kg 1.1 1.3 9.4 < 0.5

Total PAH* 0.5 mg/kg 2.2 4.6 65 < 0.5




Chlordanes - Total 0.1 mg/kg - < 0.1 - -

4.4'-DDD 0.05 mg/kg - < 0.05 - -

4.4'-DDE 0.05 mg/kg - < 0.05 - -

4.4'-DDT 0.05 mg/kg - < 0.05 - -

a-BHC 0.05 mg/kg - < 0.05 - -

Aldrin 0.05 mg/kg - < 0.05 - -

b-BHC 0.05 mg/kg - < 0.05 - -

d-BHC 0.05 mg/kg - < 0.05 - -

Dieldrin 0.05 mg/kg - < 0.05 - -

Endosulfan I 0.05 mg/kg - < 0.05 - -

Endosulfan II 0.05 mg/kg - < 0.05 - -

Endosulfan sulphate 0.05 mg/kg - < 0.05 - -

Endrin 0.05 mg/kg - < 0.05 - -

Endrin aldehyde 0.05 mg/kg - < 0.05 - -

Endrin ketone 0.05 mg/kg - < 0.05 - -

g-BHC (Lindane) 0.05 mg/kg - < 0.05 - -

Heptachlor 0.05 mg/kg - < 0.05 - -

Heptachlor epoxide 0.05 mg/kg - < 0.05 - -

Hexachlorobenzene 0.05 mg/kg - < 0.05 - -

Methoxychlor 0.2 mg/kg - < 0.2 - -

Toxaphene 1 mg/kg - < 1 - -

Dibutylchlorendate (surr.) 1 % - 97 - -

Tetrachloro-m-xylene (surr.) 1 % - 111 - -


Aroclor-1016 0.5 mg/kg - - < 0.5 -

Aroclor-1221 0.1 mg/kg - - < 0.1 -

Aroclor-1232 0.5 mg/kg - - < 0.5 -

Aroclor-1242 0.5 mg/kg - - < 0.5 -

Aroclor-1248 0.5 mg/kg - - < 0.5 -

Aroclor-1254 0.5 mg/kg - - < 0.5 -

Aroclor-1260 0.5 mg/kg - - < 0.5 -

Total PCB* 0.1 mg/kg - - < 0.1 -





Page 30 of 72








Chlorpyrifos 0.5 mg/kg - < 0.5 - -

Coumaphos 0.5 mg/kg - < 0.5 - -

Demeton (total) 1 mg/kg - < 1 - -

Diazinon 0.5 mg/kg - < 0.5 - -

Dichlorvos 0.5 mg/kg - < 0.5 - -

Dimethoate 0.5 mg/kg - < 0.5 - -

Disulfoton 0.5 mg/kg - < 0.5 - -

Ethoprop 0.5 mg/kg - < 0.5 - -

Fenitrothion 0.5 mg/kg - < 0.5 - -

Fensulfothion 0.5 mg/kg - < 0.5 - -

Fenthion 0.5 mg/kg - < 0.5 - -

Methyl azinphos 0.5 mg/kg - < 0.5 - -

Malathion 0.5 mg/kg - < 0.5 - -

Methyl parathion 0.5 mg/kg - < 0.5 - -

Mevinphos 0.5 mg/kg - < 0.5 - -

Monocrotophos 10 mg/kg - < 10 - -

Parathion 0.5 mg/kg - < 0.5 - -

Phorate 0.5 mg/kg - < 0.5 - -

Profenofos 0.5 mg/kg - < 0.5 - -

Prothiofos 0.5 mg/kg - < 0.5 - -

Ronnel 0.5 mg/kg - < 0.5 - -

Stirophos 0.5 mg/kg - < 0.5 - -

Trichloronate 0.5 mg/kg - < 0.5 - -

Triphenylphosphate (surr.) 1 % - 96 - -



% Moisture 0.1 % 21 24 14 21

Heavy Metals

Arsenic 2 mg/kg 13 6.8 12 15

Cadmium 0.4 mg/kg < 0.4 < 0.4 < 0.4 < 0.4

Chromium 5 mg/kg 12 10 10.0 14

Copper 5 mg/kg 10 19 22 16

Lead 5 mg/kg 20 120 63 20

Mercury 0.05 mg/kg < 0.05 < 0.05 0.06 < 0.05

Nickel 5 mg/kg < 5 < 5 10.0 < 5

Zinc 5 mg/kg 14 220 110 24




Page 31 of 72








TRH C6-C9 20 mg/kg < 20 < 20 < 20 < 20

TRH C10-C14 20 mg/kg < 20 < 20 < 20 < 20

TRH C15-C28 50 mg/kg 77 < 50 < 50 < 50

TRH C29-C36 50 mg/kg 250 < 50 < 50 < 50

TRH C10-36 (Total) 50 mg/kg 330 < 50 < 50 < 50

BTEX

Benzene 0.1 mg/kg < 0.1 < 0.1 < 0.1 < 0.1

Toluene 0.1 mg/kg < 0.1 < 0.1 < 0.1 < 0.1


m&p-Xylenes 0.2 mg/kg < 0.2 < 0.2 < 0.2 < 0.2

o-Xylene 0.1 mg/kg < 0.1 < 0.1 < 0.1 < 0.1





TRH C6-C10 20 mg/kg < 20 < 20 < 20 < 20


TRH >C10-C16 50 mg/kg < 50 < 50 < 50 < 50


TRH >C16-C34 100 mg/kg 270 < 100 < 100 < 100

TRH >C34-C40 100 mg/kg 200 < 100 < 100 < 100


Benzo(a)pyrene TEQ (lower bound) * 0.5 mg/kg < 0.5 < 0.5 < 0.5 < 0.5





Anthracene 0.5 mg/kg < 0.5 < 0.5 < 0.5 < 0.5

Benz(a)anthracene 0.5 mg/kg < 0.5 < 0.5 < 0.5 < 0.5

Benzo(a)pyrene 0.5 mg/kg < 0.5 < 0.5 < 0.5 < 0.5

Benzo(b&j)fluorantheneN07 0.5 mg/kg < 0.5 < 0.5 < 0.5 < 0.5



Chrysene 0.5 mg/kg < 0.5 < 0.5 < 0.5 < 0.5


Fluoranthene 0.5 mg/kg < 0.5 1.0 < 0.5 < 0.5

Fluorene 0.5 mg/kg < 0.5 < 0.5 < 0.5 < 0.5



Phenanthrene 0.5 mg/kg < 0.5 < 0.5 < 0.5 < 0.5

Pyrene 0.5 mg/kg < 0.5 0.9 < 0.5 < 0.5

Total PAH* 0.5 mg/kg < 0.5 1.9 < 0.5 < 0.5




Chlordanes - Total 0.1 mg/kg < 0.1 - - < 0.1

4.4'-DDD 0.05 mg/kg < 0.05 - - < 0.05

4.4'-DDE 0.05 mg/kg < 0.05 - - < 0.05

4.4'-DDT 0.05 mg/kg < 0.05 - - < 0.05




Page 32 of 72








a-BHC 0.05 mg/kg < 0.05 - - < 0.05

Aldrin 0.05 mg/kg < 0.05 - - < 0.05

b-BHC 0.05 mg/kg < 0.05 - - < 0.05

d-BHC 0.05 mg/kg < 0.05 - - < 0.05

Dieldrin 0.05 mg/kg < 0.05 - - < 0.05

Endosulfan I 0.05 mg/kg < 0.05 - - < 0.05

Endosulfan II 0.05 mg/kg < 0.05 - - < 0.05

Endosulfan sulphate 0.05 mg/kg < 0.05 - - < 0.05

Endrin 0.05 mg/kg < 0.05 - - < 0.05

Endrin aldehyde 0.05 mg/kg < 0.05 - - < 0.05

Endrin ketone 0.05 mg/kg < 0.05 - - < 0.05

g-BHC (Lindane) 0.05 mg/kg < 0.05 - - < 0.05

Heptachlor 0.05 mg/kg < 0.05 - - < 0.05

Heptachlor epoxide 0.05 mg/kg < 0.05 - - < 0.05

Hexachlorobenzene 0.05 mg/kg < 0.05 - - < 0.05

Methoxychlor 0.2 mg/kg < 0.2 - - < 0.2

Toxaphene 1 mg/kg < 1 - - < 1

Dibutylchlorendate (surr.) 1 % 99 - - 78

Tetrachloro-m-xylene (surr.) 1 % 107 - - 73


Chlorpyrifos 0.5 mg/kg < 0.5 - - < 0.5

Coumaphos 0.5 mg/kg < 0.5 - - < 0.5

Demeton (total) 1 mg/kg < 1 - - < 1

Diazinon 0.5 mg/kg < 0.5 - - < 0.5

Dichlorvos 0.5 mg/kg < 0.5 - - < 0.5

Dimethoate 0.5 mg/kg < 0.5 - - < 0.5

Disulfoton 0.5 mg/kg < 0.5 - - < 0.5

Ethoprop 0.5 mg/kg < 0.5 - - < 0.5

Fenitrothion 0.5 mg/kg < 0.5 - - < 0.5

Fensulfothion 0.5 mg/kg < 0.5 - - < 0.5

Fenthion 0.5 mg/kg < 0.5 - - < 0.5

Methyl azinphos 0.5 mg/kg < 0.5 - - < 0.5

Malathion 0.5 mg/kg < 0.5 - - < 0.5

Methyl parathion 0.5 mg/kg < 0.5 - - < 0.5

Mevinphos 0.5 mg/kg < 0.5 - - < 0.5

Monocrotophos 10 mg/kg < 10 - - < 10

Parathion 0.5 mg/kg < 0.5 - - < 0.5

Phorate 0.5 mg/kg < 0.5 - - < 0.5

Profenofos 0.5 mg/kg < 0.5 - - < 0.5

Prothiofos 0.5 mg/kg < 0.5 - - < 0.5

Ronnel 0.5 mg/kg < 0.5 - - < 0.5

Stirophos 0.5 mg/kg < 0.5 - - < 0.5

Trichloronate 0.5 mg/kg < 0.5 - - < 0.5

Triphenylphosphate (surr.) 1 % 104 - - 105



% Moisture 0.1 % 25 21 21 18




Page 33 of 72







Heavy Metals

Arsenic 2 mg/kg 4.2 17 11 4.4

Cadmium 0.4 mg/kg < 0.4 < 0.4 < 0.4 < 0.4

Chromium 5 mg/kg 7.5 16 10 6.7

Copper 5 mg/kg 12 15 11 14

Lead 5 mg/kg 43 26 19 58

Mercury 0.05 mg/kg < 0.05 < 0.05 < 0.05 < 0.05

Nickel 5 mg/kg < 5 < 5 < 5 5.2

Zinc 5 mg/kg 200 22 16 30







TRH C6-C9 20 mg/kg < 20 < 20 < 20 < 20

TRH C10-C14 20 mg/kg < 20 < 20 < 20 < 20

TRH C15-C28 50 mg/kg < 50 < 50 < 50 < 50

TRH C29-C36 50 mg/kg 97 < 50 < 50 < 50

TRH C10-36 (Total) 50 mg/kg 97 < 50 < 50 < 50

BTEX

Benzene 0.1 mg/kg < 0.1 < 0.1 < 0.1 < 0.1

Toluene 0.1 mg/kg < 0.1 < 0.1 < 0.1 < 0.1


m&p-Xylenes 0.2 mg/kg < 0.2 < 0.2 < 0.2 < 0.2

o-Xylene 0.1 mg/kg < 0.1 < 0.1 < 0.1 < 0.1





TRH C6-C10 20 mg/kg < 20 < 20 < 20 < 20


TRH >C10-C16 50 mg/kg < 50 < 50 < 50 < 50


TRH >C16-C34 100 mg/kg < 100 < 100 < 100 < 100

TRH >C34-C40 100 mg/kg < 100 < 100 < 100 < 100


Benzo(a)pyrene TEQ (lower bound) * 0.5 mg/kg < 0.5 < 0.5 < 0.5 1.1





Anthracene 0.5 mg/kg < 0.5 < 0.5 < 0.5 < 0.5

Benz(a)anthracene 0.5 mg/kg < 0.5 < 0.5 < 0.5 0.9

Benzo(a)pyrene 0.5 mg/kg < 0.5 < 0.5 < 0.5 0.8

Benzo(b&j)fluorantheneN07 0.5 mg/kg < 0.5 < 0.5 < 0.5 0.9


Benzo(k)fluoranthene 0.5 mg/kg < 0.5 < 0.5 < 0.5 0.7




Page 34 of 72








Chrysene 0.5 mg/kg < 0.5 < 0.5 < 0.5 0.8


Fluoranthene 0.5 mg/kg < 0.5 < 0.5 < 0.5 1.9

Fluorene 0.5 mg/kg < 0.5 < 0.5 < 0.5 < 0.5



Phenanthrene 0.5 mg/kg < 0.5 < 0.5 < 0.5 1.6

Pyrene 0.5 mg/kg < 0.5 < 0.5 < 0.5 1.9

Total PAH* 0.5 mg/kg < 0.5 < 0.5 < 0.5 9.5




Chlordanes - Total 0.1 mg/kg < 0.1 - - -

4.4'-DDD 0.05 mg/kg < 0.05 - - -

4.4'-DDE 0.05 mg/kg < 0.05 - - -

4.4'-DDT 0.05 mg/kg < 0.05 - - -

a-BHC 0.05 mg/kg < 0.05 - - -

Aldrin 0.05 mg/kg < 0.05 - - -

b-BHC 0.05 mg/kg < 0.05 - - -

d-BHC 0.05 mg/kg < 0.05 - - -

Dieldrin 0.05 mg/kg < 0.05 - - -

Endosulfan I 0.05 mg/kg < 0.05 - - -

Endosulfan II 0.05 mg/kg < 0.05 - - -

Endosulfan sulphate 0.05 mg/kg < 0.05 - - -

Endrin 0.05 mg/kg < 0.05 - - -

Endrin aldehyde 0.05 mg/kg < 0.05 - - -

Endrin ketone 0.05 mg/kg < 0.05 - - -

g-BHC (Lindane) 0.05 mg/kg < 0.05 - - -

Heptachlor 0.05 mg/kg < 0.05 - - -

Heptachlor epoxide 0.05 mg/kg < 0.05 - - -

Hexachlorobenzene 0.05 mg/kg < 0.05 - - -

Methoxychlor 0.2 mg/kg < 0.2 - - -

Toxaphene 1 mg/kg < 1 - - -



Acid Herbicides

2.4-D 0.5 mg/kg < 0.5 - - -

2.4-DB 0.5 mg/kg < 0.5 - - -

2.4.5-T 0.5 mg/kg < 0.5 - - -

2.4.5-TP 0.5 mg/kg < 0.5 - - -


Dicamba 0.5 mg/kg < 0.5 - - -



Dinoseb 0.5 mg/kg < 0.5 - - -

MCPA 0.5 mg/kg < 0.5 - - -

MCPB 0.5 mg/kg < 0.5 - - -






Page 35 of 72








Chlorpyrifos 0.5 mg/kg < 0.5 - - -

Coumaphos 0.5 mg/kg < 0.5 - - -

Demeton (total) 1 mg/kg < 1 - - -

Diazinon 0.5 mg/kg < 0.5 - - -

Dichlorvos 0.5 mg/kg < 0.5 - - -

Dimethoate 0.5 mg/kg < 0.5 - - -

Disulfoton 0.5 mg/kg < 0.5 - - -

Ethoprop 0.5 mg/kg < 0.5 - - -

Fenitrothion 0.5 mg/kg < 0.5 - - -

Fensulfothion 0.5 mg/kg < 0.5 - - -

Fenthion 0.5 mg/kg < 0.5 - - -

Methyl azinphos 0.5 mg/kg < 0.5 - - -

Malathion 0.5 mg/kg < 0.5 - - -

Methyl parathion 0.5 mg/kg < 0.5 - - -

Mevinphos 0.5 mg/kg < 0.5 - - -

Monocrotophos 10 mg/kg < 10 - - -

Parathion 0.5 mg/kg < 0.5 - - -

Phorate 0.5 mg/kg < 0.5 - - -

Profenofos 0.5 mg/kg < 0.5 - - -

Prothiofos 0.5 mg/kg < 0.5 - - -

Ronnel 0.5 mg/kg < 0.5 - - -

Stirophos 0.5 mg/kg < 0.5 - - -

Trichloronate 0.5 mg/kg < 0.5 - - -

Triphenylphosphate (surr.) 1 % 104 - - -



% Moisture 0.1 % 23 20 21 23

Heavy Metals

Arsenic 2 mg/kg 2.2 11 24 11

Cadmium 0.4 mg/kg < 0.4 < 0.4 < 0.4 < 0.4

Chromium 5 mg/kg 6.4 10 11 10

Copper 5 mg/kg 9.3 13 130 93

Lead 5 mg/kg 24 20 20 17

Mercury 0.05 mg/kg < 0.05 < 0.05 < 0.05 < 0.05

Nickel 5 mg/kg < 5 < 5 < 5 < 5

Zinc 5 mg/kg 130 18 17 15




Page 36 of 72








TRH C6-C9 20 mg/kg < 20 < 20 < 20 < 20

TRH C10-C14 20 mg/kg < 20 < 20 < 20 < 20

TRH C15-C28 50 mg/kg < 50 < 50 < 50 70

TRH C29-C36 50 mg/kg < 50 < 50 < 50 < 50

TRH C10-36 (Total) 50 mg/kg < 50 < 50 < 50 70

BTEX

Benzene 0.1 mg/kg < 0.1 < 0.1 < 0.1 < 0.1

Toluene 0.1 mg/kg < 0.1 < 0.1 < 0.1 < 0.1


m&p-Xylenes 0.2 mg/kg < 0.2 < 0.2 < 0.2 < 0.2

o-Xylene 0.1 mg/kg < 0.1 < 0.1 < 0.1 < 0.1





TRH C6-C10 20 mg/kg < 20 < 20 < 20 < 20


TRH >C10-C16 50 mg/kg < 50 < 50 < 50 < 50


TRH >C16-C34 100 mg/kg < 100 < 100 < 100 < 100

TRH >C34-C40 100 mg/kg < 100 < 100 < 100 < 100


1.1-Dichloroethane 0.5 mg/kg - < 0.5 - -

1.1-Dichloroethene 0.5 mg/kg - < 0.5 - -

1.1.1-Trichloroethane 0.5 mg/kg - < 0.5 - -

1.1.1.2-Tetrachloroethane 0.5 mg/kg - < 0.5 - -

1.1.2-Trichloroethane 0.5 mg/kg - < 0.5 - -

1.1.2.2-Tetrachloroethane 0.5 mg/kg - < 0.5 - -

1.2-Dibromoethane 0.5 mg/kg - < 0.5 - -

1.2-Dichlorobenzene 0.5 mg/kg - < 0.5 - -

1.2-Dichloroethane 0.5 mg/kg - < 0.5 - -

1.2-Dichloropropane 0.5 mg/kg - < 0.5 - -

1.2.3-Trichloropropane 0.5 mg/kg - < 0.5 - -


1.3-Dichloropropane 0.5 mg/kg - < 0.5 - -


Bromodichloromethane 0.5 mg/kg - < 0.5 - -

Bromoform 0.5 mg/kg - < 0.5 - -

Bromomethane 0.5 mg/kg - < 0.5 - -

Carbon Tetrachloride 0.5 mg/kg - < 0.5 - -

Chlorobenzene 0.5 mg/kg - < 0.5 - -

Chloroform 0.5 mg/kg - < 0.5 - -

Chloromethane 0.5 mg/kg - < 0.5 - -

cis-1.2-Dichloroethene 0.5 mg/kg - < 0.5 - -

cis-1.3-Dichloropropene 0.5 mg/kg - < 0.5 - -

Dibromochloromethane 0.5 mg/kg - < 0.5 - -

Dibromomethane 0.5 mg/kg - < 0.5 - -

Iodomethane 0.5 mg/kg - < 0.5 - -

Methylene Chloride 0.5 mg/kg - < 0.5 - -




Page 37 of 72








Tetrachloroethene 0.5 mg/kg - < 0.5 - -

trans-1.2-Dichloroethene 0.5 mg/kg - < 0.5 - -

trans-1.3-Dichloropropene 0.5 mg/kg - < 0.5 - -

Trichloroethene 0.5 mg/kg - < 0.5 - -

Trichlorofluoromethane 0.5 mg/kg - < 0.5 - -

Vinyl chloride 0.5 mg/kg - < 0.5 - -

Fluorobenzene (surr.) 1 % - 97 - -


Benzo(a)pyrene TEQ (lower bound) * 0.5 mg/kg 1.3 < 0.5 < 0.5 < 0.5





Anthracene 0.5 mg/kg < 0.5 < 0.5 < 0.5 < 0.5

Benz(a)anthracene 0.5 mg/kg 1.0 < 0.5 < 0.5 < 0.5

Benzo(a)pyrene 0.5 mg/kg 1.0 < 0.5 < 0.5 < 0.5

Benzo(b&j)fluorantheneN07 0.5 mg/kg 0.8 < 0.5 < 0.5 < 0.5


Benzo(k)fluoranthene 0.5 mg/kg 0.7 < 0.5 < 0.5 < 0.5

Chrysene 0.5 mg/kg 0.8 < 0.5 < 0.5 < 0.5


Fluoranthene 0.5 mg/kg 1.9 < 0.5 < 0.5 < 0.5

Fluorene 0.5 mg/kg < 0.5 < 0.5 < 0.5 < 0.5



Phenanthrene 0.5 mg/kg 1.0 < 0.5 < 0.5 < 0.5

Pyrene 0.5 mg/kg 1.8 < 0.5 < 0.5 < 0.5

Total PAH* 0.5 mg/kg 9.0 < 0.5 < 0.5 < 0.5




Chlordanes - Total 0.1 mg/kg < 0.1 - - -

4.4'-DDD 0.05 mg/kg < 0.05 - - -

4.4'-DDE 0.05 mg/kg < 0.05 - - -

4.4'-DDT 0.05 mg/kg < 0.05 - - -

a-BHC 0.05 mg/kg < 0.05 - - -

Aldrin 0.05 mg/kg < 0.05 - - -

b-BHC 0.05 mg/kg < 0.05 - - -

d-BHC 0.05 mg/kg < 0.05 - - -

Dieldrin 0.05 mg/kg < 0.05 - - -

Endosulfan I 0.05 mg/kg < 0.05 - - -

Endosulfan II 0.05 mg/kg < 0.05 - - -

Endosulfan sulphate 0.05 mg/kg < 0.05 - - -

Endrin 0.05 mg/kg < 0.05 - - -

Endrin aldehyde 0.05 mg/kg < 0.05 - - -

Endrin ketone 0.05 mg/kg < 0.05 - - -

g-BHC (Lindane) 0.05 mg/kg < 0.05 - - -

Heptachlor 0.05 mg/kg < 0.05 - - -

Heptachlor epoxide 0.05 mg/kg < 0.05 - - -




Page 38 of 72








Hexachlorobenzene 0.05 mg/kg < 0.05 - - -

Methoxychlor 0.2 mg/kg < 0.2 - - -

Toxaphene 1 mg/kg < 1 - - -




Aroclor-1016 0.5 mg/kg - < 0.5 - -

Aroclor-1221 0.1 mg/kg - < 0.1 - -

Aroclor-1232 0.5 mg/kg - < 0.5 - -

Aroclor-1242 0.5 mg/kg - < 0.5 - -

Aroclor-1248 0.5 mg/kg - < 0.5 - -

Aroclor-1254 0.5 mg/kg - < 0.5 - -

Aroclor-1260 0.5 mg/kg - < 0.5 - -

Total PCB* 0.1 mg/kg - < 0.1 - -

Dibutylchlorendate (surr.) 1 % - 100 - -

Tetrachloro-m-xylene (surr.) 1 % - - -


Chlorpyrifos 0.5 mg/kg < 0.5 - - -

Coumaphos 0.5 mg/kg < 0.5 - - -

Demeton (total) 1 mg/kg < 1 - - -

Diazinon 0.5 mg/kg < 0.5 - - -

Dichlorvos 0.5 mg/kg < 0.5 - - -

Dimethoate 0.5 mg/kg < 0.5 - - -

Disulfoton 0.5 mg/kg < 0.5 - - -

Ethoprop 0.5 mg/kg < 0.5 - - -

Fenitrothion 0.5 mg/kg < 0.5 - - -

Fensulfothion 0.5 mg/kg < 0.5 - - -

Fenthion 0.5 mg/kg < 0.5 - - -

Methyl azinphos 0.5 mg/kg < 0.5 - - -

Malathion 0.5 mg/kg < 0.5 - - -

Methyl parathion 0.5 mg/kg < 0.5 - - -

Mevinphos 0.5 mg/kg < 0.5 - - -

Monocrotophos 10 mg/kg < 10 - - -

Parathion 0.5 mg/kg < 0.5 - - -

Phorate 0.5 mg/kg < 0.5 - - -

Profenofos 0.5 mg/kg < 0.5 - - -

Prothiofos 0.5 mg/kg < 0.5 - - -

Ronnel 0.5 mg/kg < 0.5 - - -

Stirophos 0.5 mg/kg < 0.5 - - -

Trichloronate 0.5 mg/kg < 0.5 - - -

Triphenylphosphate (surr.) 1 % 100 - - -



% Moisture 0.1 % 12 18 19 24




Page 39 of 72







Heavy Metals

Arsenic 2 mg/kg < 2 14 10 12

Cadmium 0.4 mg/kg < 0.4 < 0.4 < 0.4 < 0.4

Chromium 5 mg/kg < 5 16 13 16

Copper 5 mg/kg 17 28 20 10

Lead 5 mg/kg 78 57 24 13

Mercury 0.05 mg/kg 0.19 0.06 < 0.05 < 0.05

Nickel 5 mg/kg < 5 8.9 13 6.5

Zinc 5 mg/kg 59 67 60 19







TRH C6-C9 20 mg/kg < 20 < 20 < 20 -

TRH C10-C14 20 mg/kg < 20 < 20 < 20 -

TRH C15-C28 50 mg/kg 130 110 < 50 -

TRH C29-C36 50 mg/kg < 50 < 50 < 50 -

TRH C10-36 (Total) 50 mg/kg 130 110 < 50 -

BTEX

Benzene 0.1 mg/kg < 0.1 < 0.1 < 0.1 -

Toluene 0.1 mg/kg < 0.1 < 0.1 < 0.1 -

Ethylbenzene 0.1 mg/kg < 0.1 < 0.1 < 0.1 -

m&p-Xylenes 0.2 mg/kg < 0.2 < 0.2 < 0.2 -

o-Xylene 0.1 mg/kg < 0.1 < 0.1 < 0.1 -

Xylenes - Total 0.3 mg/kg < 0.3 < 0.3 < 0.3 -

4-Bromofluorobenzene (surr.) 1 % 92 87 91 -


NaphthaleneN02 0.5 mg/kg < 0.5 < 0.5 < 0.5 -

TRH C6-C10 20 mg/kg < 20 < 20 < 20 -

TRH C6-C10 less BTEX (F1)N04 20 mg/kg < 20 < 20 < 20 -

TRH >C10-C16 50 mg/kg < 50 < 50 < 50 -

TRH >C10-C16 less Naphthalene (F2)N01 50 mg/kg < 50 < 50 < 50 -

TRH >C16-C34 100 mg/kg 160 120 < 100 -

TRH >C34-C40 100 mg/kg < 100 < 100 < 100 -


Benzo(a)pyrene TEQ (lower bound) * 0.5 mg/kg < 0.5 < 0.5 < 0.5 -

Benzo(a)pyrene TEQ (medium bound) * 0.5 mg/kg 0.6 0.6 0.6 -

Benzo(a)pyrene TEQ (upper bound) * 0.5 mg/kg 1.2 1.2 1.2 -

Acenaphthene 0.5 mg/kg < 0.5 < 0.5 < 0.5 -

Acenaphthylene 0.5 mg/kg < 0.5 < 0.5 < 0.5 -

Anthracene 0.5 mg/kg < 0.5 < 0.5 < 0.5 -

Benz(a)anthracene 0.5 mg/kg < 0.5 < 0.5 < 0.5 -

Benzo(a)pyrene 0.5 mg/kg < 0.5 < 0.5 < 0.5 -

Benzo(b&j)fluorantheneN07 0.5 mg/kg < 0.5 < 0.5 < 0.5 -

Benzo(g.h.i)perylene 0.5 mg/kg < 0.5 < 0.5 < 0.5 -

Benzo(k)fluoranthene 0.5 mg/kg < 0.5 < 0.5 < 0.5 -




Page 40 of 72








Chrysene 0.5 mg/kg < 0.5 < 0.5 < 0.5 -

Dibenz(a.h)anthracene 0.5 mg/kg < 0.5 < 0.5 < 0.5 -

Fluoranthene 0.5 mg/kg < 0.5 < 0.5 < 0.5 -

Fluorene 0.5 mg/kg < 0.5 < 0.5 < 0.5 -

Indeno(1.2.3-cd)pyrene 0.5 mg/kg < 0.5 < 0.5 < 0.5 -

Naphthalene 0.5 mg/kg < 0.5 < 0.5 < 0.5 -

Phenanthrene 0.5 mg/kg < 0.5 < 0.5 < 0.5 -

Pyrene 0.5 mg/kg < 0.5 < 0.5 < 0.5 -

Total PAH* 0.5 mg/kg < 0.5 < 0.5 < 0.5 -

2-Fluorobiphenyl (surr.) 1 % 115 99 107 -

p-Terphenyl-d14 (surr.) 1 % 114 100 96 -



% Moisture 0.1 % 16 19 22 23

Heavy Metals

Arsenic 2 mg/kg 4.1 11 12 35

Cadmium 0.4 mg/kg < 0.4 < 0.4 < 0.4 < 0.4


Copper 5 mg/kg 12 22 12 21

Lead 5 mg/kg 17 51 12 11

Mercury 0.05 mg/kg < 0.05 < 0.05 < 0.05 < 0.05

Nickel 5 mg/kg 9.7 < 5 < 5 8.2

Zinc 5 mg/kg 44 73 22 40

Foreign Materials - ENM

Initial Weight 0.01 kg - 8.1 - -

Foreign Material - Type I

Metal* 0.1 % - < 0.1 - -

Glass* 0.1 % - < 0.1 - -

Asphalt* 0.1 % - < 0.1 - -

Stone* 0.1 % - < 0.1 - -

Ceramic and slag (other than blast furnace slag)* 0.1 % - < 0.1 - -

Foreign Material - Type II

Plaster* 0.1 % - < 0.1 - -

Clay lumps and other friable material* 0.1 % - 48 - -

Foreign Material - Type III

Rubber* 0.05 % - < 0.05 - -

Plastic* 0.05 % - < 0.05 - -

Bitumen* 0.05 % - < 0.05 - -

Paper* 0.05 % - < 0.05 - -

Cloth* 0.05 % - < 0.05 - -

Paint* 0.05 % - < 0.05 - -

Wood and other vegetable matter* 0.05 % - 0.84 - -




Page 41 of 72


Client Sample ID TRIP SPIKE TRIP BLANK

Sample Matrix Soil Soil

Eurofins | mgt Sample No. S15-Jn20328 S15-Jn20329

Date Sampled Jun 18, 2015 Jun 18, 2015



TRH C6-C9 20 mg/kg - < 20

BTEX

Benzene 0.1 mg/kg 93% < 0.1

Toluene 0.1 mg/kg 94% < 0.1

Ethylbenzene 0.1 mg/kg 94% < 0.1

m&p-Xylenes 0.2 mg/kg 95% < 0.2

o-Xylene 0.1 mg/kg 95% < 0.1

Xylenes - Total 0.3 mg/kg 95% < 0.3

4-Bromofluorobenzene (surr.) 1 % 85 85


TRH C6-C10 20 mg/kg - < 20

TRH C6-C10 less BTEX (F1)N04 20 mg/kg - < 20

Volatile Organics

NaphthaleneN02 0.5 mg/kg - < 0.5




Page 42 of 72


Sample HistoryWhere samples are submitted/analysed over several days, the last date of extraction and analysis is reported.A recent review of our LIMS has resulted in the correction or clarification of some method identifications. Due to this, some of the method reference information on reports has changed. However,no substantive change has been made to our laboratory methods, and as such there is no change in the validity of current or previous results (regarding both quality and NATA accreditation).

