attachment ercb 33-1 · worleyparsons 100, 4500 - 16th avenue nw calgary, ab canada t3b 0m6 report...

Your P.O. #: 30102893 Your Project #: C61334026 Site: PEACE RIVER Your C.O.C. #: 67193

Attention: MELANIE EVANSWORLEYPARSONS100, 4500 - 16TH AVENUE NWCALGARY, ABCANADA T3B 0M6

Report Date: 2009/07/22

CERTIFICATE OF ANALYSIS

MAXXAM JOB #: A936113Received: 2009/07/13, 8:00

Sample Matrix: Water# Samples Received: 2

Date DateAnalyses Quantity Extracted Analyzed Laboratory Method Analytical MethodAlkalinity (pp, total), CO3,HCO3,OH 2 N/A 2009/07/18 EENVSOP-00054 SM 2320-B BTEX/F1 in Water by HS GC/MS 1 N/A 2009/07/20 EENVSOP-00004 EPA 8260C/CCME

EENVSOP-00002BTEX/F1 in Water by HS GC/MS 1 N/A 2009/07/21 EENVSOP-00004 EPA 8260C/CCME

EENVSOP-00002Cadmium - low level CCME - Dissolved 2 N/A 2009/07/18 CAL SOP-00191 EPA SW-846 6020A Cadmium - low level CCME (Total) 2 2009/07/15 2009/07/20 CAL SOP-00191 EPA SW-846 6020A Chloride by Automated Colourimetry 2 N/A 2009/07/17 EENVSOP-00055 EPA 325.2 True Colour 2 N/A 2009/07/16 EENVSOP-00065 SM 2120 B,C Total Coliforms and E.Coli 1 2009/07/13 2009/07/14 EIND SOP-00013 SM 9223 A,B Carbon (DOC) 2 N/A 2009/07/20 EENVSOP-00060 MMCW 119 Conductivity 2 N/A 2009/07/18 EENVSOP-00054 SM 2510-B Fluoride 2 N/A 2009/07/16 EENVSOP-00054 SM 4500-F C CCME Hydrocarbons in Water (F2; C10-C16) 2 2009/07/16 2009/07/17 EENVSOP-00009 EPA 8015D/3510C

EENVSOP-00008Sulphide (as H2S) 2 N/A 2009/07/16 Hardness 2 N/A 2009/07/18 CAL WI-00053 AEMM, Method 423 Mercury - Low Level (Dissolved) ( 1 ) 2 2009/07/16 2009/07/17 CAL SOP-00007 EPA 1631 Mercury - Low Level (Total) ( 1 ) 2 2009/07/16 2009/07/17 CAL SOP-00007 EPA 1631 Elements by ICP - Dissolved 2 N/A 2009/07/16 CAL SOP-00192 EPA SW846 6010B Elements by ICP - Total 2 2009/07/19 2009/07/19 CAL SOP-00192 EPA SW846 6010B Elements by ICPMS - Dissolved 2 N/A 2009/07/17 CAL SOP-00191 EPA SW-846 6020A Elements by ICPMS - Total 2 2009/07/19 2009/07/19 CAL SOP-00191 EPA SW-846 6020A Ion Balance 2 N/A 2009/07/18 CAL WI-00053 SM 1030E Sum of cations, anions 2 N/A 2009/07/18 Ammonia-N (Total) 2 N/A 2009/07/20 EENVSOP-00058 EPA 350.1 Nitrate and Nitrite 2 N/A 2009/07/20 Nitrate + Nitrite-N (calculated) 2 N/A 2009/07/20 Nitrogen, (Nitrite, Nitrate) by IC 2 N/A 2009/07/18 CAL SOP-00060 SM 4110-B Oil and Grease by IR ( 1 ) 2 2009/07/17 2009/07/20 CAL SOP-00096 Mod. EPA 9071A Benzo[a]pyrene Equivalency 2 N/A 2009/07/18 EENVSOP-00010 EPA 8270D/3510C Polycyclic Aromatic Hydrocarbons ( 2 ) 2 2009/07/16 2009/07/16 EENVSOP-00010 EPA 8270D/3510C

EENVSOP-00132pH (Alkalinity titrator) 2 N/A 2009/07/18 EENVSOP-00054 SM 4500-H+B Phenols (4-AAP) 2 N/A 2009/07/17 EENVSOP-00061 EPA 420.2 Sulphide 2 N/A 2009/07/16 EENVSOP-00096 SM 4500-S2 D Sulphate by Automated Colourimetry 2 N/A 2009/07/17 EENVSOP-00057 EPA 375.4 Total Dissolved Solids (Calculated) 2 N/A 2009/07/19 SM 1030E

../2Maxxam Analytics International Corporation o/a Maxxam Analytics Edmonton: 9331 - 48th Street T6B 2R4 Telephone(780)577-7100 FAX(780)450-4187

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Attachment ERCB 33-1

Your P.O. #: 30102893 Your Project #: C61334026 Site: PEACE RIVER Your C.O.C. #: 67193

Attention: MELANIE EVANSWORLEYPARSONS100, 4500 - 16TH AVENUE NWCALGARY, ABCANADA T3B 0M6

Report Date: 2009/07/22

CERTIFICATE OF ANALYSIS-2-

Sample Matrix: Water# Samples Received: 2

Date DateAnalyses Quantity Extracted Analyzed Laboratory Method Analytical MethodHydrocarbons (C10-C30) in Water - GC/FID 2 2009/07/16 2009/07/17 EENVSOP-00009 EPA 8015D/3510C

EENVSOP-00008Total Kjeldahl Nitrogen 2 2009/07/19 2009/07/20 EENVSOP-00145 EPA 351.1, 351.2 Carbon (Total Organic) 2 N/A 2009/07/20 EENVSOP-00060 SM 5310C TPH (C6-C30) Water Calc 1 N/A 2009/07/20 TPH (C6-C30) Water Calc 1 N/A 2009/07/21 Turbidity 2 N/A 2009/07/16 EENVSOP-00066 EPA Method 180.1

(1) This test was performed by Maxxam Calgary(2) B[a]P TPE is calculated using 1/2 of the RDL for non detect results as per Alberta Environment instructions. This protocol may not applyin other jurisdictions.

Encryption Key

Please direct all questions regarding this Certificate of Analysis to your Project Manager.

ALAINA HUNTER, Project ManagerEmail: [email protected]# (780) 577-7100

====================================================================Maxxam has procedures in place to guard against improper use of the electronic signature and have the required "signatories", as per section5.10.2 of ISO/IEC 17025:2005(E), signing the reports. SCC and CALA have approved this reporting process and electronic report format.

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Total cover pages: 2

Maxxam Analytics International Corporation o/a Maxxam Analytics Edmonton: 9331 - 48th Street T6B 2R4 Telephone(780)577-7100 FAX(780)450-4187

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WORLEYPARSONSMaxxam Job #: A936113 Client Project #: C61334026Report Date: 2009/07/22 Site Reference: PEACE RIVER

Your P.O. #: 30102893Sampler Initials: JAC

Sample Details/Parameters Result RDL Units Extracted Analyzed By Batch P 7 7 2 1 9 SW PRE Sampling Date 2009/07/11 M a t r i x W RESULTS OF CHEMICAL ANALYSES OF WATER CONVENTIONALS Total Ammonia (N) 3.3 ( 1 ) 0.05 mg/L 2009/07/20 2009/07/20 AL2 3283618 Misc. Inorganics Total Kjeldahl Nitrogen 3.2 ( 1 ) 0.05 mg/L 2009/07/19 2009/07/20 AL2 3283589 Calculated Parameters Anion Sum 65 N/A meq/L 2009/07/18 2009/07/18 3275117 Cation Sum 68 N/A meq/L 2009/07/18 2009/07/18 3275117 Hydrogen Sulphide (H2S) 0.007 0.002 mg/L 2009/07/16 2009/07/16 3275114 Ion Balance 1.0 0.01 N/A 2009/07/18 2009/07/18 3275116 Dissolved Nitrate (NO3) <0.01 0.01 mg/L 2009/07/20 2009/07/20 3275118 Nitrate plus Nitrite (N) <0.003 0.003 mg/L 2009/07/20 2009/07/20 3275119 Dissolved Nitrite (NO2) <0.01 0.01 mg/L 2009/07/20 2009/07/20 3275118 Misc. Inorganics C o n d u c t i v i t y 5400 1 uS/cm 2009/07/17 2009/07/18 MG5 3282818 Dissolved Organic Carbon (C) 9.3 ( 2 ) 0.5 mg/L 2009/07/20 2009/07/20 YY 3285973 Total Organic Carbon (C) 8.4 0.5 mg/L 2009/07/20 2009/07/20 YY 3285976 Low Level Elements Dissolved Cadmium (Cd) 0.023 0.005 ug/L 2009/07/18 2009/07/18 3275109 Total Cadmium (Cd) 0.060 0.005 ug/L 2009/07/20 2009/07/20 3275110 Anions Dissolved Fluoride (F) 2.2 ( 2 ) 0.05 mg/L 2009/07/16 2009/07/16 MG5 3277251 Dissolved Sulphate (SO4) <1 1 mg/L 2009/07/17 2009/07/17 MKA 3281486 S u l p h i d e 0.007 0.002 mg/L 2009/07/16 2009/07/16 RW3 3277509 Dissolved Chloride (Cl) 400 ( 3 ) 30 mg/L 2009/07/17 2009/07/17 MKA 3281496 Nutrients Dissolved Nitrate (N) <0.003 0.003 mg/L 2009/07/18 2009/07/18 JQ 3282945 Dissolved Nitrite (N) <0.003 0.003 mg/L 2009/07/18 2009/07/18 JQ 3282945 Misc. Organics P h e n o l s 0.004 0.002 mg/L 2009/07/17 2009/07/17 YY 3281948 Physical Properties True Colour 9 2 PtCo units 2009/07/16 2009/07/16 LF1 3276836 Physical Properties T u r b i d i t y 73 0.1 NTU 2009/07/16 2009/07/16 RW3 3276830 ELEMENTS BY ATOMIC SPECTROSCOPY (WATER) Elements Dissolved Aluminum (Al) 0.001 0.001 mg/L 2009/07/17 2009/07/17 AS7 3280112 Total Aluminum (Al) 0.63 0.001 mg/L 2009/07/19 2009/07/19 EO1 3283530 Dissolved Antimony (Sb) <0.0002 0.0002 mg/L 2009/07/17 2009/07/17 AS7 3280112 Total Antimony (Sb) 0.0002 0.0002 mg/L 2009/07/19 2009/07/19 EO1 3283530 Dissolved Arsenic (As) 0.0003 0.0002 mg/L 2009/07/17 2009/07/17 AS7 3280112 Total Arsenic (As) 0.0011 0.0002 mg/L 2009/07/19 2009/07/19 EO1 3283530 Dissolved Barium (Ba) 0.67 0.01 mg/L 2009/07/16 2009/07/16 RI3 3279352 Total Barium (Ba) 0.75 0.01 mg/L 2009/07/19 2009/07/19 SG8 3283559 Dissolved Beryllium (Be) <0.001 0.001 mg/L 2009/07/17 2009/07/17 AS7 3280112 Total Beryllium (Be) <0.001 0.001 mg/L 2009/07/19 2009/07/19 EO1 3283530 Dissolved Boron (B) 2.8 0.02 mg/L 2009/07/16 2009/07/16 RI3 3279352 Total Boron (B) 3.4 0.02 mg/L 2009/07/19 2009/07/19 SG8 3283559 Dissolved Calcium (Ca) 2.2 0.3 mg/L 2009/07/16 2009/07/16 RI3 3279352 ( 1 ) TKN < NH4: Both values fall within acceptable RPD limits for duplicates and are likely equivalent.( 2 ) Matrix spike non calculable due to high concentration of original analyte.( 3 ) Detection limits raised due to dilution to bring analyte within the calibrated range.

