analytical report 482073 - azdeq.gov · · 2014-04-16analytical report 482073 for terranext...

Analytical Report 482073for

Terranext

Project Manager: Chuck Gordon

WVBA

15-APR-14

3154-25

3725 E. Atlanta Ave, Phoenix, AZ 85040Ph: (602) 437-0330

Phoenix (EPA Lab Code: AZ00901): Arizona(AZ0757)Phoenix Mobile (EPA Lab code: AZ00901): Arizona (AZM757)

Collected By: Client

of 112 Final 1.000

Houston - Dallas - Odessa - San Antonio - Tampa - Lakeland - Atlanta - Phoenix - Oklahoma - Latin America

Recipient of the Prestigious Small Business Administration Award of Excellence in 1994.Certified and approved by numerous States and Agencies.

A Small Business and Minority Status Company that delivers SERVICE and QUALITY

Project Manager: Chuck Gordon Terranext4050 E. Cotton Center Blvd.Phoenix, AZ 85040 Reference: TWA Report No(s): 482073 WVBA Project Address:

Chuck Gordon:

We are reporting to you the results of the analyses performed on the samples received under the project namereferenced above and identified with the TWA Report Number(s) 482073. All results being reported underthis Report Number apply to the samples analyzed and properly identified with a Laboratory ID number.Subcontracted analyses are identified in this report with either the NELAC certification number of thesubcontract lab in the analyst ID field, or the complete subcontracted report attached to this report.

Unless otherwise noted in a Case Narrative, all data reported in this Analytical Report are in compliance withNELAC standards. The uncertainty of measurement associated with the results of analysis reported is availableupon request. Should insufficient sample be provided to the laboratory to meet the method and NELAC MatrixDuplicate and Matrix Spike requirements, then the data will be analyzed, evaluated and reported using allother available quality control measures.

The validity and integrity of this report will remain intact as long as it is accompanied by this letter andreproduced in full, unless written approval is granted by TransWest Analytical. This report will be filed for atleast 5 years in our archives after which time it will be destroyed without further notice, unless otherwisearranged with you. The samples received, and described as recorded in Report No. 482073 will be filed for 60days, and after that time they will be properly disposed without further notice, unless otherwise arranged withyou. We reserve the right to return to you any unused samples, extracts or solutions related to them if weconsider so necessary (e.g., samples identified as hazardous waste, sample sizes exceeding analytical standardpractices, controlled substances under regulated protocols, etc).

We thank you for selecting TransWest Analytical to serve your analytical needs. If you have any questionsconcerning this report, please feel free to contact us at any time.

Respectfully,

15-APR-14

Project ManagerSkip Harden

of 112 Final 1.000

CASE NARRATIVE

482073Work Order Number(s):15-APR-14Report Date: 3154-25Project ID:

Project Name: WVBA

Date Received:

Client Name: Terranext

03/27/2014

None

None

Sample receipt non conformances and comments:

Sample receipt non conformances and comments per sample:

of 112 Final 1.000

Flagging Criteria

R5

All method blanks, laboratory spikes, and/or matrix spikes met quality control objectives for the parametersassociated with this Work Order except as detailed below or on the Data Qualifier page of this report. DataQualifiers used in this report are in accordance with ADEQ Arizona Data Qualifiers, Revision 3.0 9/20/2007.Data qualifiers (flags) contained within this analytical report have been issued to explain a quality controldeficiency, and do not affect the quality (validity) of the data unless noted otherwise in the case narrative.

MS/MSD RPD exceeded the laboratory acceptance limit. Recovery met acceptance criteria.

Arizona Flags

of 112 Final 1.000

Sample Cross Reference 482073

Terranext, Phoenix, AZWVBA

Sample Id

43A Canal67A Canal83A CanalSalt CanalRID-105RID-106RID-107RID-96RID-108RID-109RID-110EQBRID-111RRID-113RID-114RID-104RID-102RID-103RID-101RID-100RID-99RID-97RID-95RID-94RID-93RID-91RID-92RID-90RID-89RID-88Trip Blank

03-27-14 07:2703-27-14 08:1503-27-14 08:4203-27-14 09:0403-27-14 09:2503-27-14 09:3903-27-14 09:5203-27-14 10:0003-27-14 10:0803-27-14 10:2103-27-14 10:3703-27-14 10:4303-27-14 10:3503-27-14 11:4603-27-14 11:5803-27-14 12:1503-27-14 12:3903-27-14 12:5603-27-14 13:1303-27-14 13:3203-27-14 13:4803-27-14 13:5603-27-14 14:0803-27-14 14:0003-27-14 14:3803-27-14 14:5103-27-14 15:0503-27-14 15:1803-27-14 15:3603-27-14 15:5003-27-14 07:27

Date Collected Lab Sample Id

482073-001482073-002482073-003482073-004482073-005482073-006482073-007482073-008482073-009482073-010482073-011482073-012482073-013482073-014482073-015482073-016482073-017482073-018482073-019482073-020482073-021482073-022482073-023482073-024482073-025482073-026482073-027482073-028482073-029482073-030482073-031

Sample DepthMatrix

WWWWWWWWWWWWWWWWWWWWWWWWWWWWWWW

of 112 Final 1.000

Certificate of Analytical Results 482073


03.27.14 16.40 Date Received:03.27.14 07.27 Date Collected:482073-001Lab Sample Id:WaterMatrix: 43A CanalSample Id:

Total Metals by EPA 6010B

Metals, Dissolved, by EPA 6010B

Chromium Hexavalent by SM 3500 Cr-D

Analytical Method:

Analytical Method:

Analytical Method:

MKO

MKO

TNL

Analyst:

Analyst:

Analyst:

SW3010A

SW3010A

Prep Method:

Prep Method:

04.03.14 10.10

04.07.14 11.00

Date Prep:

Date Prep:

MLI

MLI

RYR

Tech:

Tech:

Tech:

Chromium

Chromium

Chromium, Hexavalent

Parameter

Parameter

Parameter

Result

Result

Result

0.0100

0.0100

0.00500

Flag

Flag

Flag

mg/L

mg/L

mg/L

Units

Units

Units

1

1

1

Dil

Dil

Dil

Cas Number

Cas Number

Cas Number

7440-47-3

7440-47-3

18540-29-9

<0.0100

<0.0100

0.00500

938379

938352

937261

Seq Number:

Seq Number:

Seq Number:

SUB: AZ0765

SUB: AZ0765

RL

RL

RL

04.11.14 11.26

04.11.14 05.01

03.28.14 07.09

Analysis Date

Analysis Date

Analysis Date

% Moisture:

% Moisture:

% Moisture:

of 112 Final 1.000




VOCs by EPA 8260B Analytical Method:

OEMAnalyst:

SW5030CPrep Method:

03.31.14 21.52 Date Prep:

OEMTech:

Acetone Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone MTBE n-Butylbenzene Sec-Butylbenzene tert-Butylbenzene Carbon Disulfide Carbon Tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene p-Cymene (p-Isopropyltoluene) Dibromochloromethane 1,2-Dibromo-3-Chloropropane 1,2-Dibromoethane Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene

Parameter Result

20.0 0.500

1.50 0.500 0.500

1.00 5.00 5.00 2.00 2.50 1.50 2.50

0.500 0.500 0.500

4.00 0.500

5.00 1.50 2.00 1.50

0.500 2.00

0.500 0.500

1.50 1.50 1.50 2.00

0.500 0.500 0.500 0.500 0.500 0.500

1.00 0.500

1.00 1.00

Flag

ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L

Units

1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1

DilCas Number

67-64-171-43-2108-86-174-97-575-27-475-25-274-83-978-93-31634-04-4104-51-8135-98-898-06-675-15-056-23-5108-90-775-00-367-66-374-87-395-49-8106-43-499-87-6124-48-196-12-8106-93-474-95-395-50-1541-73-1106-46-775-71-875-34-3107-06-275-35-4156-59-2156-60-578-87-5142-28-9594-20-7563-58-610061-01-5

<20.0<0.500

<1.50<0.500

4.64 <1.00<5.00<5.00<2.00<2.50<1.50<2.50

<0.500<0.500<0.500

<4.006.56

<5.00<1.50<2.00<1.501.91

<2.00<0.500<0.500

<1.50<1.50<1.50<2.00

<0.500<0.5000.610 0.580

<0.500<0.500

<1.00<0.500

<1.00<1.00

937532Seq Number:

RL

04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09

Analysis Date

% Moisture:

of 112 Final 1.000





OEMAnalyst:

SW5030CPrep Method:

03.31.14 21.52 Date Prep:

OEMTech:

trans-1,3-dichloropropene Ethylbenzene Hexachlorobutadiene 2-Hexanone isopropylbenzene Methylene Chloride Iodomethane (Methyl Iodide) 4-Methyl-2-Pentanone Naphthalene n-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethylene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene o-Xylene m,p-Xylenes Vinyl Acetate Vinyl Chloride Total Xylenes

Parameter Result

0.500 2.00 5.00 5.00 2.50 3.00 2.00 5.00 5.00 2.00 1.00

0.500 0.500 0.500

2.00 5.00 5.00

0.500 0.500 0.500

2.00 1.00 2.00 1.50 1.00 2.00 5.00

0.500 1.00

Flag

ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L

Units

1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1

DilCas Number

10061-02-6100-41-487-68-3591-78-698-82-875-09-274-88-4108-10-191-20-3103-65-1100-42-5630-20-679-34-5127-18-4108-88-387-61-6120-82-171-55-679-00-579-01-675-69-496-18-495-63-6108-67-895-47-6179601-23-1108-05-475-01-41330-20-7

<0.500<2.00<5.00<5.00<2.50<3.00<2.00<5.00<5.00<2.00<1.00

<0.500<0.500

1.27 <2.00<5.00<5.00

<0.500<0.500

3.87 <2.00<1.00<2.00<1.50<1.00<2.00<5.00

<0.500<1.00

937532Seq Number:

RL

04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09

Analysis Date

Surrogate

69-13366-13970-13070-135

%Recovery Flag

%%%%

100104

9995

04.01.14 02.09 04.01.14 02.09 04.01.14 02.09 04.01.14 02.09

Cas Number

1868-53-717060-07-02037-26-5460-00-4

Units Analysis Date

Dibromofluoromethane 1,2-Dichloroethane-D4 Toluene-D8 4-Bromofluorobenzene

Limits

% Moisture:

of 112 Final 1.000







Analytical Method:

Analytical Method:

Analytical Method:

MKO

MKO

TNL

Analyst:

Analyst:

Analyst:

SW3010A

SW3010A

Prep Method:

Prep Method:

04.03.14 10.10

04.07.14 11.00

Date Prep:

Date Prep:

MLI

MLI

RYR

Tech:

Tech:

Tech:

Chromium

Chromium


Parameter

Parameter

Parameter

Result

Result

Result

0.0100

0.0100

0.00500

Flag

Flag

Flag

mg/L

mg/L

mg/L

Units

Units

Units

1

1

1

Dil

Dil

Dil

Cas Number

Cas Number

Cas Number

7440-47-3

7440-47-3

18540-29-9

<0.0100

<0.0100

<0.00500

938379

938352

937261

Seq Number:

Seq Number:

Seq Number:

SUB: AZ0765

SUB: AZ0765

RL

RL

RL

04.11.14 11.59

04.11.14 05.33

03.28.14 07.09

Analysis Date

Analysis Date

Analysis Date

% Moisture:

% Moisture:

% Moisture:

of 112 Final 1.000





OEMAnalyst:

SW5030CPrep Method:

03.31.14 21.52 Date Prep:

OEMTech:


Parameter Result

20.0 0.500

1.50 0.500 0.500

1.00 5.00 5.00 2.00 2.50 1.50 2.50

0.500 0.500 0.500

4.00 0.500

5.00 1.50 2.00 1.50

0.500 2.00

0.500 0.500

1.50 1.50 1.50 2.00

0.500 0.500 0.500 0.500 0.500 0.500

1.00 0.500

1.00 1.00

Flag


Units

1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1

DilCas Number

67-64-171-43-2108-86-174-97-575-27-475-25-274-83-978-93-31634-04-4104-51-8135-98-898-06-675-15-056-23-5108-90-775-00-367-66-374-87-395-49-8106-43-499-87-6124-48-196-12-8106-93-474-95-395-50-1541-73-1106-46-775-71-875-34-3107-06-275-35-4156-59-2156-60-578-87-5142-28-9594-20-7563-58-610061-01-5

<20.0<0.500

<1.50<0.500

3.74 <1.00<5.00<5.00<2.00<2.50<1.50<2.50

<0.500<0.500<0.500

<4.005.82

<5.00<1.50<2.00<1.501.52

<2.00<0.500<0.500

<1.50<1.50<1.50<2.00

<0.500<0.500<0.500<0.500<0.500<0.500

<1.00<0.500

<1.00<1.00

937532Seq Number:

RL

04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35

Analysis Date

% Moisture:

of 112 Final 1.000





OEMAnalyst:

SW5030CPrep Method:

03.31.14 21.52 Date Prep:

OEMTech:


Parameter Result

0.500 2.00 5.00 5.00 2.50 3.00 2.00 5.00 5.00 2.00 1.00

0.500 0.500 0.500

2.00 5.00 5.00

0.500 0.500 0.500

2.00 1.00 2.00 1.50 1.00 2.00 5.00

0.500 1.00

Flag


Units

1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1

DilCas Number

10061-02-6100-41-487-68-3591-78-698-82-875-09-274-88-4108-10-191-20-3103-65-1100-42-5630-20-679-34-5127-18-4108-88-387-61-6120-82-171-55-679-00-579-01-675-69-496-18-495-63-6108-67-895-47-6179601-23-1108-05-475-01-41330-20-7

<0.500<2.00<5.00<5.00<2.50<3.00<2.00<5.00<5.00<2.00<1.00

<0.500<0.500

1.17 <2.00<5.00<5.00

<0.500<0.500

3.56 <2.00<1.00<2.00<1.50<1.00<2.00<5.00

<0.500<1.00

937532Seq Number:

RL

04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35

Analysis Date

Surrogate

69-13366-13970-13070-135

%Recovery Flag

%%%%

100106101

95

04.01.14 02.35 04.01.14 02.35 04.01.14 02.35 04.01.14 02.35

Cas Number

1868-53-717060-07-02037-26-5460-00-4

Units Analysis Date


Limits

% Moisture:

of 112 Final 1.000







Analytical Method:

Analytical Method:

Analytical Method:

MKO

MKO

TNL

Analyst:

Analyst:

Analyst:

SW3010A

SW3010A

Prep Method:

Prep Method:

04.03.14 10.10

04.07.14 11.00

Date Prep:

Date Prep:

MLI

MLI

RYR

Tech:

Tech:

Tech:

Chromium

Chromium


Parameter

Parameter

Parameter

Result

Result

Result

0.0100

0.0100

0.00500

Flag

Flag

Flag

mg/L

mg/L

mg/L

Units

Units

Units

1

1

1

Dil

Dil

Dil

Cas Number

Cas Number

Cas Number

7440-47-3

7440-47-3

18540-29-9

<0.0100

<0.0100

<0.00500

938379

938352

937261

Seq Number:

Seq Number:

Seq Number:

SUB: AZ0765

SUB: AZ0765

RL

RL

RL

04.11.14 12.18

04.11.14 05.39

03.28.14 07.09

Analysis Date

Analysis Date

Analysis Date

% Moisture:

% Moisture:

% Moisture:

of 112 Final 1.000





OEMAnalyst:

SW5030CPrep Method:

03.31.14 21.52 Date Prep:

OEMTech:


Parameter Result

20.0 0.500

1.50 0.500 0.500

1.00 5.00 5.00 2.00 2.50 1.50 2.50

0.500 0.500 0.500

4.00 0.500

5.00 1.50 2.00 1.50

0.500 2.00

0.500 0.500

1.50 1.50 1.50 2.00

0.500 0.500 0.500 0.500 0.500 0.500

1.00 0.500

1.00 1.00

Flag


Units

1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1

DilCas Number

67-64-171-43-2108-86-174-97-575-27-475-25-274-83-978-93-31634-04-4104-51-8135-98-898-06-675-15-056-23-5108-90-775-00-367-66-374-87-395-49-8106-43-499-87-6124-48-196-12-8106-93-474-95-395-50-1541-73-1106-46-775-71-875-34-3107-06-275-35-4156-59-2156-60-578-87-5142-28-9594-20-7563-58-610061-01-5

<20.0<0.500

<1.50<0.500

2.43 <1.00<5.00<5.00<2.00<2.50<1.50<2.50

<0.500<0.500<0.500

<4.004.25

<5.00<1.50<2.00<1.501.05

<2.00<0.500<0.500

<1.50<1.50<1.50<2.00

<0.500<0.500<0.500<0.500<0.500<0.500

<1.00<0.500

<1.00<1.00

937532Seq Number:

RL

04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01

Analysis Date

% Moisture:

of 112 Final 1.000





OEMAnalyst:

SW5030CPrep Method:

03.31.14 21.52 Date Prep:

OEMTech:


Parameter Result

0.500 2.00 5.00 5.00 2.50 3.00 2.00 5.00 5.00 2.00 1.00

0.500 0.500 0.500

2.00 5.00 5.00

0.500 0.500 0.500

2.00 1.00 2.00 1.50 1.00 2.00 5.00

0.500 1.00

Flag


Units

1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1

DilCas Number

10061-02-6100-41-487-68-3591-78-698-82-875-09-274-88-4108-10-191-20-3103-65-1100-42-5630-20-679-34-5127-18-4108-88-387-61-6120-82-171-55-679-00-579-01-675-69-496-18-495-63-6108-67-895-47-6179601-23-1108-05-475-01-41330-20-7

<0.500<2.00<5.00<5.00<2.50<3.00<2.00<5.00<5.00<2.00<1.00

<0.500<0.500

1.16 <2.00<5.00<5.00

<0.500<0.500

3.29 <2.00<1.00<2.00<1.50<1.00<2.00<5.00

<0.500<1.00

937532Seq Number:

RL

04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01

Analysis Date

Surrogate

69-13366-13970-13070-135

%Recovery Flag

%%%%

96104100

96

04.01.14 03.01 04.01.14 03.01 04.01.14 03.01 04.01.14 03.01

Cas Number

1868-53-717060-07-02037-26-5460-00-4

Units Analysis Date


Limits

% Moisture:

of 112 Final 1.000



03.27.14 16.40 Date Received:03.27.14 09.04 Date Collected:482073-004Lab Sample Id:WaterMatrix: Salt CanalSample Id:




Analytical Method:

Analytical Method:

Analytical Method:

MKO

MKO

TNL

Analyst:

Analyst:

Analyst:

SW3010A

SW3010A

Prep Method:

Prep Method:

04.03.14 10.10

04.07.14 11.00

Date Prep:

Date Prep:

MLI

MLI

RYR

Tech:

Tech:

Tech:

Chromium

Chromium


Parameter

Parameter

Parameter

Result

Result

Result

0.0100

0.0100

0.00500

Flag

Flag

Flag

mg/L

mg/L

mg/L

Units

Units

Units

1

1

1

Dil

Dil

Dil

Cas Number

Cas Number

Cas Number

7440-47-3

7440-47-3

18540-29-9

<0.0100

<0.0100

0.00600

938379

938352

937261

Seq Number:

Seq Number:

Seq Number:

SUB: AZ0765

SUB: AZ0765

RL

RL

RL

04.11.14 12.25

04.11.14 05.59

03.28.14 07.09

Analysis Date

Analysis Date

Analysis Date

% Moisture:

% Moisture:

% Moisture:

of 112 Final 1.000





OEMAnalyst:

SW5030CPrep Method:

03.31.14 21.52 Date Prep:

OEMTech:


Parameter Result

20.0 0.500

1.50 0.500 0.500

1.00 5.00 5.00 2.00 2.50 1.50 2.50

0.500 0.500 0.500

4.00 0.500

5.00 1.50 2.00 1.50

0.500 2.00

0.500 0.500

1.50 1.50 1.50 2.00

0.500 0.500 0.500 0.500 0.500 0.500

1.00 0.500

1.00 1.00

Flag


Units

1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1

DilCas Number

67-64-171-43-2108-86-174-97-575-27-475-25-274-83-978-93-31634-04-4104-51-8135-98-898-06-675-15-056-23-5108-90-775-00-367-66-374-87-395-49-8106-43-499-87-6124-48-196-12-8106-93-474-95-395-50-1541-73-1106-46-775-71-875-34-3107-06-275-35-4156-59-2156-60-578-87-5142-28-9594-20-7563-58-610061-01-5

<20.0<0.500

<1.50<0.500<0.500

<1.00<5.00<5.00<2.00<2.50<1.50<2.50

<0.500<0.500<0.500

<4.002.04

<5.00<1.50<2.00<1.50

<0.500<2.00

<0.500<0.500

<1.50<1.50<1.50<2.00

<0.500<0.5000.960 0.970

<0.500<0.500

<1.00<0.500

<1.00<1.00

937532Seq Number:

RL

04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19

Analysis Date

% Moisture:

of 112 Final 1.000





OEMAnalyst:

SW5030CPrep Method:

03.31.14 21.52 Date Prep:

OEMTech:


Parameter Result

0.500 2.00 5.00 5.00 2.50 3.00 2.00 5.00 5.00 2.00 1.00

0.500 0.500 0.500

2.00 5.00 5.00

0.500 0.500 0.500

2.00 1.00 2.00 1.50 1.00 2.00 5.00

0.500 1.00

Flag


Units

1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1

DilCas Number

10061-02-6100-41-487-68-3591-78-698-82-875-09-274-88-4108-10-191-20-3103-65-1100-42-5630-20-679-34-5127-18-4108-88-387-61-6120-82-171-55-679-00-579-01-675-69-496-18-495-63-6108-67-895-47-6179601-23-1108-05-475-01-41330-20-7

<0.500<2.00<5.00<5.00<2.50<3.00<2.00<5.00<5.00<2.00<1.00

<0.500<0.500

4.32 <2.00<5.00<5.00

<0.500<0.500

7.01 <2.00<1.00<2.00<1.50<1.00<2.00<5.00

<0.500<1.00

937532Seq Number:

RL

04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19

Analysis Date

Surrogate

69-13366-13970-13070-135

%Recovery Flag

%%%%

98101

9996

04.01.14 04.19 04.01.14 04.19 04.01.14 04.19 04.01.14 04.19

Cas Number

1868-53-717060-07-02037-26-5460-00-4

Units Analysis Date


Limits

% Moisture:

of 112 Final 1.000



03.27.14 16.40 Date Received:03.27.14 09.25 Date Collected:482073-005Lab Sample Id:WaterMatrix: RID-105Sample Id:




Analytical Method:

Analytical Method:

Analytical Method:

MKO

MKO

TNL

Analyst:

Analyst:

Analyst:

SW3010A

SW3010A

Prep Method:

Prep Method:

04.03.14 10.10

04.07.14 11.00

Date Prep:

Date Prep:

MLI

MLI

RYR

Tech:

Tech:

Tech:

Chromium

Chromium


Parameter

Parameter

Parameter

Result

Result

Result

0.0100

0.0100

0.00500

Flag

Flag

Flag

mg/L

mg/L

mg/L

Units

Units

Units

1

1

1

Dil

Dil

Dil

Cas Number

Cas Number

Cas Number

7440-47-3

7440-47-3

18540-29-9

0.0130

0.0134

0.0120

938379

938352

937261

Seq Number:

Seq Number:

Seq Number:

SUB: AZ0765

SUB: AZ0765

RL

RL

RL

04.11.14 12.32

04.11.14 06.05

03.28.14 07.09

Analysis Date

Analysis Date

Analysis Date

% Moisture:

% Moisture:

% Moisture:

of 112 Final 1.000





OEMAnalyst:

SW5030CPrep Method:

03.31.14 21.52 Date Prep:

OEMTech:


Parameter Result

20.0 0.500

1.50 0.500 0.500

1.00 5.00 5.00 2.00 2.50 1.50 2.50

0.500 0.500 0.500

4.00 0.500

5.00 1.50 2.00 1.50

0.500 2.00

0.500 0.500

1.50 1.50 1.50 2.00

0.500 0.500 0.500 0.500 0.500 0.500

1.00 0.500

1.00 1.00

Flag


Units

1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1

DilCas Number

67-64-171-43-2108-86-174-97-575-27-475-25-274-83-978-93-31634-04-4104-51-8135-98-898-06-675-15-056-23-5108-90-775-00-367-66-374-87-395-49-8106-43-499-87-6124-48-196-12-8106-93-474-95-395-50-1541-73-1106-46-775-71-875-34-3107-06-275-35-4156-59-2156-60-578-87-5142-28-9594-20-7563-58-610061-01-5

<20.0<0.500

<1.50<0.500<0.500

<1.00<5.00<5.00<2.00<2.50<1.50<2.50

<0.500<0.500<0.500

<4.00<0.500

<5.00<1.50<2.00<1.50

<0.500<2.00

<0.500<0.500

<1.50<1.50<1.50<2.00

<0.500<0.500<0.500<0.500<0.500<0.500

<1.00<0.500

<1.00<1.00

937532Seq Number:

RL

04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45

Analysis Date

% Moisture:

of 112 Final 1.000





OEMAnalyst:

SW5030CPrep Method:

03.31.14 21.52 Date Prep:

OEMTech:


Parameter Result

0.500 2.00 5.00 5.00 2.50 3.00 2.00 5.00 5.00 2.00 1.00

0.500 0.500 0.500

2.00 5.00 5.00

0.500 0.500 0.500

2.00 1.00 2.00 1.50 1.00 2.00 5.00

0.500 1.00

Flag


Units

1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1

DilCas Number

10061-02-6100-41-487-68-3591-78-698-82-875-09-274-88-4108-10-191-20-3103-65-1100-42-5630-20-679-34-5127-18-4108-88-387-61-6120-82-171-55-679-00-579-01-675-69-496-18-495-63-6108-67-895-47-6179601-23-1108-05-475-01-41330-20-7