If the date and time of sampling are not provided, the Laboratory will not be responsible for compromised results should testing be performed outside the recommended holding time.

Description Testing Site Extracted Holding Time

Total Recoverable Hydrocarbons - 1999 NEPM Fractions Sydney Jun 29, 2015 14 Day

- Method: TRH C6-C36 - LTM-ORG-2010

BTEX Sydney Jun 29, 2015 14 Day


Total Recoverable Hydrocarbons - 2013 NEPM Fractions Sydney Jun 29, 2015 14 Day


Volatile Organics Sydney Jun 29, 2015 7 Day

- Method: E016 Volatile Organic Compounds (VOC)

Eurofins | mgt Suite 4

Polycyclic Aromatic Hydrocarbons Sydney Jun 29, 2015 14 Day

- Method: E007 Polyaromatic Hydrocarbons (PAH)

Halogenated Volatile Organics Sydney Jun 26, 2015 7 Day

- Method: E016 Volatile Halogenated Compounds (VHC)

Polychlorinated Biphenyls Sydney Jun 26, 2015 28 Day

Acid Herbicides Melbourne Jun 26, 2015 14 Day

- Method: MGT 530

Eurofins | mgt Suite 14

Organochlorine Pesticides Sydney Jun 29, 2015 14 Day

- Method: E013 Organochlorine Pesticides (OC)

Organophosphorus Pesticides (OP) Sydney Jun 29, 2015 14 Day

- Method: E014 Organophosphorus Pesticides (OP)

ENM Exemption 2012 - NSW Office of Environment and Heritage (excluding Foreign Materials)

Conductivity (1:5 aqueous extract at 25°C) Sydney Jul 01, 2015 7 Day

- Method: E032.2 Electrical Conductivity (EC)

pH (1:5 Aqueous extract) Sydney Jul 01, 2015 7 Day

- Method: LTM-GEN-7090 pH in soil by ISE

Metals M8 Sydney Jun 26, 2015 28 Day

- Method: LTM-MET-3040_R0 TOTAL AND DISSOLVED METALS AND MERCURY IN WATERS BY ICP-MS

% Moisture Sydney Jun 24, 2015 14 Day

- Method: LTM-GEN-7080 Moisture

Foreign Material - Type I Sydney Jun 24, 2015 180 Day

- Method: RMS Method T276

Foreign Material - Type II Sydney Jun 24, 2015 180 Day


Foreign Material - Type III Sydney Jun 24, 2015 180 Day





Page 43 of 72


.Company Name: Coffey Environments Pty Ltd Wollongong Order No.: Received: Jun 24, 2015 1:22 PMAddress: 118 Auburn Street Report #: 462743 Due: Jul 1, 2015

Wollongong Phone: 02 4201 1400 Priority: 5 DayNSW 2500 Fax: 02 4201 1401 Contact Name: Alexander Williams

Project Name: ENAUWOLL04223AA

Eurofins | mgt Client Manager: Charl Du Preez

Sample Detail

Asbestos A

bsence /Presence

HO

LD

Polychlorinated B

iphenyls

Acid H

erbicides

Metals M

8

BT

EX

Foreign M

aterials - EN

M

EN

M E

xemption 2012 - N

SW

Office of

Environm

ent and Heritage (excluding

Eurofins | m

gt Suite 14

Eurofins | m

gt Suite 4

BT

EX

and Volatile T

RH

Halogenated V

olatile Organics

Moisture S

et

Laboratory where analysis is conducted

Melbourne Laboratory - NATA Site # 1254 & 14271 X

Sydney Laboratory - NATA Site # 18217 X X X X X X X X X X X X

Brisbane Laboratory - NATA Site # 20794

External Laboratory

Sample ID Sample Date SamplingTime

Matrix LAB ID

CTP01/0.0-0.2 Jun 22, 2015 Soil S15-Jn20258 X X X X

CTP01/1.0-1.2 Jun 22, 2015 Soil S15-Jn20259 X X X

CTP01/1.4-1.6 Jun 22, 2015 Soil S15-Jn20260 X X X X X


CTP01/2.0-2.1 Jun 22, 2015 Soil S15-Jn20262 X

CTP02/1.35-1.45

Jun 22, 2015 Soil S15-Jn20263 X X X X

CTP02A/0.0-0.2

Jun 22, 2015 Soil S15-Jn20264 X X X X


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7 39

02 4

600

NA

TA #

126

1 S

ite #

207

94

Dat

e R

epor

ted:

Jul 0

1, 2

015

Eur

ofin

s | m

gt U

nit F

3, B

uild

ing

F, 1

6 M

ars

Roa

d, L

ane

Cov

e W

est,

NS

W, A

ustr

alia

, 206

6

AB

N :

50 0

05 0

85 5

21 T

elep

hone

: +61

2 9

900

8400

Fac

sim

ile: +

61 2

942

0 29

77

Pag

e 44

of 7

2

Rep

ort N

umbe

r: 4

6274

3-S

Company Name: Coffey Environments Pty Ltd Wollongong Order No.: Received: Jun 24, 2015 1:22 PMAddress: 118 Auburn Street Report #: 462743 Due: Jul 1, 2015




Sample Detail

Asbestos A

bsence /Presence

HO

LD

Polychlorinated B

iphenyls

Acid H

erbicides

Metals M

8

BT

EX

Foreign M

aterials - EN

M

EN

M E

xemption 2012 - N

SW

Office of

Environm


Eurofins | m

gt Suite 14

Eurofins | m

gt Suite 4

BT

EX

and Volatile T

RH

Halogenated V

olatile Organics

Moisture S

et





External Laboratory


CTP03/1.2-1.3 Jun 22, 2015 Soil S15-Jn20267 X


CTP04/0.3-0.4 Jun 22, 2015 Soil S15-Jn20269 X X


CTP05/0.4-0.5 Jun 22, 2015 Soil S15-Jn20271 X

QC2 Jun 22, 2015 Soil S15-Jn20272 X X X

QC1 Jun 22, 2015 Soil S15-Jn20273 X X X X X


CTP06/0.2-0.25

Jun 22, 2015 Soil S15-Jn20275 X X

CTP06/0.35- Jun 22, 2015 Soil S15-Jn20276 X X X X X X

AB

N –

50

005

085

521

e.m

ail :

Env

iroS

ales

@eu

rofin

s.co

m.a

u

w

eb :

ww

w.e

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ins.

com

.au

Mel

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Mel

bour

neM

elbo

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3-5

Kin

gsto

n To

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VIC

316

6P

hone

: +6

1 3

8564

500

0N

ATA

# 1

261

Site

# 1

254

& 1

4271

Syd

ney

Syd

ney

Syd

ney

Syd

ney

Uni

t F3,

Bui

ldin

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16 M

ars

Roa

dLa

ne C

ove

Wes

t NS

W 2

066

Pho

ne :

+61

2 99

00 8

400

NA

TA #

126

1 S

ite #

182

17

Bris

bane

Bris

bane

Bris

bane

Bris

bane

1/21

Sm

allw

ood

Pla

ceM

urar

rie Q

LD 4

172

Pho

ne :

+61

7 39

02 4

600

NA

TA #

126

1 S

ite #

207

94

Pag

e 45

of 7

2

Rep

ort N

umbe

r: 4

6274

3-S





Sample Detail

Asbestos A

bsence /Presence

HO

LD

Polychlorinated B

iphenyls

Acid H

erbicides

Metals M

8

BT

EX

Foreign M

aterials - EN

M

EN

M E

xemption 2012 - N

SW

Office of

Environm


Eurofins | m

gt Suite 14

Eurofins | m

gt Suite 4

BT

EX

and Volatile T

RH

Halogenated V

olatile Organics

Moisture S

et





External Laboratory

0.55

CTP06/0.75-0.85

Jun 22, 2015 Soil S15-Jn20277 X X


CTP07/0.3-0.4 Jun 22, 2015 Soil S15-Jn20279 X


CTP08/0.35-0.45

Jun 22, 2015 Soil S15-Jn20281 X X X



CTP10/0.45-065

Jun 23, 2015 Soil S15-Jn20284 X X X

AB

N –

50

005

085

521

e.m

ail :

Env

iroS

ales

@eu

rofin

s.co

m.a

u

w

eb :

ww

w.e

urof

ins.

com

.au

Mel

bour

neM

elbo

urne

Mel

bour

neM

elbo

urne

3-5

Kin

gsto

n To

wn

Clo

seO

akle

igh

VIC

316

6P

hone

: +6

1 3

8564

500

0N

ATA

# 1

261

Site

# 1

254

& 1

4271

Syd

ney

Syd

ney

Syd

ney

Syd

ney

Uni

t F3,

Bui

ldin

g F

16 M

ars

Roa

dLa

ne C

ove

Wes

t NS

W 2

066

Pho

ne :

+61

2 99

00 8

400

NA

TA #

126

1 S

ite #

182

17

Bris

bane

Bris

bane

Bris

bane

Bris

bane

1/21

Sm

allw

ood

Pla

ceM

urar

rie Q

LD 4

172

Pho

ne :

+61

7 39

02 4

600

NA

TA #

126

1 S

ite #

207

94

Pag

e 46

of 7

2

Rep

ort N

umbe

r: 4

6274

3-S





Sample Detail

Asbestos A

bsence /Presence

HO

LD

Polychlorinated B

iphenyls

Acid H

erbicides

Metals M

8

BT

EX

Foreign M

aterials - EN

M

EN

M E

xemption 2012 - N

SW

Office of

Environm


Eurofins | m

gt Suite 14

Eurofins | m

gt Suite 4

BT

EX

and Volatile T

RH

Halogenated V

olatile Organics

Moisture S

et





External Laboratory

CTP10/0.7-0.8 Jun 23, 2015 Soil S15-Jn20285 X




QC3 Jun 22, 2015 Soil S15-Jn20289 X


CTP12/0.25-0.45

Jun 23, 2015 Soil S15-Jn20291 X X X

CTP13/0.0-0.2 Jun 22, 2015 Soil S15-Jn20292 X X X X X X X


CTP13/0.7-0.8 Jun 22, 2015 Soil S15-Jn20294 X


AB

N –

50

005

085

521

e.m

ail :

Env

iroS

ales

@eu

rofin

s.co

m.a

u

w

eb :

ww

w.e

urof

ins.

com

.au

Mel

bour

neM

elbo

urne

Mel

bour

neM

elbo

urne

3-5

Kin

gsto

n To

wn

Clo

seO

akle

igh

VIC

316

6P

hone

: +6

1 3

8564

500

0N

ATA

# 1

261

Site

# 1

254

& 1

4271

Syd

ney

Syd

ney

Syd

ney

Syd

ney

Uni

t F3,

Bui

ldin

g F

16 M

ars

Roa

dLa

ne C

ove

Wes

t NS

W 2

066

Pho

ne :

+61

2 99

00 8

400

NA

TA #

126

1 S

ite #

182

17

Bris

bane

Bris

bane

Bris

bane

Bris

bane

1/21

Sm

allw

ood

Pla

ceM

urar

rie Q

LD 4

172

Pho

ne :

+61

7 39

02 4

600

NA

TA #

126

1 S

ite #

207

94

Pag

e 47

of 7

2

Rep

ort N

umbe

r: 4

6274

3-S





Sample Detail

Asbestos A

bsence /Presence

HO

LD

Polychlorinated B

iphenyls

Acid H

erbicides

Metals M

8

BT

EX

Foreign M

aterials - EN

M

EN

M E

xemption 2012 - N

SW

Office of

Environm


Eurofins | m

gt Suite 14

Eurofins | m

gt Suite 4

BT

EX

and Volatile T

RH

Halogenated V

olatile Organics

Moisture S

et





External Laboratory










QC6 Jun 23, 2015 Soil S15-Jn20305 X

QC5 Jun 23, 2015 Soil S15-Jn20306 X X

AB

N –

50

005

085

521

e.m

ail :

Env

iroS

ales

@eu

rofin

s.co

m.a

u

w

eb :

ww

w.e

urof

ins.

com

.au

Mel

bour

neM

elbo

urne

Mel

bour

neM

elbo

urne

3-5

Kin

gsto

n To

wn

Clo

seO

akle

igh

VIC

316

6P

hone

: +6

1 3

8564

500

0N

ATA

# 1

261

Site

# 1

254

& 1

4271

Syd

ney

Syd

ney

Syd

ney

Syd

ney

Uni

t F3,

Bui

ldin

g F

16 M

ars

Roa

dLa

ne C

ove

Wes

t NS

W 2

066

Pho

ne :

+61

2 99

00 8

400

NA

TA #

126

1 S

ite #

182

17

Bris

bane

Bris

bane

Bris

bane

Bris

bane

1/21

Sm

allw

ood

Pla

ceM

urar

rie Q

LD 4

172

Pho

ne :

+61

7 39

02 4

600

NA

TA #

126

1 S

ite #

207

94

Pag

e 48

of 7

2

Rep

ort N

umbe

r: 4

6274

3-S





Sample Detail

Asbestos A

bsence /Presence

HO

LD

Polychlorinated B

iphenyls

Acid H

erbicides

Metals M

8

BT

EX

Foreign M

aterials - EN

M

EN

M E

xemption 2012 - N

SW

Office of

Environm


Eurofins | m

gt Suite 14

Eurofins | m

gt Suite 4

BT

EX

and Volatile T

RH

Halogenated V

olatile Organics

Moisture S

et





External Laboratory




CTP18/1.7-1.9 Jun 23, 2015 Soil S15-Jn20310 X








AB

N –

50

005

085

521

e.m

ail :

Env

iroS

ales

@eu

rofin

s.co

m.a

u

w

eb :

ww

w.e

urof

ins.

com

.au

Mel

bour

neM

elbo

urne

Mel

bour

neM

elbo

urne

3-5

Kin

gsto

n To

wn

Clo

seO

akle

igh

VIC

316

6P

hone

: +6

1 3

8564

500

0N

ATA

# 1

261

Site

# 1

254

& 1

4271

Syd

ney

Syd

ney

Syd

ney

Syd

ney

Uni

t F3,

Bui

ldin

g F

16 M

ars

Roa

dLa

ne C

ove

Wes

t NS

W 2

066

Pho

ne :

+61

2 99

00 8

400

NA

TA #

126

1 S

ite #

182

17

Bris

bane

Bris

bane

Bris

bane

Bris

bane

1/21

Sm

allw

ood

Pla

ceM

urar

rie Q

LD 4

172

Pho

ne :

+61

7 39

02 4

600

NA

TA #

126

1 S

ite #

207

94

Pag

e 49

of 7

2

Rep

ort N

umbe

r: 4

6274

3-S





Sample Detail

Asbestos A

bsence /Presence

HO

LD

Polychlorinated B

iphenyls

Acid H

erbicides

Metals M

8

BT

EX

Foreign M

aterials - EN

M

EN

M E

xemption 2012 - N

SW

Office of

Environm


Eurofins | m

gt Suite 14

Eurofins | m

gt Suite 4

BT

EX

and Volatile T

RH

Halogenated V

olatile Organics

Moisture S

et





External Laboratory










CTP22/0.8-1.2ACM

Jun 23, 2015 Soil S15-Jn20327 X

TRIP SPIKE Jun 18, 2015 Soil S15-Jn20328 X

AB

N –

50

005

085

521

e.m

ail :

Env

iroS

ales

@eu

rofin

s.co

m.a

u

w

eb :

ww

w.e

urof

ins.

com

.au

Mel

bour

neM

elbo

urne

Mel

bour

neM

elbo

urne

3-5

Kin

gsto

n To

wn

Clo

seO

akle

igh

VIC

316

6P

hone

: +6

1 3

8564

500

0N

ATA

# 1

261

Site

# 1

254

& 1

4271

Syd

ney

Syd

ney

Syd

ney

Syd

ney

Uni

t F3,

Bui

ldin

g F

16 M

ars

Roa

dLa

ne C

ove

Wes

t NS

W 2

066

Pho

ne :

+61

2 99

00 8

400

NA

TA #

126

1 S

ite #

182

17

Bris

bane

Bris

bane

Bris

bane

Bris

bane

1/21

Sm

allw

ood

Pla

ceM

urar

rie Q

LD 4

172

Pho

ne :

+61

7 39

02 4

600

NA

TA #

126

1 S

ite #

207

94

Pag

e 50

of 7

2

Rep

ort N

umbe

r: 4

6274

3-S





Sample Detail

Asbestos A

bsence /Presence

HO

LD

Polychlorinated B

iphenyls

Acid H

erbicides

Metals M

8

BT

EX

Foreign M

aterials - EN

M

EN

M E

xemption 2012 - N

SW

Office of

Environm


Eurofins | m

gt Suite 14

Eurofins | m

gt Suite 4

BT

EX

and Volatile T

RH

Halogenated V

olatile Organics

Moisture S

et





External Laboratory

TRIP BLANK Jun 18, 2015 Soil S15-Jn20329 X

TSLAB Jun 18, 2015 Soil S15-Jn20330 X

AB

N –

50

005

085

521

e.m

ail :

Env

iroS

ales

@eu

rofin

s.co

m.a

u

w

eb :

ww

w.e

urof

ins.

com

.au

Mel

bour

neM

elbo

urne

Mel

bour

neM

elbo

urne

3-5

Kin

gsto

n To

wn

Clo

seO

akle

igh

VIC

316

6P

hone

: +6

1 3

8564

500

0N

ATA

# 1

261

Site

# 1

254

& 1

4271

Syd

ney

Syd

ney

Syd

ney

Syd

ney

Uni

t F3,

Bui

ldin

g F

16 M

ars

Roa

dLa

ne C

ove

Wes

t NS

W 2

066

Pho

ne :

+61

2 99

00 8

400

NA

TA #

126

1 S

ite #

182

17

Bris

bane

Bris

bane

Bris

bane

Bris

bane

1/21

Sm

allw

ood

Pla

ceM

urar

rie Q

LD 4

172

Pho

ne :

+61

7 39

02 4

600

NA

TA #

126

1 S

ite #

207

94

Pag

e 51

of 7

2

Rep

ort N

umbe

r: 4

6274

3-S

Eurofins | mgt Internal Quality Control Review and Glossary

General

Holding Times

UNITS

TERMS

QC - ACCEPTANCE CRITERIA

QC DATA GENERAL COMMENTS

1. Laboratory QC results for Method Blanks, Duplicates, Matrix Spikes, and Laboratory Control Samples are included in this QC report where applicable. Additional QC data may be available on

request.

2. All soil results are reported on a dry basis, unless otherwise stated.

3. Actual LORs are matrix dependant. Quoted LORs may be raised where sample extracts are diluted due to interferences.

4. Results are uncorrected for matrix spikes or surrogate recoveries.

5. SVOC analysis on waters are performed on homogenised, unfiltered samples, unless noted otherwise.

6. Samples were analysed on an 'as received' basis. 7. This report replaces any interim results previously issued.

Please refer to 'Sample Preservation and Container Guide' for holding times (QS3001).

For samples received on the last day of holding time, notification of testing requirements should have been received at least 6 hours prior to sample receipt deadlines as stated on the Sample

Receipt Advice.

If the Laboratory did not receive the information in the required timeframe, and regardless of any other integrity issues, suitably qualified results may still be reported.

Holding times apply from the date of sampling, therefore compliance to these may be outside the laboratory's control.

**NOTE: pH duplicates are reported as a range NOT as RPD

mg/kg: milligrams per Kilogram mg/l: milligrams per litre

ug/l: micrograms per litre ppm: Parts per million

ppb: Parts per billion %: Percentage

org/100ml: Organisms per 100 millilitres NTU: Nephelometric Turbidity Units

MPN/100mL: Most Probable Number of organisms per 100 millilitres

Dry Where a moisture has been determined on a solid sample the result is expressed on a dry basis.

LOR Limit of Reporting.

SPIKE Addition of the analyte to the sample and reported as percentage recovery.

RPD Relative Percent Difference between two Duplicate pieces of analysis.

LCS Laboratory Control Sample - reported as percent recovery

CRM Certified Reference Material - reported as percent recovery

Method Blank In the case of solid samples these are performed on laboratory certified clean sands.

In the case of water samples these are performed on de-ionised water.

Surr - Surrogate The addition of a like compound to the analyte target and reported as percentage recovery.

Duplicate A second piece of analysis from the same sample and reported in the same units as the result to show comparison.

Batch Duplicate A second piece of analysis from a sample outside of the clients batch of samples but run within the laboratory batch of analysis.

Batch SPIKE Spike recovery reported on a sample from outside of the clients batch of samples but run within the laboratory batch of analysis.

USEPA United States Environmental Protection Agency

APHA American Public Health Association

ASLP Australian Standard Leaching Procedure (AS4439.3)

TCLP Toxicity Characteristic Leaching Procedure

COC Chain of Custody

SRA Sample Receipt Advice

CP Client Parent - QC was performed on samples pertaining to this report

NCP Non-Client Parent - QC performed on samples not pertaining to this report, QC is representative of the sequence or batch that client samples were analysed within

TEQ Toxic Equivalency Quotient

RPD Duplicates: Global RPD Duplicates Acceptance Criteria is 30% however the following acceptance guidelines are equally applicable:

Results <10 times the LOR : No Limit

Results between 10-20 times the LOR : RPD must lie between 0-50%

Results >20 times the LOR : RPD must lie between 0-30%

Surrogate Recoveries : Recoveries must lie between 50-150% - Phenols 20-130%.

1. Where a result is reported as a less than (<), higher than the nominated LOR, this is due to either matrix interference, extract dilution required due to interferences or contaminant levels within

the sample, high moisture content or insufficient sample provided.

2. Duplicate data shown within this report that states the word "BATCH" is a Batch Duplicate from outside of your sample batch, but within the laboratory sample batch at a 1:10 ratio. The Parent

and Duplicate data shown is not data from your samples.

3. Organochlorine Pesticide analysis - where reporting LCS data, Toxophene & Chlordane are not added to the LCS.

4. Organochlorine Pesticide analysis - where reporting Spike data, Toxophene is not added to the Spike.

5. Total Recoverable Hydrocarbons - where reporting Spike & LCS data, a single spike of commercial Hydrocarbon products in the range of C12-C30 is added and it's Total Recovery is reported

in the C10-C14 cell of the Report.

6. pH and Free Chlorine analysed in the laboratory - Analysis on this test must begin within 30 minutes of sampling.Therefore laboratory analysis is unlikely to be completed within holding time.

Analysis will begin as soon as possible after sample receipt.

7. Recovery Data (Spikes & Surrogates) - where chromatographic interference does not allow the determination of Recovery the term "INT" appears against that analyte.

8. Polychlorinated Biphenyls are spiked only using Arochlor 1260 in Matrix Spikes and LCS's.

9. For Matrix Spikes and LCS results a dash " -" in the report means that the specific analyte was not added to the QC sample.