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Sample Details/Parameters Result RDL Units Extracted Analyzed By Batch P 7 7 2 1 9 SW PRE Sampling Date 2009/07/11 M a t r i x W ELEMENTS BY ATOMIC SPECTROSCOPY (WATER) Elements Total Calcium (Ca) 3.1 0.3 mg/L 2009/07/19 2009/07/19 SG8 3283559 Dissolved Chromium (Cr) 0.002 0.001 mg/L 2009/07/17 2009/07/17 AS7 3280112 Total Chromium (Cr) 0.038 0.001 mg/L 2009/07/19 2009/07/19 EO1 3283530 Dissolved Cobalt (Co) 0.0005 0.0003 mg/L 2009/07/17 2009/07/17 AS7 3280112 Total Cobalt (Co) 0.0022 0.0003 mg/L 2009/07/19 2009/07/19 EO1 3283530 Dissolved Copper (Cu) 0.0013 0.0002 mg/L 2009/07/17 2009/07/17 AS7 3280112 Total Copper (Cu) 0.0047 0.0002 mg/L 2009/07/19 2009/07/19 EO1 3283530 Dissolved Iron (Fe) 3.9 0.06 mg/L 2009/07/16 2009/07/16 RI3 3279352 Total Iron (Fe) 7.3 0.06 mg/L 2009/07/19 2009/07/19 SG8 3283559 Dissolved Lead (Pb) 0.0010 0.0002 mg/L 2009/07/17 2009/07/17 AS7 3280112 Total Lead (Pb) 0.0043 0.0002 mg/L 2009/07/19 2009/07/19 EO1 3283530 Dissolved Lithium (Li) 0.38 0.02 mg/L 2009/07/16 2009/07/16 RI3 3279352 Total Lithium (Li) 0.43 0.02 mg/L 2009/07/19 2009/07/19 SG8 3283559 Dissolved Magnesium (Mg) 2.2 0.2 mg/L 2009/07/16 2009/07/16 RI3 3279352 Total Magnesium (Mg) 3.6 0.2 mg/L 2009/07/19 2009/07/19 SG8 3283559 Dissolved Manganese (Mn) 0.054 0.004 mg/L 2009/07/16 2009/07/16 RI3 3279352 Total Manganese (Mn) 0.083 0.004 mg/L 2009/07/19 2009/07/19 SG8 3283559 Dissolved Molybdenum (Mo) 0.0020 0.0002 mg/L 2009/07/17 2009/07/17 AS7 3280112 Total Molybdenum (Mo) 0.0040 0.0002 mg/L 2009/07/19 2009/07/19 EO1 3283530 Dissolved Nickel (Ni) 0.0055 0.0005 mg/L 2009/07/17 2009/07/17 AS7 3280112 Total Nickel (Ni) 0.024 0.0005 mg/L 2009/07/19 2009/07/19 EO1 3283530 Dissolved Phosphorus (P) 0.8 0.1 mg/L 2009/07/16 2009/07/16 RI3 3279352 Total Phosphorus (P) 0.5 0.1 mg/L 2009/07/19 2009/07/19 SG8 3283559 Dissolved Potassium (K) 4.2 0.3 mg/L 2009/07/16 2009/07/16 RI3 3279352 Total Potassium (K) 6.0 0.3 mg/L 2009/07/19 2009/07/19 SG8 3283559 Dissolved Selenium (Se) <0.0002 0.0002 mg/L 2009/07/17 2009/07/17 AS7 3280112 Total Selenium (Se) 0.0005 0.0002 mg/L 2009/07/19 2009/07/19 EO1 3283530 Dissolved Silicon (Si) 2.6 0.1 mg/L 2009/07/16 2009/07/16 RI3 3279352 Total Silicon (Si) 4.7 0.1 mg/L 2009/07/19 2009/07/19 SG8 3283559 Dissolved Silver (Ag) <0.0001 0.0001 mg/L 2009/07/17 2009/07/17 AS7 3280112 Total Silver (Ag) <0.0001 0.0001 mg/L 2009/07/19 2009/07/19 EO1 3283530 Dissolved Sodium (Na) 1500 ( 1 ) 5 mg/L 2009/07/16 2009/07/16 RI3 3279352 Total Sodium (Na) 1500 ( 1 ) 5 mg/L 2009/07/19 2009/07/19 SG8 3283559 Dissolved Strontium (Sr) 0.35 0.02 mg/L 2009/07/16 2009/07/16 RI3 3279352 Total Strontium (Sr) 0.38 0.02 mg/L 2009/07/19 2009/07/19 SG8 3283559 Dissolved Sulphur (S) 0.5 0.2 mg/L 2009/07/16 2009/07/16 RI3 3279352 Total Sulphur (S) 1.2 0.2 mg/L 2009/07/19 2009/07/19 SG8 3283559 Dissolved Thallium (Tl) <0.0002 0.0002 mg/L 2009/07/17 2009/07/17 AS7 3280112 Total Thallium (Tl) <0.0002 0.0002 mg/L 2009/07/19 2009/07/19 EO1 3283530 Dissolved Tin (Sn) <0.001 0.001 mg/L 2009/07/17 2009/07/17 AS7 3280112 Total Tin (Sn) <0.001 0.001 mg/L 2009/07/19 2009/07/19 EO1 3283530 Dissolved Titanium (Ti) 0.001 0.001 mg/L 2009/07/17 2009/07/17 AS7 3280112 Total Titanium (Ti) 0.010 0.001 mg/L 2009/07/19 2009/07/19 EO1 3283530 Dissolved Uranium (U) <0.0001 0.0001 mg/L 2009/07/17 2009/07/17 AS7 3280112 Total Uranium (U) 0.0002 0.0001 mg/L 2009/07/19 2009/07/19 EO1 3283530 Dissolved Vanadium (V) <0.001 0.001 mg/L 2009/07/17 2009/07/17 AS7 3280112 Total Vanadium (V) 0.004 0.001 mg/L 2009/07/19 2009/07/19 EO1 3283530 Dissolved Zinc (Zn) 0.15 0.003 mg/L 2009/07/17 2009/07/17 AS7 3280112 Total Zinc (Zn) 0.033 0.003 mg/L 2009/07/19 2009/07/19 EO1 3283530 ( 1 ) Detection limits raised due to dilution to bring analyte within the calibrated range.