<0.500<2.00<5.00<5.00<2.50<3.00<2.00<5.00<5.00<2.00<1.00

<0.500<0.500

2.39 <2.00<5.00<5.00

<0.500<0.5000.590 <2.00<1.00<2.00<1.50<1.00<2.00<5.00

<0.500<1.00

937532Seq Number:

RL

04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45

Analysis Date

Surrogate

69-13366-13970-13070-135

%Recovery Flag

%%%%

113113107100

04.01.14 04.45 04.01.14 04.45 04.01.14 04.45 04.01.14 04.45

Cas Number

1868-53-717060-07-02037-26-5460-00-4

Units Analysis Date


Limits

% Moisture:

of 112 Final 1.000







Analytical Method:

Analytical Method:

Analytical Method:

MKO

MKO

TNL

Analyst:

Analyst:

Analyst:

SW3010A

SW3010A

Prep Method:

Prep Method:

04.03.14 10.10

04.07.14 11.00

Date Prep:

Date Prep:

MLI

MLI

RYR

Tech:

Tech:

Tech:

Chromium

Chromium


Parameter

Parameter

Parameter

Result

Result

Result

0.0100

0.0100

0.00500

Flag

Flag

Flag

mg/L

mg/L

mg/L

Units

Units

Units

1

1

1

Dil

Dil

Dil

Cas Number

Cas Number

Cas Number

7440-47-3

7440-47-3

18540-29-9

<0.0100

<0.0100

0.00700

938379

938352

937261

Seq Number:

Seq Number:

Seq Number:

SUB: AZ0765

SUB: AZ0765

RL

RL

RL

04.11.14 12.38

04.11.14 06.12

03.28.14 07.09

Analysis Date

Analysis Date

Analysis Date

% Moisture:

% Moisture:

% Moisture:

of 112 Final 1.000





OEMAnalyst:

SW5030CPrep Method:

03.31.14 21.52 Date Prep:

OEMTech:


Parameter Result

20.0 0.500

1.50 0.500 0.500

1.00 5.00 5.00 2.00 2.50 1.50 2.50

0.500 0.500 0.500

4.00 0.500

5.00 1.50 2.00 1.50

0.500 2.00

0.500 0.500

1.50 1.50 1.50 2.00

0.500 0.500 0.500 0.500 0.500 0.500

1.00 0.500

1.00 1.00

Flag


Units

1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1

DilCas Number

67-64-171-43-2108-86-174-97-575-27-475-25-274-83-978-93-31634-04-4104-51-8135-98-898-06-675-15-056-23-5108-90-775-00-367-66-374-87-395-49-8106-43-499-87-6124-48-196-12-8106-93-474-95-395-50-1541-73-1106-46-775-71-875-34-3107-06-275-35-4156-59-2156-60-578-87-5142-28-9594-20-7563-58-610061-01-5

<20.0<0.500

<1.50<0.500<0.500

<1.00<5.00<5.00<2.00<2.50<1.50<2.50

<0.500<0.500<0.500

<4.001.69

<5.00<1.50<2.00<1.50

<0.500<2.00

<0.500<0.500

<1.50<1.50<1.50<2.00

<0.500<0.500

4.66 0.960

<0.500<0.500

<1.00<0.500

<1.00<1.00

937532Seq Number:

RL

04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11

Analysis Date

% Moisture:

of 112 Final 1.000





OEMAnalyst:

SW5030CPrep Method:

03.31.14 21.52 Date Prep:

OEMTech:


Parameter Result

0.500 2.00 5.00 5.00 2.50 3.00 2.00 5.00 5.00 2.00 1.00

0.500 0.500 0.500

2.00 5.00 5.00

0.500 0.500 0.500

2.00 1.00 2.00 1.50 1.00 2.00 5.00

0.500 1.00

Flag


Units

1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1

DilCas Number

10061-02-6100-41-487-68-3591-78-698-82-875-09-274-88-4108-10-191-20-3103-65-1100-42-5630-20-679-34-5127-18-4108-88-387-61-6120-82-171-55-679-00-579-01-675-69-496-18-495-63-6108-67-895-47-6179601-23-1108-05-475-01-41330-20-7

<0.500<2.00<5.00<5.00<2.50<3.00<2.00<5.00<5.00<2.00<1.00

<0.500<0.500

21.5 <2.00<5.00<5.00

<0.500<0.500

8.06 <2.00<1.00<2.00<1.50<1.00<2.00<5.00

<0.500<1.00

937532Seq Number:

RL

04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11

Analysis Date

Surrogate

69-13366-13970-13070-135

%Recovery Flag

%%%%

96102101

94

04.01.14 05.11 04.01.14 05.11 04.01.14 05.11 04.01.14 05.11

Cas Number

1868-53-717060-07-02037-26-5460-00-4

Units Analysis Date


Limits

% Moisture:

of 112 Final 1.000







Analytical Method:

Analytical Method:

Analytical Method:

MKO

MKO

TNL

Analyst:

Analyst:

Analyst:

SW3010A

SW3010A

Prep Method:

Prep Method:

04.03.14 10.10

04.07.14 11.00

Date Prep:

Date Prep:

MLI

MLI

RYR

Tech:

Tech:

Tech:

Chromium

Chromium


Parameter

Parameter

Parameter

Result

Result

Result

0.0100

0.0100

0.00500

Flag

Flag

Flag

mg/L

mg/L

mg/L

Units

Units

Units

1

1

1

Dil

Dil

Dil

Cas Number

Cas Number

Cas Number

7440-47-3

7440-47-3

18540-29-9

<0.0100

<0.0100

0.00600

938379

938352

937261

Seq Number:

Seq Number:

Seq Number:

SUB: AZ0765

SUB: AZ0765

RL

RL

RL

04.11.14 12.45

04.11.14 06.18

03.28.14 07.09

Analysis Date

Analysis Date

Analysis Date

% Moisture:

% Moisture:

% Moisture:

of 112 Final 1.000





OEMAnalyst:

SW5030CPrep Method:

03.31.14 21.52 Date Prep:

OEMTech:


Parameter Result

20.0 0.500

1.50 0.500 0.500

1.00 5.00 5.00 2.00 2.50 1.50 2.50

0.500 0.500 0.500

4.00 0.500

5.00 1.50 2.00 1.50

0.500 2.00

0.500 0.500

1.50 1.50 1.50 2.00

0.500 0.500 0.500 0.500 0.500 0.500

1.00 0.500

1.00 1.00

Flag


Units

1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1

DilCas Number

67-64-171-43-2108-86-174-97-575-27-475-25-274-83-978-93-31634-04-4104-51-8135-98-898-06-675-15-056-23-5108-90-775-00-367-66-374-87-395-49-8106-43-499-87-6124-48-196-12-8106-93-474-95-395-50-1541-73-1106-46-775-71-875-34-3107-06-275-35-4156-59-2156-60-578-87-5142-28-9594-20-7563-58-610061-01-5