10. Duplicate RPD's are calculated from raw analytical data thus it is possible to have two sets of data.




Page 52 of 72


Quality Control Results

Test Units Result 1 AcceptanceLimits

PassLimits

QualifyingCode

Method Blank


TRH C6-C9 mg/kg < 20 20 Pass




Method Blank

BTEX

Benzene mg/kg < 0.1 0.1 Pass

Toluene mg/kg < 0.1 0.1 Pass

Ethylbenzene mg/kg < 0.1 0.1 Pass

m&p-Xylenes mg/kg < 0.2 0.2 Pass

o-Xylene mg/kg < 0.1 0.1 Pass

Xylenes - Total mg/kg < 0.3 0.3 Pass

Method Blank


Naphthalene mg/kg < 0.5 0.5 Pass



TRH C6-C10 less BTEX (F1) mg/kg < 20 20 Pass

TRH C6-C10 less BTEX (F1) mg/kg < 20 20 Pass

TRH >C10-C16 mg/kg < 50 50 Pass

TRH >C16-C34 mg/kg < 100 100 Pass

TRH >C34-C40 mg/kg < 100 100 Pass

Method Blank

Volatile Organics


Method Blank


1.1-Dichloroethane mg/kg < 0.5 0.5 Pass

1.1-Dichloroethene mg/kg < 0.5 0.5 Pass

1.1.1-Trichloroethane mg/kg < 0.5 0.5 Pass

1.1.1.2-Tetrachloroethane mg/kg < 0.5 0.5 Pass



1.2-Dibromoethane mg/kg < 0.5 0.5 Pass

1.2-Dichlorobenzene mg/kg < 0.5 0.5 Pass


1.2-Dichloropropane mg/kg < 0.5 0.5 Pass

1.2.3-Trichloropropane mg/kg < 0.5 0.5 Pass




Bromodichloromethane mg/kg < 0.5 0.5 Pass

Bromoform mg/kg < 0.5 0.5 Pass

Bromomethane mg/kg < 0.5 0.5 Pass

Carbon Tetrachloride mg/kg < 0.5 0.5 Pass

Chlorobenzene mg/kg < 0.5 0.5 Pass

Chloroform mg/kg < 0.5 0.5 Pass

Chloromethane mg/kg < 0.5 0.5 Pass

cis-1.2-Dichloroethene mg/kg < 0.5 0.5 Pass

cis-1.3-Dichloropropene mg/kg < 0.5 0.5 Pass




Page 53 of 72



PassLimits

QualifyingCode

Dibromochloromethane mg/kg < 0.5 0.5 Pass

Dibromomethane mg/kg < 0.5 0.5 Pass

Iodomethane mg/kg < 0.5 0.5 Pass

Methylene Chloride mg/kg < 0.5 0.5 Pass

Tetrachloroethene mg/kg < 0.5 0.5 Pass

trans-1.2-Dichloroethene mg/kg < 0.5 0.5 Pass

trans-1.3-Dichloropropene mg/kg < 0.5 0.5 Pass

Trichloroethene mg/kg < 0.5 0.5 Pass

Trichlorofluoromethane mg/kg < 0.5 0.5 Pass

Vinyl chloride mg/kg < 0.5 0.5 Pass

Method Blank


Acenaphthene mg/kg < 0.5 0.5 Pass

Acenaphthylene mg/kg < 0.5 0.5 Pass

Anthracene mg/kg < 0.5 0.5 Pass

Benz(a)anthracene mg/kg < 0.5 0.5 Pass

Benzo(a)pyrene mg/kg < 0.5 0.5 Pass

Benzo(b&j)fluoranthene mg/kg < 0.5 0.5 Pass

Benzo(g.h.i)perylene mg/kg < 0.5 0.5 Pass

Benzo(k)fluoranthene mg/kg < 0.5 0.5 Pass

Chrysene mg/kg < 0.5 0.5 Pass

Dibenz(a.h)anthracene mg/kg < 0.5 0.5 Pass

Fluoranthene mg/kg < 0.5 0.5 Pass

Fluorene mg/kg < 0.5 0.5 Pass

Indeno(1.2.3-cd)pyrene mg/kg < 0.5 0.5 Pass


Phenanthrene mg/kg < 0.5 0.5 Pass

Pyrene mg/kg < 0.5 0.5 Pass

Method Blank


Chlordanes - Total mg/kg < 0.1 0.1 Pass

4.4'-DDD mg/kg < 0.05 0.05 Pass

4.4'-DDE mg/kg < 0.05 0.05 Pass

4.4'-DDT mg/kg < 0.05 0.05 Pass

a-BHC mg/kg < 0.05 0.05 Pass

Aldrin mg/kg < 0.05 0.05 Pass

b-BHC mg/kg < 0.05 0.05 Pass

d-BHC mg/kg < 0.05 0.05 Pass

Dieldrin mg/kg < 0.05 0.05 Pass

Endosulfan I mg/kg < 0.05 0.05 Pass

Endosulfan II mg/kg < 0.05 0.05 Pass

Endosulfan sulphate mg/kg < 0.05 0.05 Pass

Endrin mg/kg < 0.05 0.05 Pass

Endrin aldehyde mg/kg < 0.05 0.05 Pass

Endrin ketone mg/kg < 0.05 0.05 Pass

g-BHC (Lindane) mg/kg < 0.05 0.05 Pass

Heptachlor mg/kg < 0.05 0.05 Pass

Heptachlor epoxide mg/kg < 0.05 0.05 Pass

Hexachlorobenzene mg/kg < 0.05 0.05 Pass

Methoxychlor mg/kg < 0.2 0.2 Pass

Toxaphene mg/kg < 1 1 Pass

Method Blank


Aroclor-1016 mg/kg < 0.5 0.5 Pass




Page 54 of 72



PassLimits

QualifyingCode







Total PCB* mg/kg < 0.1 0.1 Pass

Method Blank

Acid Herbicides

2.4-D mg/kg < 0.5 0.5 Pass

2.4-DB mg/kg < 0.5 0.5 Pass

2.4.5-T mg/kg < 0.5 0.5 Pass

2.4.5-TP mg/kg < 0.5 0.5 Pass

Actril (loxynil) mg/kg < 0.5 0.5 Pass

Dicamba mg/kg < 0.5 0.5 Pass

Dichlorprop mg/kg < 0.5 0.5 Pass

Dinitro-o-cresol mg/kg < 0.5 0.5 Pass

Dinoseb mg/kg < 0.5 0.5 Pass

MCPA mg/kg < 0.5 0.5 Pass

MCPB mg/kg < 0.5 0.5 Pass

Mecoprop mg/kg < 0.5 0.5 Pass

Method Blank


Chlorpyrifos mg/kg < 0.5 0.5 Pass

Coumaphos mg/kg < 0.5 0.5 Pass

Demeton (total) mg/kg < 1 1 Pass

Diazinon mg/kg < 0.5 0.5 Pass

Dichlorvos mg/kg < 0.5 0.5 Pass

Dimethoate mg/kg < 0.5 0.5 Pass

Disulfoton mg/kg < 0.5 0.5 Pass

Ethoprop mg/kg < 0.5 0.5 Pass

Fenitrothion mg/kg < 0.5 0.5 Pass

Fensulfothion mg/kg < 0.5 0.5 Pass

Fenthion mg/kg < 0.5 0.5 Pass

Methyl azinphos mg/kg < 0.5 0.5 Pass

Malathion mg/kg < 0.5 0.5 Pass

Methyl parathion mg/kg < 0.5 0.5 Pass

Mevinphos mg/kg < 0.5 0.5 Pass

Monocrotophos mg/kg < 10 10 Pass

Parathion mg/kg < 0.5 0.5 Pass

Phorate mg/kg < 0.5 0.5 Pass

Profenofos mg/kg < 0.5 0.5 Pass

Prothiofos mg/kg < 0.5 0.5 Pass

Ronnel mg/kg < 0.5 0.5 Pass

Stirophos mg/kg < 0.5 0.5 Pass

Method Blank

Conductivity (1:5 aqueous extract at 25°C) uS/cm < 5 5 Pass

Method Blank

Heavy Metals

Arsenic mg/kg < 2 2 Pass

Cadmium mg/kg < 0.4 0.4 Pass

Chromium mg/kg < 5 5 Pass

Copper mg/kg < 5 5 Pass

Lead mg/kg < 5 5 Pass




Page 55 of 72



PassLimits

QualifyingCode

Mercury mg/kg < 0.05 0.05 Pass

Nickel mg/kg < 5 5 Pass

Zinc mg/kg < 5 5 Pass

LCS - % Recovery


TRH C6-C9 % 90 70-130 Pass

TRH C10-C14 % 82 70-130 Pass

LCS - % Recovery

BTEX

Benzene % 95 70-130 Pass

Toluene % 95 70-130 Pass

Ethylbenzene % 94 70-130 Pass

m&p-Xylenes % 96 70-130 Pass

o-Xylene % 95 70-130 Pass

Xylenes - Total % 96 70-130 Pass

LCS - % Recovery


Naphthalene % 112 70-130 Pass

TRH C6-C10 % 96 70-130 Pass

TRH C6-C10 % 113 70-130 Pass

TRH >C10-C16 % 78 70-130 Pass

LCS - % Recovery

Volatile Organics


LCS - % Recovery


1.1-Dichloroethane % 113 75-125 Pass

1.1-Dichloroethene % 111 70-130 Pass

1.1.1-Trichloroethane % 112 70-130 Pass

1.1.1.2-Tetrachloroethane % 104 70-130 Pass



1.2-Dibromoethane % 119 70-130 Pass

1.2-Dichlorobenzene % 118 70-130 Pass


1.2-Dichloropropane % 123 70-130 Pass

1.2.3-Trichloropropane % 122 70-130 Pass




Bromodichloromethane % 103 70-130 Pass

Bromoform % 101 70-130 Pass

Bromomethane % 123 70-130 Pass

Carbon Tetrachloride % 115 70-130 Pass

Chlorobenzene % 120 70-130 Pass

Chloroform % 122 70-130 Pass

Chloromethane % 125 70-130 Pass

cis-1.2-Dichloroethene % 123 70-130 Pass

cis-1.3-Dichloropropene % 102 70-130 Pass

Dibromochloromethane % 107 70-130 Pass

Dibromomethane % 119 70-130 Pass

Iodomethane % 80 70-130 Pass

Methylene Chloride % 119 70-130 Pass

Tetrachloroethene % 114 70-130 Pass




Page 56 of 72



PassLimits

QualifyingCode

trans-1.2-Dichloroethene % 115 70-130 Pass

trans-1.3-Dichloropropene % 102 70-130 Pass

Trichloroethene % 117 70-130 Pass

Trichlorofluoromethane % 70 70-130 Pass

Vinyl chloride % 124 70-130 Pass

LCS - % Recovery


Acenaphthene % 95 70-130 Pass

Acenaphthylene % 91 70-130 Pass

Anthracene % 98 70-130 Pass

Benz(a)anthracene % 101 70-130 Pass

Benzo(a)pyrene % 110 70-130 Pass

Benzo(b&j)fluoranthene % 93 70-130 Pass

Benzo(g.h.i)perylene % 85 70-130 Pass

Benzo(k)fluoranthene % 89 70-130 Pass

Chrysene % 107 70-130 Pass

Dibenz(a.h)anthracene % 86 70-130 Pass

Fluoranthene % 97 70-130 Pass

Fluorene % 97 70-130 Pass

Indeno(1.2.3-cd)pyrene % 87 70-130 Pass


Phenanthrene % 91 70-130 Pass

Pyrene % 100 70-130 Pass

LCS - % Recovery


Chlordanes - Total % 101 70-130 Pass

4.4'-DDD % 101 70-130 Pass

4.4'-DDE % 102 70-130 Pass

4.4'-DDT % 91 70-130 Pass

a-BHC % 105 70-130 Pass

Aldrin % 107 70-130 Pass

b-BHC % 106 70-130 Pass

d-BHC % 101 70-130 Pass

Dieldrin % 103 70-130 Pass

Endosulfan I % 103 70-130 Pass

Endosulfan II % 100 70-130 Pass

Endosulfan sulphate % 95 70-130 Pass

Endrin % 99 70-130 Pass

Endrin aldehyde % 94 70-130 Pass

Endrin ketone % 98 70-130 Pass

g-BHC (Lindane) % 104 70-130 Pass

Heptachlor % 103 70-130 Pass

Heptachlor epoxide % 102 70-130 Pass

Methoxychlor % 81 70-130 Pass

LCS - % Recovery


Aroclor-1260 % 87 70-130 Pass

LCS - % Recovery

Acid Herbicides

2.4-D % 124 70-130 Pass

2.4-DB % 79 70-130 Pass

2.4.5-T % 100 70-130 Pass

2.4.5-TP % 97 70-130 Pass

Actril (loxynil) % 105 70-130 Pass




Page 57 of 72



PassLimits

QualifyingCode

Dicamba % 95 70-130 Pass

Dichlorprop % 72 70-130 Pass

Dinitro-o-cresol % 92 70-130 Pass

Dinoseb % 99 70-130 Pass

MCPA % 104 70-130 Pass

MCPB % 77 70-130 Pass

Mecoprop % 91 70-130 Pass

LCS - % Recovery


Chlorpyrifos % 90 70-130 Pass

Dimethoate % 117 70-130 Pass

Disulfoton % 109 70-130 Pass

Methyl azinphos % 83 70-130 Pass

Methyl parathion % 90 70-130 Pass

Parathion % 91 70-130 Pass

Phorate % 102 70-130 Pass

LCS - % Recovery

Heavy Metals

Arsenic % 109 70-130 Pass

Cadmium % 105 70-130 Pass

Chromium % 108 70-130 Pass

Copper % 108 70-130 Pass

Lead % 110 70-130 Pass

Mercury % 112 70-130 Pass

Nickel % 106 70-130 Pass

Zinc % 109 70-130 Pass

Test Lab Sample ID QASource Units Result 1 Acceptance

LimitsPass

LimitsQualifying

Code

Spike - % Recovery

Acid Herbicides Result 1

2.4-D S15-Jn19778 NCP % 83 70-130 Pass

Actril (loxynil) S15-Jn19778 NCP % 93 70-130 Pass

Dichlorprop S15-Jn19778 NCP % 84 70-130 Pass

MCPA S15-Jn19778 NCP % 85 70-130 Pass

MCPB M15-Jn18690 NCP % 71 70-130 Pass

Spike - % Recovery

Total Recoverable Hydrocarbons - 1999 NEPM Fractions Result 1

TRH C10-C14 S15-Jn20260 CP % 112 70-130 Pass

Spike - % Recovery


TRH >C10-C16 S15-Jn20260 CP % 125 70-130 Pass

Spike - % Recovery

Heavy Metals Result 1

Arsenic S15-Jn20261 CP % 101 70-130 Pass

Cadmium S15-Jn20261 CP % 86 70-130 Pass

Chromium S15-Jn20261 CP % 96 70-130 Pass

Lead S15-Jn20261 CP % 113 70-130 Pass

Mercury S15-Jn20261 CP % 97 70-130 Pass

Nickel S15-Jn20261 CP % 90 70-130 Pass

Spike - % Recovery

Organochlorine Pesticides Result 1

Chlordanes - Total S15-Jn20264 CP % 119 70-130 Pass

4.4'-DDD S15-Jn20264 CP % 129 70-130 Pass

4.4'-DDE S15-Jn20264 CP % 118 70-130 Pass

4.4'-DDT S15-Jn20264 CP % 73 70-130 Pass




Page 58 of 72



LimitsPass

LimitsQualifying

Code

a-BHC S15-Jn20264 CP % 126 70-130 Pass

Aldrin S15-Jn20264 CP % 130 70-130 Pass

b-BHC S15-Jn20264 CP % 121 70-130 Pass

d-BHC S15-Jn20264 CP % 123 70-130 Pass

Dieldrin S15-Jn20264 CP % 120 70-130 Pass

Endosulfan I S15-Jn20264 CP % 116 70-130 Pass

Endosulfan II S15-Jn20264 CP % 114 70-130 Pass

Endosulfan sulphate S15-Jn20264 CP % 110 70-130 Pass

Endrin S15-Jn20264 CP % 115 70-130 Pass

Endrin aldehyde S15-Jn20264 CP % 123 70-130 Pass

Endrin ketone S15-Jn20264 CP % 110 70-130 Pass

g-BHC (Lindane) S15-Jn20264 CP % 122 70-130 Pass

Heptachlor S15-Jn20264 CP % 122 70-130 Pass

Heptachlor epoxide S15-Jn20264 CP % 121 70-130 Pass

Methoxychlor S15-Jn20264 CP % 123 70-130 Pass

Spike - % Recovery

BTEX Result 1

Benzene S15-Jn20273 CP % 102 70-130 Pass

Toluene S15-Jn20273 CP % 101 70-130 Pass

Ethylbenzene S15-Jn20273 CP % 103 70-130 Pass

m&p-Xylenes S15-Jn20273 CP % 107 70-130 Pass

o-Xylene S15-Jn20273 CP % 105 70-130 Pass

Spike - % Recovery


Naphthalene S15-Jn20273 CP % 94 70-130 Pass

Spike - % Recovery

Halogenated Volatile Organics Result 1

1.1-Dichloroethane S15-Jn20273 CP % 99 75-125 Pass

1.1-Dichloroethene S15-Jn20273 CP % 88 70-130 Pass

1.1.1-Trichloroethane S15-Jn20273 CP % 95 70-130 Pass

1.1.1.2-Tetrachloroethane S15-Jn20273 CP % 85 70-130 Pass

1.1.2-Trichloroethane S15-Jn20273 CP % 100 70-130 Pass

1.1.2.2-Tetrachloroethane S15-Jn20273 CP % 105 70-130 Pass

1.2-Dibromoethane S15-Jn20273 CP % 95 70-130 Pass

1.2-Dichlorobenzene S15-Jn20273 CP % 97 70-130 Pass

1.2-Dichloroethane S15-Jn20273 CP % 105 70-130 Pass

1.2-Dichloropropane S15-Jn20273 CP % 103 70-130 Pass

1.2.3-Trichloropropane S15-Jn20273 CP % 103 70-130 Pass


1.3-Dichloropropane S15-Jn20273 CP % 104 70-130 Pass


Bromodichloromethane S15-Jn20273 CP % 80 70-130 Pass

Bromoform S15-Jn20273 CP % 78 70-130 Pass

Bromomethane S15-Jn20273 CP % 85 70-130 Pass

Carbon Tetrachloride S15-Jn20273 CP % 98 70-130 Pass

Chlorobenzene S15-Jn20273 CP % 103 70-130 Pass

Chloroform S15-Jn20273 CP % 109 70-130 Pass

Chloromethane S15-Jn20273 CP % 123 70-130 Pass

cis-1.2-Dichloroethene S15-Jn20273 CP % 110 70-130 Pass

cis-1.3-Dichloropropene S15-Jn20273 CP % 75 70-130 Pass

Dibromochloromethane S15-Jn20273 CP % 81 70-130 Pass

Dibromomethane S15-Jn20273 CP % 94 70-130 Pass

Iodomethane S15-Jn20273 CP % 72 70-130 Pass

Methylene Chloride S15-Jn20273 CP % 98 70-130 Pass




Page 59 of 72



LimitsPass

LimitsQualifying

Code

Tetrachloroethene S15-Jn20273 CP % 95 70-130 Pass

trans-1.2-Dichloroethene S15-Jn20273 CP % 98 70-130 Pass

trans-1.3-Dichloropropene S15-Jn20273 CP % 75 70-130 Pass

Trichloroethene S15-Jn20273 CP % 96 70-130 Pass

Trichlorofluoromethane S15-Jn20273 CP % 79 70-130 Pass

Vinyl chloride S15-Jn20273 CP % 110 70-130 Pass

Spike - % Recovery





Copper S15-Jn20274 CP % 95 70-130 Pass

Lead S15-Jn20274 CP % 97 70-130 Pass



Spike - % Recovery


TRH C6-C9 S15-Jn20276 CP % 82 70-130 Pass

Spike - % Recovery

BTEX Result 1






Xylenes - Total S15-Jn20276 CP % 86 70-130 Pass

Spike - % Recovery



TRH C6-C10 S15-Jn20276 CP % 87 70-130 Pass

Spike - % Recovery






Lead S15-Jn20287 CP % 79 70-130 Pass



Spike - % Recovery


TRH C6-C9 S15-Jn20290 CP % 84 70-130 Pass

TRH C10-C14 S15-Jn20290 CP % 83 70-130 Pass

Spike - % Recovery

BTEX Result 1







Spike - % Recovery






Page 60 of 72



LimitsPass

LimitsQualifying

Code

TRH C6-C10 S15-Jn20290 CP % 79 70-130 Pass

TRH >C10-C16 S15-Jn20290 CP % 79 70-130 Pass

Spike - % Recovery

Polycyclic Aromatic Hydrocarbons Result 1

Acenaphthene S15-Jn20295 CP % 95 70-130 Pass

Acenaphthylene S15-Jn20295 CP % 95 70-130 Pass

Anthracene S15-Jn20295 CP % 98 70-130 Pass

Benz(a)anthracene S15-Jn20295 CP % 107 70-130 Pass

Benzo(a)pyrene S15-Jn20295 CP % 101 70-130 Pass

Benzo(b&j)fluoranthene S15-Jn20295 CP % 120 70-130 Pass

Benzo(g.h.i)perylene S15-Jn20295 CP % 93 70-130 Pass

Benzo(k)fluoranthene S15-Jn20295 CP % 109 70-130 Pass

Chrysene S15-Jn20295 CP % 97 70-130 Pass

Dibenz(a.h)anthracene S15-Jn20295 CP % 88 70-130 Pass

Fluoranthene S15-Jn20295 CP % 111 70-130 Pass

Fluorene S15-Jn20295 CP % 96 70-130 Pass

Indeno(1.2.3-cd)pyrene S15-Jn20295 CP % 91 70-130 Pass


Phenanthrene S15-Jn20295 CP % 102 70-130 Pass

Pyrene S15-Jn20295 CP % 111 70-130 Pass

Spike - % Recovery

Organophosphorus Pesticides (OP) Result 1

Chlorpyrifos S15-Jn20298 CP % 95 70-130 Pass

Dimethoate S15-Jn20298 CP % 115 70-130 Pass

Disulfoton S15-Jn20298 CP % 87 70-130 Pass

Methyl azinphos S15-Jn20298 CP % 102 70-130 Pass

Methyl parathion S15-Jn20298 CP % 93 70-130 Pass

Parathion S15-Jn20298 CP % 106 70-130 Pass

Phorate S15-Jn20298 CP % 98 70-130 Pass

Spike - % Recovery






Lead S15-Jn20299 CP % 109 70-130 Pass



Zinc S15-Jn20299 CP % 117 70-130 Pass

Spike - % Recovery


TRH C6-C9 S15-Jn20303 CP % 82 70-130 Pass

Spike - % Recovery

BTEX Result 1







Spike - % Recovery



TRH C6-C10 S15-Jn20303 CP % 87 70-130 Pass




Page 61 of 72



LimitsPass

LimitsQualifying

Code

Spike - % Recovery


TRH C10-C14 S15-Jn20304 CP % 104 70-130 Pass

Spike - % Recovery


TRH >C10-C16 S15-Jn20304 CP % 106 70-130 Pass

Spike - % Recovery


Acenaphthene S15-Jn20307 CP % 93 70-130 Pass

Acenaphthylene S15-Jn20307 CP % 94 70-130 Pass

Anthracene S15-Jn20307 CP % 95 70-130 Pass

Benz(a)anthracene S15-Jn20307 CP % 112 70-130 Pass

Benzo(a)pyrene S15-Jn20307 CP % 86 70-130 Pass

Benzo(b&j)fluoranthene S15-Jn20307 CP % 95 70-130 Pass

Benzo(g.h.i)perylene S15-Jn20307 CP % 79 70-130 Pass

Benzo(k)fluoranthene S15-Jn20307 CP % 84 70-130 Pass

Chrysene S15-Jn20307 CP % 82 70-130 Pass

Dibenz(a.h)anthracene S15-Jn20307 CP % 76 70-130 Pass

Fluoranthene S15-Jn20307 CP % 110 70-130 Pass

Fluorene S15-Jn20307 CP % 94 70-130 Pass

Indeno(1.2.3-cd)pyrene S15-Jn20307 CP % 77 70-130 Pass


Phenanthrene S15-Jn20307 CP % 124 70-130 Pass

Pyrene S15-Jn20307 CP % 110 70-130 Pass

Spike - % Recovery



4.4'-DDD S15-Jn20307 CP % 98 70-130 Pass

4.4'-DDE S15-Jn20307 CP % 95 70-130 Pass

4.4'-DDT S15-Jn20307 CP % 83 70-130 Pass

a-BHC S15-Jn20307 CP % 99 70-130 Pass


b-BHC S15-Jn20307 CP % 89 70-130 Pass

d-BHC S15-Jn20307 CP % 94 70-130 Pass












Spike - % Recovery






Lead S15-Jn20311 CP % 75 70-130 Pass






Page 62 of 72



LimitsPass

LimitsQualifying

Code

Zinc S15-Jn20311 CP % 83 70-130 Pass

Spike - % Recovery



4.4'-DDD S15-Jn20314 CP % 128 70-130 Pass

4.4'-DDE S15-Jn20314 CP % 103 70-130 Pass

4.4'-DDT S15-Jn20314 CP % 116 70-130 Pass

a-BHC S15-Jn20314 CP % 106 70-130 Pass


b-BHC S15-Jn20314 CP % 97 70-130 Pass

d-BHC S15-Jn20314 CP % 102 70-130 Pass












Spike - % Recovery


TRH C6-C9 S15-Jn20315 CP % 90 70-130 Pass

TRH C10-C14 S15-Jn20315 CP % 90 70-130 Pass

Spike - % Recovery

BTEX Result 1







Spike - % Recovery



TRH C6-C10 S15-Jn20315 CP % 96 70-130 Pass

TRH >C10-C16 S15-Jn20315 CP % 91 70-130 Pass

Spike - % Recovery

Polychlorinated Biphenyls Result 1

Aroclor-1260 S15-Jn20320 CP % 74 70-130 Pass

Spike - % Recovery






Lead S15-Jn20321 CP % 75 70-130 Pass



Zinc S15-Jn20321 CP % 101 70-130 Pass

Spike - % Recovery





Page 63 of 72



LimitsPass

LimitsQualifying

Code

TRH C6-C9 S15-Jn20325 CP % 86 70-130 Pass

Spike - % Recovery

BTEX Result 1







Spike - % Recovery



TRH C6-C10 S15-Jn20325 CP % 90 70-130 Pass


LimitsPass

LimitsQualifying

Code

Duplicate

Acid Herbicides Result 1 Result 2 RPD

2.4-D S15-Jn19801 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

2.4-DB S15-Jn19801 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

2.4.5-T S15-Jn19801 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

2.4.5-TP S15-Jn19801 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Actril (loxynil) S15-Jn19801 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Dicamba S15-Jn19801 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Dichlorprop S15-Jn19801 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Dinitro-o-cresol S15-Jn19801 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Dinoseb S15-Jn19801 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

MCPA S15-Jn19801 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

MCPB S15-Jn19801 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Mecoprop S15-Jn19801 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Duplicate

Result 1 Result 2 RPD

Conductivity (1:5 aqueous extractat 25°C) S15-Jn20258 CP uS/cm 35 35 1.0 30% Pass