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Sample Details/Parameters Result RDL Units Extracted Analyzed By Batch P 7 7 2 1 9 SW PRE Sampling Date 2009/07/11 M a t r i x W ELEMENTS BY ATOMIC SPECTROSCOPY (WATER) Low Level Elements Dissolved Mercury (Hg) <0.001 0.001 ug/L 2009/07/16 2009/07/17 VH2 3277865 Total Mercury (Hg) 0.003 0.001 ug/L 2009/07/16 2009/07/17 VH2 3277868 PETROLEUM HYDROCARBONS (CCME) Hydrocarbons F2 (C10-C16 Hydrocarbons) <0.1 0.1 mg/L 2009/07/16 2009/07/17 JM7 3276686 O-TERPHENYL (sur.) 98 70 - 130 % 2009/07/16 2009/07/17 JM7 3276686 SEMIVOLATILE ORGANICS BY GC-MS (WATER) Polycyclic Aromatics A c e n a p h t h e n e <0.10 0.10 ug/L 2009/07/16 2009/07/16 MB7 3271880 A c e n a p h t h y l e n e <0.10 0.10 ug/L 2009/07/16 2009/07/16 MB7 3271880 A c r i d i n e <0.20 0.20 ug/L 2009/07/16 2009/07/16 MB7 3271880 A n t h r a c e n e <0.010 0.010 ug/L 2009/07/16 2009/07/16 MB7 3271880 B e n z o ( a ) a n t h r a c e n e <0.0085 0.0085 ug/L 2009/07/16 2009/07/16 MB7 3271880 B e n z o ( b & j ) f l u o r a n t h e n e <0.0085 0.0085 ug/L 2009/07/16 2009/07/16 MB7 3271880 B e n z o ( k ) f l u o r a n t h e n e <0.0085 0.0085 ug/L 2009/07/16 2009/07/16 MB7 3271880 B e n z o ( g , h , i ) p e r y l e n e 0.011 0.0085 ug/L 2009/07/16 2009/07/16 MB7 3271880 B e n z o ( c ) p h e n a n t h r e n e <0.050 0.050 ug/L 2009/07/16 2009/07/16 MB7 3271880 B e n z o ( a ) p y r e n e <0.0075 0.0075 ug/L 2009/07/16 2009/07/16 MB7 3271880 B e n z o [ e ] p y r e n e <0.050 0.050 ug/L 2009/07/16 2009/07/16 MB7 3271880 C h r y s e n e <0.0085 0.0085 ug/L 2009/07/16 2009/07/16 MB7 3271880 D i b e n z ( a , h ) a n t h r a c e n e <0.0075 0.0075 ug/L 2009/07/16 2009/07/16 MB7 3271880 F l u o r a n t h e n e <0.040 0.040 ug/L 2009/07/16 2009/07/16 MB7 3271880 F l u o r e n e 0.064 0.050 ug/L 2009/07/16 2009/07/16 MB7 3271880 I n d e n o ( 1 , 2 , 3 - c d ) p y r e n e 0.014 0.0085 ug/L 2009/07/16 2009/07/16 MB7 3271880 2 - M e t h y l n a p h t h a l e n e 0.24 0.10 ug/L 2009/07/16 2009/07/16 MB7 3271880 N a p h t h a l e n e <0.10 0.10 ug/L 2009/07/16 2009/07/16 MB7 3271880 P h e n a n t h r e n e 0.28 0.050 ug/L 2009/07/16 2009/07/16 MB7 3271880 P e r y l e n e <0.050 0.050 ug/L 2009/07/16 2009/07/16 MB7 3271880 P y r e n e <0.020 0.020 ug/L 2009/07/16 2009/07/16 MB7 3271880 Q u i n o l i n e <0.20 0.20 ug/L 2009/07/16 2009/07/16 MB7 3271880 D10-ANTHRACENE (sur.) 101 30 - 130 % 2009/07/16 2009/07/16 MB7 3271880 D12-BENZO(A)PYRENE (sur.) 89 30 - 130 % 2009/07/16 2009/07/16 MB7 3271880 D8-ACENAPHTHYLENE (sur.) 88 30 - 130 % 2009/07/16 2009/07/16 MB7 3271880 TERPHENYL-D14 (sur.) 102 30 - 130 % 2009/07/16 2009/07/16 MB7 3271880 TOTAL PETROLEUM HYDROCARBONS (WATER) Hydrocarbons Total Extractables C10 to C30 0.3 0.1 mg/L 2009/07/16 2009/07/17 JM7 3276700 Total hydrocarbons C5-C30 0.3 0.2 mg/L 2009/07/20 2009/07/20 3275124 O-TERPHENYL (sur.) 97 60 - 130 % 2009/07/16 2009/07/17 JM7 3276700 VOLATILE ORGANICS BY GC-MS (WATER) Volatiles B e n z e n e <40 40 ug/L 2009/07/15 2009/07/20 CD1 3276059 T o l u e n e <40 40 ug/L 2009/07/15 2009/07/20 CD1 3276059 E t h y l b e n z e n e <40 40 ug/L 2009/07/15 2009/07/20 CD1 3276059 o - X y l e n e <40 40 ug/L 2009/07/15 2009/07/20 CD1 3276059 m & p-Xylene <80 80 ug/L 2009/07/15 2009/07/20 CD1 3276059 Xylenes (Total) <80 80 ug/L 2009/07/15 2009/07/20 CD1 3276059 F1 (C6-C10) - BTEX <100 100 ug/L 2009/07/15 2009/07/20 CD1 3276059 LH (C5-C10) <100 100 ug/L 2009/07/15 2009/07/20 CD1 3276059 ( C 6 - C 1 0 ) <100 100 ug/L 2009/07/15 2009/07/20 CD1 3276059 4-BROMOFLUOROBENZENE (sur.) 92 70 - 130 % 2009/07/15 2009/07/20 CD1 3276059 D4-1,2-DICHLOROETHANE (sur.) 105 70 - 130 % 2009/07/15 2009/07/20 CD1 3276059 D8-TOLUENE (sur.) 96 70 - 130 % 2009/07/15 2009/07/20 CD1 3276059

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Sample Details/Parameters Result RDL Units Extracted Analyzed By Batch P 7 7 2 1 9 SW PRE Sampling Date 2009/07/11 M a t r i x W RESULTS OF CHEMICAL ANALYSES OF WATER Calculated Parameters Hardness (CaCO3) 14 0.5 mg/L 2009/07/18 2009/07/18 3275115 Total Dissolved Solids 3600 10 mg/L 2009/07/19 2009/07/19 3275123 Misc. Inorganics p H 8.27 N/A N/A 2009/07/17 2009/07/18 MG5 3282817 Anions Alkalinity (PP as CaCO3) <0.5 0.5 mg/L 2009/07/17 2009/07/18 MG5 3282799 Alkalinity (Total as CaCO3) 2700 0.5 mg/L 2009/07/17 2009/07/18 MG5 3282799 Bicarbonate (HCO3) 3300 0.5 mg/L 2009/07/17 2009/07/18 MG5 3282799 Carbonate (CO3) <0.5 0.5 mg/L 2009/07/17 2009/07/18 MG5 3282799 Hydroxide (OH) <0.5 0.5 mg/L 2009/07/17 2009/07/18 MG5 3282799 Misc. Organics Oil and grease 3 2 mg/L 2009/07/17 2009/07/20 CL4 3279937 SEMIVOLATILE ORGANICS BY GC-MS (WATER) Polycyclic Aromatics Benzo[a]pyrene equivalency <0.01 0.01 ug/L 2009/07/18 2009/07/18 3275120 P 7 7 2 4 6 SW POST Sampling Date 2009/07/12 M a t r i x W RESULTS OF CHEMICAL ANALYSES OF WATER CONVENTIONALS Total Ammonia (N) 3.5 ( 1 ) 0.05 mg/L 2009/07/20 2009/07/20 AL2 3283618 Misc. Inorganics Total Kjeldahl Nitrogen 3.2 ( 1 ) 0.05 mg/L 2009/07/19 2009/07/20 AL2 3283589 Calculated Parameters Anion Sum 65 N/A meq/L 2009/07/18 2009/07/18 3275117 Cation Sum 67 N/A meq/L 2009/07/18 2009/07/18 3275117 Hydrogen Sulphide (H2S) <0.002 0.002 mg/L 2009/07/16 2009/07/16 3275114 Ion Balance 1.0 0.01 N/A 2009/07/18 2009/07/18 3275116 Dissolved Nitrate (NO3) <0.01 0.01 mg/L 2009/07/20 2009/07/20 3275118 Nitrate plus Nitrite (N) <0.003 0.003 mg/L 2009/07/20 2009/07/20 3275119 Dissolved Nitrite (NO2) <0.01 0.01 mg/L 2009/07/20 2009/07/20 3275118 Misc. Inorganics C o n d u c t i v i t y 5400 1 uS/cm 2009/07/17 2009/07/18 MG5 3282818 Dissolved Organic Carbon (C) 8.3 0.5 mg/L 2009/07/20 2009/07/20 YY 3285973 Total Organic Carbon (C) 9.0 0.5 mg/L 2009/07/20 2009/07/20 YY 3285976 Low Level Elements Dissolved Cadmium (Cd) 0.054 0.005 ug/L 2009/07/18 2009/07/18 3275109 Total Cadmium (Cd) 0.019 0.005 ug/L 2009/07/20 2009/07/20 3275110 Anions Dissolved Fluoride (F) 2.2 0.05 mg/L 2009/07/16 2009/07/16 MG5 3277251 Dissolved Sulphate (SO4) <1 1 mg/L 2009/07/17 2009/07/17 MKA 3281486 S u l p h i d e <0.002 0.002 mg/L 2009/07/16 2009/07/16 RW3 3277509 Dissolved Chloride (Cl) 410 ( 2 ) 30 mg/L 2009/07/17 2009/07/17 MKA 3281496 Microbiological Param. E.Coli DST <1 1 mpn/100mL 2009/07/13 2009/07/14 JA6 3275087 Total Coliforms DST 1120 1 mpn/100mL 2009/07/13 2009/07/14 JA6 3275087 ( 1 ) TKN < NH4: Both values fall within acceptable RPD limits for duplicates and are likely equivalent.( 2 ) Detection limits raised due to dilution to bring analyte within the calibrated range.