pH (1:5 Aqueous extract) S15-Jn20258 CP pH Units 6.4 6.4 pass 30% Pass

% Moisture S15-Jn20258 CP % 27 28 4.0 30% Pass

Duplicate

Total Recoverable Hydrocarbons - 1999 NEPM Fractions Result 1 Result 2 RPD

TRH C10-C14 S15-Jn20259 CP mg/kg < 20 < 20 <1 30% Pass



Duplicate


TRH >C10-C16 S15-Jn20259 CP mg/kg < 50 < 50 <1 30% Pass



Duplicate

Halogenated Volatile Organics Result 1 Result 2 RPD

1.1-Dichloroethane S15-Jn20260 CP mg/kg < 0.5 < 0.5 <1 30% Pass

1.1-Dichloroethene S15-Jn20260 CP mg/kg < 0.5 < 0.5 <1 30% Pass

1.1.1-Trichloroethane S15-Jn20260 CP mg/kg < 0.5 < 0.5 <1 30% Pass

1.1.1.2-Tetrachloroethane S15-Jn20260 CP mg/kg < 0.5 < 0.5 <1 30% Pass

1.1.2-Trichloroethane S15-Jn20260 CP mg/kg < 0.5 < 0.5 <1 30% Pass

1.1.2.2-Tetrachloroethane S15-Jn20260 CP mg/kg < 0.5 < 0.5 <1 30% Pass

1.2-Dibromoethane S15-Jn20260 CP mg/kg < 0.5 < 0.5 <1 30% Pass

1.2-Dichlorobenzene S15-Jn20260 CP mg/kg < 0.5 < 0.5 <1 30% Pass




Page 64 of 72


Duplicate


1.2-Dichloroethane S15-Jn20260 CP mg/kg < 0.5 < 0.5 <1 30% Pass

1.2-Dichloropropane S15-Jn20260 CP mg/kg < 0.5 < 0.5 <1 30% Pass

1.2.3-Trichloropropane S15-Jn20260 CP mg/kg < 0.5 < 0.5 <1 30% Pass


1.3-Dichloropropane S15-Jn20260 CP mg/kg < 0.5 < 0.5 <1 30% Pass


Bromodichloromethane S15-Jn20260 CP mg/kg < 0.5 < 0.5 <1 30% Pass

Bromoform S15-Jn20260 CP mg/kg < 0.5 < 0.5 <1 30% Pass

Bromomethane S15-Jn20260 CP mg/kg < 0.5 < 0.5 <1 30% Pass

Carbon Tetrachloride S15-Jn20260 CP mg/kg < 0.5 < 0.5 <1 30% Pass

Chlorobenzene S15-Jn20260 CP mg/kg < 0.5 < 0.5 <1 30% Pass

Chloroform S15-Jn20260 CP mg/kg < 0.5 < 0.5 <1 30% Pass

Chloromethane S15-Jn20260 CP mg/kg < 0.5 < 0.5 <1 30% Pass

cis-1.2-Dichloroethene S15-Jn20260 CP mg/kg < 0.5 < 0.5 <1 30% Pass

cis-1.3-Dichloropropene S15-Jn20260 CP mg/kg < 0.5 < 0.5 <1 30% Pass

Dibromochloromethane S15-Jn20260 CP mg/kg < 0.5 < 0.5 <1 30% Pass

Dibromomethane S15-Jn20260 CP mg/kg < 0.5 < 0.5 <1 30% Pass

Iodomethane S15-Jn20260 CP mg/kg < 0.5 < 0.5 <1 30% Pass

Methylene Chloride S15-Jn20260 CP mg/kg < 0.5 < 0.5 <1 30% Pass

Tetrachloroethene S15-Jn20260 CP mg/kg < 0.5 < 0.5 <1 30% Pass

trans-1.2-Dichloroethene S15-Jn20260 CP mg/kg < 0.5 < 0.5 <1 30% Pass

trans-1.3-Dichloropropene S15-Jn20260 CP mg/kg < 0.5 < 0.5 <1 30% Pass

Trichloroethene S15-Jn20260 CP mg/kg < 0.5 < 0.5 <1 30% Pass

Trichlorofluoromethane S15-Jn20260 CP mg/kg < 0.5 < 0.5 <1 30% Pass

Vinyl chloride S15-Jn20260 CP mg/kg < 0.5 < 0.5 <1 30% Pass

Duplicate

Heavy Metals Result 1 Result 2 RPD

Arsenic S15-Jn20260 CP mg/kg 9.4 11 20 30% Pass

Cadmium S15-Jn20260 CP mg/kg < 0.4 < 0.4 <1 30% Pass

Chromium S15-Jn20260 CP mg/kg 14 16 17 30% Pass

Copper S15-Jn20260 CP mg/kg 37 35 5.0 30% Pass

Lead S15-Jn20260 CP mg/kg 320 280 15 30% Pass

Mercury S15-Jn20260 CP mg/kg 0.25 0.28 10 30% Pass

Nickel S15-Jn20260 CP mg/kg 5.5 5.7 3.0 30% Pass

Zinc S15-Jn20260 CP mg/kg 150 140 10 30% Pass

Duplicate

Organochlorine Pesticides Result 1 Result 2 RPD

Chlordanes - Total S15-Jn20263 CP mg/kg < 0.1 < 0.1 <1 30% Pass

4.4'-DDD S15-Jn20263 CP mg/kg < 0.05 < 0.05 <1 30% Pass

4.4'-DDE S15-Jn20263 CP mg/kg < 0.05 < 0.05 <1 30% Pass

4.4'-DDT S15-Jn20263 CP mg/kg < 0.05 < 0.05 <1 30% Pass

a-BHC S15-Jn20263 CP mg/kg < 0.05 < 0.05 <1 30% Pass

Aldrin S15-Jn20263 CP mg/kg < 0.05 < 0.05 <1 30% Pass

b-BHC S15-Jn20263 CP mg/kg < 0.05 < 0.05 <1 30% Pass

d-BHC S15-Jn20263 CP mg/kg < 0.05 < 0.05 <1 30% Pass

Dieldrin S15-Jn20263 CP mg/kg < 0.05 < 0.05 <1 30% Pass

Endosulfan I S15-Jn20263 CP mg/kg < 0.05 < 0.05 <1 30% Pass

Endosulfan II S15-Jn20263 CP mg/kg < 0.05 < 0.05 <1 30% Pass

Endosulfan sulphate S15-Jn20263 CP mg/kg < 0.05 < 0.05 <1 30% Pass

Endrin S15-Jn20263 CP mg/kg < 0.05 < 0.05 <1 30% Pass

Endrin aldehyde S15-Jn20263 CP mg/kg < 0.05 < 0.05 <1 30% Pass

Endrin ketone S15-Jn20263 CP mg/kg < 0.05 < 0.05 <1 30% Pass

g-BHC (Lindane) S15-Jn20263 CP mg/kg < 0.05 < 0.05 <1 30% Pass

Heptachlor S15-Jn20263 CP mg/kg < 0.05 < 0.05 <1 30% Pass




Page 65 of 72


Duplicate


Heptachlor epoxide S15-Jn20263 CP mg/kg < 0.05 < 0.05 <1 30% Pass

Hexachlorobenzene S15-Jn20263 CP mg/kg < 0.05 < 0.05 <1 30% Pass

Methoxychlor S15-Jn20263 CP mg/kg < 0.2 < 0.2 <1 30% Pass

Toxaphene S15-Jn20263 CP mg/kg < 1 < 1 <1 30% Pass

Duplicate



Duplicate


Arsenic S15-Jn20273 CP mg/kg 15 13 9.0 30% Pass


Chromium S15-Jn20273 CP mg/kg 20 19 4.0 30% Pass



Mercury S15-Jn20273 CP mg/kg 0.11 0.08 28 30% Pass

Nickel S15-Jn20273 CP mg/kg 11 21 65 30% Fail Q15


Duplicate



Duplicate

BTEX Result 1 Result 2 RPD

Benzene S15-Jn20274 CP mg/kg < 0.1 < 0.1 <1 30% Pass

Toluene S15-Jn20274 CP mg/kg < 0.1 < 0.1 <1 30% Pass

Ethylbenzene S15-Jn20274 CP mg/kg < 0.1 < 0.1 <1 30% Pass

m&p-Xylenes S15-Jn20274 CP mg/kg < 0.2 < 0.2 <1 30% Pass

o-Xylene S15-Jn20274 CP mg/kg < 0.1 < 0.1 <1 30% Pass

Xylenes - Total S15-Jn20274 CP mg/kg < 0.3 < 0.3 <1 30% Pass

Duplicate


Naphthalene S15-Jn20274 CP mg/kg < 0.5 < 0.5 <1 30% Pass


TRH C6-C10 less BTEX (F1) S15-Jn20274 CP mg/kg < 20 < 20 <1 30% Pass

Duplicate




Duplicate

Organophosphorus Pesticides (OP) Result 1 Result 2 RPD

Chlorpyrifos S15-Jn20277 CP mg/kg < 0.5 < 0.5 <1 30% Pass

Coumaphos S15-Jn20277 CP mg/kg < 0.5 < 0.5 <1 30% Pass

Demeton (total) S15-Jn20277 CP mg/kg < 1 < 1 <1 30% Pass

Diazinon S15-Jn20277 CP mg/kg < 0.5 < 0.5 <1 30% Pass

Dichlorvos S15-Jn20277 CP mg/kg < 0.5 < 0.5 <1 30% Pass

Dimethoate S15-Jn20277 CP mg/kg < 0.5 < 0.5 <1 30% Pass

Disulfoton S15-Jn20277 CP mg/kg < 0.5 < 0.5 <1 30% Pass

Ethoprop S15-Jn20277 CP mg/kg < 0.5 < 0.5 <1 30% Pass

Fenitrothion S15-Jn20277 CP mg/kg < 0.5 < 0.5 <1 30% Pass

Fensulfothion S15-Jn20277 CP mg/kg < 0.5 < 0.5 <1 30% Pass

Fenthion S15-Jn20277 CP mg/kg < 0.5 < 0.5 <1 30% Pass

Methyl azinphos S15-Jn20277 CP mg/kg < 0.5 < 0.5 <1 30% Pass

Malathion S15-Jn20277 CP mg/kg < 0.5 < 0.5 <1 30% Pass

Methyl parathion S15-Jn20277 CP mg/kg < 0.5 < 0.5 <1 30% Pass




Page 66 of 72


Duplicate


Mevinphos S15-Jn20277 CP mg/kg < 0.5 < 0.5 <1 30% Pass

Monocrotophos S15-Jn20277 CP mg/kg < 10 < 10 <1 30% Pass

Parathion S15-Jn20277 CP mg/kg < 0.5 < 0.5 <1 30% Pass

Phorate S15-Jn20277 CP mg/kg < 0.5 < 0.5 <1 30% Pass

Profenofos S15-Jn20277 CP mg/kg < 0.5 < 0.5 <1 30% Pass

Prothiofos S15-Jn20277 CP mg/kg < 0.5 < 0.5 <1 30% Pass

Ronnel S15-Jn20277 CP mg/kg < 0.5 < 0.5 <1 30% Pass

Stirophos S15-Jn20277 CP mg/kg < 0.5 < 0.5 <1 30% Pass

Duplicate























Duplicate



Duplicate


Arsenic S15-Jn20286 CP mg/kg 3.5 4.4 23 30% Pass


Chromium S15-Jn20286 CP mg/kg 7.0 7.5 7.0 30% Pass

Copper S15-Jn20286 CP mg/kg 12 14 14 30% Pass


Mercury S15-Jn20286 CP mg/kg 0.05 < 0.05 6.0 30% Pass

Nickel S15-Jn20286 CP mg/kg < 5 < 5 <1 30% Pass


Duplicate



Duplicate











Page 67 of 72


Duplicate





Duplicate




Duplicate


Chlorpyrifos S15-Jn20295 CP mg/kg < 0.5 < 0.5 <1 30% Pass

Coumaphos S15-Jn20295 CP mg/kg < 0.5 < 0.5 <1 30% Pass

Demeton (total) S15-Jn20295 CP mg/kg < 1 < 1 <1 30% Pass

Diazinon S15-Jn20295 CP mg/kg < 0.5 < 0.5 <1 30% Pass

Dichlorvos S15-Jn20295 CP mg/kg < 0.5 < 0.5 <1 30% Pass

Dimethoate S15-Jn20295 CP mg/kg < 0.5 < 0.5 <1 30% Pass

Disulfoton S15-Jn20295 CP mg/kg < 0.5 < 0.5 <1 30% Pass

Ethoprop S15-Jn20295 CP mg/kg < 0.5 < 0.5 <1 30% Pass

Fenitrothion S15-Jn20295 CP mg/kg < 0.5 < 0.5 <1 30% Pass

Fensulfothion S15-Jn20295 CP mg/kg < 0.5 < 0.5 <1 30% Pass

Fenthion S15-Jn20295 CP mg/kg < 0.5 < 0.5 <1 30% Pass

Methyl azinphos S15-Jn20295 CP mg/kg < 0.5 < 0.5 <1 30% Pass

Malathion S15-Jn20295 CP mg/kg < 0.5 < 0.5 <1 30% Pass

Methyl parathion S15-Jn20295 CP mg/kg < 0.5 < 0.5 <1 30% Pass

Mevinphos S15-Jn20295 CP mg/kg < 0.5 < 0.5 <1 30% Pass

Monocrotophos S15-Jn20295 CP mg/kg < 10 < 10 <1 30% Pass

Parathion S15-Jn20295 CP mg/kg < 0.5 < 0.5 <1 30% Pass

Phorate S15-Jn20295 CP mg/kg < 0.5 < 0.5 <1 30% Pass

Profenofos S15-Jn20295 CP mg/kg < 0.5 < 0.5 <1 30% Pass

Prothiofos S15-Jn20295 CP mg/kg < 0.5 < 0.5 <1 30% Pass

Ronnel S15-Jn20295 CP mg/kg < 0.5 < 0.5 <1 30% Pass

Stirophos S15-Jn20295 CP mg/kg < 0.5 < 0.5 <1 30% Pass

Duplicate


% Moisture S15-Jn20295 CP % 20 20 <1 30% Pass

Duplicate


Arsenic S15-Jn20298 CP mg/kg 4.2 3.6 16 30% Pass


Chromium S15-Jn20298 CP mg/kg 8.6 7.4 15 30% Pass



Mercury S15-Jn20298 CP mg/kg 0.06 0.06 7.0 30% Pass



Duplicate









Page 68 of 72


Duplicate








Duplicate








Duplicate























Duplicate





Duplicate

Polychlorinated Biphenyls Result 1 Result 2 RPD

Aroclor-1016 S15-Jn20308 CP mg/kg < 0.5 < 0.5 <1 30% Pass










Page 69 of 72


Duplicate


Arsenic S15-Jn20309 CP mg/kg 15 11 28 30% Pass




Lead S15-Jn20309 CP mg/kg 20 19 7.0 30% Pass

Mercury S15-Jn20309 CP mg/kg < 0.05 < 0.05 <1 30% Pass



Duplicate






Duplicate








Duplicate








Duplicate

Polycyclic Aromatic Hydrocarbons Result 1 Result 2 RPD

Acenaphthene S15-Jn20317 CP mg/kg < 0.5 < 0.5 <1 30% Pass

Acenaphthylene S15-Jn20317 CP mg/kg < 0.5 < 0.5 <1 30% Pass

Anthracene S15-Jn20317 CP mg/kg < 0.5 < 0.5 <1 30% Pass

Benz(a)anthracene S15-Jn20317 CP mg/kg < 0.5 < 0.5 <1 30% Pass

Benzo(a)pyrene S15-Jn20317 CP mg/kg < 0.5 < 0.5 <1 30% Pass

Benzo(b&j)fluoranthene S15-Jn20317 CP mg/kg < 0.5 < 0.5 <1 30% Pass

Benzo(g.h.i)perylene S15-Jn20317 CP mg/kg < 0.5 < 0.5 <1 30% Pass

Benzo(k)fluoranthene S15-Jn20317 CP mg/kg < 0.5 < 0.5 <1 30% Pass

Chrysene S15-Jn20317 CP mg/kg < 0.5 < 0.5 <1 30% Pass

Dibenz(a.h)anthracene S15-Jn20317 CP mg/kg < 0.5 < 0.5 <1 30% Pass

Fluoranthene S15-Jn20317 CP mg/kg < 0.5 < 0.5 <1 30% Pass

Fluorene S15-Jn20317 CP mg/kg < 0.5 < 0.5 <1 30% Pass

Indeno(1.2.3-cd)pyrene S15-Jn20317 CP mg/kg < 0.5 < 0.5 <1 30% Pass


Phenanthrene S15-Jn20317 CP mg/kg < 0.5 < 0.5 <1 30% Pass

Pyrene S15-Jn20317 CP mg/kg < 0.5 < 0.5 <1 30% Pass

Duplicate








Page 70 of 72


Duplicate


Arsenic S15-Jn20320 CP mg/kg 14 11 22 30% Pass



Copper S15-Jn20320 CP mg/kg 28 24 14 30% Pass


Mercury S15-Jn20320 CP mg/kg 0.06 0.06 <1 30% Pass

Nickel S15-Jn20320 CP mg/kg 8.9 6.4 33 30% Fail Q15


Duplicate



Duplicate








Duplicate








Page 71 of 72


Comments

Sample IntegrityCustody Seals Intact (if used) N/A

Attempt to Chill was evident Yes

Sample correctly preserved Yes

Appropriate sample containers have been used Yes

Sample containers for volatile analysis received with minimal headspace Yes

Samples received within HoldingTime Yes

Some samples have been subcontracted No

Qualifier Codes/Comments

Code Description

N01F2 is determined by arithmetically subtracting the "naphthalene" value from the ">C10-C16" value. The naphthalene value used in this calculation is obtained from volatiles(Purge & Trap analysis).

N02

Where we have reported both volatile (P&T GCMS) and semivolatile (GCMS) naphthalene data, results may not be identical. Provided correct sample handling protocols havebeen followed, any observed differences in results are likely to be due to procedural differences within each methodology. Results determined by both techniques have passedall QAQC acceptance criteria, and are entirely technically valid.

N04F1 is determined by arithmetically subtracting the "Total BTEX" value from the "C6-C10" value. The "Total BTEX" value is obtained by summing the concentrations of BTEXanalytes. The "C6-C10" value is obtained by quantitating against a standard of mixed aromatic/aliphatic analytes.

N07Please note:- These two PAH isomers closely co-elute using the most contemporary analytical methods and both the reported concentration (and the TEQ) apply specifically tothe total of the two co-eluting PAHs

Q15 The RPD reported passes Eurofins | mgt's Acceptance Criteria as stipulated in SOP 05. Refer to Glossary Page of this report for further details

Authorised By

Charl Du Preez Analytical Services Manager

Bob Symons Senior Analyst-Inorganic (NSW)

Carroll Lee Senior Analyst-Organic (VIC)

Ivan Taylor Senior Analyst-Metal (NSW)

Nibha Vaidya Senior Analyst-Asbestos (NSW)

Ryan Hamilton Senior Analyst-Organic (NSW)

Ryan Hamilton Senior Analyst-Volatile (NSW)

Glenn Jackson

National Laboratory Manager

- Indicates Not Requested

* Indicates NATA accreditation does not cover the performance of this service

Uncertainty data is available on requestEurofins | mgt shall not be liable for loss, cost, damages or expenses incurred by the client, or any other person or company, resulting from the use of any information or interpretation given in this report. In no case shall Eurofins | mgt be liable for consequential damages including, but notlimited to, lost profits, damages for failure to meet deadlines and lost production arising from this report. This document shall not be reproduced except in full and relates only to the items tested. Unless indicated otherwise, the tests were performed on the samples as received.




Page 72 of 72



Coffey Environments Pty Ltd Wollongong118 Auburn StreetWollongongNSW 2500

Attention: Alexander WilliamsReport 462743-AIDProject Name ENAUWOLL04223AAReceived Date Jun 24, 2015Date Reported Jul 01, 2015

Methodology:Asbestos ID Conducted in accordance with the Australian Standard AS 4964 – 2004: Method for the

Qualitative Identification of Asbestos in Bulk Samples and in-house Method LTM-ASB-8020 bypolarised light microscopy (PLM) and dispersion staining (DS) techniques. Bulk samplesinclude building materials, soils and ores.

Subsampling SoilSamples

The whole sample submitted is first dried and then sieved through a 10mm sieve followed by a2mm sieve. All fibrous matter viz greater than 10mm, greater than 2mm as well as the materialpassing through the 2mm sieve are retained and analysed for the presence of asbestos. If thesub 2mm fraction is greater than approximately 30 to 60g then a sub-sampling routine based onISO 3082:2009(E) Iron ores - Sampling and Sample preparation procedures is employed.Depending on the nature and size of the soil sample, the sub-2 mm residue material may needto be sub-sampled for trace analysis in accordance with AS 4964-2004.

Bondedasbestos-containingmaterial (ACM)

The material is first examined and any fibres isolated and where required interfering organicfibres or matter may be removed by treating the sample for several hours at a temperature notexceeding 400 ± 30°C. The resultant material is then ground and examined in accordance withAS 4964-2004.

Limit of Reporting The nominal detection limit of the AS4964 method is around 0.01%. The examination of largesample sizes (at least 500 ml is recommended) may improve the likelihood of identifyingasbestos material in the greater than 2 mm fraction. The NEPM screening level of 0.001% w/wasbestos in soil for FA and AF (i.e. non-bonded/friable asbestos) only applies where the FA andAF are able to be quantified by gravimetric procedures. This screening level is not applicable tofree fibres. NOTE: NATA News, September 2011 – page 34, states, “Weighing of fibres isproblematic and can lead to loss of fibres and potential exposure for laboratory analysts. Torequest laboratories to report information which is outside the scope of AS 4964-2004 and thescope of their accreditation is misleading and is most unwise” therefore such values reportedare outside the scope of Eurofins | mgt NATA accreditation as designated by an asterisk.

First Reported: Jul 01, 2015




Page 1 of

Report Number: 462743-AID

16


Accredited for compliance with ISO/IEC 17025.The results of the tests, calibrations and/ormeasurements included in this document aretraceable to Australian/national standards.

Project Name ENAUWOLL04223AAProject IDDate Sampled Jun 22, 2015 to Jun 23, 2015Report 462743-AID

Client Sample ID Eurofins | mgtSample No. Date Sampled Sample Description Result

CTP01/0.0-0.2 15-Jn20258 Jun 22, 2015 Approximate Sample 140gSample consisted of: Brown fine-grained soil and rocks

No asbestos detected.Organic fibre detected.No respirable fibres detected.





CTP02A/0.0-0.2 15-Jn20264 Jun 22, 2015Approximate Sample 190gSample consisted of: Dark brown coarse-grained sandy soil and plantmatter


CTP03/0.0-0.2 15-Jn20265 Jun 22, 2015 Approximate Sample 233gSample consisted of: Dark brown coarse-grained sandy soil


CTP03/0.8-1.0 15-Jn20266 Jun 22, 2015 Approximate Sample 238gSample consisted of: Dark brown fine-grained soil and rocks














Page 2 of


16




CTP07/0.0-0.2 15-Jn20278 Jun 22, 2015Approximate Sample 158gSample consisted of: Dark brown coarse-grained sandy soil and plantmatter








CTP10/0.45-065 15-Jn20284 Jun 23, 2015 Approximate Sample 170gSample consisted of: Brown fine-grained soil and rocks















Chrysotile, amosite and crocidolite asbestos detected in aweathered fibre cement fragment.Approximate raw weight of asbestos containing material = 0.0328g

Organic fibre detected.No respirable fibres detected.





Page 3 of


16














CTP17/0.0-0.2 15-Jn20303 Jun 23, 2015Approximate Sample 180gSample consisted of: Dark brown coarse-grained sandy soil and plantmatter


CTP17/0.9-1.1 15-Jn20304 Jun 23, 2015 Approximate Sample 351gSample consisted of: Greyish brown fine-grained soil and rocks


CTP18/0.0-0.2 15-Jn20307 Jun 23, 2015 Approximate Sample 317gSample consisted of: Dark brown coarse-grained soil and rocks

Chrysotile and amosite asbestos detected in the form of loose fibrebundles.Approximate raw weight of asbestos = 0.0005g*

Organic fibre detected.No respirable fibres detected.

CTP18/0.8-0.9 15-Jn20308 Jun 23, 2015 Approximate Sample 230gSample consisted of: Greyish brown fine-grained soil and rocks




CTP19/0.0-0.2 15-Jn20311 Jun 23, 2015 Approximate Sample 300gSample consisted of: Dark brown coarse-grained sandy soil and rocks








Page 4 of


16














CTP21/0.0-0.2 15-Jn20319 Jun 23, 2015 Approximate Sample 323gSample consisted of: Greyish brown coarse-grained sandy soil






CTP22/0.0-0.2 15-Jn20323 Jun 23, 2015 Approximate Sample 204gSample consisted of: Greyish brown coarse-grained soil and rocks






CTP22/0.8-1.2 ACM 15-Jn20327 Jun 23, 2015 Approximate Sample 3g / 48x24x5mmSample consisted of: Brown compressed fibre cement material Chrysotile and amosite asbestos detected.





Page 5 of


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Sample HistoryWhere samples are submitted/analysed over several days, the last date of extraction and analysis is reported.A recent review of our LIMS has resulted in the correction or clarification of some method identifications. Due to this,some of the method reference information on reports has changed. However, no substantive change has beenmade to our laboratory methods, and as such there is no change in the validity of current or previous results(regarding both quality and NATA accreditation).

If the date and time of sampling are not provided, the Laboratory will not be responsible for compromised resultsshould testing be performed outside the recommended holding time.


Asbestos - LTM-ASB-8020 Sydney Jun 26, 2015 Indefinite





Page 6 of


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V2

ABN – 50 005 085 521 e.mail : [email protected] web : www.eurofins.com.au

Melbourne3-5 Kingston Town CloseOakleigh VIC 3166Phone : +61 3 8564 5000NATA # 1261Site # 1254 & 14271

SydneyUnit F3, Building F16 Mars RoadLane Cove West NSW 2066Phone : +61 2 9900 8400NATA # 1261 Site # 18217

Brisbane1/21 Smallwood PlaceMurarrie QLD 4172Phone : +61 7 3902 4600NATA # 1261 Site # 20794





Sample Detail

Asbestos A

bsence /Presence

HO

LD

Polychlorinated B

iphenyls

Acid H

erbicides

Metals M

8

BT

EX

Foreign M

aterials - EN

M

EN

M E

xemption 2012 - N

SW

Office of

Environm


Eurofins | m

gt Suite 14

Eurofins | m

gt Suite 4

BT

EX

and Volatile T

RH

Halogenated V

olatile Organics

Moisture S

et





External Laboratory


Matrix LAB ID





CTP01/2.0-2.1 Jun 22, 2015 Soil S15-Jn20262 X

CTP02/1.35-1.45

Jun 22, 2015 Soil S15-Jn20263 X X X X

CTP02A/0.0-0.2

Jun 22, 2015 Soil S15-Jn20264 X X X X






Page 7 of


16

V2









Sample Detail

Asbestos A

bsence /Presence

HO

LD

Polychlorinated B

iphenyls

Acid H

erbicides

Metals M

8

BT

EX

Foreign M

aterials - EN

M

EN

M E

xemption 2012 - N

SW

Office of

Environm


Eurofins | m

gt Suite 14

Eurofins | m

gt Suite 4

BT

EX

and Volatile T

RH

Halogenated V

olatile Organics

Moisture S

et





External Laboratory


CTP03/1.2-1.3 Jun 22, 2015 Soil S15-Jn20267 X




CTP05/0.4-0.5 Jun 22, 2015 Soil S15-Jn20271 X




CTP06/0.2-0.25

Jun 22, 2015 Soil S15-Jn20275 X X






Page 8 of


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V2









Sample Detail

Asbestos A

bsence /Presence

HO

LD

Polychlorinated B

iphenyls

Acid H

erbicides

Metals M

8

BT

EX

Foreign M

aterials - EN

M

EN

M E

xemption 2012 - N

SW

Office of

Environm


Eurofins | m

gt Suite 14

Eurofins | m

gt Suite 4

BT

EX

and Volatile T

RH

Halogenated V

olatile Organics

Moisture S

et





External Laboratory

0.55

CTP06/0.75-0.85

Jun 22, 2015 Soil S15-Jn20277 X X


CTP07/0.3-0.4 Jun 22, 2015 Soil S15-Jn20279 X


CTP08/0.35-0.45

Jun 22, 2015 Soil S15-Jn20281 X X X



CTP10/0.45-065

Jun 23, 2015 Soil S15-Jn20284 X X X





Page 9 of


16

V2









Sample Detail

Asbestos A

bsence /Presence

HO

LD

Polychlorinated B

iphenyls

Acid H

erbicides

Metals M

8

BT

EX

Foreign M

aterials - EN

M

EN

M E

xemption 2012 - N

SW

Office of

Environm


Eurofins | m

gt Suite 14

Eurofins | m

gt Suite 4

BT

EX

and Volatile T

RH

Halogenated V

olatile Organics

Moisture S

et





External Laboratory

CTP10/0.7-0.8 Jun 23, 2015 Soil S15-Jn20285 X




QC3 Jun 22, 2015 Soil S15-Jn20289 X


CTP12/0.25-0.45

Jun 23, 2015 Soil S15-Jn20291 X X X



CTP13/0.7-0.8 Jun 22, 2015 Soil S15-Jn20294 X






Page 10 of


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V2









Sample Detail

Asbestos A

bsence /Presence

HO

LD

Polychlorinated B

iphenyls

Acid H

erbicides

Metals M

8

BT

EX

Foreign M

aterials - EN

M

EN

M E

xemption 2012 - N

SW

Office of

Environm


Eurofins | m

gt Suite 14

Eurofins | m

gt Suite 4

BT

EX

and Volatile T

RH

Halogenated V

olatile Organics

Moisture S

et





External Laboratory










QC6 Jun 23, 2015 Soil S15-Jn20305 X

QC5 Jun 23, 2015 Soil S15-Jn20306 X X





Page 11 of


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V2









Sample Detail

Asbestos A

bsence /Presence

HO

LD

Polychlorinated B

iphenyls

Acid H

erbicides

Metals M

8

BT

EX

Foreign M

aterials - EN

M

EN

M E

xemption 2012 - N

SW

Office of

Environm


Eurofins | m

gt Suite 14

Eurofins | m

gt Suite 4

BT

EX

and Volatile T

RH

Halogenated V

olatile Organics

Moisture S

et





External Laboratory




CTP18/1.7-1.9 Jun 23, 2015 Soil S15-Jn20310 X












Page 12 of


16

V2









Sample Detail

Asbestos A

bsence /Presence

HO

LD

Polychlorinated B

iphenyls

Acid H

erbicides

Metals M

8

BT

EX

Foreign M

aterials - EN

M

EN

M E

xemption 2012 - N

SW

Office of

Environm


Eurofins | m

gt Suite 14

Eurofins | m

gt Suite 4

BT

EX

and Volatile T

RH

Halogenated V

olatile Organics

Moisture S

et





External Laboratory










CTP22/0.8-1.2ACM

Jun 23, 2015 Soil S15-Jn20327 X






Page 13 of


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V2









Sample Detail

Asbestos A

bsence /Presence

HO

LD

Polychlorinated B

iphenyls

Acid H

erbicides

Metals M

8

BT

EX

Foreign M

aterials - EN

M

EN

M E

xemption 2012 - N

SW

Office of

Environm


Eurofins | m

gt Suite 14

Eurofins | m

gt Suite 4

BT

EX

and Volatile T

RH

Halogenated V

olatile Organics

Moisture S

et





External Laboratory






Page 14 of


16


General1. QC data may be available on request.


3. Samples were analysed on an 'as received' basis.

4. This report replaces any interim results previously issued.

Holding TimesPlease refer to 'Sample Preservation and Container Guide' for holding times (QS3001).


Receipt Advice.



UNITS% w/w: weight for weight basis grams per kilogram

Filter loading: fibres/100 graticule areas

Reported Concentration: fibres/mL

Flowrate: L/min

TERMSDry Where a moisture has been determined on a solid sample the result is expressed on a dry basis.


COC Chain of custody


ISO International Stardards Organisation

AS Australian Standards

WA DOH Western Australia Department of Health

NOHSC National Occupational Health and Safety Commission

ACM Bonded asbestos-containing material means any material containing more than 1% asbestos and comprises asbestos-containing-material which is in sound condition,

although possibly broken or fragmented, and where the asbestos is bound in a matrix such as cement or resin. Common examples of ACM include but are not limited

to: pipe and boiler insulation, sprayed-on fireproofing, troweled-on acoustical plaster, floor tile and mastic, floor linoleum, transite shingles, roofing materials, wall and

ceiling plaster, ceiling tiles, and gasket materials. This term is restricted to material that cannot pass a 7 mm x 7 mm sieve. This sieve size is selected because it

approximates the thickness of common asbestos cement sheeting and for fragments to be smaller than this would imply a high degree of damage and hence potential

for fibre release.

FA FA comprises friable asbestos material and includes severely weathered cement sheet, insulation products and woven asbestos material. This type of friable asbestos

is defined here as asbestos material that is in a degraded condition such that it can be broken or crumbled by hand pressure. This material is typically unbonded or

was previously bonded and is now significantly degraded (crumbling).

PACM Presumed Asbestos-Containing Material means thermal system insulation and surfacing material found in buildings, vessels, and vessel sections constructed no later

than 1980 that are assumed to contain greater than one percent asbestos but have not been sampled or analyzed to verify or negate the presence of asbestos.

AF Asbestos fines (AF) are defined as free fibres, or fibre bundles, smaller than 7mm. It is the free fibres which present the greatest risk to human health, although very

small fibres (< 5 microns in length) are not considered to be such a risk. AF also includes small fragments of bonded ACM that pass through a 7 mm x 7 mm sieve.

(Note that for bonded ACM fragments to pass through a 7 mm x 7 mm sieve implies a substatntial degree of damage which increases the potential for fibre release.)

AC Asbestos cement means a mixture of cement and asbestos fibres (typically 90:10 ratios).





Page 15 of


16

Comments









Code DescriptionN/A Not applicable

Authorised by:

Nibha Vaidya Senior Analyst-Asbestos (NSW)

Glenn Jackson









Page 16 of


16

Final Report – this report replaces any previously issued Report


MelbourneMelbourneMelbourneMelbourne3-5 Kingston Town CloseOakleigh Vic 3166Phone : +61 3 8564 5000NATA # 1261Site # 1254 & 14271

SydneySydneySydneySydneyUnit F3, Building F16 Mars RoadLane Cove West NSW 2066Phone : +61 2 9900 8400NATA # 1261 Site # 18217

BrisbaneBrisbaneBrisbaneBrisbane1/21 Smallwood PlaceMurarrie QLD 4172Phone : +61 7 3902 4600NATA # 1261 Site # 20794

Environmental LaboratoryAir AnalysisWater AnalysisSoil Contamination Analysis

NATA AccreditationStack Emission Sampling & AnalysisTrade Waste Sampling & AnalysisGroundwater Sampling & Analysis

38 Years of Environmental Analysis & Experience38 Years of Environmental Analysis & Experience38 Years of Environmental Analysis & Experience38 Years of Environmental Analysis & Experience

Sample Receipt AdviceSample Receipt AdviceSample Receipt AdviceSample Receipt Advice

Company name: Coffey Environments Pty Ltd WollongongCoffey Environments Pty Ltd WollongongCoffey Environments Pty Ltd WollongongCoffey Environments Pty Ltd Wollongong

Contact name: Alexander WilliamsProject name: ENAUWOLL04223AACOC number: Not providedTurn around time: 5 DayDate/Time received: Jun 24, 2015 1:22 PMEurofins | mgt reference: 462743462743462743462743

Sample informationSample informationSample informationSample information

☑ A detailed list of analytes logged into our LIMS, is included in the attached summary table.

☑ Sample Temperature of a random sample selected from the batch as recorded by Eurofins | mgtSample Receipt : 6.5 degrees Celsius.

☑ All samples have been received as described on the above COC.

☑ COC has been completed correctly.

☑ Attempt to chill was evident.

☑ Appropriately preserved sample containers have been used.

☑ All samples were received in good condition.

☑ Samples have been provided with adequate time to commence analysis in accordance with therelevant holding times.

☑ Appropriate sample containers have been used.

☒ Some samples have been subcontracted.

N/A Custody Seals intact (if used).

Contact notesContact notesContact notesContact notes

If you have any questions with respect to these samples please contact:

Charl Du Preez on Phone : or by e.mail: [email protected]

Results will be delivered electronically via e.mail to Alexander Williams - [email protected].

.Company Name: Coffey Environments Pty Ltd Wollongong Order No.: Received: Jun 24, 2015 1:22 PMAddress: 118 Auburn Street Report #: 462743 Due: Jul 1, 2015




Sample Detail

Asbestos A

bsence /Presence

HO

LD

Polychlorinated B

iphenyls

Acid H

erbicides

Metals M

8

BT

EX

Foreign M

aterials - EN

M

EN

M E

xemption 2012 - N

SW

Office of

Environm


Eurofins | m

gt Suite 14

Eurofins | m

gt Suite 4

BT

EX

and Volatile T

RH

Halogenated V

olatile Organics

Moisture S

et





External Laboratory


Matrix LAB ID





CTP01/2.0-2.1 Jun 22, 2015 Soil S15-Jn20262 X

CTP02/1.35-1.45

Jun 22, 2015 Soil S15-Jn20263 X X X X

CTP02A/0.0-0.2

Jun 22, 2015 Soil S15-Jn20264 X X X X


AB

N –

50

005

085

521

e.m

ail :

Env

iroS

ales

@eu

rofin

s.co

m.a

u

w

eb :

ww

w.e

urof

ins.

com

.au

Mel

bour

neM

elbo

urne

Mel

bour

neM

elbo

urne

3-5

Kin

gsto

n To

wn

Clo

seO

akle

igh

VIC

316

6P

hone

: +6

1 3

8564

500

0N

ATA

# 1

261

Site

# 1

254

& 1

4271

Syd

ney

Syd

ney

Syd

ney

Syd

ney

Uni

t F3,

Bui

ldin

g F

16 M

ars

Roa

dLa

ne C

ove

Wes

t NS

W 2

066

Pho

ne :

+61

2 99

00 8

400

NA

TA #

126

1 S

ite #

182

17

Bris

bane

Bris

bane

Bris

bane

Bris

bane

1/21

Sm

allw

ood

Pla

ceM

urar

rie Q

LD 4

172

Pho

ne :

+61

7 39

02 4

600

NA

TA #

126

1 S

ite #

207

94





Sample Detail

Asbestos A

bsence /Presence

HO

LD

Polychlorinated B

iphenyls

Acid H

erbicides

Metals M

8

BT

EX

Foreign M

aterials - EN

M

EN

M E

xemption 2012 - N

SW

Office of

Environm


Eurofins | m

gt Suite 14

Eurofins | m

gt Suite 4

BT

EX

and Volatile T

RH

Halogenated V

olatile Organics

Moisture S

et





External Laboratory


CTP03/1.2-1.3 Jun 22, 2015 Soil S15-Jn20267 X




CTP05/0.4-0.5 Jun 22, 2015 Soil S15-Jn20271 X




CTP06/0.2-0.25

Jun 22, 2015 Soil S15-Jn20275 X X


AB

N –

50

005

085

521

e.m

ail :

Env

iroS

ales

@eu

rofin

s.co

m.a

u

w

eb :

ww

w.e

urof

ins.

com

.au

Mel

bour

neM

elbo

urne

Mel

bour

neM

elbo

urne

3-5

Kin

gsto

n To

wn

Clo

seO

akle

igh

VIC

316

6P

hone

: +6

1 3

8564

500

0N

ATA

# 1

261

Site

# 1

254

& 1

4271

Syd

ney

Syd

ney

Syd

ney

Syd

ney

Uni

t F3,

Bui

ldin

g F

16 M

ars

Roa

dLa

ne C

ove

Wes

t NS

W 2

066

Pho

ne :

+61

2 99

00 8

400

NA

TA #

126

1 S

ite #

182

17

Bris

bane

Bris

bane

Bris

bane

Bris

bane

1/21

Sm

allw

ood

Pla

ceM

urar

rie Q

LD 4

172

Pho

ne :

+61

7 39

02 4

600

NA

TA #

126

1 S

ite #

207

94





Sample Detail

Asbestos A

bsence /Presence

HO

LD

Polychlorinated B

iphenyls

Acid H

erbicides

Metals M

8

BT

EX

Foreign M

aterials - EN

M

EN

M E

xemption 2012 - N

SW

Office of

Environm


Eurofins | m

gt Suite 14

Eurofins | m

gt Suite 4

BT

EX

and Volatile T

RH

Halogenated V

olatile Organics

Moisture S

et





External Laboratory

0.55

CTP06/0.75-0.85

Jun 22, 2015 Soil S15-Jn20277 X X


CTP07/0.3-0.4 Jun 22, 2015 Soil S15-Jn20279 X


CTP08/0.35-0.45

Jun 22, 2015 Soil S15-Jn20281 X X X



CTP10/0.45-065

Jun 23, 2015 Soil S15-Jn20284 X X X

AB

N –

50

005

085

521

e.m

ail :

Env

iroS

ales

@eu

rofin

s.co

m.a

u

w

eb :

ww

w.e

urof

ins.

com

.au

Mel

bour

neM

elbo

urne

Mel

bour

neM

elbo

urne

3-5

Kin

gsto

n To

wn

Clo

seO

akle

igh

VIC

316

6P

hone

: +6

1 3

8564

500

0N

ATA

# 1

261

Site

# 1

254

& 1

4271

Syd

ney

Syd

ney

Syd

ney

Syd

ney

Uni

t F3,

Bui

ldin

g F

16 M

ars

Roa

dLa

ne C

ove

Wes

t NS

W 2

066

Pho

ne :

+61

2 99

00 8

400

NA

TA #

126

1 S

ite #

182

17

Bris

bane

Bris

bane

Bris

bane

Bris

bane

1/21

Sm

allw

ood

Pla

ceM

urar

rie Q

LD 4

172

Pho

ne :

+61

7 39

02 4

600

NA

TA #

126

1 S

ite #

207

94





Sample Detail

Asbestos A

bsence /Presence

HO

LD

Polychlorinated B

iphenyls

Acid H

erbicides

Metals M

8

BT

EX

Foreign M

aterials - EN

M

EN

M E

xemption 2012 - N

SW

Office of

Environm


Eurofins | m

gt Suite 14

Eurofins | m

gt Suite 4

BT

EX

and Volatile T

RH

Halogenated V

olatile Organics

Moisture S

et





External Laboratory

CTP10/0.7-0.8 Jun 23, 2015 Soil S15-Jn20285 X




QC3 Jun 22, 2015 Soil S15-Jn20289 X


CTP12/0.25-0.45

Jun 23, 2015 Soil S15-Jn20291 X X X



CTP13/0.7-0.8 Jun 22, 2015 Soil S15-Jn20294 X


AB

N –

50

005

085

521

e.m

ail :

Env

iroS

ales

@eu

rofin

s.co

m.a

u

w

eb :

ww

w.e

urof

ins.

com

.au

Mel

bour

neM

elbo

urne

Mel

bour

neM

elbo

urne

3-5

Kin

gsto

n To

wn

Clo

seO

akle

igh

VIC

316

6P

hone

: +6

1 3

8564

500

0N

ATA

# 1

261

Site

# 1

254

& 1

4271

Syd

ney

Syd

ney

Syd

ney

Syd

ney

Uni

t F3,

Bui

ldin

g F

16 M

ars

Roa

dLa

ne C

ove

Wes

t NS

W 2

066

Pho

ne :

+61

2 99

00 8

400

NA

TA #

126

1 S

ite #

182

17

Bris

bane

Bris

bane

Bris

bane

Bris

bane

1/21

Sm

allw

ood

Pla

ceM

urar

rie Q

LD 4

172

Pho

ne :

+61

7 39

02 4

600

NA

TA #

126

1 S

ite #

207

94





Sample Detail

Asbestos A

bsence /Presence

HO

LD

Polychlorinated B

iphenyls

Acid H

erbicides

Metals M

8

BT

EX

Foreign M

aterials - EN

M

EN

M E

xemption 2012 - N

SW

Office of

Environm


Eurofins | m

gt Suite 14

Eurofins | m

gt Suite 4

BT

EX

and Volatile T

RH

Halogenated V

olatile Organics

Moisture S

et





External Laboratory










QC6 Jun 23, 2015 Soil S15-Jn20305 X

QC5 Jun 23, 2015 Soil S15-Jn20306 X X

AB

N –

50

005

085

521

e.m

ail :

Env

iroS

ales

@eu

rofin

s.co

m.a

u

w

eb :

ww

w.e

urof

ins.

com

.au

Mel

bour

neM

elbo

urne

Mel

bour

neM

elbo

urne

3-5

Kin

gsto

n To

wn

Clo

seO

akle

igh

VIC

316

6P

hone

: +6

1 3

8564

500

0N

ATA

# 1

261

Site

# 1

254

& 1

4271

Syd

ney

Syd

ney

Syd

ney

Syd

ney

Uni

t F3,

Bui

ldin

g F

16 M

ars

Roa

dLa

ne C

ove

Wes

t NS

W 2

066

Pho

ne :

+61

2 99

00 8

400

NA

TA #

126

1 S

ite #

182

17

Bris

bane

Bris

bane

Bris

bane

Bris

bane

1/21

Sm

allw

ood

Pla

ceM

urar

rie Q

LD 4

172

Pho

ne :

+61

7 39

02 4

600

NA

TA #

126

1 S

ite #

207

94





Sample Detail

Asbestos A

bsence /Presence

HO

LD

Polychlorinated B

iphenyls

Acid H

erbicides

Metals M

8

BT

EX

Foreign M

aterials - EN

M

EN

M E

xemption 2012 - N

SW

Office of

Environm


Eurofins | m

gt Suite 14

Eurofins | m

gt Suite 4

BT

EX

and Volatile T

RH

Halogenated V

olatile Organics

Moisture S

et





External Laboratory




CTP18/1.7-1.9 Jun 23, 2015 Soil S15-Jn20310 X








AB

N –

50

005

085

521

e.m

ail :

Env

iroS

ales

@eu

rofin

s.co

m.a

u

w

eb :

ww

w.e

urof

ins.

com

.au

Mel

bour

neM

elbo

urne

Mel

bour

neM

elbo

urne

3-5

Kin

gsto

n To

wn

Clo

seO

akle

igh

VIC

316

6P

hone

: +6

1 3

8564

500

0N

ATA

# 1

261

Site

# 1

254

& 1

4271

Syd

ney

Syd

ney

Syd

ney

Syd

ney

Uni

t F3,

Bui

ldin

g F

16 M

ars

Roa

dLa

ne C

ove

Wes

t NS

W 2

066

Pho

ne :

+61

2 99

00 8

400

NA

TA #

126

1 S

ite #

182

17

Bris

bane

Bris

bane

Bris

bane

Bris

bane

1/21

Sm

allw

ood

Pla

ceM

urar

rie Q

LD 4

172

Pho

ne :

+61

7 39

02 4

600

NA

TA #

126

1 S

ite #

207

94





Sample Detail

Asbestos A

bsence /Presence

HO

LD

Polychlorinated B

iphenyls

Acid H

erbicides

Metals M

8

BT

EX

Foreign M

aterials - EN

M

EN

M E

xemption 2012 - N

SW

Office of

Environm


Eurofins | m

gt Suite 14

Eurofins | m

gt Suite 4

BT

EX

and Volatile T

RH

Halogenated V

olatile Organics

Moisture S

et





External Laboratory










CTP22/0.8-1.2ACM

Jun 23, 2015 Soil S15-Jn20327 X


AB

N –

50

005

085

521

e.m

ail :

Env

iroS

ales

@eu

rofin

s.co

m.a

u

w

eb :

ww

w.e

urof

ins.

com

.au

Mel

bour

neM

elbo

urne

Mel

bour

neM

elbo

urne

3-5

Kin

gsto

n To

wn

Clo

seO

akle

igh

VIC

316

6P

hone

: +6

1 3

8564

500

0N

ATA

# 1

261

Site

# 1

254

& 1

4271

Syd

ney

Syd

ney

Syd

ney

Syd

ney

Uni

t F3,

Bui

ldin

g F

16 M

ars

Roa

dLa

ne C

ove

Wes

t NS

W 2

066

Pho

ne :

+61

2 99

00 8

400

NA

TA #

126

1 S

ite #

182

17

Bris

bane

Bris

bane

Bris

bane

Bris

bane

1/21

Sm

allw

ood

Pla

ceM

urar

rie Q

LD 4

172

Pho

ne :

+61

7 39

02 4

600

NA

TA #

126

1 S

ite #

207

94





Sample Detail

Asbestos A

bsence /Presence

HO

LD

Polychlorinated B

iphenyls

Acid H

erbicides

Metals M

8

BT

EX

Foreign M

aterials - EN

M

EN

M E

xemption 2012 - N

SW

Office of

Environm


Eurofins | m

gt Suite 14

Eurofins | m

gt Suite 4

BT

EX

and Volatile T

RH

Halogenated V

olatile Organics

Moisture S

et





External Laboratory


TSLAB Jun 18, 2015 Soil S15-Jn20330 X

AB

N –

50

005

085

521

e.m

ail :

Env

iroS

ales

@eu

rofin

s.co

m.a

u

w

eb :

ww

w.e

urof

ins.

com

.au

Mel

bour

neM

elbo

urne

Mel

bour

neM

elbo

urne

3-5

Kin

gsto

n To

wn

Clo

seO

akle

igh

VIC

316

6P

hone

: +6

1 3

8564

500

0N

ATA

# 1

261

Site

# 1

254

& 1

4271

Syd

ney

Syd

ney

Syd

ney

Syd

ney

Uni

t F3,

Bui

ldin

g F

16 M

ars

Roa

dLa

ne C

ove

Wes

t NS

W 2

066

Pho

ne :

+61

2 99

00 8

400

NA

TA #

126

1 S

ite #

182

17

Bris

bane

Bris

bane

Bris

bane

Bris

bane

1/21

Sm

allw

ood

Pla

ceM

urar

rie Q

LD 4

172

Pho

ne :

+61

7 39

02 4

600

NA

TA #

126

1 S

ite #

207

94



118 Auburn Street

Wollongong

NSW 2500


Report 463922-S

Project name ADDITIONAL : ENAUWOLL04223AA

Received Date Jul 03, 2015



Eurofins | mgt Sample No. S15-Jl02410 S15-Jl04411 S15-Jl04412 S15-Jl04413





1.1-Dichloroethene 0.5 mg/kg < 0.5 - - -





1.2-Dibromoethane 0.5 mg/kg < 0.5 - - -




1.2.3-Trichloropropane 0.5 mg/kg < 0.5 - - -




Bromodichloromethane 0.5 mg/kg < 0.5 - - -

Bromoform 0.5 mg/kg < 0.5 - - -

Bromomethane 0.5 mg/kg < 0.5 - - -

Carbon Tetrachloride 0.5 mg/kg < 0.5 - - -

Chlorobenzene 0.5 mg/kg < 0.5 - - -

Chloroform 0.5 mg/kg < 0.5 - - -

Chloromethane 0.5 mg/kg < 0.5 - - -

cis-1.2-Dichloroethene 0.5 mg/kg < 0.5 - - -

cis-1.3-Dichloropropene 0.5 mg/kg < 0.5 - - -

Dibromochloromethane 0.5 mg/kg < 0.5 - - -

Dibromomethane 0.5 mg/kg < 0.5 - - -

Iodomethane 0.5 mg/kg < 0.5 - - -

Methylene Chloride 0.5 mg/kg < 0.5 - - -

Tetrachloroethene 0.5 mg/kg < 0.5 - - -

trans-1.2-Dichloroethene 0.5 mg/kg < 0.5 - - -

trans-1.3-Dichloropropene 0.5 mg/kg < 0.5 - - -

Trichloroethene 0.5 mg/kg < 0.5 - - -

Trichlorofluoromethane 0.5 mg/kg < 0.5 - - -

Vinyl chloride 0.5 mg/kg < 0.5 - - -

Fluorobenzene (surr.) 1 % 95 - - -




Page 1 of 15










Aroclor-1016 0.5 mg/kg < 0.5 - - -

Aroclor-1221 0.1 mg/kg < 0.1 - - -

Aroclor-1232 0.5 mg/kg < 0.5 - - -

Aroclor-1242 0.5 mg/kg < 0.5 - - -

Aroclor-1248 0.5 mg/kg < 0.5 - - -

Aroclor-1254 0.5 mg/kg < 0.5 - - -

Aroclor-1260 0.5 mg/kg < 0.5 - - -

Total PCB* 0.1 mg/kg < 0.1 - - -


Tetrachloro-m-xylene (surr.) 1 % - - -

TRH - 2013 NEPM Fractions (after silica gel clean-up)

TRH >C10-C16 (after silica gel clean-up) 50 mg/kg - < 50 < 50 < 50




TRH C10-C14 (after silica gel clean-up) 50 mg/kg - < 50 < 50 < 50



Heavy Metals

Arsenic 2 mg/kg 2.4 - - -

Cadmium 0.4 mg/kg < 0.4 - - -

Chromium 5 mg/kg 6.2 - - -

Copper 5 mg/kg 7.7 - - -

Lead 5 mg/kg 17 - - -

Mercury 0.05 mg/kg < 0.05 - - -

Nickel 5 mg/kg < 5 - - -

Zinc 5 mg/kg 110 - - -

% Moisture 0.1 % 20 19 22 23







Benzo(a)pyrene TEQ (lower bound) * 0.5 mg/kg < 0.5 < 0.5 < 0.5 -

Benzo(a)pyrene TEQ (medium bound) * 0.5 mg/kg 0.6 0.6 0.6 -

Benzo(a)pyrene TEQ (upper bound) * 0.5 mg/kg 1.2 1.2 1.2 -

Acenaphthene 0.5 mg/kg < 0.5 < 0.5 < 0.5 -

Acenaphthylene 0.5 mg/kg < 0.5 < 0.5 < 0.5 -

Anthracene 0.5 mg/kg < 0.5 < 0.5 < 0.5 -

Benz(a)anthracene 0.5 mg/kg < 0.5 < 0.5 < 0.5 -

Benzo(a)pyrene 0.5 mg/kg < 0.5 < 0.5 < 0.5 -

Benzo(b&j)fluorantheneN07 0.5 mg/kg < 0.5 < 0.5 < 0.5 -

Benzo(g.h.i)perylene 0.5 mg/kg < 0.5 < 0.5 < 0.5 -

Benzo(k)fluoranthene 0.5 mg/kg < 0.5 < 0.5 < 0.5 -

Chrysene 0.5 mg/kg < 0.5 < 0.5 < 0.5 -




Page 2 of 15








Dibenz(a.h)anthracene 0.5 mg/kg < 0.5 < 0.5 < 0.5 -

Fluoranthene 0.5 mg/kg < 0.5 < 0.5 < 0.5 -

Fluorene 0.5 mg/kg < 0.5 < 0.5 < 0.5 -

Indeno(1.2.3-cd)pyrene 0.5 mg/kg < 0.5 < 0.5 < 0.5 -

Naphthalene 0.5 mg/kg < 0.5 < 0.5 < 0.5 -

Phenanthrene 0.5 mg/kg < 0.5 < 0.5 < 0.5 -

Pyrene 0.5 mg/kg < 0.5 < 0.5 < 0.5 -

Total PAH* 0.5 mg/kg < 0.5 < 0.5 < 0.5 -

2-Fluorobiphenyl (surr.) 1 % 122 121 126 -

p-Terphenyl-d14 (surr.) 1 % 127 121 123 -

Heavy Metals

Arsenic 2 mg/kg - 5.0 - 6.0

Cadmium 0.4 mg/kg - < 0.4 - < 0.4

Chromium 5 mg/kg - 15 - 10

Copper 5 mg/kg - 23 - 21

Lead 5 mg/kg 17 13 - 10

Mercury 0.05 mg/kg - < 0.05 - < 0.05

Nickel 5 mg/kg - < 5 - < 5

Zinc 5 mg/kg 13 33 - 14

% Moisture 0.1 % 20 20 19 22


Sample Matrix Soil Soil Soil

Eurofins | mgt Sample No. S15-Jl04418 S15-Jl04420 S15-Jl04421

Date Sampled Jun 22, 2015 Jun 22, 2015 Jun 22, 2015


Heavy Metals

Arsenic 2 mg/kg - 35 -

Cadmium 0.4 mg/kg - < 0.4 -

Chromium 5 mg/kg - 11 -

Copper 5 mg/kg - 26 -

Lead 5 mg/kg 14 13 13

Mercury 0.05 mg/kg - < 0.05 -

Nickel 5 mg/kg - < 5 -

Zinc 5 mg/kg 55 14 25

% Moisture 0.1 % 23 18 20




Page 3 of 15





Halogenated Volatile Organics Sydney Jul 03, 2015 7 Day

- Method: E016 Volatile Halogenated Compounds (VHC)

Polycyclic Aromatic Hydrocarbons Sydney Jul 06, 2015 14 Day

- Method: E007 Polyaromatic Hydrocarbons (PAH)

Polychlorinated Biphenyls Sydney Jul 03, 2015 28 Day

Metals M8 Sydney Jul 06, 2015 28 Day

- Method: LTM-MET-3040_R0 TOTAL AND DISSOLVED METALS AND MERCURY IN WATERS BY ICP-MS

Heavy Metals Sydney Jul 06, 2015 180 Day

- Method: E022 Acid Extractable metals in Soils

TRH - 2013 NEPM Fractions (after silica gel clean-up) Sydney Jul 06, 2015 14 Day

- Method: LM-LTM-ORG2010

TRH - 1999 NEPM Fractions (after silica gel clean-up) Sydney Jul 06, 2015 14 Day

- Method: LM-LTM-ORG2010

% Moisture Sydney Jul 06, 2015 14 Day

- Method: LTM-GEN-7080 Moisture




Page 4 of 15


.Company Name: Coffey Environments Pty Ltd Wollongong Order No.: Received: Jul 3, 2015 5:15 PMAddress: 118 Auburn Street Report #: 463922 Due: Jul 9, 2015


Project Name: ADDITIONAL : ENAUWOLL04223AA


Sample Detail

Arsenic

CA

NC

ELLE

D

Lead

Zinc

Polycyclic A

romatic H

ydrocarbons

Polychlorinated B

iphenyls

US

A Leaching P

rocedure

Metals M

8

Benzo[a]pyrene

Halogenated V

olatile Organics

TR

H (after S

ilica Gel cleanup)

Moisture S

et


Melbourne Laboratory - NATA Site # 1254 & 14271



External Laboratory


Matrix LAB ID

QC3 Jun 22, 2015 Soil S15-Jl02410 X X X X

CTP01/1.4-1.6 Jun 22, 2015 TCLP S15-Jl04401 X X X


CTP08/0.0-0.2 Jun 22, 2015 TCLP S15-Jl04403 X X


CTP2A/0.0-0.2 Jun 22, 2015 TCLP S15-Jl04405 X X


QC2 Jun 22, 2015 TCLP S15-Jl04407 X X

CTP10/0.45-0.65

Jun 22, 2015 TCLP S15-Jl04408 X X

AB

N –

50

005

085

521

e.m

ail :

Env

iroS

ales

@eu

rofin

s.co

m.a

u

w

eb :

ww

w.e

urof

ins.

com

.au

Mel

bour

neM

elbo

urne

Mel

bour

neM

elbo

urne

3-5

Kin

gsto

n To

wn

Clo

seO

akle

igh

VIC

316

6P

hone

: +6

1 3

8564

500

0N

ATA

# 1

261

Site

# 1

254

& 1

4271

Syd

ney

Syd

ney

Syd

ney

Syd

ney

Uni

t F3,

Bui

ldin

g F

16 M

ars

Roa

dLa

ne C

ove

Wes

t NS

W 2

066

Pho

ne :

+61

2 99

00 8

400

NA

TA #

126

1 S

ite #

182

17

Bris

bane

Bris

bane

Bris

bane

Bris

bane

1/21

Sm

allw

ood

Pla

ceM

urar

rie Q

LD 4

172

Pho

ne :

+61

7 39

02 4

600

NA

TA #

126

1 S

ite #

207

94

Dat

e R

epor

ted:

Jul 0

9, 2

015

Eur

ofin

s | m

gt U

nit F

3, B

uild

ing

F, 1

6 M

ars

Roa

d, L

ane

Cov

e W

est,

NS

W, A

ustr

alia

, 206

6

AB

N :

50 0

05 0

85 5

21 T

elep

hone

: +61

2 9

900

8400

Fac

sim

ile: +

61 2

942

0 29

77

Pag

e 5

of 1

5

Rep

ort N

umbe

r: 4

6392

2-S

Company Name: Coffey Environments Pty Ltd Wollongong Order No.: Received: Jul 3, 2015 5:15 PMAddress: 118 Auburn Street Report #: 463922 Due: Jul 9, 2015




Sample Detail

Arsenic

CA

NC

ELLE

D

Lead

Zinc

Polycyclic A

romatic H

ydrocarbons

Polychlorinated B

iphenyls

US

A Leaching P

rocedure

Metals M

8

Benzo[a]pyrene

Halogenated V

olatile Organics

TR

H (after S

ilica Gel cleanup)

Moisture S

et





External Laboratory



CTP05/0.0-0.2 Jun 22, 2015 Soil S15-Jl04411 X X



CTP03/1.2-1.3 Jun 22, 2015 Soil S15-Jl04414 X X X X

CTP10/0.7-0.8 Jun 22, 2015 Soil S15-Jl04415 X X X



CTP06/0.75-0.85

Jun 22, 2015 Soil S15-Jl04418 X X X

CTP07/0.3-0.4 Jun 22, 2015 Soil S15-Jl04419 X

AB

N –

50

005

085

521

e.m

ail :

Env

iroS

ales

@eu

rofin

s.co

m.a

u

w

eb :

ww

w.e

urof

ins.

com

.au

Mel

bour

neM

elbo

urne

Mel

bour

neM

elbo

urne

3-5

Kin

gsto

n To

wn

Clo

seO

akle

igh

VIC

316

6P

hone

: +6

1 3

8564

500

0N

ATA

# 1

261

Site

# 1

254

& 1

4271

Syd

ney

Syd

ney

Syd

ney

Syd

ney

Uni

t F3,

Bui

ldin

g F

16 M

ars

Roa

dLa

ne C

ove

Wes

t NS

W 2

066

Pho

ne :

+61

2 99

00 8

400

NA

TA #

126

1 S

ite #

182

17

Bris

bane

Bris

bane

Bris

bane

Bris

bane

1/21

Sm

allw

ood

Pla

ceM

urar

rie Q

LD 4

172

Pho

ne :

+61

7 39

02 4

600

NA

TA #

126

1 S

ite #

207

94

Pag

e 6

of 1

5

Rep

ort N

umbe

r: 4

6392

2-S





Sample Detail

Arsenic

CA

NC

ELLE

D

Lead

Zinc

Polycyclic A

romatic H

ydrocarbons

Polychlorinated B

iphenyls

US

A Leaching P

rocedure

Metals M

8

Benzo[a]pyrene

Halogenated V

olatile Organics

TR

H (after S

ilica Gel cleanup)

Moisture S

et





External Laboratory



AB

N –

50

005

085

521

e.m

ail :

Env

iroS

ales

@eu

rofin

s.co

m.a

u

w

eb :

ww

w.e

urof

ins.

com

.au

Mel

bour

neM

elbo

urne

Mel

bour

neM

elbo

urne

3-5

Kin

gsto

n To

wn

Clo

seO

akle

igh

VIC

316

6P

hone

: +6

1 3

8564

500

0N

ATA

# 1

261

Site

# 1

254

& 1

4271

Syd

ney

Syd

ney

Syd

ney

Syd

ney

Uni

t F3,

Bui

ldin

g F

16 M

ars

Roa

dLa

ne C

ove

Wes

t NS

W 2

066

Pho

ne :

+61

2 99

00 8

400

NA

TA #

126

1 S

ite #

182

17

Bris

bane

Bris

bane

Bris

bane

Bris

bane

1/21

Sm

allw

ood

Pla

ceM

urar

rie Q

LD 4

172

Pho

ne :

+61

7 39

02 4

600

NA

TA #

126

1 S

ite #

207

94

Pag

e 7

of 1

5

Rep

ort N

umbe

r: 4

6392

2-S


General

Holding Times

UNITS

TERMS




request.








Receipt Advice.




















































Page 8 of 15




PassLimits

QualifyingCode

Method Blank



1.1-Dichloroethene mg/kg < 0.5 0.5 Pass





1.2-Dibromoethane mg/kg < 0.5 0.5 Pass




1.2.3-Trichloropropane mg/kg < 0.5 0.5 Pass




Bromodichloromethane mg/kg < 0.5 0.5 Pass

Bromoform mg/kg < 0.5 0.5 Pass

Bromomethane mg/kg < 0.5 0.5 Pass

Carbon Tetrachloride mg/kg < 0.5 0.5 Pass

Chlorobenzene mg/kg < 0.5 0.5 Pass

Chloroform mg/kg < 0.5 0.5 Pass

Chloromethane mg/kg < 0.5 0.5 Pass

cis-1.2-Dichloroethene mg/kg < 0.5 0.5 Pass

cis-1.3-Dichloropropene mg/kg < 0.5 0.5 Pass

Dibromochloromethane mg/kg < 0.5 0.5 Pass

Dibromomethane mg/kg < 0.5 0.5 Pass

Iodomethane mg/kg < 0.5 0.5 Pass

Methylene Chloride mg/kg < 0.5 0.5 Pass

Tetrachloroethene mg/kg < 0.5 0.5 Pass

trans-1.2-Dichloroethene mg/kg < 0.5 0.5 Pass

trans-1.3-Dichloropropene mg/kg < 0.5 0.5 Pass

Trichloroethene mg/kg < 0.5 0.5 Pass

Trichlorofluoromethane mg/kg < 0.5 0.5 Pass

Vinyl chloride mg/kg < 0.5 0.5 Pass

Method Blank


Acenaphthene mg/kg < 0.5 0.5 Pass

Acenaphthylene mg/kg < 0.5 0.5 Pass

Anthracene mg/kg < 0.5 0.5 Pass

Benz(a)anthracene mg/kg < 0.5 0.5 Pass

Benzo(a)pyrene mg/kg < 0.5 0.5 Pass

Benzo(b&j)fluoranthene mg/kg < 0.5 0.5 Pass

Benzo(g.h.i)perylene mg/kg < 0.5 0.5 Pass

Benzo(k)fluoranthene mg/kg < 0.5 0.5 Pass

Chrysene mg/kg < 0.5 0.5 Pass

Dibenz(a.h)anthracene mg/kg < 0.5 0.5 Pass

Fluoranthene mg/kg < 0.5 0.5 Pass

Fluorene mg/kg < 0.5 0.5 Pass

Indeno(1.2.3-cd)pyrene mg/kg < 0.5 0.5 Pass


Phenanthrene mg/kg < 0.5 0.5 Pass




Page 9 of 15



PassLimits

QualifyingCode

Pyrene mg/kg < 0.5 0.5 Pass

Method Blank









Total PCB* mg/kg < 0.1 0.1 Pass

Method Blank


TRH >C10-C16 (after silica gel clean-up) mg/kg < 50 50 Pass



Method Blank


TRH C10-C14 (after silica gel clean-up) mg/kg < 50 50 Pass



Method Blank

Heavy Metals

Arsenic mg/kg < 2 2 Pass

Cadmium mg/kg < 0.4 0.4 Pass

Chromium mg/kg < 5 5 Pass

Copper mg/kg < 5 5 Pass

Lead mg/kg < 5 5 Pass

Mercury mg/kg < 0.05 0.05 Pass

Nickel mg/kg < 5 5 Pass

Zinc mg/kg < 5 5 Pass

LCS - % Recovery



1.1-Dichloroethene % 110 70-130 Pass





1.2-Dibromoethane % 115 70-130 Pass




1.2.3-Trichloropropane % 115 70-130 Pass




Bromodichloromethane % 115 70-130 Pass

Bromoform % 112 70-130 Pass

Bromomethane % 74 70-130 Pass

Carbon Tetrachloride % 119 70-130 Pass

Chlorobenzene % 113 70-130 Pass

Chloroform % 123 70-130 Pass

Chloromethane % 123 70-130 Pass




Page 10 of 15



PassLimits

QualifyingCode

cis-1.2-Dichloroethene % 123 70-130 Pass

cis-1.3-Dichloropropene % 110 70-130 Pass

Dibromochloromethane % 117 70-130 Pass

Dibromomethane % 118 70-130 Pass

Iodomethane % 102 70-130 Pass

Methylene Chloride % 114 70-130 Pass

Tetrachloroethene % 121 70-130 Pass

trans-1.2-Dichloroethene % 116 70-130 Pass

trans-1.3-Dichloropropene % 110 70-130 Pass

Trichloroethene % 122 70-130 Pass

Trichlorofluoromethane % 111 70-130 Pass

Vinyl chloride % 109 70-130 Pass

LCS - % Recovery


Acenaphthene % 103 70-130 Pass

Acenaphthylene % 100 70-130 Pass

Anthracene % 104 70-130 Pass

Benz(a)anthracene % 114 70-130 Pass

Benzo(a)pyrene % 110 70-130 Pass

Benzo(b&j)fluoranthene % 127 70-130 Pass

Benzo(g.h.i)perylene % 92 70-130 Pass

Benzo(k)fluoranthene % 106 70-130 Pass

Chrysene % 110 70-130 Pass

Dibenz(a.h)anthracene % 93 70-130 Pass

Fluoranthene % 102 70-130 Pass

Fluorene % 100 70-130 Pass

Indeno(1.2.3-cd)pyrene % 95 70-130 Pass


Phenanthrene % 97 70-130 Pass

Pyrene % 106 70-130 Pass

LCS - % Recovery


Aroclor-1260 % 81 70-130 Pass

LCS - % Recovery


TRH >C10-C16 (after silica gel clean-up) % 80 70-130 Pass

LCS - % Recovery


TRH C10-C14 (after silica gel clean-up) % 84 70-130 Pass

LCS - % Recovery

Heavy Metals

Arsenic % 104 70-130 Pass

Cadmium % 100 70-130 Pass

Chromium % 103 70-130 Pass

Copper % 105 70-130 Pass

Lead % 100 70-130 Pass

Mercury % 106 70-130 Pass

Nickel % 104 70-130 Pass

Zinc % 96 70-130 Pass




Page 11 of 15



LimitsPass

LimitsQualifying

Code

Spike - % Recovery

Polychlorinated Biphenyls Result 1

Aroclor-1260 S15-Jl04390 NCP % 100 70-130 Pass

Spike - % Recovery


Arsenic S15-Jl06159 NCP % 85 70-130 Pass

Cadmium S15-Jl06159 NCP % 89 70-130 Pass

Chromium S15-Jl06159 NCP % 99 70-130 Pass

Copper S15-Jl06159 NCP % 91 70-130 Pass

Mercury S15-Jl06159 NCP % 97 70-130 Pass

Nickel S15-Jl06159 NCP % 98 70-130 Pass

Spike - % Recovery

TRH - 2013 NEPM Fractions (after silica gel clean-up) Result 1

TRH >C10-C16 (after silica gelclean-up) S15-Jl04412 CP % 75 70-130 Pass

Spike - % Recovery

TRH - 1999 NEPM Fractions (after silica gel clean-up) Result 1

TRH C10-C14 (after silica gelclean-up) S15-Jl04412 CP % 78 70-130 Pass

Spike - % Recovery


Acenaphthene S15-Jl04481 NCP % 104 70-130 Pass

Acenaphthylene S15-Jl04481 NCP % 125 70-130 Pass

Anthracene S15-Jl04481 NCP % 112 70-130 Pass

Benz(a)anthracene S15-Jl04481 NCP % 102 70-130 Pass

Benzo(a)pyrene S15-Jl04481 NCP % 89 70-130 Pass

Benzo(b&j)fluoranthene S15-Jl04481 NCP % 116 70-130 Pass

Benzo(g.h.i)perylene S15-Jl04481 NCP % 101 70-130 Pass

Benzo(k)fluoranthene S15-Jl04481 NCP % 90 70-130 Pass

Chrysene S15-Jl04481 NCP % 95 70-130 Pass

Dibenz(a.h)anthracene S15-Jl04481 NCP % 103 70-130 Pass

Fluoranthene S15-Jl04481 NCP % 81 70-130 Pass

Fluorene S15-Jl04481 NCP % 104 70-130 Pass

Indeno(1.2.3-cd)pyrene S15-Jl04481 NCP % 105 70-130 Pass

Naphthalene S15-Jl04481 NCP % 108 70-130 Pass

Phenanthrene S15-Jl04481 NCP % 105 70-130 Pass

Pyrene S15-Jl04481 NCP % 86 70-130 Pass


LimitsPass

LimitsQualifying

Code

Duplicate


1.1-Dichloroethane S15-Jl00715 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

1.1-Dichloroethene S15-Jl00715 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

1.1.1-Trichloroethane S15-Jl00715 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

1.1.1.2-Tetrachloroethane S15-Jl00715 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

1.1.2-Trichloroethane S15-Jl00715 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

1.1.2.2-Tetrachloroethane S15-Jl00715 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

1.2-Dibromoethane S15-Jl00715 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