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Sample Details/Parameters Result RDL Units Extracted Analyzed By Batch P 7 7 2 4 6 SW POST Sampling Date 2009/07/12 M a t r i x W RESULTS OF CHEMICAL ANALYSES OF WATER Nutrients Dissolved Nitrate (N) <0.003 0.003 mg/L 2009/07/18 2009/07/18 JQ 3282945 Dissolved Nitrite (N) <0.003 0.003 mg/L 2009/07/18 2009/07/18 JQ 3282945 Misc. Organics P h e n o l s 0.004 0.002 mg/L 2009/07/17 2009/07/17 YY 3281948 Physical Properties True Colour 9 2 PtCo units 2009/07/16 2009/07/16 LF1 3276836 Physical Properties T u r b i d i t y 7.8 0.1 NTU 2009/07/16 2009/07/16 RW3 3276830 ELEMENTS BY ATOMIC SPECTROSCOPY (WATER) Elements Dissolved Aluminum (Al) 0.005 0.001 mg/L 2009/07/17 2009/07/17 AS7 3280112 Total Aluminum (Al) 0.080 0.001 mg/L 2009/07/19 2009/07/19 EO1 3283530 Dissolved Antimony (Sb) <0.0002 0.0002 mg/L 2009/07/17 2009/07/17 AS7 3280112 Total Antimony (Sb) <0.0002 0.0002 mg/L 2009/07/19 2009/07/19 EO1 3283530 Dissolved Arsenic (As) 0.0002 0.0002 mg/L 2009/07/17 2009/07/17 AS7 3280112 Total Arsenic (As) <0.0002 0.0002 mg/L 2009/07/19 2009/07/19 EO1 3283530 Dissolved Barium (Ba) 0.73 0.01 mg/L 2009/07/16 2009/07/16 RI3 3279352 Total Barium (Ba) 0.75 0.01 mg/L 2009/07/19 2009/07/19 SG8 3283559 Dissolved Beryllium (Be) <0.001 0.001 mg/L 2009/07/17 2009/07/17 AS7 3280112 Total Beryllium (Be) <0.001 0.001 mg/L 2009/07/19 2009/07/19 EO1 3283530 Dissolved Boron (B) 3.0 0.02 mg/L 2009/07/16 2009/07/16 RI3 3279352 Total Boron (B) 3.4 0.02 mg/L 2009/07/19 2009/07/19 SG8 3283559 Dissolved Calcium (Ca) 2.2 0.3 mg/L 2009/07/16 2009/07/16 RI3 3279352 Total Calcium (Ca) 2.7 0.3 mg/L 2009/07/19 2009/07/19 SG8 3283559 Dissolved Chromium (Cr) <0.001 0.001 mg/L 2009/07/17 2009/07/17 AS7 3280112 Total Chromium (Cr) 0.002 0.001 mg/L 2009/07/19 2009/07/19 EO1 3283530 Dissolved Cobalt (Co) 0.0003 0.0003 mg/L 2009/07/17 2009/07/17 AS7 3280112 Total Cobalt (Co) 0.0004 0.0003 mg/L 2009/07/19 2009/07/19 EO1 3283530 Dissolved Copper (Cu) 0.0004 0.0002 mg/L 2009/07/17 2009/07/17 AS7 3280112 Total Copper (Cu) 0.0006 0.0002 mg/L 2009/07/19 2009/07/19 EO1 3283530 Dissolved Iron (Fe) 2.3 0.06 mg/L 2009/07/16 2009/07/16 RI3 3279352 Total Iron (Fe) 3.3 0.06 mg/L 2009/07/19 2009/07/19 SG8 3283559 Dissolved Lead (Pb) <0.0002 0.0002 mg/L 2009/07/17 2009/07/17 AS7 3280112 Total Lead (Pb) 0.0004 0.0002 mg/L 2009/07/19 2009/07/19 EO1 3283530 Dissolved Lithium (Li) 0.41 0.02 mg/L 2009/07/16 2009/07/16 RI3 3279352 Total Lithium (Li) 0.43 0.02 mg/L 2009/07/19 2009/07/19 SG8 3283559 Dissolved Magnesium (Mg) 2.5 0.2 mg/L 2009/07/16 2009/07/16 RI3 3279352 Total Magnesium (Mg) 3.4 0.2 mg/L 2009/07/19 2009/07/19 SG8 3283559 Dissolved Manganese (Mn) 0.035 0.004 mg/L 2009/07/16 2009/07/16 RI3 3279352 Total Manganese (Mn) 0.041 0.004 mg/L 2009/07/19 2009/07/19 SG8 3283559 Dissolved Molybdenum (Mo) 0.0014 0.0002 mg/L 2009/07/17 2009/07/17 AS7 3280112 Total Molybdenum (Mo) 0.0018 0.0002 mg/L 2009/07/19 2009/07/19 EO1 3283530 Dissolved Nickel (Ni) 0.0032 0.0005 mg/L 2009/07/17 2009/07/17 AS7 3280112 Total Nickel (Ni) 0.0034 0.0005 mg/L 2009/07/19 2009/07/19 EO1 3283530 Dissolved Phosphorus (P) 0.7 0.1 mg/L 2009/07/16 2009/07/16 RI3 3279352 Total Phosphorus (P) 0.5 0.1 mg/L 2009/07/19 2009/07/19 SG8 3283559 Dissolved Potassium (K) 4.5 0.3 mg/L 2009/07/16 2009/07/16 RI3 3279352 Total Potassium (K) 5.7 0.3 mg/L 2009/07/19 2009/07/19 SG8 3283559 Dissolved Selenium (Se) 0.0003 0.0002 mg/L 2009/07/17 2009/07/17 AS7 3280112 Total Selenium (Se) 0.0004 0.0002 mg/L 2009/07/19 2009/07/19 EO1 3283530 Dissolved Silicon (Si) 2.8 0.1 mg/L 2009/07/16 2009/07/16 RI3 3279352 Total Silicon (Si) 3.4 0.1 mg/L 2009/07/19 2009/07/19 SG8 3283559 Dissolved Silver (Ag) <0.0001 0.0001 mg/L 2009/07/17 2009/07/17 AS7 3280112 Total Silver (Ag) <0.0001 0.0001 mg/L 2009/07/19 2009/07/19 EO1 3283530 Dissolved Sodium (Na) 1500 ( 1 ) 5 mg/L 2009/07/16 2009/07/16 RI3 3279352

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( 1 ) Detection limits raised due to dilution to bring analyte within the calibrated range.

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Sample Details/Parameters Result RDL Units Extracted Analyzed By Batch P 7 7 2 4 6 SW POST Sampling Date 2009/07/12 M a t r i x W ELEMENTS BY ATOMIC SPECTROSCOPY (WATER) Elements Total Sodium (Na) 1500 ( 1 ) 5 mg/L 2009/07/19 2009/07/19 SG8 3283559 Dissolved Strontium (Sr) 0.36 0.02 mg/L 2009/07/16 2009/07/16 RI3 3279352 Total Strontium (Sr) 0.37 0.02 mg/L 2009/07/19 2009/07/19 SG8 3283559 Dissolved Sulphur (S) 0.5 0.2 mg/L 2009/07/16 2009/07/16 RI3 3279352 Total Sulphur (S) 0.6 0.2 mg/L 2009/07/19 2009/07/19 SG8 3283559 Dissolved Thallium (Tl) <0.0002 0.0002 mg/L 2009/07/17 2009/07/17 AS7 3280112 Total Thallium (Tl) <0.0002 0.0002 mg/L 2009/07/19 2009/07/19 EO1 3283530 Dissolved Tin (Sn) <0.001 0.001 mg/L 2009/07/17 2009/07/17 AS7 3280112 Total Tin (Sn) <0.001 0.001 mg/L 2009/07/19 2009/07/19 EO1 3283530 Dissolved Titanium (Ti) <0.001 0.001 mg/L 2009/07/17 2009/07/17 AS7 3280112 Total Titanium (Ti) 0.002 0.001 mg/L 2009/07/19 2009/07/19 EO1 3283530 Dissolved Uranium (U) <0.0001 0.0001 mg/L 2009/07/17 2009/07/17 AS7 3280112 Total Uranium (U) <0.0001 0.0001 mg/L 2009/07/19 2009/07/19 EO1 3283530 Dissolved Vanadium (V) <0.001 0.001 mg/L 2009/07/17 2009/07/17 AS7 3280112 Total Vanadium (V) <0.001 0.001 mg/L 2009/07/19 2009/07/19 EO1 3283530 Dissolved Zinc (Zn) 0.050 0.003 mg/L 2009/07/17 2009/07/17 AS7 3280112 Total Zinc (Zn) 0.005 0.003 mg/L 2009/07/19 2009/07/19 EO1 3283530 Low Level Elements Dissolved Mercury (Hg) <0.001 0.001 ug/L 2009/07/16 2009/07/17 VH2 3277865 Total Mercury (Hg) <0.001 0.001 ug/L 2009/07/16 2009/07/17 VH2 3277868 PETROLEUM HYDROCARBONS (CCME) Hydrocarbons F2 (C10-C16 Hydrocarbons) <0.1 0.1 mg/L 2009/07/16 2009/07/17 JM7 3276686 O-TERPHENYL (sur.) 100 70 - 130 % 2009/07/16 2009/07/17 JM7 3276686 SEMIVOLATILE ORGANICS BY GC-MS (WATER) Polycyclic Aromatics A c e n a p h t h e n e <0.10 0.10 ug/L 2009/07/16 2009/07/16 MB7 3271880 A c e n a p h t h y l e n e <0.10 0.10 ug/L 2009/07/16 2009/07/16 MB7 3271880 A c r i d i n e <0.20 0.20 ug/L 2009/07/16 2009/07/16 MB7 3271880 A n t h r a c e n e <0.010 0.010 ug/L 2009/07/16 2009/07/16 MB7 3271880 B e n z o ( a ) a n t h r a c e n e <0.0085 0.0085 ug/L 2009/07/16 2009/07/16 MB7 3271880 B e n z o ( b & j ) f l u o r a n t h e n e <0.0085 0.0085 ug/L 2009/07/16 2009/07/16 MB7 3271880 B e n z o ( k ) f l u o r a n t h e n e <0.0085 0.0085 ug/L 2009/07/16 2009/07/16 MB7 3271880 B e n z o ( g , h , i ) p e r y l e n e <0.0085 0.0085 ug/L 2009/07/16 2009/07/16 MB7 3271880 B e n z o ( c ) p h e n a n t h r e n e <0.050 0.050 ug/L 2009/07/16 2009/07/16 MB7 3271880 B e n z o ( a ) p y r e n e <0.0075 0.0075 ug/L 2009/07/16 2009/07/16 MB7 3271880 B e n z o [ e ] p y r e n e <0.050 0.050 ug/L 2009/07/16 2009/07/16 MB7 3271880 C h r y s e n e <0.0085 0.0085 ug/L 2009/07/16 2009/07/16 MB7 3271880 D i b e n z ( a , h ) a n t h r a c e n e 0.011 0.0075 ug/L 2009/07/16 2009/07/16 MB7 3271880 F l u o r a n t h e n e <0.040 0.040 ug/L 2009/07/16 2009/07/16 MB7 3271880 F l u o r e n e <0.050 0.050 ug/L 2009/07/16 2009/07/16 MB7 3271880 I n d e n o ( 1 , 2 , 3 - c d ) p y r e n e 0.011 0.0085 ug/L 2009/07/16 2009/07/16 MB7 3271880 2 - M e t h y l n a p h t h a l e n e <0.10 0.10 ug/L 2009/07/16 2009/07/16 MB7 3271880 N a p h t h a l e n e <0.10 0.10 ug/L 2009/07/16 2009/07/16 MB7 3271880 P h e n a n t h r e n e <0.050 0.050 ug/L 2009/07/16 2009/07/16 MB7 3271880 P e r y l e n e <0.050 0.050 ug/L 2009/07/16 2009/07/16 MB7 3271880 P y r e n e <0.020 0.020 ug/L 2009/07/16 2009/07/16 MB7 3271880 Q u i n o l i n e <0.20 0.20 ug/L 2009/07/16 2009/07/16 MB7 3271880 D10-ANTHRACENE (sur.) 107 30 - 130 % 2009/07/16 2009/07/16 MB7 3271880 ( 1 ) Detection limits raised due to dilution to bring analyte within the calibrated range.