1.2-Dichlorobenzene S15-Jl00715 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

1.2-Dichloroethane S15-Jl00715 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

1.2-Dichloropropane S15-Jl00715 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

1.2.3-Trichloropropane S15-Jl00715 NCP mg/kg < 0.5 < 0.5 <1 30% Pass


1.3-Dichloropropane S15-Jl00715 NCP mg/kg < 0.5 < 0.5 <1 30% Pass





Page 12 of 15



LimitsPass

LimitsQualifying

Code

Duplicate


Bromodichloromethane S15-Jl00715 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Bromoform S15-Jl00715 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Bromomethane S15-Jl00715 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Carbon Tetrachloride S15-Jl00715 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Chlorobenzene S15-Jl00715 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Chloroform S15-Jl00715 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Chloromethane S15-Jl00715 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

cis-1.2-Dichloroethene S15-Jl00715 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

cis-1.3-Dichloropropene S15-Jl00715 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Dibromochloromethane S15-Jl00715 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Dibromomethane S15-Jl00715 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Iodomethane S15-Jl00715 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Methylene Chloride S15-Jl00715 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Tetrachloroethene S15-Jl00715 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

trans-1.2-Dichloroethene S15-Jl00715 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

trans-1.3-Dichloropropene S15-Jl00715 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Trichloroethene S15-Jl00715 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Trichlorofluoromethane S15-Jl00715 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Vinyl chloride S15-Jl00715 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Duplicate


Arsenic S15-Jl06158 NCP mg/kg 3.8 3.1 19 30% Pass

Cadmium S15-Jl06158 NCP mg/kg 0.50 0.40 17 30% Pass

Chromium S15-Jl06158 NCP mg/kg 18 16 12 30% Pass

Copper S15-Jl06158 NCP mg/kg 99 92 8.0 30% Pass

Lead S15-Jl06158 NCP mg/kg 79 83 5.0 30% Pass

Mercury S15-Jl06158 NCP mg/kg < 0.05 < 0.05 <1 30% Pass

Nickel S15-Jl06158 NCP mg/kg 6.2 6.8 9.0 30% Pass

Zinc S15-Jl06158 NCP mg/kg 260 250 6.0 30% Pass

Duplicate


% Moisture S15-Jl02410 CP % 20 20 4.0 30% Pass

Duplicate

TRH - 2013 NEPM Fractions (after silica gel clean-up) Result 1 Result 2 RPD

TRH >C10-C16 (after silica gelclean-up) S15-Jl04411 CP mg/kg < 50 < 50 <1 30% Pass



Duplicate

TRH - 1999 NEPM Fractions (after silica gel clean-up) Result 1 Result 2 RPD

TRH C10-C14 (after silica gelclean-up) S15-Jl04411 CP mg/kg < 50 < 50 <1 30% Pass



Duplicate


Acenaphthene S15-Jl04445 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Acenaphthylene S15-Jl04445 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Anthracene S15-Jl04445 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Benz(a)anthracene S15-Jl04445 NCP mg/kg < 0.5 < 0.5 <1 30% Pass




Page 13 of 15


Duplicate


Benzo(a)pyrene S15-Jl04445 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Benzo(b&j)fluoranthene S15-Jl04445 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Benzo(g.h.i)perylene S15-Jl04445 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Benzo(k)fluoranthene S15-Jl04445 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Chrysene S15-Jl04445 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Dibenz(a.h)anthracene S15-Jl04445 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Fluoranthene S15-Jl04445 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Fluorene S15-Jl04445 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Indeno(1.2.3-cd)pyrene S15-Jl04445 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Naphthalene S15-Jl04445 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Phenanthrene S15-Jl04445 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Pyrene S15-Jl04445 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Duplicate


% Moisture S15-Jl04416 CP % 19 19 1.0 30% Pass




Page 14 of 15


Comments









Code Description

N07Please note:- These two PAH isomers closely co-elute using the most contemporary analytical methods and both the reported concentration (and the TEQ) apply specifically tothe total of the two co-eluting PAHs

Authorised By


Bob Symons Senior Analyst-Inorganic (NSW)



Ryan Hamilton Senior Analyst-Volatile (NSW)

Glenn Jackson








Page 15 of 15




118 Auburn Street

Wollongong

NSW 2500


Report 463922-L

Project name ADDITIONAL : ENAUWOLL04223AA

Received Date Jul 03, 2015


Sample Matrix TCLP TCLP TCLP TCLP




Benzo[a]pyrene

Benzo(a)pyrene 0.001 mg/L < 0.001 < 0.001 - -

p-Terphenyl-d14 (surr.) 1 % 71 51 - -

2-Fluorobiphenyl (surr.) 1 % 82 51 - -

Heavy Metals

Lead 0.01 mg/L 0.09 0.16 < 0.01 0.02

USA Leaching Procedure

Leachate FluidC01 comment 1.0 1.0 1.0 1.0

pH (initial) 0.1 pH Units 7.2 7.1 6.5 7.0

pH (off) 0.1 pH Units 5.2 5.2 5.1 5.1

pH (USA HCl addition) 0.1 pH Units 2.2 2.6 2.2 2.2

Client Sample ID CTP2A/0.0-0.2 CTP04/0.0-0.2 QC2CTP10/0.45-0.65

Sample Matrix TCLP TCLP TCLP TCLP




Benzo[a]pyrene

Benzo(a)pyrene 0.001 mg/L - < 0.001 < 0.001 < 0.001



Heavy Metals

Arsenic 0.01 mg/L < 0.01 - - -


Leachate FluidC01 comment 1.0 1.0 1.0 1.0

pH (initial) 0.1 pH Units 7.9 7.2 7.1 6.4

pH (off) 0.1 pH Units 5.3 5.1 5.1 5.1

pH (USA HCl addition) 0.1 pH Units 2.7 2.3 2.2 2.2




Page 1 of 9

Report Number: 463922-L



Client Sample ID CTP14/1.0-1.2 CTP18/0.8-0.9

Sample Matrix TCLP TCLP

Eurofins | mgt Sample No. S15-Jl04409 S15-Jl04410

Date Sampled Jun 22, 2015 Jun 22, 2015


Benzo[a]pyrene

Benzo(a)pyrene 0.001 mg/L < 0.001 < 0.001

p-Terphenyl-d14 (surr.) 1 % 86 80

2-Fluorobiphenyl (surr.) 1 % 87 74


Leachate FluidC01 comment 1.0 1.0

pH (initial) 0.1 pH Units 7.3 7.9

pH (off) 0.1 pH Units 5.1 5.2

pH (USA HCl addition) 0.1 pH Units 2.2 2.3




Page 2 of 9





Benzo[a]pyrene Sydney Jul 08, 2015 7 Day

- Method: E007 Benzo[a]pyrene

Heavy Metals Sydney Jul 06, 2015 180 Day

- Method: E022 Acid Extractable metals in Soils

USA Leaching Procedure Sydney Jul 06, 2015 14 Day

- Method: E019 TCLP Preparation




Page 3 of 9






Sample Detail

Arsenic

CA

NC

ELLE

D

Lead

Zinc

Polycyclic A

romatic H

ydrocarbons

Polychlorinated B

iphenyls

US

A Leaching P

rocedure

Metals M

8

Benzo[a]pyrene

Halogenated V

olatile Organics

TR

H (after S

ilica Gel cleanup)

Moisture S

et





External Laboratory


Matrix LAB ID








QC2 Jun 22, 2015 TCLP S15-Jl04407 X X

CTP10/0.45-0.65

Jun 22, 2015 TCLP S15-Jl04408 X X

AB

N –

50

005

085

521

e.m

ail :

Env

iroS

ales

@eu

rofin

s.co

m.a

u

w

eb :

ww

w.e

urof

ins.

com

.au

Mel

bour

neM

elbo

urne

Mel

bour

neM

elbo

urne

3-5

Kin

gsto

n To

wn

Clo

seO

akle

igh

VIC

316

6P

hone

: +6

1 3

8564

500

0N

ATA

# 1

261

Site

# 1

254

& 1

4271

Syd

ney

Syd

ney

Syd

ney

Syd

ney

Uni

t F3,

Bui

ldin

g F

16 M

ars

Roa

dLa

ne C

ove

Wes

t NS

W 2

066

Pho

ne :

+61

2 99

00 8

400

NA

TA #

126

1 S

ite #

182

17

Bris

bane

Bris

bane

Bris

bane

Bris

bane

1/21

Sm

allw

ood

Pla

ceM

urar

rie Q

LD 4

172

Pho

ne :

+61

7 39

02 4

600

NA

TA #

126

1 S

ite #

207

94

Dat

e R

epor

ted:

Jul 0

9, 2

015

Eur

ofin

s | m

gt U

nit F

3, B

uild

ing

F, 1

6 M

ars

Roa

d, L

ane

Cov

e W

est,

NS

W, A

ustr

alia

, 206

6

AB

N :

50 0

05 0

85 5

21 T

elep

hone

: +61

2 9

900

8400

Fac

sim

ile: +

61 2

942

0 29

77

Pag

e 4

of 9

Rep

ort N

umbe

r: 4

6392

2-L





Sample Detail

Arsenic

CA

NC

ELLE

D

Lead

Zinc

Polycyclic A

romatic H

ydrocarbons

Polychlorinated B

iphenyls

US

A Leaching P

rocedure

Metals M

8

Benzo[a]pyrene

Halogenated V

olatile Organics

TR

H (after S

ilica Gel cleanup)

Moisture S

et





External Laboratory










CTP06/0.75-0.85

Jun 22, 2015 Soil S15-Jl04418 X X X

CTP07/0.3-0.4 Jun 22, 2015 Soil S15-Jl04419 X

AB

N –

50

005

085

521

e.m

ail :

Env

iroS

ales

@eu

rofin

s.co

m.a

u

w

eb :

ww

w.e

urof

ins.

com

.au

Mel

bour

neM

elbo

urne

Mel

bour

neM

elbo

urne

3-5

Kin

gsto

n To

wn

Clo

seO

akle

igh

VIC

316

6P

hone

: +6

1 3

8564

500

0N

ATA

# 1

261

Site

# 1

254

& 1

4271

Syd

ney

Syd

ney

Syd

ney

Syd

ney

Uni

t F3,

Bui

ldin

g F

16 M

ars

Roa

dLa

ne C

ove

Wes

t NS

W 2

066

Pho

ne :

+61

2 99

00 8

400

NA

TA #

126

1 S

ite #

182

17

Bris

bane

Bris

bane

Bris

bane

Bris

bane

1/21

Sm

allw

ood

Pla

ceM

urar

rie Q

LD 4

172

Pho

ne :

+61

7 39

02 4

600

NA

TA #

126

1 S

ite #

207

94

Pag

e 5

of 9

Rep

ort N

umbe

r: 4

6392

2-L





Sample Detail

Arsenic

CA

NC

ELLE

D

Lead

Zinc

Polycyclic A

romatic H

ydrocarbons

Polychlorinated B

iphenyls

US

A Leaching P

rocedure

Metals M

8

Benzo[a]pyrene

Halogenated V

olatile Organics

TR

H (after S

ilica Gel cleanup)

Moisture S

et





External Laboratory



AB

N –

50

005

085

521

e.m

ail :

Env

iroS

ales

@eu

rofin

s.co

m.a

u

w

eb :

ww

w.e

urof

ins.

com

.au

Mel

bour

neM

elbo

urne

Mel

bour

neM

elbo

urne

3-5

Kin

gsto

n To

wn

Clo

seO

akle

igh

VIC

316

6P

hone

: +6

1 3

8564

500

0N

ATA

# 1

261

Site

# 1

254

& 1

4271

Syd

ney

Syd

ney

Syd

ney

Syd

ney

Uni

t F3,

Bui

ldin

g F

16 M

ars

Roa

dLa

ne C

ove

Wes

t NS

W 2

066

Pho

ne :

+61

2 99

00 8

400

NA

TA #

126

1 S

ite #

182

17

Bris

bane

Bris

bane

Bris

bane

Bris

bane

1/21

Sm

allw

ood

Pla

ceM

urar

rie Q

LD 4

172

Pho

ne :

+61

7 39

02 4

600

NA

TA #

126

1 S

ite #

207

94

Pag

e 6

of 9

Rep

ort N

umbe

r: 4

6392

2-L


General

Holding Times

UNITS

TERMS




request.








Receipt Advice.




















































Page 7 of 9




PassLimits

QualifyingCode

Method Blank

Benzo[a]pyrene

Benzo(a)pyrene mg/L < 0.001 0.001 Pass

Method Blank

Heavy Metals

Arsenic mg/L < 0.01 0.01 Pass

Lead mg/L < 0.01 0.01 Pass


LimitsPass

LimitsQualifying

Code

Spike - % Recovery


Arsenic S15-Jl04402 CP % 104 70-130 Pass

Lead S15-Jl04402 CP % 93 70-130 Pass


LimitsPass

LimitsQualifying

Code

Duplicate


Arsenic S15-Jl04401 CP mg/L < 0.01 < 0.01 <1 30% Pass

Lead S15-Jl04401 CP mg/L 0.09 0.09 1.0 30% Pass




Page 8 of 9


Comments









Code DescriptionC01 Leachate Fluid Key: 1 - pH 5.0; 2 - pH 2.9; 3 - pH 9.2; 4 - Reagent (DI) water; 5 - Client sample, 6 - other

Authorised By




Glenn Jackson








Page 9 of 9



MelbourneMelbourneMelbourneMelbourne3-5 Kingston Town CloseOakleigh Vic 3166Phone : +61 3 8564 5000NATA # 1261Site # 1254 & 14271

SydneySydneySydneySydneyUnit F3, Building F16 Mars RoadLane Cove West NSW 2066Phone : +61 2 9900 8400NATA # 1261 Site # 18217

BrisbaneBrisbaneBrisbaneBrisbane1/21 Smallwood PlaceMurarrie QLD 4172Phone : +61 7 3902 4600NATA # 1261 Site # 20794

Environmental LaboratoryAir AnalysisWater AnalysisSoil Contamination Analysis

NATA AccreditationStack Emission Sampling & AnalysisTrade Waste Sampling & AnalysisGroundwater Sampling & Analysis

38 Years of Environmental Analysis & Experience38 Years of Environmental Analysis & Experience38 Years of Environmental Analysis & Experience38 Years of Environmental Analysis & Experience

Sample Receipt AdviceSample Receipt AdviceSample Receipt AdviceSample Receipt Advice

Company name: Coffey Environments Pty Ltd WollongongCoffey Environments Pty Ltd WollongongCoffey Environments Pty Ltd WollongongCoffey Environments Pty Ltd Wollongong

Contact name: Alexander WilliamsProject name: ADDITIONAL : ENAUWOLL04223AACOC number: Not providedTurn around time: 4 DayDate/Time received: Jul 3, 2015 11:13 AMEurofins | mgt reference: 463922463922463922463922

Sample informationSample informationSample informationSample information

☑ A detailed list of analytes logged into our LIMS, is included in the attached summary table.

☑ Sample Temperature of a random sample selected from the batch as recorded by Eurofins | mgtSample Receipt : 6.5 degrees Celsius.

☑ All samples have been received as described on the above COC.

☑ COC has been completed correctly.

☑ Attempt to chill was evident.

☑ Appropriately preserved sample containers have been used.

☑ All samples were received in good condition.

☑ Samples have been provided with adequate time to commence analysis in accordance with therelevant holding times.

☑ Appropriate sample containers have been used.

☒ Some samples have been subcontracted.

N/A Custody Seals intact (if used).

NotesNotesNotesNotes

Additional from report

Contact notesContact notesContact notesContact notes

If you have any questions with respect to these samples please contact:

Charl Du Preez on Phone : or by e.mail: [email protected]

Results will be delivered electronically via e.mail to Alexander Williams - [email protected].





Sample Detail

Arsenic

CA

NC

ELLE

D

Lead

Zinc

Polycyclic A

romatic H

ydrocarbons

Polychlorinated B

iphenyls

US

A Leaching P

rocedure

Metals M

8

Benzo[a]pyrene

Halogenated V

olatile Organics

TR

H (after S

ilica Gel cleanup)

Moisture S

et





External Laboratory


Matrix LAB ID








QC2 Jun 22, 2015 TCLP S15-Jl04407 X X

CTP10/0.45-0.65

Jun 22, 2015 TCLP S15-Jl04408 X X

AB

N –

50

005

085

521

e.m

ail :

Env

iroS

ales

@eu

rofin

s.co

m.a

u

w

eb :

ww

w.e

urof

ins.

com

.au

Mel

bour

neM

elbo

urne

Mel

bour

neM

elbo

urne

3-5

Kin

gsto

n To

wn

Clo

seO

akle

igh

VIC

316

6P

hone

: +6

1 3

8564

500

0N

ATA

# 1

261

Site

# 1

254

& 1

4271

Syd

ney

Syd

ney

Syd

ney

Syd

ney

Uni

t F3,

Bui

ldin

g F

16 M

ars

Roa

dLa

ne C

ove

Wes

t NS

W 2

066

Pho

ne :

+61

2 99

00 8

400

NA

TA #

126

1 S

ite #

182

17

Bris

bane

Bris

bane

Bris

bane

Bris

bane

1/21

Sm

allw

ood

Pla

ceM

urar

rie Q

LD 4

172

Pho

ne :

+61

7 39

02 4

600

NA

TA #

126

1 S

ite #

207

94





Sample Detail

Arsenic

CA

NC

ELLE

D

Lead

Zinc

Polycyclic A

romatic H

ydrocarbons

Polychlorinated B

iphenyls

US

A Leaching P

rocedure

Metals M

8

Benzo[a]pyrene

Halogenated V

olatile Organics

TR

H (after S

ilica Gel cleanup)

Moisture S

et





External Laboratory










CTP06/0.75-0.85

Jun 22, 2015 Soil S15-Jl04418 X X X

CTP07/0.3-0.4 Jun 22, 2015 Soil S15-Jl04419 X

AB

N –

50

005

085

521

e.m

ail :

Env

iroS

ales

@eu

rofin

s.co

m.a

u

w

eb :

ww

w.e

urof

ins.

com

.au

Mel

bour

neM

elbo

urne

Mel

bour

neM

elbo

urne

3-5

Kin

gsto

n To

wn

Clo

seO

akle

igh

VIC

316

6P

hone

: +6

1 3

8564

500

0N

ATA

# 1

261

Site

# 1

254

& 1

4271

Syd

ney

Syd

ney

Syd

ney

Syd

ney

Uni

t F3,

Bui

ldin

g F

16 M

ars

Roa

dLa

ne C

ove

Wes

t NS

W 2

066

Pho

ne :

+61

2 99

00 8

400

NA

TA #

126

1 S

ite #

182

17

Bris

bane

Bris

bane

Bris

bane

Bris

bane

1/21

Sm

allw

ood

Pla

ceM

urar

rie Q

LD 4

172

Pho

ne :

+61

7 39

02 4

600

NA

TA #

126

1 S

ite #

207

94





Sample Detail

Arsenic

CA

NC

ELLE

D

Lead

Zinc

Polycyclic A

romatic H

ydrocarbons

Polychlorinated B

iphenyls

US

A Leaching P

rocedure

Metals M

8

Benzo[a]pyrene

Halogenated V

olatile Organics

TR

H (after S

ilica Gel cleanup)

Moisture S

et





External Laboratory



AB

N –

50

005

085

521

e.m

ail :

Env

iroS

ales

@eu

rofin

s.co

m.a

u

w

eb :

ww

w.e

urof

ins.

com

.au

Mel

bour

neM

elbo

urne

Mel

bour

neM

elbo

urne

3-5

Kin

gsto

n To

wn

Clo

seO

akle

igh

VIC

316

6P

hone

: +6

1 3

8564

500

0N

ATA

# 1

261

Site

# 1

254

& 1

4271

Syd

ney

Syd

ney

Syd

ney

Syd

ney

Uni

t F3,

Bui

ldin

g F

16 M

ars

Roa

dLa

ne C

ove

Wes

t NS

W 2

066

Pho

ne :

+61

2 99

00 8

400

NA

TA #

126

1 S

ite #

182

17

Bris

bane

Bris

bane

Bris

bane

Bris

bane

1/21

Sm

allw

ood

Pla

ceM

urar

rie Q

LD 4

172

Pho

ne :

+61

7 39

02 4

600

NA

TA #

126

1 S

ite #

207

94

4 4.00 True

CERTIFICATE OF ANALYSISWork Order : Page : 1 of 6ES1524748

:: LaboratoryClient COFFEY ENVIRONMENTS PTY LTD Environmental Division Sydney

: :ContactContact MR ALEXANDER WILLIAMS

:: AddressAddress LEVEL 19, 799 PACIFIC HIGHWAY Tower B - Citadel Tower

CHATSWOOD NSW, AUSTRALIA 2067

277-289 Woodpark Road Smithfield NSW Australia 2164

:: E-mailE-mail [email protected]

:: TelephoneTelephone +61 02 9406 1000 +61-2-8784 8555

:: FacsimileFacsimile ---- +61-2-8784 8500

:Project ENAVWOLL04223AA QC Level : NEPM 2013 Schedule B(3) and ALS QCS3 requirement

:Order number ---- Date Samples Received : 25-Jun-2015 11:00

:C-O-C number 9467 Date Analysis Commenced : 25-Jun-2015

Sampler : ALEXANDER WILLIAMS Issue Date : 02-Jul-2015 14:24

Site : ----

2:No. of samples received

Quote number : ---- 2:No. of samples analysed

This report supersedes any previous report(s) with this reference. Results apply to the sample(s) as submitted.

This Certificate of Analysis contains the following information:

l General Comments

l Analytical Results

SignatoriesThis document has been electronically signed by the authorized signatories indicated below. Electronic signing has been

carried out in compliance with procedures specified in 21 CFR Part 11.

Signatories Accreditation CategoryPosition

Ankit Joshi Inorganic Chemist Sydney Inorganics

Celine Conceicao Senior Spectroscopist Sydney Inorganics

Pabi Subba Senior Organic Chemist Sydney Inorganics

Pabi Subba Senior Organic Chemist Sydney Organics

NATA Accredited Laboratory 825

Accredited for compliance with

ISO/IEC 17025.

R I G H T S O L U T I O N S | R I G H T P A R T N E R

2 of 6:Page

Work Order :

:Client

ES1524748

ENAVWOLL04223AA:Project

COFFEY ENVIRONMENTS PTY LTD

General Comments

The analytical procedures used by the Environmental Division have been developed from established internationally recognized procedures such as those published by the USEPA, APHA, AS and NEPM. In house

developed procedures are employed in the absence of documented standards or by client request.

Where moisture determination has been performed, results are reported on a dry weight basis.

Where a reported less than (<) result is higher than the LOR, this may be due to primary sample extract/digestate dilution and/or insufficient sample for analysis.

Where the LOR of a reported result differs from standard LOR, this may be due to high moisture content, insufficient sample (reduced weight employed) or matrix interference.

When sampling time information is not provided by the client, sampling dates are shown without a time component. In these instances, the time component has been assumed by the laboratory for processing purposes.

CAS Number = CAS registry number from database maintained by Chemical Abstracts Services. The Chemical Abstracts Service is a division of the American Chemical Society.

LOR = Limit of reporting

^ = This result is computed from individual analyte detections at or above the level of reporting

ø = ALS is not NATA accredited for these tests.

Key :

EP071: Result of sample QC4A has been confirmed by re-extraction and re-analysis.l

Benzo(a)pyrene Toxicity Equivalent Quotient (TEQ) is the sum total of the concentration of the eight carcinogenic PAHs multiplied by their Toxicity Equivalence Factor (TEF) relative to Benzo(a)pyrene. TEF values

are provided in brackets as follows: Benz(a)anthracene (0.1), Chrysene (0.01), Benzo(b+j) & Benzo(k)fluoranthene (0.1), Benzo(a)pyrene (1.0), Indeno(1.2.3.cd)pyrene (0.1), Dibenz(a.h)anthracene (1.0),

Benzo(g.h.i)perylene (0.01). Less than LOR results for 'TEQ Zero' are treated as zero, for 'TEQ 1/2LOR' are treated as half the reported LOR, and for 'TEQ LOR' are treated as being equal to the reported LOR.

Note: TEQ 1/2LOR and TEQ LOR will calculate as 0.6mg/Kg and 1.2mg/Kg respectively for samples with non-detects for all of the eight TEQ PAHs.

l

3 of 6:Page

Work Order :

:Client

ES1524748



Analytical Results

------------QC4AQC2AClient sample IDSub-Matrix: SOIL

(Matrix: SOIL)

------------[23-Jun-2015][22-Jun-2015]Client sampling date / time

------------------------ES1524748-002ES1524748-001UnitLORCAS NumberCompound

Result Result Result Result Result

EA002 : pH (Soils)

6.3 6.5 ---- ---- ----pH Unit0.1----pH Value

EA010: Conductivity

28 22 ---- ---- ----µS/cm1----Electrical Conductivity @ 25°C

EA055: Moisture Content

21.1^ 24.4 ---- ---- ----%1----Moisture Content (dried @ 103°C)

EG005T: Total Metals by ICP-AES

10Arsenic <5 ---- ---- ----mg/kg57440-38-2

<1Cadmium <1 ---- ---- ----mg/kg17440-43-9

15Chromium 7 ---- ---- ----mg/kg27440-47-3

25Copper 9 ---- ---- ----mg/kg57440-50-8

236Lead 55 ---- ---- ----mg/kg57439-92-1

6Nickel 4 ---- ---- ----mg/kg27440-02-0

382Zinc 188 ---- ---- ----mg/kg57440-66-6

EG035T: Total Recoverable Mercury by FIMS

0.1Mercury <0.1 ---- ---- ----mg/kg0.17439-97-6

EP068A: Organochlorine Pesticides (OC)

<0.05alpha-BHC ---- ---- ---- ----mg/kg0.05319-84-6

<0.05Hexachlorobenzene (HCB) ---- ---- ---- ----mg/kg0.05118-74-1

<0.05beta-BHC ---- ---- ---- ----mg/kg0.05319-85-7

<0.05gamma-BHC ---- ---- ---- ----mg/kg0.0558-89-9

<0.05delta-BHC ---- ---- ---- ----mg/kg0.05319-86-8

<0.05Heptachlor ---- ---- ---- ----mg/kg0.0576-44-8

<0.05Aldrin ---- ---- ---- ----mg/kg0.05309-00-2

<0.05Heptachlor epoxide ---- ---- ---- ----mg/kg0.051024-57-3

<0.05^ ---- ---- ---- ----mg/kg0.05----Total Chlordane (sum)

<0.05trans-Chlordane ---- ---- ---- ----mg/kg0.055103-74-2

<0.05alpha-Endosulfan ---- ---- ---- ----mg/kg0.05959-98-8

<0.05cis-Chlordane ---- ---- ---- ----mg/kg0.055103-71-9

<0.05Dieldrin ---- ---- ---- ----mg/kg0.0560-57-1

<0.054.4`-DDE ---- ---- ---- ----mg/kg0.0572-55-9

<0.05Endrin ---- ---- ---- ----mg/kg0.0572-20-8

<0.05beta-Endosulfan ---- ---- ---- ----mg/kg0.0533213-65-9

<0.05^ Endosulfan (sum) ---- ---- ---- ----mg/kg0.05115-29-7

<0.054.4`-DDD ---- ---- ---- ----mg/kg0.0572-54-8

<0.05Endrin aldehyde ---- ---- ---- ----mg/kg0.057421-93-4

4 of 6:Page

Work Order :

:Client

ES1524748



Analytical Results


(Matrix: SOIL)




EP068A: Organochlorine Pesticides (OC) - Continued

<0.05Endosulfan sulfate ---- ---- ---- ----mg/kg0.051031-07-8

<0.24.4`-DDT ---- ---- ---- ----mg/kg0.250-29-3

<0.05Endrin ketone ---- ---- ---- ----mg/kg0.0553494-70-5

<0.2Methoxychlor ---- ---- ---- ----mg/kg0.272-43-5

<0.05^ Sum of Aldrin + Dieldrin ---- ---- ---- ----mg/kg0.05309-00-2/60-57-1

<0.05^ ---- ---- ---- ----mg/kg0.05----Sum of DDD + DDE + DDT

EP068B: Organophosphorus Pesticides (OP)

<0.05Dichlorvos ---- ---- ---- ----mg/kg0.0562-73-7

<0.05Demeton-S-methyl ---- ---- ---- ----mg/kg0.05919-86-8

<0.2Monocrotophos ---- ---- ---- ----mg/kg0.26923-22-4

<0.05Dimethoate ---- ---- ---- ----mg/kg0.0560-51-5

<0.05Diazinon ---- ---- ---- ----mg/kg0.05333-41-5

<0.05Chlorpyrifos-methyl ---- ---- ---- ----mg/kg0.055598-13-0

<0.2Parathion-methyl ---- ---- ---- ----mg/kg0.2298-00-0

<0.05Malathion ---- ---- ---- ----mg/kg0.05121-75-5

<0.05Fenthion ---- ---- ---- ----mg/kg0.0555-38-9

<0.05Chlorpyrifos ---- ---- ---- ----mg/kg0.052921-88-2

<0.2Parathion ---- ---- ---- ----mg/kg0.256-38-2

<0.05Pirimphos-ethyl ---- ---- ---- ----mg/kg0.0523505-41-1

<0.05Chlorfenvinphos ---- ---- ---- ----mg/kg0.05470-90-6

<0.05Bromophos-ethyl ---- ---- ---- ----mg/kg0.054824-78-6

<0.05Fenamiphos ---- ---- ---- ----mg/kg0.0522224-92-6

<0.05Prothiofos ---- ---- ---- ----mg/kg0.0534643-46-4

<0.05Ethion ---- ---- ---- ----mg/kg0.05563-12-2

<0.05Carbophenothion ---- ---- ---- ----mg/kg0.05786-19-6

<0.05Azinphos Methyl ---- ---- ---- ----mg/kg0.0586-50-0

EP075(SIM)B: Polynuclear Aromatic Hydrocarbons

<0.5Naphthalene <0.5 ---- ---- ----mg/kg0.591-20-3

<0.5Acenaphthylene <0.5 ---- ---- ----mg/kg0.5208-96-8

<0.5Acenaphthene <0.5 ---- ---- ----mg/kg0.583-32-9

<0.5Fluorene <0.5 ---- ---- ----mg/kg0.586-73-7

<0.5Phenanthrene <0.5 ---- ---- ----mg/kg0.585-01-8

<0.5Anthracene <0.5 ---- ---- ----mg/kg0.5120-12-7

1.2Fluoranthene <0.5 ---- ---- ----mg/kg0.5206-44-0

1.3Pyrene <0.5 ---- ---- ----mg/kg0.5129-00-0

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Analytical Results


(Matrix: SOIL)




EP075(SIM)B: Polynuclear Aromatic Hydrocarbons - Continued

0.6Benz(a)anthracene <0.5 ---- ---- ----mg/kg0.556-55-3

0.6Chrysene <0.5 ---- ---- ----mg/kg0.5218-01-9

0.7Benzo(b+j)fluoranthene <0.5 ---- ---- ----mg/kg0.5205-99-2 205-82-3

<0.5Benzo(k)fluoranthene <0.5 ---- ---- ----mg/kg0.5207-08-9

0.5Benzo(a)pyrene <0.5 ---- ---- ----mg/kg0.550-32-8

<0.5Indeno(1.2.3.cd)pyrene <0.5 ---- ---- ----mg/kg0.5193-39-5

<0.5Dibenz(a.h)anthracene <0.5 ---- ---- ----mg/kg0.553-70-3

<0.5Benzo(g.h.i)perylene <0.5 ---- ---- ----mg/kg0.5191-24-2

4.9^ <0.5 ---- ---- ----mg/kg0.5----Sum of polycyclic aromatic hydrocarbons

0.6^ <0.5 ---- ---- ----mg/kg0.5----Benzo(a)pyrene TEQ (zero)

0.9^ 0.6 ---- ---- ----mg/kg0.5----Benzo(a)pyrene TEQ (half LOR)

1.2^ 1.2 ---- ---- ----mg/kg0.5----Benzo(a)pyrene TEQ (LOR)

EP080/071: Total Petroleum Hydrocarbons

<10 <10 ---- ---- ----mg/kg10----C6 - C9 Fraction

<50 <50 ---- ---- ----mg/kg50----C10 - C14 Fraction

<100 <100 ---- ---- ----mg/kg100----C15 - C28 Fraction

<100 <100 ---- ---- ----mg/kg100----C29 - C36 Fraction

<50^ <50 ---- ---- ----mg/kg50----C10 - C36 Fraction (sum)

EP080/071: Total Recoverable Hydrocarbons - NEPM 2013 Fractions

<10C6 - C10 Fraction <10 ---- ---- ----mg/kg10C6_C10

<10^ C6 - C10 Fraction minus BTEX

(F1)

<10 ---- ---- ----mg/kg10C6_C10-BTEX

<50>C10 - C16 Fraction <50 ---- ---- ----mg/kg50>C10_C16

<100 160 ---- ---- ----mg/kg100---->C16 - C34 Fraction

<100 <100 ---- ---- ----mg/kg100---->C34 - C40 Fraction

<50^ 160 ---- ---- ----mg/kg50---->C10 - C40 Fraction (sum)

<50^ <50 ---- ---- ----mg/kg50---->C10 - C16 Fraction minus Naphthalene

(F2)

EP080: BTEXN

<0.2Benzene <0.2 ---- ---- ----mg/kg0.271-43-2

<0.5Toluene <0.5 ---- ---- ----mg/kg0.5108-88-3

<0.5Ethylbenzene <0.5 ---- ---- ----mg/kg0.5100-41-4

<0.5meta- & para-Xylene <0.5 ---- ---- ----mg/kg0.5108-38-3 106-42-3

<0.5ortho-Xylene <0.5 ---- ---- ----mg/kg0.595-47-6

<0.2^ <0.2 ---- ---- ----mg/kg0.2----Sum of BTEX

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Analytical Results


(Matrix: SOIL)




EP080: BTEXN - Continued

<0.5^ Total Xylenes <0.5 ---- ---- ----mg/kg0.51330-20-7

<1Naphthalene <1 ---- ---- ----mg/kg191-20-3

EP068S: Organochlorine Pesticide Surrogate

83.0Dibromo-DDE ---- ---- ---- ----%0.0521655-73-2

EP068T: Organophosphorus Pesticide Surrogate

80.7DEF ---- ---- ---- ----%0.0578-48-8

EP075(SIM)S: Phenolic Compound Surrogates

83.1Phenol-d6 88.0 ---- ---- ----%0.513127-88-3

88.22-Chlorophenol-D4 92.8 ---- ---- ----%0.593951-73-6

66.12.4.6-Tribromophenol 65.2 ---- ---- ----%0.5118-79-6

EP075(SIM)T: PAH Surrogates

84.42-Fluorobiphenyl 89.0 ---- ---- ----%0.5321-60-8

119Anthracene-d10 111 ---- ---- ----%0.51719-06-8

82.44-Terphenyl-d14 88.7 ---- ---- ----%0.51718-51-0

EP080S: TPH(V)/BTEX Surrogates

77.41.2-Dichloroethane-D4 81.2 ---- ---- ----%0.217060-07-0

85.4Toluene-D8 92.4 ---- ---- ----%0.22037-26-5

78.74-Bromofluorobenzene 80.7 ---- ---- ----%0.2460-00-4

False 4 4.00True

QUALITY CONTROL REPORTWork Order : ES1524748 Page : 1 of 10

:: LaboratoryClient Environmental Division SydneyCOFFEY ENVIRONMENTS PTY LTD

:Contact MR ALEXANDER WILLIAMS :Contact

:Address LEVEL 19, 799 PACIFIC HIGHWAY Tower B - Citadel Tower


Address : 277-289 Woodpark Road Smithfield NSW Australia 2164


::Telephone +61 02 9406 1000 +61-2-8784 8555:Telephone


QC Level : NEPM 2013 Schedule B(3) and ALS QCS3 requirement:Project ENAVWOLL04223AA

Date Samples Received : 25-Jun-2015:Order number ----

Date Analysis Commenced : 25-Jun-2015:C-O-C number 9467

Issue Date : 02-Jul-2015Sampler : ALEXANDER WILLIAMS

No. of samples received 2:Site : ----

No. of samples analysed 2:Quote number : ----

This report supersedes any previous report(s) with this reference. Results apply to the sample(s) as submitted.

This Quality Control Report contains the following information:

l Laboratory Duplicate (DUP) Report; Relative Percentage Difference (RPD) and Acceptance Limits

l Method Blank (MB) and Laboratory Control Spike (LCS) Report ; Recovery and Acceptance Limits

l Matrix Spike (MS) Report; Recovery and Acceptance Limits

SignatoriesThis document has been electronically signed by the authorized signatories indicated below. Electronic signing has been carried out in

compliance with procedures specified in 21 CFR Part 11.

Signatories Accreditation CategoryPosition

Ankit Joshi Inorganic Chemist Sydney Inorganics

Celine Conceicao Senior Spectroscopist Sydney Inorganics

Pabi Subba Senior Organic Chemist Sydney Inorganics

Pabi Subba Senior Organic Chemist Sydney Organics

NATA Accredited

Laboratory 825

Accredited for

compliance with

ISO/IEC 17025.


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General Comments

The analytical procedures used by the Environmental Division have been developed from established internationally recognized procedures such as those published by the USEPA, APHA, AS and NEPM. In house

developed procedures are employed in the absence of documented standards or by client request.

Where moisture determination has been performed, results are reported on a dry weight basis.

Where a reported less than (<) result is higher than the LOR, this may be due to primary sample extract/digestate dilution and/or insufficient sample for analysis. Where the LOR of a reported result differs from standard LOR, this may be due to high moisture content, insufficient sample (reduced weight employed) or matrix interference.

Anonymous = Refers to samples which are not specifically part of this work order but formed part of the QC process lot

CAS Number = CAS registry number from database maintained by Chemical Abstracts Services. The Chemical Abstracts Service is a division of the American Chemical Society.

LOR = Limit of reporting

RPD = Relative Percentage Difference

# = Indicates failed QC

Key :

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Laboratory Duplicate (DUP) Report

The quality control term Laboratory Duplicate refers to a randomly selected intralaboratory split. Laboratory duplicates provide information regarding method precision and sample heterogeneity. The permitted ranges

for the Relative Percent Deviation (RPD) of Laboratory Duplicates are specified in ALS Method QWI -EN/38 and are dependent on the magnitude of results in comparison to the level of reporting: Result < 10 times LOR:

No Limit; Result between 10 and 20 times LOR:- 0% - 50%; Result > 20 times LOR:0% - 20%.

Sub-Matrix: SOIL Laboratory Duplicate (DUP) Report

Original Result RPD (%)Laboratory sample ID Client sample ID Method: Compound CAS Number LOR Unit Duplicate Result Recovery Limits (%)

EA002 : pH (Soils) (QC Lot: 137388)

EA002: pH Value ---- 0.1 pH Unit 5.4 5.3 0.00 0% - 20%Anonymous ES1524724-001

EA002: pH Value ---- 0.1 pH Unit 8.5 8.7 2.33 0% - 20%Anonymous ES1524725-002

EA010: Conductivity (QC Lot: 137389)

EA010: Electrical Conductivity @ 25°C ---- 1 µS/cm 311 294 5.52 0% - 20%Anonymous ES1524724-001

EA010: Electrical Conductivity @ 25°C ---- 1 µS/cm 298 283 5.19 0% - 20%Anonymous ES1524725-002

EA055: Moisture Content (QC Lot: 136561)

EA055-103: Moisture Content (dried @ 103°C) ---- 1 % 15.8 15.3 3.15 0% - 50%Anonymous ES1524724-009

EA055-103: Moisture Content (dried @ 103°C) ---- 1 % 24.4 23.0 6.01 0% - 20%QC4A ES1524748-002

EG005T: Total Metals by ICP-AES (QC Lot: 138797)

EG005T: Cadmium 7440-43-9 1 mg/kg <1 <1 0.00 No LimitAnonymous ES1524729-006

EG005T: Chromium 7440-47-3 2 mg/kg 25 21 18.4 0% - 50%

EG005T: Nickel 7440-02-0 2 mg/kg 6 6 0.00 No Limit

EG005T: Arsenic 7440-38-2 5 mg/kg <5 <5 0.00 No Limit

EG005T: Copper 7440-50-8 5 mg/kg 11 12 0.00 No Limit

EG005T: Lead 7439-92-1 5 mg/kg 10 10 0.00 No Limit

EG005T: Zinc 7440-66-6 5 mg/kg 12 13 8.07 No Limit

EG005T: Cadmium 7440-43-9 1 mg/kg <1 <1 0.00 No LimitQC2A ES1524748-001

EG005T: Chromium 7440-47-3 2 mg/kg 15 18 19.7 No Limit

EG005T: Nickel 7440-02-0 2 mg/kg 6 6 0.00 No Limit

EG005T: Arsenic 7440-38-2 5 mg/kg 10 12 20.2 No Limit

EG005T: Copper 7440-50-8 5 mg/kg 25 27 4.74 No Limit

EG005T: Lead 7439-92-1 5 mg/kg 236 231 1.84 0% - 20%

EG005T: Zinc 7440-66-6 5 mg/kg 382 416 8.58 0% - 20%

EG035T: Total Recoverable Mercury by FIMS (QC Lot: 138798)

EG035T: Mercury 7439-97-6 0.1 mg/kg <0.1 <0.1 0.00 No LimitAnonymous ES1524729-006

EG035T: Mercury 7439-97-6 0.1 mg/kg 0.1 0.1 0.00 No LimitQC2A ES1524748-001

EP068A: Organochlorine Pesticides (OC) (QC Lot: 136517)

EP068: 4.4`-DDD 72-54-8 0.05 mg/kg <0.05 <0.05 0.00 No LimitQC2A ES1524748-001

EP068: 4.4`-DDE 72-55-9 0.05 mg/kg <0.05 <0.05 0.00 No Limit

EP068: Aldrin 309-00-2 0.05 mg/kg <0.05 <0.05 0.00 No Limit

EP068: alpha-BHC 319-84-6 0.05 mg/kg <0.05 <0.05 0.00 No Limit

EP068: alpha-Endosulfan 959-98-8 0.05 mg/kg <0.05 <0.05 0.00 No Limit

EP068: beta-BHC 319-85-7 0.05 mg/kg <0.05 <0.05 0.00 No Limit

EP068: beta-Endosulfan 33213-65-9 0.05 mg/kg <0.05 <0.05 0.00 No Limit

EP068: cis-Chlordane 5103-71-9 0.05 mg/kg <0.05 <0.05 0.00 No Limit

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EP068A: Organochlorine Pesticides (OC) (QC Lot: 136517) - continued

EP068: delta-BHC 319-86-8 0.05 mg/kg <0.05 <0.05 0.00 No LimitQC2A ES1524748-001

EP068: Dieldrin 60-57-1 0.05 mg/kg <0.05 <0.05 0.00 No Limit

EP068: Endosulfan sulfate 1031-07-8 0.05 mg/kg <0.05 <0.05 0.00 No Limit

EP068: Endrin 72-20-8 0.05 mg/kg <0.05 <0.05 0.00 No Limit

EP068: Endrin aldehyde 7421-93-4 0.05 mg/kg <0.05 <0.05 0.00 No Limit

EP068: Endrin ketone 53494-70-5 0.05 mg/kg <0.05 <0.05 0.00 No Limit

EP068: gamma-BHC 58-89-9 0.05 mg/kg <0.05 <0.05 0.00 No Limit

EP068: Heptachlor 76-44-8 0.05 mg/kg <0.05 <0.05 0.00 No Limit

EP068: Heptachlor epoxide 1024-57-3 0.05 mg/kg <0.05 <0.05 0.00 No Limit

EP068: Hexachlorobenzene (HCB) 118-74-1 0.05 mg/kg <0.05 <0.05 0.00 No Limit

EP068: trans-Chlordane 5103-74-2 0.05 mg/kg <0.05 <0.05 0.00 No Limit

EP068: 4.4`-DDT 50-29-3 0.2 mg/kg <0.2 <0.2 0.00 No Limit

EP068: Methoxychlor 72-43-5 0.2 mg/kg <0.2 <0.2 0.00 No Limit

EP068B: Organophosphorus Pesticides (OP) (QC Lot: 136517)

EP068: Azinphos Methyl 86-50-0 0.05 mg/kg <0.05 <0.05 0.00 No LimitQC2A ES1524748-001

EP068: Bromophos-ethyl 4824-78-6 0.05 mg/kg <0.05 <0.05 0.00 No Limit

EP068: Carbophenothion 786-19-6 0.05 mg/kg <0.05 <0.05 0.00 No Limit

EP068: Chlorfenvinphos 470-90-6 0.05 mg/kg <0.05 <0.05 0.00 No Limit

EP068: Chlorpyrifos 2921-88-2 0.05 mg/kg <0.05 <0.05 0.00 No Limit

EP068: Chlorpyrifos-methyl 5598-13-0 0.05 mg/kg <0.05 <0.05 0.00 No Limit

EP068: Demeton-S-methyl 919-86-8 0.05 mg/kg <0.05 <0.05 0.00 No Limit

EP068: Diazinon 333-41-5 0.05 mg/kg <0.05 <0.05 0.00 No Limit

EP068: Dichlorvos 62-73-7 0.05 mg/kg <0.05 <0.05 0.00 No Limit

EP068: Dimethoate 60-51-5 0.05 mg/kg <0.05 <0.05 0.00 No Limit

EP068: Ethion 563-12-2 0.05 mg/kg <0.05 <0.05 0.00 No Limit

EP068: Fenamiphos 22224-92-6 0.05 mg/kg <0.05 <0.05 0.00 No Limit

EP068: Fenthion 55-38-9 0.05 mg/kg <0.05 <0.05 0.00 No Limit

EP068: Malathion 121-75-5 0.05 mg/kg <0.05 <0.05 0.00 No Limit

EP068: Pirimphos-ethyl 23505-41-1 0.05 mg/kg <0.05 <0.05 0.00 No Limit

EP068: Prothiofos 34643-46-4 0.05 mg/kg <0.05 <0.05 0.00 No Limit

EP068: Monocrotophos 6923-22-4 0.2 mg/kg <0.2 <0.2 0.00 No Limit

EP068: Parathion 56-38-2 0.2 mg/kg <0.2 <0.2 0.00 No Limit

EP068: Parathion-methyl 298-00-0 0.2 mg/kg <0.2 <0.2 0.00 No Limit

EP075(SIM)B: Polynuclear Aromatic Hydrocarbons (QC Lot: 136516)

EP075(SIM): Acenaphthene 83-32-9 0.5 mg/kg <0.5 <0.5 0.00 No LimitAnonymous ES1524351-004

EP075(SIM): Acenaphthylene 208-96-8 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP075(SIM): Anthracene 120-12-7 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP075(SIM): Benz(a)anthracene 56-55-3 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP075(SIM): Benzo(a)pyrene 50-32-8 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP075(SIM): Benzo(a)pyrene TEQ (zero) ---- 0.5 mg/kg <0.5 <0.5 0.00 No Limit

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EP075(SIM)B: Polynuclear Aromatic Hydrocarbons (QC Lot: 136516) - continued

EP075(SIM): Benzo(b+j)fluoranthene 205-99-2

205-82-3

0.5 mg/kg <0.5 <0.5 0.00 No LimitAnonymous ES1524351-004

EP075(SIM): Benzo(g.h.i)perylene 191-24-2 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP075(SIM): Benzo(k)fluoranthene 207-08-9 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP075(SIM): Chrysene 218-01-9 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP075(SIM): Dibenz(a.h)anthracene 53-70-3 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP075(SIM): Fluoranthene 206-44-0 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP075(SIM): Fluorene 86-73-7 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP075(SIM): Indeno(1.2.3.cd)pyrene 193-39-5 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP075(SIM): Naphthalene 91-20-3 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP075(SIM): Phenanthrene 85-01-8 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP075(SIM): Pyrene 129-00-0 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP075(SIM): Sum of polycyclic aromatic

hydrocarbons

---- 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP080/071: Total Petroleum Hydrocarbons (QC Lot: 136515)

EP071: C15 - C28 Fraction ---- 100 mg/kg 200 240 15.8 No LimitAnonymous ES1524351-067

EP071: C29 - C36 Fraction ---- 100 mg/kg 160 210 25.4 No Limit

EP071: C10 - C14 Fraction ---- 50 mg/kg <50 <50 0.00 No Limit

EP071: C15 - C28 Fraction ---- 100 mg/kg <100 <100 0.00 No LimitAnonymous ES1524351-004



EP080/071: Total Petroleum Hydrocarbons (QC Lot: 137009)



EP080/071: Total Recoverable Hydrocarbons - NEPM 2013 Fractions (QC Lot: 136515)

EP071: >C16 - C34 Fraction ---- 100 mg/kg 320 390 19.7 No LimitAnonymous ES1524351-067

EP071: >C34 - C40 Fraction ---- 100 mg/kg <100 <100 0.00 No Limit

EP071: >C10 - C16 Fraction >C10_C16 50 mg/kg <50 <50 0.00 No Limit

EP071: >C16 - C34 Fraction ---- 100 mg/kg <100 <100 0.00 No LimitAnonymous ES1524351-004

EP071: >C34 - C40 Fraction ---- 100 mg/kg <100 <100 0.00 No Limit

EP071: >C10 - C16 Fraction >C10_C16 50 mg/kg <50 <50 0.00 No Limit

EP080/071: Total Recoverable Hydrocarbons - NEPM 2013 Fractions (QC Lot: 137009)

EP080: C6 - C10 Fraction C6_C10 10 mg/kg <10 <10 0.00 No LimitAnonymous ES1524734-001

EP080: C6 - C10 Fraction C6_C10 10 mg/kg <10 <10 0.00 No LimitAnonymous ES1524737-001

EP080: BTEXN (QC Lot: 137009)

EP080: Benzene 71-43-2 0.2 mg/kg <0.2 <0.2 0.00 No LimitAnonymous ES1524734-001

EP080: Ethylbenzene 100-41-4 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP080: meta- & para-Xylene 108-38-3

106-42-3

0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP080: ortho-Xylene 95-47-6 0.5 mg/kg <0.5 <0.5 0.00 No Limit

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EP080: BTEXN (QC Lot: 137009) - continued

EP080: Toluene 108-88-3 0.5 mg/kg <0.5 <0.5 0.00 No LimitAnonymous ES1524734-001

EP080: Naphthalene 91-20-3 1 mg/kg <1 <1 0.00 No Limit

EP080: Benzene 71-43-2 0.2 mg/kg <0.2 <0.2 0.00 No LimitAnonymous ES1524737-001

EP080: Ethylbenzene 100-41-4 0.5 mg/kg <0.5 <0.5 0.00 No Limit


106-42-3

0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP080: ortho-Xylene 95-47-6 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP080: Toluene 108-88-3 0.5 mg/kg <0.5 <0.5 0.00 No Limit

EP080: Naphthalene 91-20-3 1 mg/kg <1 <1 0.00 No Limit

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Method Blank (MB) and Laboratory Control Spike (LCS) Report

The quality control term Method / Laboratory Blank refers to an analyte free matrix to which all reagents are added in the same volumes or proportions as used in standard sample preparation. The purpose of this QC

parameter is to monitor potential laboratory contamination. The quality control term Laboratory Control Sample (LCS) refers to a certified reference material, or a known interference free matrix spiked with target

analytes. The purpose of this QC parameter is to monitor method precision and accuracy independent of sample matrix. Dynamic Recovery Limits are based on statistical evaluation of processed LCS.

Sub-Matrix: SOIL Method Blank (MB)

Report

Laboratory Control Spike (LCS) Report

Spike Spike Recovery (%) Recovery Limits (%)

Result Concentration HighLowLCSMethod: Compound CAS Number LOR Unit

EA010: Conductivity (QCLot: 137389)

EA010: Electrical Conductivity @ 25°C ---- 1 µS/cm <1 95.41412 µS/cm 13070

EG005T: Total Metals by ICP-AES (QCLot: 138797)

EG005T: Arsenic 7440-38-2 5 mg/kg <5 11721.7 mg/kg 13092

EG005T: Cadmium 7440-43-9 1 mg/kg <1 1014.64 mg/kg 12187

EG005T: Chromium 7440-47-3 2 mg/kg <2 10043.9 mg/kg 13680

EG005T: Copper 7440-50-8 5 mg/kg <5 10232 mg/kg 12793

EG005T: Lead 7439-92-1 5 mg/kg <5 10940 mg/kg 12486

EG005T: Nickel 7440-02-0 2 mg/kg <2 10655 mg/kg 13193

EG005T: Zinc 7440-66-6 5 mg/kg <5 10860.8 mg/kg 13381

EG035T: Total Recoverable Mercury by FIMS (QCLot: 138798)

EG035T: Mercury 7439-97-6 0.1 mg/kg <0.1 88.32.57 mg/kg 10570

EP068A: Organochlorine Pesticides (OC) (QCLot: 136517)

EP068: 4.4`-DDD 72-54-8 0.05 mg/kg <0.05 98.60.5 mg/kg 12076

EP068: 4.4`-DDE 72-55-9 0.05 mg/kg <0.05 97.00.5 mg/kg 11769

EP068: 4.4`-DDT 50-29-3 0.2 mg/kg <0.2 83.30.5 mg/kg 12767

EP068: Aldrin 309-00-2 0.05 mg/kg <0.05 97.90.5 mg/kg 11868

EP068: alpha-BHC 319-84-6 0.05 mg/kg <0.05 99.60.5 mg/kg 11371

EP068: alpha-Endosulfan 959-98-8 0.05 mg/kg <0.05 91.30.5 mg/kg 11969

EP068: beta-BHC 319-85-7 0.05 mg/kg <0.05 1000.5 mg/kg 11969

EP068: beta-Endosulfan 33213-65-9 0.05 mg/kg <0.05 95.60.5 mg/kg 12076

EP068: cis-Chlordane 5103-71-9 0.05 mg/kg <0.05 98.90.5 mg/kg 12167

EP068: delta-BHC 319-86-8 0.05 mg/kg <0.05 87.60.5 mg/kg 11365

EP068: Dieldrin 60-57-1 0.05 mg/kg <0.05 95.50.5 mg/kg 11866

EP068: Endosulfan sulfate 1031-07-8 0.05 mg/kg <0.05 83.00.5 mg/kg 12460

EP068: Endrin 72-20-8 0.05 mg/kg <0.05 87.50.5 mg/kg 12367

EP068: Endrin aldehyde 7421-93-4 0.05 mg/kg <0.05 80.50.5 mg/kg 11557

EP068: Endrin ketone 53494-70-5 0.05 mg/kg <0.05 90.70.5 mg/kg 12365

EP068: gamma-BHC 58-89-9 0.05 mg/kg <0.05 99.70.5 mg/kg 11571

EP068: Heptachlor 76-44-8 0.05 mg/kg <0.05 95.60.5 mg/kg 11668

EP068: Heptachlor epoxide 1024-57-3 0.05 mg/kg <0.05 99.50.5 mg/kg 11668

EP068: Hexachlorobenzene (HCB) 118-74-1 0.05 mg/kg <0.05 96.70.5 mg/kg 12266

EP068: Methoxychlor 72-43-5 0.2 mg/kg <0.2 74.90.5 mg/kg 12965

EP068: trans-Chlordane 5103-74-2 0.05 mg/kg <0.05 99.00.5 mg/kg 12068

EP068B: Organophosphorus Pesticides (OP) (QCLot: 136517)

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EP068B: Organophosphorus Pesticides (OP) (QCLot: 136517) - continued

EP068: Azinphos Methyl 86-50-0 0.05 mg/kg <0.05 95.70.5 mg/kg 12642

EP068: Bromophos-ethyl 4824-78-6 0.05 mg/kg <0.05 1030.5 mg/kg 11668

EP068: Carbophenothion 786-19-6 0.05 mg/kg <0.05 1010.5 mg/kg 12367

EP068: Chlorfenvinphos 470-90-6 0.05 mg/kg <0.05 87.60.5 mg/kg 11870

EP068: Chlorpyrifos 2921-88-2 0.05 mg/kg <0.05 1020.5 mg/kg 11468

EP068: Chlorpyrifos-methyl 5598-13-0 0.05 mg/kg <0.05 89.10.5 mg/kg 11955

EP068: Demeton-S-methyl 919-86-8 0.05 mg/kg <0.05 86.00.5 mg/kg 12864

EP068: Diazinon 333-41-5 0.05 mg/kg <0.05 1020.5 mg/kg 11773

EP068: Dichlorvos 62-73-7 0.05 mg/kg <0.05 94.60.5 mg/kg 12656

EP068: Dimethoate 60-51-5 0.05 mg/kg <0.05 92.80.5 mg/kg 12464

EP068: Ethion 563-12-2 0.05 mg/kg <0.05 96.00.5 mg/kg 11870

EP068: Fenamiphos 22224-92-6 0.05 mg/kg <0.05 81.40.5 mg/kg 12064

EP068: Fenthion 55-38-9 0.05 mg/kg <0.05 1010.5 mg/kg 11571

EP068: Malathion 121-75-5 0.05 mg/kg <0.05 78.00.5 mg/kg 12070

EP068: Monocrotophos 6923-22-4 0.2 mg/kg <0.2 1080.5 mg/kg 12254

EP068: Parathion 56-38-2 0.2 mg/kg <0.2 81.60.5 mg/kg 12268

EP068: Parathion-methyl 298-00-0 0.2 mg/kg <0.2 93.40.5 mg/kg 12369

EP068: Pirimphos-ethyl 23505-41-1 0.05 mg/kg <0.05 1020.5 mg/kg 11569

EP068: Prothiofos 34643-46-4 0.05 mg/kg <0.05 1030.5 mg/kg 11668

EP075(SIM)B: Polynuclear Aromatic Hydrocarbons (QCLot: 136516)

EP075(SIM): Acenaphthene 83-32-9 0.5 mg/kg <0.5 1026 mg/kg 12379

EP075(SIM): Acenaphthylene 208-96-8 0.5 mg/kg <0.5 91.96 mg/kg 12377

EP075(SIM): Anthracene 120-12-7 0.5 mg/kg <0.5 97.56 mg/kg 12379

EP075(SIM): Benz(a)anthracene 56-55-3 0.5 mg/kg <0.5 92.06 mg/kg 12173

EP075(SIM): Benzo(a)pyrene 50-32-8 0.5 mg/kg <0.5 95.26 mg/kg 12276

EP075(SIM): Benzo(b+j)fluoranthene 205-99-2

205-82-3

0.5 mg/kg <0.5 98.76 mg/kg 11870

EP075(SIM): Benzo(g.h.i)perylene 191-24-2 0.5 mg/kg <0.5 1006 mg/kg 11472

EP075(SIM): Benzo(k)fluoranthene 207-08-9 0.5 mg/kg <0.5 1016 mg/kg 12377

EP075(SIM): Chrysene 218-01-9 0.5 mg/kg <0.5 93.46 mg/kg 12381

EP075(SIM): Dibenz(a.h)anthracene 53-70-3 0.5 mg/kg <0.5 90.66 mg/kg 11372

EP075(SIM): Fluoranthene 206-44-0 0.5 mg/kg <0.5 87.86 mg/kg 12379

EP075(SIM): Fluorene 86-73-7 0.5 mg/kg <0.5 1016 mg/kg 12377

EP075(SIM): Indeno(1.2.3.cd)pyrene 193-39-5 0.5 mg/kg <0.5 89.16 mg/kg 11371

EP075(SIM): Naphthalene 91-20-3 0.5 mg/kg <0.5 1006 mg/kg 12480

EP075(SIM): Phenanthrene 85-01-8 0.5 mg/kg <0.5 99.96 mg/kg 12379

EP075(SIM): Pyrene 129-00-0 0.5 mg/kg <0.5 91.86 mg/kg 12579

EP080/071: Total Petroleum Hydrocarbons (QCLot: 136515)

EP071: C10 - C14 Fraction ---- 50 mg/kg <50 103200 mg/kg 13171

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EP080/071: Total Petroleum Hydrocarbons (QCLot: 136515) - continued




EP080: C6 - C9 Fraction ---- 10 mg/kg <10 89.326 mg/kg 12868

EP080/071: Total Recoverable Hydrocarbons - NEPM 2013 Fractions (QCLot: 136515)

EP071: >C10 - C16 Fraction >C10_C16 50 mg/kg <50 105250 mg/kg 13070

EP071: >C16 - C34 Fraction ---- 100 mg/kg <100 116350 mg/kg 13874

EP071: >C34 - C40 Fraction ---- 100 mg/kg <100 87.5200 mg/kg 13163


EP080: C6 - C10 Fraction C6_C10 10 mg/kg <10 88.831 mg/kg 12868

EP080: BTEXN (QCLot: 137009)

EP080: Benzene 71-43-2 0.2 mg/kg <0.2 84.91 mg/kg 11662

EP080: Ethylbenzene 100-41-4 0.5 mg/kg <0.5 82.41 mg/kg 11858


106-42-3

0.5 mg/kg <0.5 86.62 mg/kg 12060

EP080: Naphthalene 91-20-3 1 mg/kg <1 85.91 mg/kg 13862

EP080: ortho-Xylene 95-47-6 0.5 mg/kg <0.5 91.71 mg/kg 12060

EP080: Toluene 108-88-3 0.5 mg/kg <0.5 94.91 mg/kg 12862

Matrix Spike (MS) ReportThe quality control term Matrix Spike (MS) refers to an intralaboratory split sample spiked with a representative set of target analytes. The purpose of this QC parameter is to monitor potential matrix effects on

analyte recoveries. Static Recovery Limits as per laboratory Data Quality Objectives (DQOs). Ideal recovery ranges stated may be waived in the event of sample matrix interference.