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Sample Details/Parameters Result RDL Units Extracted Analyzed By Batch P 7 7 2 4 6 SW POST Sampling Date 2009/07/12 M a t r i x W SEMIVOLATILE ORGANICS BY GC-MS (WATER) Polycyclic Aromatics D12-BENZO(A)PYRENE (sur.) 94 30 - 130 % 2009/07/16 2009/07/16 MB7 3271880 D8-ACENAPHTHYLENE (sur.) 93 30 - 130 % 2009/07/16 2009/07/16 MB7 3271880 TERPHENYL-D14 (sur.) 107 30 - 130 % 2009/07/16 2009/07/16 MB7 3271880 TOTAL PETROLEUM HYDROCARBONS (WATER) Hydrocarbons Total Extractables C10 to C30 <0.1 0.1 mg/L 2009/07/16 2009/07/17 JM7 3276700 Total hydrocarbons C5-C30 <0.2 0.2 mg/L 2009/07/21 2009/07/21 3275124 O-TERPHENYL (sur.) 96 60 - 130 % 2009/07/16 2009/07/17 JM7 3276700 VOLATILE ORGANICS BY GC-MS (WATER) Volatiles B e n z e n e <0.4 0.4 ug/L 2009/07/16 2009/07/21 CD1 3276635 T o l u e n e <0.4 0.4 ug/L 2009/07/16 2009/07/21 CD1 3276635 E t h y l b e n z e n e <0.4 0.4 ug/L 2009/07/16 2009/07/21 CD1 3276635 o - X y l e n e <0.4 0.4 ug/L 2009/07/16 2009/07/21 CD1 3276635 m & p-Xylene <0.8 0.8 ug/L 2009/07/16 2009/07/21 CD1 3276635 Xylenes (Total) <0.8 0.8 ug/L 2009/07/16 2009/07/21 CD1 3276635 F1 (C6-C10) - BTEX <100 100 ug/L 2009/07/16 2009/07/21 CD1 3276635 LH (C5-C10) <100 100 ug/L 2009/07/16 2009/07/21 CD1 3276635 ( C 6 - C 1 0 ) <100 100 ug/L 2009/07/16 2009/07/21 CD1 3276635 4-BROMOFLUOROBENZENE (sur.) 96 70 - 130 % 2009/07/16 2009/07/21 CD1 3276635 D4-1,2-DICHLOROETHANE (sur.) 110 70 - 130 % 2009/07/16 2009/07/21 CD1 3276635 D8-TOLUENE (sur.) 99 70 - 130 % 2009/07/16 2009/07/21 CD1 3276635 RESULTS OF CHEMICAL ANALYSES OF WATER Calculated Parameters Hardness (CaCO3) 16 0.5 mg/L 2009/07/18 2009/07/18 3275115 Total Dissolved Solids 3600 10 mg/L 2009/07/19 2009/07/19 3275123 Misc. Inorganics p H 8.28 N/A N/A 2009/07/17 2009/07/18 MG5 3282817 Anions Alkalinity (PP as CaCO3) <0.5 0.5 mg/L 2009/07/17 2009/07/18 MG5 3282799 Alkalinity (Total as CaCO3) 2700 0.5 mg/L 2009/07/17 2009/07/18 MG5 3282799 Bicarbonate (HCO3) 3300 0.5 mg/L 2009/07/17 2009/07/18 MG5 3282799 Carbonate (CO3) <0.5 0.5 mg/L 2009/07/17 2009/07/18 MG5 3282799 Hydroxide (OH) <0.5 0.5 mg/L 2009/07/17 2009/07/18 MG5 3282799 Misc. Organics Oil and grease 3 2 mg/L 2009/07/17 2009/07/20 CL4 3279937 SEMIVOLATILE ORGANICS BY GC-MS (WATER) Polycyclic Aromatics Benzo[a]pyrene equivalency 0.01 0.01 ug/L 2009/07/18 2009/07/18 3275120

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General Comments

Sample P77219-01: Dissolved Metals > Total Metals for some parameters; analysis from separate sample bottles.

Sample P77246-01: Dissolved Metals > Total Metals for some parameters; analysis from separate sample bottles

Results relate only to the items tested.

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WORLEYPARSONSAttention: MELANIE EVANS Client Project #: C61334026P.O. #: 30102893Site Reference: PEACE RIVER

Quality Assurance ReportMaxxam Job Number: EA936113

QA/QC DateBatch AnalyzedNum Init QC Type Parameter yyyy/mm/dd Value Recovery Units QC Limits

3271880 MB7 MATRIX SPIKE D10-ANTHRACENE (sur.) 2009/07/16 100 % 30 - 130D12-BENZO(A)PYRENE (sur.) 2009/07/16 89 % 30 - 130D8-ACENAPHTHYLENE (sur.) 2009/07/16 85 % 30 - 130TERPHENYL-D14 (sur.) 2009/07/16 96 % 30 - 130Acenaphthene 2009/07/16 86 % 30 - 130Acenaphthylene 2009/07/16 90 % 30 - 130Acridine 2009/07/16 76 % 30 - 130Anthracene 2009/07/16 78 % 30 - 130Benzo(a)anthracene 2009/07/16 81 % 30 - 130Benzo(b&j)fluoranthene 2009/07/16 80 % 30 - 130Benzo(k)fluoranthene 2009/07/16 87 % 30 - 130Benzo(g,h,i)perylene 2009/07/16 86 % 30 - 130Benzo(c)phenanthrene 2009/07/16 90 % 30 - 130Benzo(a)pyrene 2009/07/16 81 % 30 - 130Benzo[e]pyrene 2009/07/16 87 % 30 - 130Chrysene 2009/07/16 94 % 30 - 130Dibenz(a,h)anthracene 2009/07/16 107 % 30 - 130Fluoranthene 2009/07/16 85 % 30 - 130Fluorene 2009/07/16 88 % 30 - 130Indeno(1,2,3-cd)pyrene 2009/07/16 74 % 30 - 1302-Methylnaphthalene 2009/07/16 93 % 30 - 130Naphthalene 2009/07/16 89 % 30 - 130Phenanthrene 2009/07/16 88 % 30 - 130Perylene 2009/07/16 82 % 30 - 130Pyrene 2009/07/16 84 % 30 - 130Quinoline 2009/07/16 18 ( 1 ) % 30 - 130

SPIKE D10-ANTHRACENE (sur.) 2009/07/16 110 % 30 - 130D12-BENZO(A)PYRENE (sur.) 2009/07/16 97 % 30 - 130D8-ACENAPHTHYLENE (sur.) 2009/07/16 92 % 30 - 130TERPHENYL-D14 (sur.) 2009/07/16 106 % 30 - 130Acenaphthene 2009/07/16 96 % 30 - 130Acenaphthylene 2009/07/16 96 % 30 - 130Acridine 2009/07/16 80 % 30 - 130Anthracene 2009/07/16 91 % 30 - 130Benzo(a)anthracene 2009/07/16 95 % 30 - 130Benzo(b&j)fluoranthene 2009/07/16 90 % 30 - 130Benzo(k)fluoranthene 2009/07/16 102 % 30 - 130Benzo(g,h,i)perylene 2009/07/16 96 % 30 - 130Benzo(c)phenanthrene 2009/07/16 101 % 30 - 130Benzo(a)pyrene 2009/07/16 100 % 30 - 130Benzo[e]pyrene 2009/07/16 99 % 30 - 130Chrysene 2009/07/16 107 % 30 - 130Dibenz(a,h)anthracene 2009/07/16 108 % 30 - 130Fluoranthene 2009/07/16 95 % 30 - 130Fluorene 2009/07/16 96 % 30 - 130Indeno(1,2,3-cd)pyrene 2009/07/16 96 % 30 - 1302-Methylnaphthalene 2009/07/16 96 % 30 - 130Naphthalene 2009/07/16 94 % 30 - 130Phenanthrene 2009/07/16 96 % 30 - 130Perylene 2009/07/16 94 % 30 - 130Pyrene 2009/07/16 96 % 30 - 130Quinoline 2009/07/16 15 ( 1 ) % 30 - 130

BLANK D10-ANTHRACENE (sur.) 2009/07/15 109 % 30 - 130D12-BENZO(A)PYRENE (sur.) 2009/07/15 93 % 30 - 130D8-ACENAPHTHYLENE (sur.) 2009/07/15 92 % 30 - 130


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Quality Assurance Report (Continued)Maxxam Job Number: EA936113


3271880 MB7 BLANK TERPHENYL-D14 (sur.) 2009/07/15 108 % 30 - 130Acenaphthene 2009/07/15 <0.10 ug/LAcenaphthylene 2009/07/15 <0.10 ug/LAcridine 2009/07/15 <0.20 ug/LAnthracene 2009/07/15 <0.010 ug/LBenzo(a)anthracene 2009/07/15 <0.0085 ug/LBenzo(b&j)fluoranthene 2009/07/15 <0.0085 ug/LBenzo(k)fluoranthene 2009/07/15 <0.0085 ug/LBenzo(g,h,i)perylene 2009/07/15 <0.0085 ug/LBenzo(c)phenanthrene 2009/07/15 <0.050 ug/LBenzo(a)pyrene 2009/07/15 <0.0075 ug/LBenzo[e]pyrene 2009/07/15 <0.050 ug/LChrysene 2009/07/15 <0.0085 ug/LDibenz(a,h)anthracene 2009/07/15 0.0092, RDL=0.0075 ug/LFluoranthene 2009/07/15 <0.040 ug/LFluorene 2009/07/15 <0.050 ug/LIndeno(1,2,3-cd)pyrene 2009/07/15 0.0088, RDL=0.0085 ug/L2-Methylnaphthalene 2009/07/15 <0.10 ug/LNaphthalene 2009/07/15 <0.10 ug/LPhenanthrene 2009/07/15 <0.050 ug/LPerylene 2009/07/15 <0.050 ug/LPyrene 2009/07/15 <0.020 ug/LQuinoline 2009/07/15 <0.20 ug/L

RPD Acenaphthene 2009/07/16 NC % 40Acenaphthylene 2009/07/16 NC % 40Anthracene 2009/07/16 NC % 40Benzo(a)anthracene 2009/07/16 NC % 40Benzo(b&j)fluoranthene 2009/07/16 NC % 40Benzo(k)fluoranthene 2009/07/16 NC % 40Benzo(g,h,i)perylene 2009/07/16 NC % 40Benzo(a)pyrene 2009/07/16 NC % 40Chrysene 2009/07/16 NC % 40Dibenz(a,h)anthracene 2009/07/16 NC % 40Fluoranthene 2009/07/16 NC % 40Fluorene 2009/07/16 NC % 40Indeno(1,2,3-cd)pyrene 2009/07/16 NC % 40Naphthalene 2009/07/16 NC % 40Phenanthrene 2009/07/16 NC % 40Pyrene 2009/07/16 NC % 40