Sub-Matrix: SOIL Matrix Spike (MS) Report

SpikeRecovery(%) Recovery Limits (%)Spike

HighLowMSConcentrationLaboratory sample ID Client sample ID Method: Compound CAS Number

EG005T: Total Metals by ICP-AES (QCLot: 138797)

Anonymous ES1524729-006 7440-38-2EG005T: Arsenic 11650 mg/kg 13070

7440-43-9EG005T: Cadmium 10750 mg/kg 13070

7440-47-3EG005T: Chromium 10050 mg/kg 13070

7440-50-8EG005T: Copper 109250 mg/kg 13070

7439-92-1EG005T: Lead 106250 mg/kg 13070

7440-02-0EG005T: Nickel 10550 mg/kg 13070

7440-66-6EG005T: Zinc 107250 mg/kg 13070

EG035T: Total Recoverable Mercury by FIMS (QCLot: 138798)

Anonymous ES1524729-006 7439-97-6EG035T: Mercury 74.85 mg/kg 13070

EP068A: Organochlorine Pesticides (OC) (QCLot: 136517)

QC2A ES1524748-001 50-29-3EP068: 4.4`-DDT 76.12 mg/kg 13070

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Sub-Matrix: SOIL Matrix Spike (MS) Report

SpikeRecovery(%) Recovery Limits (%)Spike

HighLowMSConcentrationLaboratory sample ID Client sample ID Method: Compound CAS Number

EP068A: Organochlorine Pesticides (OC) (QCLot: 136517) - continued

QC2A ES1524748-001 309-00-2EP068: Aldrin 77.20.5 mg/kg 13070

60-57-1EP068: Dieldrin 80.70.5 mg/kg 13070

72-20-8EP068: Endrin 91.92 mg/kg 13070

58-89-9EP068: gamma-BHC 91.10.5 mg/kg 13070

76-44-8EP068: Heptachlor 81.80.5 mg/kg 13070

EP068B: Organophosphorus Pesticides (OP) (QCLot: 136517)

QC2A ES1524748-001 4824-78-6EP068: Bromophos-ethyl 80.00.5 mg/kg 13070

5598-13-0EP068: Chlorpyrifos-methyl 92.70.5 mg/kg 13070

333-41-5EP068: Diazinon 80.10.5 mg/kg 13070

23505-41-1EP068: Pirimphos-ethyl 80.40.5 mg/kg 13070

34643-46-4EP068: Prothiofos 76.60.5 mg/kg 13070

EP075(SIM)B: Polynuclear Aromatic Hydrocarbons (QCLot: 136516)

Anonymous ES1524351-004 83-32-9EP075(SIM): Acenaphthene 10210 mg/kg 13070

129-00-0EP075(SIM): Pyrene 11610 mg/kg 13070


Anonymous ES1524351-004 ----EP071: C10 - C14 Fraction 106523 mg/kg 13773

----EP071: C15 - C28 Fraction 1042319 mg/kg 13153

----EP071: C29 - C36 Fraction 1261714 mg/kg 13252


Anonymous ES1524734-001 ----EP080: C6 - C9 Fraction 10232.5 mg/kg 13070


Anonymous ES1524351-004 >C10_C16EP071: >C10 - C16 Fraction 99.8860 mg/kg 13773

----EP071: >C16 - C34 Fraction 1223223 mg/kg 13153

----EP071: >C34 - C40 Fraction 1071058 mg/kg 13252


Anonymous ES1524734-001 C6_C10EP080: C6 - C10 Fraction 10137.5 mg/kg 13070

EP080: BTEXN (QCLot: 137009)

Anonymous ES1524734-001 71-43-2EP080: Benzene 92.32.5 mg/kg 13070

100-41-4EP080: Ethylbenzene 91.62.5 mg/kg 13070

108-38-3

106-42-3

EP080: meta- & para-Xylene 88.82.5 mg/kg 13070

91-20-3EP080: Naphthalene 88.52.5 mg/kg 13070

95-47-6EP080: ortho-Xylene 1012.5 mg/kg 13070

108-88-3EP080: Toluene 91.62.5 mg/kg 13070

True

QA/QC Compliance Assessment for DQO ReportingWork Order : ES1524748 Page : 1 of 5


:Contact MR ALEXANDER WILLIAMS Telephone : +61-2-8784 8555

:Project ENAVWOLL04223AA Date Samples Received : 25-Jun-2015

Site : ---- Issue Date : 02-Jul-2015

ALEXANDER WILLIAMS:Sampler No. of samples received : 2

:Order number ---- No. of samples analysed : 2

This report is automatically generated by the ALS LIMS through interpretation of the ALS Quality Control Report and several Quality Assurance parameters measured by ALS. This automated

reporting highlights any non-conformances, facilitates faster and more accurate data validation and is designed to assist internal expert and external Auditor review. Many components of this

report contribute to the overall DQO assessment and reporting for guideline compliance.

Brief method summaries and references are also provided to assist in traceability.

Summary of Outliers

Outliers : Quality Control Samples

This report highlights outliers flagged in the Quality Control (QC) Report.

l NO Method Blank value outliers occur.

l NO Duplicate outliers occur.

l NO Laboratory Control outliers occur.

l NO Matrix Spike outliers occur.

l For all regular sample matrices, NO surrogate recovery outliers occur.

Outliers : Analysis Holding Time Compliance

l NO Analysis Holding Time Outliers exist.

Outliers : Frequency of Quality Control Samples

l NO Quality Control Sample Frequency Outliers exist.


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This report summarizes extraction / preparation and analysis times and compares each with ALS recommended holding times (referencing USEPA SW 846, APHA, AS and NEPM) based on the sample container

provided. Dates reported represent first date of extraction or analysis and preclude subsequent dilutions and reruns. A listing of breaches (if any) is provided herein.

Holding time for leachate methods (e.g. TCLP) vary according to the analytes reported. Assessment compares the leach date with the shortest analyte holding time for the equivalent soil method. These are: organics

14 days, mercury 28 days & other metals 180 days. A recorded breach does not guarantee a breach for all non-volatile parameters.

Holding times for VOC in soils vary according to analytes of interest. Vinyl Chloride and Styrene holding time is 7 days; others 14 days. A recorded breach does not guarantee a breach for all VOC analytes and

should be verified in case the reported breach is a false positive or Vinyl Chloride and Styrene are not key analytes of interest/concern.

Analysis Holding Time Compliance

Matrix: SOIL Evaluation: û = Holding time breach ; ü = Within holding time.

AnalysisExtraction / PreparationSample DateMethod

EvaluationDue for analysisDate analysedEvaluationDue for extractionDate extractedContainer / Client Sample ID(s)

EA002 : pH (Soils)

Soil Glass Jar - Unpreserved (EA002)

QC2A 26-Jun-201529-Jun-2015 26-Jun-201526-Jun-201522-Jun-2015 ü üSoil Glass Jar - Unpreserved (EA002)

QC4A 26-Jun-201530-Jun-2015 26-Jun-201526-Jun-201523-Jun-2015 ü üEA010: Conductivity

Soil Glass Jar - Unpreserved (EA010)

QC2A 24-Jul-201529-Jun-2015 26-Jun-201526-Jun-201522-Jun-2015 ü üSoil Glass Jar - Unpreserved (EA010)

QC4A 24-Jul-201530-Jun-2015 26-Jun-201526-Jun-201523-Jun-2015 ü üEA055: Moisture Content

Soil Glass Jar - Unpreserved (EA055-103)

QC2A 06-Jul-2015---- 25-Jun-2015----22-Jun-2015 ---- üSoil Glass Jar - Unpreserved (EA055-103)

QC4A 07-Jul-2015---- 25-Jun-2015----23-Jun-2015 ---- üEG005T: Total Metals by ICP-AES

Soil Glass Jar - Unpreserved (EG005T)

QC2A 19-Dec-201519-Dec-2015 29-Jun-201529-Jun-201522-Jun-2015 ü üSoil Glass Jar - Unpreserved (EG005T)

QC4A 20-Dec-201520-Dec-2015 29-Jun-201529-Jun-201523-Jun-2015 ü üEG035T: Total Recoverable Mercury by FIMS

Soil Glass Jar - Unpreserved (EG035T)

QC2A 20-Jul-201520-Jul-2015 01-Jul-201529-Jun-201522-Jun-2015 ü üSoil Glass Jar - Unpreserved (EG035T)

QC4A 21-Jul-201521-Jul-2015 01-Jul-201529-Jun-201523-Jun-2015 ü üEP068A: Organochlorine Pesticides (OC)

Soil Glass Jar - Unpreserved (EP068)

QC2A 04-Aug-201506-Jul-2015 27-Jun-201525-Jun-201522-Jun-2015 ü üEP080/071: Total Petroleum Hydrocarbons


QC2A 04-Aug-201506-Jul-2015 26-Jun-201525-Jun-201522-Jun-2015 ü üSoil Glass Jar - Unpreserved (EP071)

QC4A 04-Aug-201507-Jul-2015 26-Jun-201525-Jun-201523-Jun-2015 ü ü

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Matrix: SOIL Evaluation: û = Holding time breach ; ü = Within holding time.

AnalysisExtraction / PreparationSample DateMethod

EvaluationDue for analysisDate analysedEvaluationDue for extractionDate extractedContainer / Client Sample ID(s)

EP075(SIM)B: Polynuclear Aromatic Hydrocarbons

Soil Glass Jar - Unpreserved (EP075(SIM))

QC2A 04-Aug-201506-Jul-2015 26-Jun-201525-Jun-201522-Jun-2015 ü üSoil Glass Jar - Unpreserved (EP075(SIM))

QC4A 04-Aug-201507-Jul-2015 26-Jun-201525-Jun-201523-Jun-2015 ü üEP080/071: Total Petroleum Hydrocarbons


QC2A 06-Jul-201506-Jul-2015 29-Jun-201526-Jun-201522-Jun-2015 ü üSoil Glass Jar - Unpreserved (EP080)

QC4A 07-Jul-201507-Jul-2015 29-Jun-201526-Jun-201523-Jun-2015 ü ü

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Quality Control Parameter Frequency ComplianceThe following report summarises the frequency of laboratory QC samples analysed within the analytical lot(s) in which the submitted sample(s) was(were) processed. Actual rate should be greater than or equal to

the expected rate. A listing of breaches is provided in the Summary of Outliers.

Matrix: SOIL Evaluation: û = Quality Control frequency not within specification ; ü = Quality Control frequency within specification.

Quality Control SpecificationQuality Control Sample Type

ExpectedQC Regular Actual

Rate (%)Quality Control Sample Type CountEvaluationAnalytical Methods Method

Laboratory Duplicates (DUP)

NEPM 2013 Schedule B(3) and ALS QCS3 requirement 10.00 10.002 20 üElectrical Conductivity (1:5) EA010

NEPM 2013 Schedule B(3) and ALS QCS3 requirement 13.33 10.002 15 üMoisture Content EA055-103

NEPM 2013 Schedule B(3) and ALS QCS3 requirement 12.50 10.001 8 üPAH/Phenols (SIM) EP075(SIM)

NEPM 2013 Schedule B(3) and ALS QCS3 requirement 100.00 10.001 1 üPesticides by GCMS EP068

NEPM 2013 Schedule B(3) and ALS QCS3 requirement 10.00 10.002 20 üpH (1:5) EA002

NEPM 2013 Schedule B(3) and ALS QCS3 requirement 13.33 10.002 15 üTotal Mercury by FIMS EG035T

NEPM 2013 Schedule B(3) and ALS QCS3 requirement 13.33 10.002 15 üTotal Metals by ICP-AES EG005T

NEPM 2013 Schedule B(3) and ALS QCS3 requirement 12.50 10.002 16 üTRH - Semivolatile Fraction EP071

NEPM 2013 Schedule B(3) and ALS QCS3 requirement 10.00 10.002 20 üTRH Volatiles/BTEX EP080

Laboratory Control Samples (LCS)








Method Blanks (MB)








Matrix Spikes (MS)







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Brief Method SummariesThe analytical procedures used by the Environmental Division have been developed from established internationally recognized procedures such as those published by the US EPA, APHA, AS and NEPM. In house

developed procedures are employed in the absence of documented standards or by client request. The following report provides brief descriptions of the analytical procedures employed for results reported in the

Certificate of Analysis. Sources from which ALS methods have been developed are provided within the Method Descriptions.

Analytical Methods Method DescriptionsMatrixMethod

In house: Referenced to APHA 4500H+. pH is determined on soil samples after a 1:5 soil/water leach. This

method is compliant with NEPM (2013) Schedule B(3) (Method 103)

pH (1:5) EA002 SOIL

In house: Referenced to APHA 2510. Conductivity is determined on soil samples using a 1:5 soil/water leach.

This method is compliant with NEPM (2013) Schedule B(3) (Method 104)

Electrical Conductivity (1:5) EA010 SOIL

In-house. A gravimetric procedure based on weight loss over a 12 hour drying period at 103-105 degrees C.

This method is compliant with NEPM (2013) Schedule B(3) Section 7.1 and Table 1 (14 day holding time).

Moisture Content EA055-103 SOIL

In house: Referenced to APHA 3120; USEPA SW 846 - 6010. Metals are determined following an appropriate

acid digestion of the soil. The ICPAES technique ionises samples in a plasma, emitting a characteristic

spectrum based on metals present. Intensities at selected wavelengths are compared against those of matrix

matched standards. This method is compliant with NEPM (2013) Schedule B(3)

Total Metals by ICP-AES EG005T SOIL

In house: Referenced to AS 3550, APHA 3112 Hg - B (Flow-injection (SnCl2)(Cold Vapour generation) AAS)

FIM-AAS is an automated flameless atomic absorption technique. Mercury in solids are determined following an

appropriate acid digestion. Ionic mercury is reduced online to atomic mercury vapour by SnCl2 which is then

purged into a heated quartz cell. Quantification is by comparing absorbance against a calibration curve. This

method is compliant with NEPM (2013) Schedule B(3)

Total Mercury by FIMS EG035T SOIL

(USEPA SW 846 - 8270B) Extracts are analysed by Capillary GC/MS and quantification is by comparison against

an established 5 point calibration curve. This technique is compliant with NEPM (2013) Schedule B(3) (Method

504,505)

Pesticides by GCMS EP068 SOIL

(USEPA SW 846 - 8015A) Sample extracts are analysed by Capillary GC/FID and quantified against alkane

standards over the range C10 - C40.

TRH - Semivolatile Fraction EP071 SOIL

(USEPA SW 846 - 8270B) Extracts are analysed by Capillary GC/MS in Selective Ion Mode (SIM) and

quantification is by comparison against an established 5 point calibration curve. This method is compliant with

NEPM (2013) Schedule B(3) (Method 502 and 507)

PAH/Phenols (SIM) EP075(SIM) SOIL

(USEPA SW 846 - 8260B) Extracts are analysed by Purge and Trap, Capillary GC/MS. Quantification is by

comparison against an established 5 point calibration curve.

TRH Volatiles/BTEX EP080 SOIL

Preparation Methods Method DescriptionsMatrixMethod

(USEPA SW 846 - 5030A) 5g of solid is shaken with surrogate and 10mL methanol prior to analysis by Purge

and Trap - GC/MS.

Methanolic Extraction of Soils for Purge

and Trap

* ORG16 SOIL

In-house, Mechanical agitation (tumbler). 10g of sample, Na2SO4 and surrogate are extracted with 30mL 1:1

DCM/Acetone by end over end tumble. The solvent is decanted, dehydrated and concentrated (by KD) to the

desired volume for analysis.

Tumbler Extraction of Solids ORG17 SOIL

SAMPLE RECEIPT NOTIFICATION (SRN)Work Order : ES1524748


: :ContactContact MR ALEXANDER WILLIAMS

:: AddressAddress LEVEL 19, 799 PACIFIC HIGHWAY

Tower B - Citadel Tower


277-289 Woodpark Road Smithfield

NSW Australia 2164


:: TelephoneTelephone +61 02 9406 1000 +61-2-8784 8555


::Project ENAVWOLL04223AA Page 1 of 2

:Order number ---- :Quote number ES2014COFENV0369 (EN/077/14)

:C-O-C number 9467 :QC Level NEPM 2013 Schedule B(3) and ALS

QCS3 requirementSite : ----

Sampler : ALEXANDER WILLIAMS

DatesDate Samples Received : 25-Jun-2015 Issue Date : 25-Jun-2015

Scheduled Reporting Date: 02-Jul-2015:Client Requested Due

Date

02-Jul-2015

Delivery DetailsMode of Delivery : :Carrier Intact.Security Seal

No. of coolers/boxes : :1 Temperature 1.8'C - Ice present

: : 2 / 2Receipt Detail No. of samples received / analysed

General Comments

This report contains the following information:l

- Sample Container(s)/Preservation Non-Compliances

- Summary of Sample(s) and Requested Analysis

- Proactive Holding Time Report

- Requested Deliverables

l Please refer to the Proactive Holding Time Report table below which summarises breaches of

recommended holding times that have occurred prior to samples/instructions being received at

the laboratory. The absence of this summary table indicates that all samples have been received

within the recommended holding times for the analysis requested.l Sample(s) requiring volatile organic compound analysis received in airtight containers (ZHE).l Please direct any queries you have regarding this work order to the above ALS laboratory contact.

l Analytical work for this work order will be conducted at ALS Sydney.

l Sample Disposal - Aqueous (14 days), Solid (60 days) from date of completion of work order.


:Client COFFEY ENVIRONMENTS PTY LTD

Work Order : ES1524748 Amendment 02 of 2:Page

25-Jun-2015:Issue Date

Sample Container(s)/Preservation Non-Compliances

All comparisons are made against pretreatment/preservation AS, APHA, USEPA standards.

l No sample container / preservation non-compliance exist.

Summary of Sample(s) and Requested Analysis

Some items described below may be part of a laboratory

process necessary for the execution of client requested

tasks. Packages may contain additional analyses, such

as the determination of moisture content and preparation

tasks, that are included in the package.

SO

IL -

EA

055

-10

3

Mois

ture

Co

nte

nt

SO

IL -

IN

-4S

pH

plu

s E

C (

1:5

)

SO

IL -

S-1

2

OC

/OP

Pest

icid

es

SO

IL -

S-2

6

8 m

eta

ls/T

RH

/BT

EX

N/P

AH

ES1524748-001 [ 22-Jun-2015 ] QC2A ü ü ü ü

ES1524748-002 [ 23-Jun-2015 ] QC4A ü ü ü

Matrix: SOIL

Client sample IDLaboratory sample

ID

Client sampling

date / time

Proactive Holding Time Report

Sample(s) have been received within the recommended holding times for the requested analysis.

Requested Deliverables

ALEXANDER WILLIAMS

- *AU Certificate of Analysis - NATA (COA) Email [email protected]

- *AU Interpretive QC Report - DEFAULT (Anon QCI Rep) (QCI) Email [email protected]

- *AU QC Report - DEFAULT (Anon QC Rep) - NATA (QC) Email [email protected]

- A4 - AU Sample Receipt Notification - Environmental HT (SRN) Email [email protected]

- A4 - AU Tax Invoice (INV) Email [email protected]

- Chain of Custody (CoC) (COC) Email [email protected]

- EDI Format - ENMRG (ENMRG) Email [email protected]

- EDI Format - ESDAT (ESDAT) Email [email protected]

MANUEL FERNANDEZ

- *AU Certificate of Analysis - NATA (COA) Email [email protected]

- *AU Interpretive QC Report - DEFAULT (Anon QCI Rep) (QCI) Email [email protected]

- *AU QC Report - DEFAULT (Anon QC Rep) - NATA (QC) Email [email protected]

- A4 - AU Sample Receipt Notification - Environmental HT (SRN) Email [email protected]

- A4 - AU Tax Invoice (INV) Email [email protected]

- Attachment - Report (SUBCO) Email [email protected]

- Chain of Custody (CoC) (COC) Email [email protected]

- EDI Format - ENMRG (ENMRG) Email [email protected]

- EDI Format - ESDAT (ESDAT) Email [email protected]

Accredited for compliance with ISO/IEC 17025. The results of the tests, calibrations and/ormeasurements included in this document are traceableto Australian/national standards.

6/07/2015

Material Test Report

Report No: ASM:FYSH15W00725

Issue No: 1

Client:

Date of Issue:

NATA Accredited Laboratory Number:431

Approved Signatory: Rod Wilkins

(Senior Geotechnician)Project Name: ENAUWOLL04223AA - 25A Barker Road, Strathfield

ABN 92 114 364 046

Fyshwick,Canberra Laboratory

Coffey Testing Pty Ltd

16 Mildura StreetFyshwick ACT 2609

Phone: +61 2 6260 7288Fax: +61 2 6260 7211

Project No.: INFOFYSH00659AA

Principal:

Lot No.: CTP01 - CTP08 TRN: Work Order 1 of 4

118, Auburn streetWollongong NSW 2500

Coffey Environments Pty Ltd (Wollongong)

Material Details

ResultsForeign Materials Content RMS T276

Other Test Results

MethodDescription Limits

Sample Details

Type I (%)Metal.Glass.Asphalt.Stone.Ceramics and Slag :Type II (%)Plaster.Clay lumps and other Friable Material :Type III (%)Rubber.Plastic.Bitumen.Paper.Cloth.Wood and otherVegetable Matter:Retained on 4.75mm sieve (%)

InsituSourceProposed Carpark, 25A Barker Rd, StrathfieldLocationSampled by Coffey EnvironmentsSampling Method

Investigation - General FillDescriptionRMS GradingSpecification

Sampled From

Sample ID

Field Sample ID

Date Sampled

Date Submitted:

Sample Location:

FYSH15S-0117100001

22/06/2015

26/06/2015

CTP 01

0.0 - 0.2m

Type III

Result

<0.05%

0.0

0.0

0.0

7.0

FYSH15S-0117200002

22/06/2015

26/06/2015

CTP 01

1.0 - 1.2m

Type III

Result

<0.05%

0.0

0.0

0.0

0.0

FYSH15S-0117300003

22/06/2015

26/06/2015

CTP 01

1.4 - 1.6m

Type III

Result

<0.05%

0.0

0.0

0.0

2.7

FYSH15S-0117400004

22/06/2015

26/06/2015

CTP 02A

0.0 - 0.2m

Type III

Result

<0.05%

0.0

0.0

0.0

1.0

FYSH15S-0117500005

22/06/2015

26/06/2015

CTP 03

0.0 - 0.2m

Type III

Result

<0.05%

1.3

0.0

0.0

8.0

FYSH15S-0117600006

22/06/2015

26/06/2015

CTP 03

0.8 - 1.0m

Type III

Result

<0.05%

0.0

0.0

0.0

0.7

Page 1 of 2© 2000-2013 QESTLab by SpectraQEST.comForm No: 18980, Report No: ASM:FYSH15W00725

Testing performed on Topsoil and Sandy Clay/Clayey Sand material.Clay lumps not included in Type II.Type III does not include "other vegetable matter" (natural organic matter) as per Client Specification.

Comments


6/07/2015



Issue No: 1

Client:

Date of Issue:




ABN 92 114 364 046




Phone: +61 2 6260 7288Fax: +61 2 6260 7211


Principal:




Material Details


Other Test Results


Sample Details




Sampled From

Sample ID

Field Sample ID

Date Sampled

Date Submitted:

Sample Location:

FYSH15S-0117700007

22/06/2015

26/06/2015

CTP 04

0.0 - 0.2m

Type III

Result

<0.05%

0.0

0.0

0.0

1.5

FYSH15S-0117800008

22/06/2015

26/06/2015

CTP 05

0.0 - 0.2m

Type III

Result

<0.05%

0.0

0.0

0.0

0.3

FYSH15S-0117900009

22/06/2015

26/06/2015

CTP 06

0.0 - 0.2m

Type III

Result

<0.05%

0.0

0.0

0.0

1.5

FYSH15S-0118000010

22/06/2015

26/06/2015

CTP 06

0.35 - 0.55mType III

Result

<0.05%

0.7

0.1

0.0

9.0

FYSH15S-0118100011

22/06/2015

26/06/2015

CTP 07

0.0 - 0.2m

Type III

Result

<0.05%

0.0

0.0

0.0

0.9

FYSH15S-0118200012

22/06/2015

26/06/2015

CTP 08

0.0 - 0.2m

Type III

Result

<0.05%

0.0

0.0

0.0

0.2



Comments


6/07/2015



Issue No: 1

Client:

Date of Issue:




ABN 92 114 364 046




Phone: +61 2 6260 7288Fax: +61 2 6260 7211


Principal:




Material Details


Other Test Results


Sample Details




Sampled From

Sample ID

Field Sample ID

Date Sampled

Date Submitted:

Sample Location:

FYSH15S-0118300013

22/06/2015

26/06/2015

CTP 09

0.0 - 0.2m

Type III

Result

<0.05%

0.0

0.0

0.0

0.2

FYSH15S-0118400014

23/06/2015

26/06/2015

CTP 10

0.0 - 0.2m

Type III

Result

<0.05%

0.0

0.2

0.0

3.4

FYSH15S-0118500015

23/06/2015

26/06/2015

CTP 10


Result

<0.05%

0.0

0.0

0.0

10.9

FYSH15S-0118600016

23/06/2015

26/06/2015

CTP 11

0.0 - 0.2m

Type III

Result

<0.05%

0.0

0.0

0.0

0.3

FYSH15S-0118700017

23/06/2015

26/06/2015

CTP 11

0.3 - 0.5m

Type III

Result

<0.05%

0.0

0.0

0.0

13.0

FYSH15S-0118800018

23/06/2015

26/06/2015

CTP 12

0.0 - 0.2m

Type III

Result

<0.05%

0.0

0.0

0.0

0.1



Comments


6/07/2015



Issue No: 1

Client:

Date of Issue:




ABN 92 114 364 046




Phone: +61 2 6260 7288Fax: +61 2 6260 7211


Principal:




Material Details


Other Test Results


Sample Details




Sampled From

Sample ID

Field Sample ID

Date Sampled

Date Submitted:

Sample Location:

FYSH15S-0118900019

23/06/2015

26/06/2015

CTP 12


Result

<0.05%

0.0

0.0

0.0

6.3

FYSH15S-0119000020

22/06/2015

26/06/2015

CTP 13

0.0 - 0.2m

Type III

Result

<0.05%

0.0

0.0

0.0

0.9

FYSH15S-0119100021

23/06/2015

26/06/2015

CTP 14

0.0 - 0.2m

Type III

Result

<0.05%

0.0

0.0

0.0

1.9

FYSH15S-0119200022

23/06/2015

26/06/2015

CTP 14

1.0 - 1.2m

Type III

Result

0.05%

0.0

0.5

0.1

10.2

FYSH15S-0119300023

23/06/2015

26/06/2015

CTP 15

0.0 - 0.2m

Type III

Result

<0.05%

0.0

0.0

0.0

0.4

FYSH15S-0119400024

23/06/2015

26/06/2015

CTP 15

1.0 - 1.1m

Type III

Result

<0.05%

0.0

0.0

0.0

4.4



Comments


6/07/2015



Issue No: 1

Client:

Date of Issue:




ABN 92 114 364 046




Phone: +61 2 6260 7288Fax: +61 2 6260 7211


Principal:




Material Details


Other Test Results


Sample Details




Sampled From

Sample ID

Field Sample ID

Date Sampled

Date Submitted:

Sample Location:

FYSH15S-0119500025

23/06/2015

26/06/2015

CTP 16

0.0 - 0.2m

Type III

Result

<0.05%

0.0

0.0

0.0

0.1

FYSH15S-0119600026

23/06/2015

26/06/2015

CTP 16

1.2 - 1.4m

Type III

Result

<0.05%

0.0

0.0

0.0

5.6

FYSH15S-0119700027

23/06/2015

26/06/2015

CTP 16

1.5 - 1.7m

Type III

Result

<0.05%

0.0

0.0

0.0

13.0

FYSH15S-0119800028

23/06/2015

26/06/2015

CTP 17

0.0 - 0.2m

Type III

Result

<0.05%

0.0

0.0

0.0

0.2

FYSH15S-0119900029

23/06/2015

26/06/2015

CTP 17

0.9 - 1.1m

Type III

Result

<0.05%

0.0

0.0

0.0

4.2

FYSH15S-0120000030

23/06/2015

26/06/2015

CTP 18

0.0 - 0.2m

Type III

Result

<0.05%

0.0

0.0

0.0

2.5



Comments


6/07/2015



Issue No: 1

Client:

Date of Issue:




ABN 92 114 364 046




Phone: +61 2 6260 7288Fax: +61 2 6260 7211


Principal:




Material Details


Other Test Results


Sample Details




Sampled From

Sample ID

Field Sample ID

Date Sampled

Date Submitted:

Sample Location:

FYSH15S-0120100031

23/06/2015

26/06/2015

CTP 18

0.8 - 0.9m

Type III

Result

<0.05%

0.0

0.0

0.0

12.9

FYSH15S-0120200032

23/06/2015

26/06/2015

CTP 18

1.4 - 1.6m

Type III

Result

<0.05%

0.0

0.0

0.0

6.1

FYSH15S-0120300033

23/06/2015

26/06/2015

CTP 19

0.0 - 0.2m

Type III

Result

<0.05%

0.1

0.0

0.0

3.7

FYSH15S-0120400034

23/06/2015

26/06/2015

CTP 19

1.0 - 1.2m

Type III

Result

<0.05%

0.0

0.0

0.0

2.6

FYSH15S-0120500035

23/06/2015

26/06/2015

CTP 19

1.8 - 1.9m

Type III

Result

<0.05%

0.0

0.0

0.0

3.0



Comments


6/07/2015



Issue No: 1

Client:

Date of Issue:




ABN 92 114 364 046




Phone: +61 2 6260 7288Fax: +61 2 6260 7211


Principal:




Material Details


Other Test Results


Sample Details




Sampled From

Sample ID

Field Sample ID

Date Sampled

Date Submitted:

Sample Location:

FYSH15S-0120600036

23/06/2015

26/06/2015

CTP 20

0.0 - 0.2m

Type III

Result

<0.05%

0.0

0.0

0.0

0.0

FYSH15S-0120700037

23/06/2015

26/06/2015

CTP 20

1.0 - 1.1m

Type III

Result

<0.05%

0.0

0.0

0.0

4.4

FYSH15S-0120800038

23/06/2015

26/06/2015

CTP 20

1.9 - 2.1m

Type III

Result

<0.05%

0.0

0.0

0.0

4.4

FYSH15S-0120900039

23/06/2015

26/06/2015

CTP 20

2.3 - 2.5m

Type III

Result

<0.05%

0.0

0.0

0.0

7.5

FYSH15S-0121000040

23/06/2015

26/06/2015

CTP 21

0.0 - 0.2m

Type III

Result

<0.05%

0.0

0.0

0.0

3.3

FYSH15S-0121100041

23/06/2015

26/06/2015

CTP 21

0.9 - 1.0m

Type III

Result

<0.05%

0.0

0.0

0.0

13.8



Comments


6/07/2015



Issue No: 1

Client:

Date of Issue:




ABN 92 114 364 046




Phone: +61 2 6260 7288Fax: +61 2 6260 7211


Principal:




Material Details


Other Test Results


Sample Details




Sampled From

Sample ID

Field Sample ID

Date Sampled

Date Submitted:

Sample Location:

FYSH15S-0121200042

23/06/2015

26/06/2015

CTP 21

1.8 - 2.0m

Type III

Result

<0.05%

0.0

0.0

0.0

15.0

FYSH15S-0121300043

23/06/2015

26/06/2015

CTP 22

0.0 - 0.2m

Type III

Result

<0.05%

0.0

0.0

0.0

2.5

FYSH15S-0121400044

23/06/2015

26/06/2015

CTP 22

1.9 - 2.1m

Type III

Result

<0.05%

0.0

0.0

0.0

3.7



Comments

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