3275087 JA6 BLANK E.Coli DST 2009/07/14 <1 mpn/100mLTotal Coliforms DST 2009/07/14 <1 mpn/100mL

3276059 CD1 MATRIX SPIKE 4-BROMOFLUOROBENZENE (sur.) 2009/07/17 101 % 70 - 130D4-1,2-DICHLOROETHANE (sur.) 2009/07/17 98 % 70 - 130D8-TOLUENE (sur.) 2009/07/17 100 % 70 - 130Benzene 2009/07/17 99 % 70 - 130Toluene 2009/07/17 93 % 70 - 130Ethylbenzene 2009/07/17 103 % 70 - 130o-Xylene 2009/07/17 105 % 70 - 130m & p-Xylene 2009/07/17 105 % 70 - 130(C6-C10) 2009/07/17 83 % 70 - 130

SPIKE 4-BROMOFLUOROBENZENE (sur.) 2009/07/18 97 % 70 - 130D4-1,2-DICHLOROETHANE (sur.) 2009/07/18 120 % 70 - 130D8-TOLUENE (sur.) 2009/07/18 93 % 70 - 130Benzene 2009/07/18 95 % 70 - 130Toluene 2009/07/18 79 % 70 - 130


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3276059 CD1 SPIKE Ethylbenzene 2009/07/18 86 % 70 - 130o-Xylene 2009/07/18 88 % 70 - 130m & p-Xylene 2009/07/18 88 % 70 - 130(C6-C10) 2009/07/18 103 % 80 - 120

BLANK 4-BROMOFLUOROBENZENE (sur.) 2009/07/18 96 % 70 - 130D4-1,2-DICHLOROETHANE (sur.) 2009/07/18 111 % 70 - 130D8-TOLUENE (sur.) 2009/07/18 96 % 70 - 130Benzene 2009/07/18 <0.4 ug/LToluene 2009/07/18 <0.4 ug/LEthylbenzene 2009/07/18 <0.4 ug/Lo-Xylene 2009/07/18 <0.4 ug/Lm & p-Xylene 2009/07/18 <0.8 ug/LXylenes (Total) 2009/07/18 <0.8 ug/LF1 (C6-C10) - BTEX 2009/07/18 <100 ug/L(C6-C10) 2009/07/18 <100 ug/L

RPD Benzene 2009/07/20 NC % 40Toluene 2009/07/20 NC % 40Ethylbenzene 2009/07/20 NC % 40o-Xylene 2009/07/20 12.9 % 40m & p-Xylene 2009/07/20 15.1 % 40Xylenes (Total) 2009/07/20 14.1 % 40F1 (C6-C10) - BTEX 2009/07/20 4 9 . 3 ( 1 ) % 40(C6-C10) 2009/07/20 4 8 . 7 ( 2 ) % 40

3276635 CD1 MATRIX SPIKE 4-BROMOFLUOROBENZENE (sur.) 2009/07/17 100 % 70 - 130D4-1,2-DICHLOROETHANE (sur.) 2009/07/17 104 % 70 - 130D8-TOLUENE (sur.) 2009/07/17 97 % 70 - 130Benzene 2009/07/17 101 % 70 - 130Toluene 2009/07/17 92 % 70 - 130Ethylbenzene 2009/07/17 103 % 70 - 130o-Xylene 2009/07/17 103 % 70 - 130m & p-Xylene 2009/07/17 105 % 70 - 130(C6-C10) 2009/07/17 99 % 70 - 130

SPIKE 4-BROMOFLUOROBENZENE (sur.) 2009/07/17 95 % 70 - 130D4-1,2-DICHLOROETHANE (sur.) 2009/07/17 101 % 70 - 130D8-TOLUENE (sur.) 2009/07/17 97 % 70 - 130Benzene 2009/07/17 96 % 70 - 130Toluene 2009/07/17 87 % 70 - 130Ethylbenzene 2009/07/17 97 % 70 - 130o-Xylene 2009/07/17 99 % 70 - 130m & p-Xylene 2009/07/17 100 % 70 - 130(C6-C10) 2009/07/17 117 % 80 - 120

BLANK 4-BROMOFLUOROBENZENE (sur.) 2009/07/20 98 % 70 - 130D4-1,2-DICHLOROETHANE (sur.) 2009/07/20 104 % 70 - 130D8-TOLUENE (sur.) 2009/07/20 98 % 70 - 130Benzene 2009/07/20 <0.4 ug/LToluene 2009/07/20 <0.4 ug/LEthylbenzene 2009/07/20 <0.4 ug/Lo-Xylene 2009/07/20 <0.4 ug/Lm & p-Xylene 2009/07/20 <0.8 ug/LXylenes (Total) 2009/07/20 <0.8 ug/LF1 (C6-C10) - BTEX 2009/07/20 <100 ug/L(C6-C10) 2009/07/20 <100 ug/L

RPD Benzene 2009/07/20 NC % 40Toluene 2009/07/20 NC % 40Ethylbenzene 2009/07/20 NC % 40


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3276635 CD1 RPD o-Xylene 2009/07/20 NC % 40m & p-Xylene 2009/07/20 NC % 40Xylenes (Total) 2009/07/20 NC % 40F1 (C6-C10) - BTEX 2009/07/20 NC % 40(C6-C10) 2009/07/20 NC % 40

3276686 JM7 SPIKE O-TERPHENYL (sur.) 2009/07/17 98 % 70 - 130F2 (C10-C16 Hydrocarbons) 2009/07/17 97 % 80 - 120

BLANK O-TERPHENYL (sur.) 2009/07/17 101 % 70 - 130F2 (C10-C16 Hydrocarbons) 2009/07/17 <0.1 mg/L

3276700 JM7 SPIKE O-TERPHENYL (sur.) 2009/07/17 99 % 60 - 130Total Extractables C10 to C30 2009/07/17 87 % 70 - 130

BLANK O-TERPHENYL (sur.) 2009/07/17 101 % 60 - 130Total Extractables C10 to C30 2009/07/17 <0.1 mg/L

3276830 RW3 Calibration Check Turbidity 2009/07/16 100 % 80 - 120BLANK Turbidity 2009/07/16 <0.1 NTURPD Turbidity 2009/07/16 2.4 % 20

3276836 LF1 Calibration Check True Colour 2009/07/16 104 % 80 - 120BLANK True Colour 2009/07/16 <2 PtCo unitsRPD True Colour 2009/07/16 NC % 25

3277251 MG5 Calibration Check Dissolved Fluoride (F) 2009/07/16 92 % 80 - 120MATRIX SPIKE[P77219-01] Dissolved Fluoride (F) 2009/07/16 NC % 80 - 120BLANK Dissolved Fluoride (F) 2009/07/16 <0.05 mg/LRPD [ P 7 7 2 1 9 - 0 1 ] Dissolved Fluoride (F) 2009/07/16 0.6 % 20

3277509 RW3 Calibration Check Sulphide 2009/07/16 108 % 77 - 127BLANK Sulphide 2009/07/16 <0.002 mg/LRPD Sulphide 2009/07/16 NC % 20

3277865 VH2 MATRIX SPIKE Dissolved Mercury (Hg) 2009/07/17 87 % 80 - 120SPIKE Dissolved Mercury (Hg) 2009/07/17 100 % 80 - 120BLANK Dissolved Mercury (Hg) 2009/07/17 <0.001 ug/LRPD Dissolved Mercury (Hg) 2009/07/17 NC % 20

3277868 VH2 MATRIX SPIKE Total Mercury (Hg) 2009/07/17 91 % 80 - 120SPIKE Total Mercury (Hg) 2009/07/17 89 % 80 - 120BLANK Total Mercury (Hg) 2009/07/17 <0.001 ug/LRPD Total Mercury (Hg) 2009/07/17 NC % 20

3279352 RI3 Calibration Check Dissolved Barium (Ba) 2009/07/16 95 % 80 - 120Dissolved Boron (B) 2009/07/16 99 % 80 - 120Dissolved Calcium (Ca) 2009/07/16 98 % 80 - 120Dissolved Iron (Fe) 2009/07/16 91 % 80 - 120Dissolved Lithium (Li) 2009/07/16 98 % 80 - 120Dissolved Magnesium (Mg) 2009/07/16 97 % 80 - 120Dissolved Manganese (Mn) 2009/07/16 97 % 80 - 120Dissolved Phosphorus (P) 2009/07/16 104 % 80 - 120Dissolved Potassium (K) 2009/07/16 97 % 80 - 120Dissolved Silicon (Si) 2009/07/16 102 % 80 - 120Dissolved Sodium (Na) 2009/07/16 96 % 80 - 120Dissolved Strontium (Sr) 2009/07/16 96 % 80 - 120

MATRIX SPIKE Dissolved Barium (Ba) 2009/07/16 95 % 80 - 120Dissolved Boron (B) 2009/07/16 95 % 80 - 120Dissolved Calcium (Ca) 2009/07/16 NC % 80 - 120Dissolved Iron (Fe) 2009/07/16 84 % 80 - 120Dissolved Lithium (Li) 2009/07/16 97 % 80 - 120Dissolved Magnesium (Mg) 2009/07/16 93 % 80 - 120Dissolved Manganese (Mn) 2009/07/16 NC % 80 - 120Dissolved Phosphorus (P) 2009/07/16 108 % 80 - 120


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3279352 RI3 MATRIX SPIKE Dissolved Potassium (K) 2009/07/16 93 % 80 - 120Dissolved Silicon (Si) 2009/07/16 98 % 80 - 120Dissolved Sodium (Na) 2009/07/16 95 % 80 - 120Dissolved Strontium (Sr) 2009/07/16 93 % 80 - 120

SPIKE Dissolved Sulphur (S) 2009/07/16 103 % 80 - 120BLANK Dissolved Barium (Ba) 2009/07/16 <0.01 mg/L

Dissolved Boron (B) 2009/07/16 <0.02 mg/LDissolved Calcium (Ca) 2009/07/16 <0.3 mg/LDissolved Iron (Fe) 2009/07/16 <0.06 mg/LDissolved Lithium (Li) 2009/07/16 <0.02 mg/LDissolved Magnesium (Mg) 2009/07/16 <0.2 mg/LDissolved Manganese (Mn) 2009/07/16 <0.004 mg/LDissolved Phosphorus (P) 2009/07/16 <0.1 mg/LDissolved Potassium (K) 2009/07/16 <0.3 mg/LDissolved Silicon (Si) 2009/07/16 <0.1 mg/LDissolved Sodium (Na) 2009/07/16 <0.5 mg/LDissolved Strontium (Sr) 2009/07/16 <0.02 mg/LDissolved Sulphur (S) 2009/07/16 <0.2 mg/L

3279937 CL4 MATRIX SPIKE Oil and grease 2009/07/20 96 % 70 - 130SPIKE Oil and grease 2009/07/20 94 % 70 - 130BLANK Oil and grease 2009/07/20 <2 mg/LRPD Oil and grease 2009/07/20 NC % 40

3280112 AS7 Calibration Check Dissolved Aluminum (Al) 2009/07/17 110 % 80 - 120Dissolved Antimony (Sb) 2009/07/17 101 % 80 - 120Dissolved Arsenic (As) 2009/07/17 101 % 80 - 120Dissolved Beryllium (Be) 2009/07/17 112 % 80 - 120Dissolved Chromium (Cr) 2009/07/17 97 % 80 - 120Dissolved Cobalt (Co) 2009/07/17 103 % 80 - 120Dissolved Copper (Cu) 2009/07/17 100 % 80 - 120Dissolved Lead (Pb) 2009/07/17 102 % 80 - 120Dissolved Molybdenum (Mo) 2009/07/17 102 % 80 - 120Dissolved Nickel (Ni) 2009/07/17 101 % 80 - 120Dissolved Selenium (Se) 2009/07/17 102 % 80 - 120Dissolved Silver (Ag) 2009/07/17 100 % 80 - 120Dissolved Thallium (Tl) 2009/07/17 103 % 80 - 120Dissolved Tin (Sn) 2009/07/17 105 % 80 - 120Dissolved Titanium (Ti) 2009/07/17 104 % 80 - 120Dissolved Uranium (U) 2009/07/17 105 % 80 - 120Dissolved Vanadium (V) 2009/07/17 105 % 80 - 120Dissolved Zinc (Zn) 2009/07/17 105 % 80 - 120

MATRIX SPIKE Dissolved Aluminum (Al) 2009/07/17 NC % 80 - 120Dissolved Antimony (Sb) 2009/07/17 101 % 80 - 120Dissolved Arsenic (As) 2009/07/17 113 % 80 - 120Dissolved Beryllium (Be) 2009/07/17 120 % 80 - 120Dissolved Chromium (Cr) 2009/07/17 107 % 80 - 120Dissolved Cobalt (Co) 2009/07/17 112 % 80 - 120Dissolved Copper (Cu) 2009/07/17 107 % 80 - 120Dissolved Lead (Pb) 2009/07/17 110 % 80 - 120Dissolved Molybdenum (Mo) 2009/07/17 102 % 80 - 120Dissolved Nickel (Ni) 2009/07/17 107 % 80 - 120Dissolved Selenium (Se) 2009/07/17 117 % 80 - 120Dissolved Silver (Ag) 2009/07/17 109 % 80 - 120Dissolved Thallium (Tl) 2009/07/17 111 % 80 - 120Dissolved Tin (Sn) 2009/07/17 101 % 80 - 120Dissolved Titanium (Ti) 2009/07/17 118 % 80 - 120


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3280112 AS7 MATRIX SPIKE Dissolved Uranium (U) 2009/07/17 118 % 80 - 120Dissolved Vanadium (V) 2009/07/17 117 % 80 - 120Dissolved Zinc (Zn) 2009/07/17 113 % 80 - 120

BLANK Dissolved Aluminum (Al) 2009/07/17 <0.001 mg/LDissolved Antimony (Sb) 2009/07/17 <0.0002 mg/LDissolved Arsenic (As) 2009/07/17 <0.0002 mg/LDissolved Beryllium (Be) 2009/07/17 <0.001 mg/LDissolved Chromium (Cr) 2009/07/17 <0.001 mg/LDissolved Cobalt (Co) 2009/07/17 <0.0003 mg/LDissolved Copper (Cu) 2009/07/17 <0.0002 mg/LDissolved Lead (Pb) 2009/07/17 <0.0002 mg/LDissolved Molybdenum (Mo) 2009/07/17 <0.0002 mg/LDissolved Nickel (Ni) 2009/07/17 <0.0005 mg/LDissolved Selenium (Se) 2009/07/17 <0.0002 mg/LDissolved Silver (Ag) 2009/07/17 <0.0001 mg/LDissolved Thallium (Tl) 2009/07/17 <0.0002 mg/LDissolved Tin (Sn) 2009/07/17 <0.001 mg/LDissolved Titanium (Ti) 2009/07/17 <0.001 mg/LDissolved Uranium (U) 2009/07/17 <0.0001 mg/LDissolved Vanadium (V) 2009/07/17 <0.001 mg/LDissolved Zinc (Zn) 2009/07/17 <0.003 mg/L

RPD Dissolved Aluminum (Al) 2009/07/17 5.5 % 20Dissolved Antimony (Sb) 2009/07/17 NC % 20Dissolved Arsenic (As) 2009/07/17 1.4 % 20Dissolved Beryllium (Be) 2009/07/17 NC % 20Dissolved Chromium (Cr) 2009/07/17 NC % 20Dissolved Cobalt (Co) 2009/07/17 0.4 % 20Dissolved Copper (Cu) 2009/07/17 1.4 % 20Dissolved Lead (Pb) 2009/07/17 1.2 % 20Dissolved Molybdenum (Mo) 2009/07/17 NC % 20Dissolved Nickel (Ni) 2009/07/17 0.4 % 20Dissolved Selenium (Se) 2009/07/17 NC % 20Dissolved Silver (Ag) 2009/07/17 NC % 20Dissolved Thallium (Tl) 2009/07/17 NC % 20Dissolved Tin (Sn) 2009/07/17 NC % 20Dissolved Titanium (Ti) 2009/07/17 19.4 % 20Dissolved Uranium (U) 2009/07/17 2.4 % 20Dissolved Vanadium (V) 2009/07/17 NC % 20Dissolved Zinc (Zn) 2009/07/17 1.2 % 20

3281486 MKA MATRIX SPIKE Dissolved Sulphate (SO4) 2009/07/17 N/C % 80 - 120SPIKE Dissolved Sulphate (SO4) 2009/07/17 110 % 80 - 120BLANK Dissolved Sulphate (SO4) 2009/07/17 <1 mg/LRPD Dissolved Sulphate (SO4) 2009/07/17 6.0 ( 3 ) % 20

3281496 MKA MATRIX SPIKE Dissolved Chloride (Cl) 2009/07/17 N/C % 80 - 120SPIKE Dissolved Chloride (Cl) 2009/07/17 109 % 80 - 120BLANK Dissolved Chloride (Cl) 2009/07/17 <1 mg/LRPD Dissolved Chloride (Cl) 2009/07/17 1 ( 3 ) % 20

3281948 YY MATRIX SPIKE Phenols 2009/07/17 105 % 80 - 120SPIKE Phenols 2009/07/17 100 % 80 - 120BLANK Phenols 2009/07/17 <0.002 mg/LRPD Phenols 2009/07/17 NC % 20

3282799 MG5 Calibration Check Alkalinity (PP as CaCO3) TBA % N/AAlkalinity (Total as CaCO3) TBA % 80 - 120Bicarbonate (HCO3) TBA % N/ACarbonate (CO3) TBA % N/A


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3282799 MG5 Calibration Check Hydroxide (OH) TBA % N/ABLANK Alkalinity (PP as CaCO3) 2009/07/18 <0.5 mg/L

Alkalinity (Total as CaCO3) 2009/07/18 0.5, RDL=0.5 mg/LBicarbonate (HCO3) 2009/07/18 0.6, RDL=0.5 mg/LCarbonate (CO3) 2009/07/18 <0.5 mg/LHydroxide (OH) 2009/07/18 <0.5 mg/L

RPD Alkalinity (PP as CaCO3) 2009/07/18 NC % 20Alkalinity (Total as CaCO3) 2009/07/18 0.1 % 20Bicarbonate (HCO3) 2009/07/18 0.1 % 20Carbonate (CO3) 2009/07/18 NC % 20Hydroxide (OH) 2009/07/18 NC % 20

3282817 MG5 Calibration Check pH 2009/07/18 100 % 97 - 103RPD pH 2009/07/18 0.6 % 5

3282818 MG5 Calibration Check Conductivity 2009/07/18 101 % 80 - 120BLANK Conductivity 2009/07/18 1, RDL=1 uS/cmRPD Conductivity 2009/07/18 0.2 % 20

3282945 JQ Calibration Check Dissolved Nitrate (N) 2009/07/18 99 % 90 - 110Dissolved Nitrite (N) 2009/07/18 96 % 90 - 110

MATRIX SPIKE[P77219-01] Dissolved Nitrate (N) 2009/07/18 103 % 80 - 120

Dissolved Nitrite (N) 2009/07/18 101 % 80 - 120BLANK Dissolved Nitrate (N) 2009/07/18 <0.003 mg/L

Dissolved Nitrite (N) 2009/07/18 <0.003 mg/LRPD [ P 7 7 2 1 9 - 0 1 ] Dissolved Nitrate (N) 2009/07/18 NC % 20

Dissolved Nitrite (N) 2009/07/18 NC % 203283530 EO1 Calibration Check Total Aluminum (Al) 2009/07/19 105 % 80 - 120

Total Antimony (Sb) 2009/07/19 87 % 80 - 120Total Arsenic (As) 2009/07/19 81 % 80 - 120Total Beryllium (Be) 2009/07/19 92 % 80 - 120Total Chromium (Cr) 2009/07/19 91 % 80 - 120Total Cobalt (Co) 2009/07/19 95 % 80 - 120Total Copper (Cu) 2009/07/19 87 % 80 - 120Total Lead (Pb) 2009/07/19 94 % 80 - 120Total Molybdenum (Mo) 2009/07/19 99 % 80 - 120Total Nickel (Ni) 2009/07/19 92 % 80 - 120Total Selenium (Se) 2009/07/19 81 % 80 - 120Total Silver (Ag) 2009/07/19 95 % 80 - 120Total Thallium (Tl) 2009/07/19 95 % 80 - 120Total Tin (Sn) 2009/07/19 98 % 80 - 120Total Titanium (Ti) 2009/07/19 95 % 80 - 120Total Uranium (U) 2009/07/19 94 % 80 - 120Total Vanadium (V) 2009/07/19 95 % 80 - 120Total Zinc (Zn) 2009/07/19 80 % 80 - 120

MATRIX SPIKE Total Aluminum (Al) 2009/07/19 NC % 80 - 120Total Antimony (Sb) 2009/07/19 117 % 80 - 120Total Arsenic (As) 2009/07/19 95 % 80 - 120Total Beryllium (Be) 2009/07/19 100 % 80 - 120Total Chromium (Cr) 2009/07/19 101 % 80 - 120Total Cobalt (Co) 2009/07/19 104 % 80 - 120Total Copper (Cu) 2009/07/19 91 % 80 - 120Total Lead (Pb) 2009/07/19 97 % 80 - 120Total Molybdenum (Mo) 2009/07/19 NC % 80 - 120Total Nickel (Ni) 2009/07/19 97 % 80 - 120Total Selenium (Se) 2009/07/19 85 % 80 - 120Total Silver (Ag) 2009/07/19 102 % 80 - 120


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3283530 EO1 MATRIX SPIKE Total Thallium (Tl) 2009/07/19 99 % 80 - 120Total Tin (Sn) 2009/07/19 114 % 80 - 120Total Titanium (Ti) 2009/07/19 109 % 80 - 120Total Uranium (U) 2009/07/19 104 % 80 - 120Total Vanadium (V) 2009/07/19 111 % 80 - 120Total Zinc (Zn) 2009/07/19 87 % 80 - 120

BLANK Total Aluminum (Al) 2009/07/19 <0.001 mg/LTotal Antimony (Sb) 2009/07/19 <0.0002 mg/LTotal Arsenic (As) 2009/07/19 <0.0002 mg/LTotal Beryllium (Be) 2009/07/19 <0.001 mg/LTotal Chromium (Cr) 2009/07/19 <0.001 mg/LTotal Cobalt (Co) 2009/07/19 <0.0003 mg/LTotal Copper (Cu) 2009/07/19 <0.0002 mg/LTotal Lead (Pb) 2009/07/19 <0.0002 mg/LTotal Molybdenum (Mo) 2009/07/19 0.0004, RDL=0.0002 mg/LTotal Nickel (Ni) 2009/07/19 <0.0005 mg/LTotal Selenium (Se) 2009/07/19 <0.0002 mg/LTotal Silver (Ag) 2009/07/19 <0.0001 mg/LTotal Thallium (Tl) 2009/07/19 <0.0002 mg/LTotal Tin (Sn) 2009/07/19 <0.001 mg/LTotal Titanium (Ti) 2009/07/19 <0.001 mg/LTotal Uranium (U) 2009/07/19 <0.0001 mg/LTotal Vanadium (V) 2009/07/19 <0.001 mg/LTotal Zinc (Zn) 2009/07/19 <0.003 mg/L

RPD Total Aluminum (Al) 2009/07/19 10.8 % 20Total Antimony (Sb) 2009/07/19 NC % 20Total Arsenic (As) 2009/07/19 3.0 % 20Total Beryllium (Be) 2009/07/19 NC % 20Total Chromium (Cr) 2009/07/19 NC % 20Total Cobalt (Co) 2009/07/19 NC % 20Total Copper (Cu) 2009/07/19 4.8 % 20Total Lead (Pb) 2009/07/19 NC % 20Total Molybdenum (Mo) 2009/07/19 1.9 % 20Total Nickel (Ni) 2009/07/19 NC % 20Total Selenium (Se) 2009/07/19 NC % 20Total Silver (Ag) 2009/07/19 NC % 20Total Thallium (Tl) 2009/07/19 NC % 20Total Tin (Sn) 2009/07/19 NC % 20Total Titanium (Ti) 2009/07/19 NC % 20Total Uranium (U) 2009/07/19 7.3 % 20Total Vanadium (V) 2009/07/19 NC % 20Total Zinc (Zn) 2009/07/19 NC % 20

3283559 SG8 Calibration Check Total Barium (Ba) 2009/07/19 96 % 80 - 120Total Boron (B) 2009/07/19 101 % 80 - 120Total Calcium (Ca) 2009/07/19 99 % 80 - 120Total Iron (Fe) 2009/07/19 95 % 80 - 120Total Lithium (Li) 2009/07/19 99 % 80 - 120Total Magnesium (Mg) 2009/07/19 100 % 80 - 120Total Manganese (Mn) 2009/07/19 99 % 80 - 120Total Phosphorus (P) 2009/07/19 107 % 80 - 120Total Potassium (K) 2009/07/19 100 % 80 - 120Total Silicon (Si) 2009/07/19 100 % 80 - 120Total Sodium (Na) 2009/07/19 99 % 80 - 120Total Strontium (Sr) 2009/07/19 99 % 80 - 120

MATRIX SPIKE Total Barium (Ba) 2009/07/19 94 % 80 - 120


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3283559 SG8 MATRIX SPIKE Total Boron (B) 2009/07/19 100 % 80 - 120Total Calcium (Ca) 2009/07/19 NC % 80 - 120Total Iron (Fe) 2009/07/19 90 % 80 - 120Total Lithium (Li) 2009/07/19 98 % 80 - 120Total Magnesium (Mg) 2009/07/19 95 % 80 - 120Total Manganese (Mn) 2009/07/19 97 % 80 - 120Total Phosphorus (P) 2009/07/19 106 % 80 - 120Total Potassium (K) 2009/07/19 98 % 80 - 120Total Silicon (Si) 2009/07/19 96 % 80 - 120Total Sodium (Na) 2009/07/19 NC % 80 - 120Total Strontium (Sr) 2009/07/19 94 % 80 - 120

SPIKE Total Sulphur (S) 2009/07/19 103 % 80 - 120BLANK Total Barium (Ba) 2009/07/19 <0.01 mg/L

Total Boron (B) 2009/07/19 <0.02 mg/LTotal Calcium (Ca) 2009/07/19 <0.3 mg/LTotal Iron (Fe) 2009/07/19 <0.06 mg/LTotal Lithium (Li) 2009/07/19 <0.02 mg/LTotal Magnesium (Mg) 2009/07/19 <0.2 mg/LTotal Manganese (Mn) 2009/07/19 <0.004 mg/LTotal Phosphorus (P) 2009/07/19 0.1, RDL=0.1 mg/LTotal Potassium (K) 2009/07/19 <0.3 mg/LTotal Silicon (Si) 2009/07/19 <0.1 mg/LTotal Sodium (Na) 2009/07/19 <0.5 mg/LTotal Strontium (Sr) 2009/07/19 <0.02 mg/LTotal Sulphur (S) 2009/07/19 <0.2 mg/L

RPD Total Barium (Ba) 2009/07/19 3.4 % 20Total Boron (B) 2009/07/19 NC % 20Total Calcium (Ca) 2009/07/19 4.2 % 20Total Iron (Fe) 2009/07/19 NC % 20Total Lithium (Li) 2009/07/19 NC % 20Total Magnesium (Mg) 2009/07/19 3.3 % 20Total Manganese (Mn) 2009/07/19 3.1 % 20Total Phosphorus (P) 2009/07/19 3.4 % 20Total Potassium (K) 2009/07/19 3.4 % 20Total Silicon (Si) 2009/07/19 5.8 % 20Total Sodium (Na) 2009/07/19 3.4 % 20Total Strontium (Sr) 2009/07/19 3.4 % 20Total Sulphur (S) 2009/07/19 4.1 % 20

3283589 AL2 SPIKE Total Kjeldahl Nitrogen 2009/07/20 103 % 80 - 120BLANK Total Kjeldahl Nitrogen 2009/07/20 <0.05 mg/LRPD Total Kjeldahl Nitrogen 2009/07/20 NC % 20

3283618 AL2 MATRIX SPIKE Total Ammonia (N) 2009/07/20 110 % 80 - 120SPIKE Total Ammonia (N) 2009/07/20 99 % 86 - 110BLANK Total Ammonia (N) 2009/07/20 <0.05 mg/LRPD Total Ammonia (N) 2009/07/20 NC % 20

3285973 YY MATRIX SPIKE[P77219-06] Dissolved Organic Carbon (C) 2009/07/20 NC % 80 - 120SPIKE Dissolved Organic Carbon (C) 2009/07/20 100 % 80 - 120BLANK Dissolved Organic Carbon (C) 2009/07/20 <0.5 mg/LRPD [ P 7 7 2 1 9 - 0 6 ] Dissolved Organic Carbon (C) 2009/07/20 1.5 % 20

3285976 YY MATRIX SPIKE Total Organic Carbon (C) 2009/07/20 NC % 80 - 120SPIKE Total Organic Carbon (C) 2009/07/20 104 % 80 - 120BLANK Total Organic Carbon (C) 2009/07/20 <0.5 mg/LRPD Total Organic Carbon (C) 2009/07/20 3.0 % 20

N/A = Not Applicable


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TBA = Result to followNC = Non-calculableRPD = Relative Percent Difference( 1 ) Please note that the recovery of some compounds are outside control limits however the overall quality control for this analysis meets ouracceptability criteria.( 2 ) Duplicate exceeds acceptance criteria due to sample matrix. Reanalysis yields similar results( 3 ) Detection limits raised due to dilution to bring analyte within the calibrated range.


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Validation Signature Page

Maxxam Job #: A936113

The analytical data and all QC contained in this report were reviewed and validated by the following individual(s).

DIANE ZACHARKIW, Scientific Specialist

HUA WO,

LISA CUMMINGS, Extractables Supervisor

LUBA SHYMUSHOVSKA, Senior Analyst, Organic Department

LILI ZHOU, Senior analyst, Inorganic department.

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Validation Signature Page

Maxxam Job #: A936113

The analytical data and all QC contained in this report were reviewed and validated by the following individual(s).

PETER CHOW, Senior Analyst

ROBERT VIVIAN, Senior Analyst

====================================================================Maxxam has procedures in place to guard against improper use of the electronic signature and have the required "signatories", as per section 5.10.2 ofISO/IEC 17025:2005(E), signing the reports. SCC and CALA have approved this reporting process and electronic report format.

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