<20.0<0.500

<1.50<0.500<0.500

<1.00<5.00<5.00<2.00<2.50<1.50<2.50

<0.500<0.500<0.500

<4.001.11

<5.00<1.50<2.00<1.50

<0.500<2.00

<0.500<0.500

<1.50<1.50<1.50<2.00

<0.500<0.500

2.38 <0.500<0.500<0.500

<1.00<0.500

<1.00<1.00

937532Seq Number:

RL

04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37

Analysis Date

% Moisture:

of 112 Final 1.000





OEMAnalyst:

SW5030CPrep Method:

03.31.14 21.52 Date Prep:

OEMTech:


Parameter Result

0.500 2.00 5.00 5.00 2.50 3.00 2.00 5.00 5.00 2.00 1.00

0.500 0.500 0.500

2.00 5.00 5.00

0.500 0.500 0.500

2.00 1.00 2.00 1.50 1.00 2.00 5.00

0.500 1.00

Flag


Units

1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1

DilCas Number

10061-02-6100-41-487-68-3591-78-698-82-875-09-274-88-4108-10-191-20-3103-65-1100-42-5630-20-679-34-5127-18-4108-88-387-61-6120-82-171-55-679-00-579-01-675-69-496-18-495-63-6108-67-895-47-6179601-23-1108-05-475-01-41330-20-7

<0.500<2.00<5.00<5.00<2.50<3.00<2.00<5.00<5.00<2.00<1.00

<0.500<0.500

5.95 <2.00<5.00<5.00

<0.500<0.500

8.11 <2.00<1.00<2.00<1.50<1.00<2.00<5.00

<0.500<1.00

937532Seq Number:

RL

04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37

Analysis Date

Surrogate

69-13366-13970-13070-135

%Recovery Flag

%%%%

98102101

97

04.01.14 05.37 04.01.14 05.37 04.01.14 05.37 04.01.14 05.37

Cas Number

1868-53-717060-07-02037-26-5460-00-4

Units Analysis Date


Limits

% Moisture:

of 112 Final 1.000







Analytical Method:

Analytical Method:

Analytical Method:

MKO

MKO

TNL

Analyst:

Analyst:

Analyst:

SW3010A

SW3010A

Prep Method:

Prep Method:

04.03.14 10.10

04.07.14 11.00

Date Prep:

Date Prep:

MLI

MLI

RYR

Tech:

Tech:

Tech:

Chromium

Chromium


Parameter

Parameter

Parameter

Result

Result

Result

0.0100

0.0100

0.00500

Flag

Flag

Flag

mg/L

mg/L

mg/L

Units

Units

Units

1

1

1

Dil

Dil

Dil

Cas Number

Cas Number

Cas Number

7440-47-3

7440-47-3

18540-29-9

<0.0100

<0.0100

0.00800

938379

938352

937261

Seq Number:

Seq Number:

Seq Number:

SUB: AZ0765

SUB: AZ0765

RL

RL

RL

04.11.14 12.51

04.11.14 06.25

03.28.14 07.09

Analysis Date

Analysis Date

Analysis Date

% Moisture:

% Moisture:

% Moisture:

of 112 Final 1.000





OEMAnalyst:

SW5030CPrep Method:

03.31.14 21.52 Date Prep:

OEMTech:


Parameter Result

20.0 0.500

1.50 0.500 0.500

1.00 5.00 5.00 2.00 2.50 1.50 2.50

0.500 0.500 0.500

4.00 0.500

5.00 1.50 2.00 1.50

0.500 2.00

0.500 0.500

1.50 1.50 1.50 2.00

0.500 0.500 0.500 0.500 0.500 0.500

1.00 0.500

1.00 1.00

Flag


Units

1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1

DilCas Number

67-64-171-43-2108-86-174-97-575-27-475-25-274-83-978-93-31634-04-4104-51-8135-98-898-06-675-15-056-23-5108-90-775-00-367-66-374-87-395-49-8106-43-499-87-6124-48-196-12-8106-93-474-95-395-50-1541-73-1106-46-775-71-875-34-3107-06-275-35-4156-59-2156-60-578-87-5142-28-9594-20-7563-58-610061-01-5

<20.0<0.500

<1.50<0.500<0.500

<1.00<5.00<5.00<2.00<2.50<1.50<2.50

<0.500<0.500<0.500

<4.000.650 <5.00<1.50<2.00<1.50

<0.500<2.00

<0.500<0.500

<1.50<1.50<1.50<2.00

<0.500<0.5000.600

<0.500<0.500<0.500

<1.00<0.500

<1.00<1.00

937532Seq Number:

RL

04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03

Analysis Date

% Moisture:

of 112 Final 1.000





OEMAnalyst:

SW5030CPrep Method:

03.31.14 21.52 Date Prep:

OEMTech:


Parameter Result

0.500 2.00 5.00 5.00 2.50 3.00 2.00 5.00 5.00 2.00 1.00

0.500 0.500 0.500

2.00 5.00 5.00

0.500 0.500 0.500

2.00 1.00 2.00 1.50 1.00 2.00 5.00

0.500 1.00

Flag


Units

1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1

DilCas Number

10061-02-6100-41-487-68-3591-78-698-82-875-09-274-88-4108-10-191-20-3103-65-1100-42-5630-20-679-34-5127-18-4108-88-387-61-6120-82-171-55-679-00-579-01-675-69-496-18-495-63-6108-67-895-47-6179601-23-1108-05-475-01-41330-20-7

<0.500<2.00<5.00<5.00<2.50<3.00<2.00<5.00<5.00<2.00<1.00

<0.500<0.500

5.19 <2.00<5.00<5.00

<0.500<0.500

2.85 <2.00<1.00<2.00<1.50<1.00<2.00<5.00

<0.500<1.00

937532Seq Number:

RL

04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03

Analysis Date

Surrogate

69-13366-13970-13070-135

%Recovery Flag

%%%%

97103102

97

04.01.14 06.03 04.01.14 06.03 04.01.14 06.03 04.01.14 06.03

Cas Number

1868-53-717060-07-02037-26-5460-00-4

Units Analysis Date


Limits

% Moisture:

of 112 Final 1.000







Analytical Method:

Analytical Method:

Analytical Method:

MKO

MKO

TNL

Analyst:

Analyst:

Analyst:

SW3010A

SW3010A

Prep Method:

Prep Method:

04.03.14 10.10

04.07.14 11.00

Date Prep:

Date Prep:

MLI

MLI

RYR

Tech:

Tech:

Tech:

Chromium

Chromium


Parameter

Parameter

Parameter

Result

Result

Result

0.0100

0.0100

0.00500

Flag

Flag

Flag

mg/L

mg/L

mg/L

Units

Units

Units

1

1

1

Dil

Dil

Dil

Cas Number

Cas Number

Cas Number

7440-47-3

7440-47-3

18540-29-9

<0.0100

<0.0100

0.00900

938379

938352

937261

Seq Number:

Seq Number:

Seq Number:

SUB: AZ0765

SUB: AZ0765

RL

RL

RL

04.11.14 12.58

04.11.14 06.31

03.28.14 07.09

Analysis Date

Analysis Date

Analysis Date

% Moisture:

% Moisture:

% Moisture:

of 112 Final 1.000





OEMAnalyst:

SW5030CPrep Method:

03.31.14 21.52 Date Prep:

OEMTech:


Parameter Result

20.0 0.500

1.50 0.500 0.500

1.00 5.00 5.00 2.00 2.50 1.50 2.50

0.500 0.500 0.500

4.00 0.500

5.00 1.50 2.00 1.50

0.500 2.00

0.500 0.500

1.50 1.50 1.50 2.00

0.500 0.500 0.500 0.500 0.500 0.500

1.00 0.500

1.00 1.00

Flag


Units

1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1

DilCas Number

67-64-171-43-2108-86-174-97-575-27-475-25-274-83-978-93-31634-04-4104-51-8135-98-898-06-675-15-056-23-5108-90-775-00-367-66-374-87-395-49-8106-43-499-87-6124-48-196-12-8106-93-474-95-395-50-1541-73-1106-46-775-71-875-34-3107-06-275-35-4156-59-2156-60-578-87-5142-28-9594-20-7563-58-610061-01-5

<20.0<0.500

<1.50<0.500<0.500

<1.00<5.00<5.00<2.00<2.50<1.50<2.50

<0.500<0.500<0.500

<4.000.620 <5.00<1.50<2.00<1.50

<0.500<2.00

<0.500<0.500

<1.50<1.50<1.50<2.00

<0.500<0.500<0.500<0.500<0.500<0.500

<1.00<0.500

<1.00<1.00

937532Seq Number:

RL

04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29

Analysis Date

% Moisture:

of 112 Final 1.000





OEMAnalyst:

SW5030CPrep Method:

03.31.14 21.52 Date Prep:

OEMTech:


Parameter Result

0.500 2.00 5.00 5.00 2.50 3.00 2.00 5.00 5.00 2.00 1.00

0.500 0.500 0.500

2.00 5.00 5.00

0.500 0.500 0.500

2.00 1.00 2.00 1.50 1.00 2.00 5.00

0.500 1.00

Flag


Units

1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1

DilCas Number

10061-02-6100-41-487-68-3591-78-698-82-875-09-274-88-4108-10-191-20-3103-65-1100-42-5630-20-679-34-5127-18-4108-88-387-61-6120-82-171-55-679-00-579-01-675-69-496-18-495-63-6108-67-895-47-6179601-23-1108-05-475-01-41330-20-7

<0.500<2.00<5.00<5.00<2.50<3.00<2.00<5.00<5.00<2.00<1.00

<0.500<0.500

4.90 <2.00<5.00<5.00

<0.500<0.500

2.69 <2.00<1.00<2.00<1.50<1.00<2.00<5.00

<0.500<1.00

937532Seq Number:

RL

04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29

Analysis Date

Surrogate

69-13366-13970-13070-135

%Recovery Flag

%%%%

98104100

96

04.01.14 06.29 04.01.14 06.29 04.01.14 06.29 04.01.14 06.29

Cas Number

1868-53-717060-07-02037-26-5460-00-4

Units Analysis Date


Limits

% Moisture:

of 112 Final 1.000







Analytical Method:

Analytical Method:

Analytical Method:

MKO

MKO

TNL

Analyst:

Analyst:

Analyst:

SW3010A

SW3010A

Prep Method:

Prep Method:

04.03.14 10.10

04.07.14 11.00

Date Prep:

Date Prep:

MLI

MLI

RYR

Tech:

Tech:

Tech:

Chromium

Chromium


Parameter

Parameter

Parameter

Result

Result

Result

0.0100

0.0100

0.00500

Flag

Flag

Flag

mg/L

mg/L

mg/L

Units

Units

Units

1

1

1

Dil

Dil

Dil

Cas Number

Cas Number

Cas Number

7440-47-3

7440-47-3

18540-29-9

<0.0100

<0.0100

0.00900

938379

938352

937261

Seq Number:

Seq Number:

Seq Number:

SUB: AZ0765

SUB: AZ0765

RL

RL

RL

04.11.14 13.04

04.11.14 06.38

03.28.14 07.09

Analysis Date

Analysis Date

Analysis Date

% Moisture:

% Moisture:

% Moisture:

of 112 Final 1.000





OEMAnalyst:

SW5030CPrep Method:

03.31.14 21.52 Date Prep:

OEMTech:


Parameter Result

20.0 0.500

1.50 0.500 0.500

1.00 5.00 5.00 2.00 2.50 1.50 2.50

0.500 0.500 0.500

4.00 0.500

5.00 1.50 2.00 1.50

0.500 2.00

0.500 0.500

1.50 1.50 1.50 2.00

0.500 0.500 0.500 0.500 0.500 0.500

1.00 0.500

1.00 1.00

Flag


Units

1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1

DilCas Number

67-64-171-43-2108-86-174-97-575-27-475-25-274-83-978-93-31634-04-4104-51-8135-98-898-06-675-15-056-23-5108-90-775-00-367-66-374-87-395-49-8106-43-499-87-6124-48-196-12-8106-93-474-95-395-50-1541-73-1106-46-775-71-875-34-3107-06-275-35-4156-59-2156-60-578-87-5142-28-9594-20-7563-58-610061-01-5

<20.0<0.500

<1.50<0.500<0.500

<1.00<5.00<5.00<2.00<2.50<1.50<2.50

<0.500<0.500<0.500

<4.002.26

<5.00<1.50<2.00<1.50

<0.500<2.00

<0.500<0.500

<1.50<1.50<1.50<2.00

<0.500<0.500

2.60 <0.500<0.500<0.500

<1.00<0.500

<1.00<1.00

937532Seq Number:

RL

04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55

Analysis Date

% Moisture:

of 112 Final 1.000





OEMAnalyst:

SW5030CPrep Method:

03.31.14 21.52 Date Prep:

OEMTech:


Parameter Result

0.500 2.00 5.00 5.00 2.50 3.00 2.00 5.00 5.00 2.00 1.00

0.500 0.500 0.500

2.00 5.00 5.00

0.500 0.500 0.500

2.00 1.00 2.00 1.50 1.00 2.00 5.00

0.500 1.00

Flag


Units

1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1

DilCas Number

10061-02-6100-41-487-68-3591-78-698-82-875-09-274-88-4108-10-191-20-3103-65-1100-42-5630-20-679-34-5127-18-4108-88-387-61-6120-82-171-55-679-00-579-01-675-69-496-18-495-63-6108-67-895-47-6179601-23-1108-05-475-01-41330-20-7

<0.500<2.00<5.00<5.00<2.50<3.00<2.00<5.00<5.00<2.00<1.00

<0.500<0.500

10.6 <2.00<5.00<5.00

<0.500<0.500

7.15 <2.00<1.00<2.00<1.50<1.00<2.00<5.00

<0.500<1.00

937532Seq Number:

RL

04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55

Analysis Date

Surrogate

69-13366-13970-13070-135

%Recovery Flag

%%%%

97102

9995

04.01.14 06.55 04.01.14 06.55 04.01.14 06.55 04.01.14 06.55

Cas Number

1868-53-717060-07-02037-26-5460-00-4

Units Analysis Date


Limits

% Moisture:

of 112 Final 1.000







Analytical Method:

Analytical Method:

Analytical Method:

MKO

MKO

TNL

Analyst:

Analyst:

Analyst:

SW3010A

SW3010A

Prep Method:

Prep Method:

04.03.14 10.10

04.07.14 11.00

Date Prep:

Date Prep:

MLI

MLI

RYR

Tech:

Tech:

Tech:

Chromium

Chromium


Parameter

Parameter

Parameter

Result

Result

Result

0.0100

0.0100

0.00500

Flag

Flag

Flag

mg/L

mg/L

mg/L

Units

Units

Units

1

1

1

Dil

Dil

Dil

Cas Number

Cas Number

Cas Number

7440-47-3

7440-47-3

18540-29-9

<0.0100

<0.0100

<0.00500

938379

938352

937261

Seq Number:

Seq Number:

Seq Number:

SUB: AZ0765

SUB: AZ0765

RL

RL

RL

04.11.14 13.11

04.11.14 06.44

03.28.14 07.09

Analysis Date

Analysis Date

Analysis Date

% Moisture:

% Moisture:

% Moisture:

of 112 Final 1.000





OEMAnalyst:

SW5030CPrep Method:

03.31.14 21.52 Date Prep:

OEMTech:


Parameter Result

20.0 0.500

1.50 0.500 0.500

1.00 5.00 5.00 2.00 2.50 1.50 2.50

0.500 0.500 0.500

4.00 0.500

5.00 1.50 2.00 1.50

0.500 2.00

0.500 0.500

1.50 1.50 1.50 2.00

0.500 0.500 0.500 0.500 0.500 0.500

1.00 0.500

1.00 1.00

Flag


Units

1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1

DilCas Number

67-64-171-43-2108-86-174-97-575-27-475-25-274-83-978-93-31634-04-4104-51-8135-98-898-06-675-15-056-23-5108-90-775-00-367-66-374-87-395-49-8106-43-499-87-6124-48-196-12-8106-93-474-95-395-50-1541-73-1106-46-775-71-875-34-3107-06-275-35-4156-59-2156-60-578-87-5142-28-9594-20-7563-58-610061-01-5

<20.0<0.500

<1.50<0.500<0.500

<1.00<5.00<5.00<2.00<2.50<1.50<2.50

<0.500<0.500<0.500

<4.003.32

<5.00<1.50<2.00<1.50

<0.500<2.00

<0.500<0.500

<1.50<1.50<1.50<2.00

<0.500<0.500<0.500<0.500<0.500<0.500

<1.00<0.500

<1.00<1.00

937532Seq Number:

RL

04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21

Analysis Date

% Moisture:

of 112 Final 1.000





OEMAnalyst:

SW5030CPrep Method:

03.31.14 21.52 Date Prep:

OEMTech:


Parameter Result

0.500 2.00 5.00 5.00 2.50 3.00 2.00 5.00 5.00 2.00 1.00

0.500 0.500 0.500

2.00 5.00 5.00

0.500 0.500 0.500

2.00 1.00 2.00 1.50 1.00 2.00 5.00

0.500 1.00

Flag


Units

1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1

DilCas Number

10061-02-6100-41-487-68-3591-78-698-82-875-09-274-88-4108-10-191-20-3103-65-1100-42-5630-20-679-34-5127-18-4108-88-387-61-6120-82-171-55-679-00-579-01-675-69-496-18-495-63-6108-67-895-47-6179601-23-1108-05-475-01-41330-20-7

<0.500<2.00<5.00<5.00<2.50<3.00<2.00<5.00<5.00<2.00<1.00

<0.500<0.500

8.16 <2.00<5.00<5.00

<0.500<0.500

1.53 <2.00<1.00<2.00<1.50<1.00<2.00<5.00

<0.500<1.00

937532Seq Number:

RL

04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21

Analysis Date

Surrogate

69-13366-13970-13070-135

%Recovery Flag

%%%%

97103

9994

04.01.14 07.21 04.01.14 07.21 04.01.14 07.21 04.01.14 07.21

Cas Number

1868-53-717060-07-02037-26-5460-00-4

Units Analysis Date


Limits

% Moisture:

of 112 Final 1.000



03.27.14 16.40 Date Received:03.27.14 10.43 Date Collected:482073-012Lab Sample Id:WaterMatrix: EQBSample Id:




Analytical Method:

Analytical Method:

Analytical Method:

MKO

MKO

TNL

Analyst:

Analyst:

Analyst:

SW3010A

SW3010A

Prep Method:

Prep Method:

04.03.14 10.10

04.07.14 11.00

Date Prep:

Date Prep:

MLI

MLI

RYR

Tech:

Tech:

Tech:

Chromium

Chromium


Parameter

Parameter

Parameter

Result

Result

Result

0.0100

0.0100

0.00500

Flag

Flag

Flag

mg/L

mg/L

mg/L

Units

Units

Units

1

1

1

Dil

Dil

Dil

Cas Number

Cas Number

Cas Number

7440-47-3

7440-47-3

18540-29-9

<0.0100

<0.0100

<0.00500

938379

938352

937261

Seq Number:

Seq Number:

Seq Number:

SUB: AZ0765

SUB: AZ0765

RL

RL

RL

04.11.14 13.17

04.11.14 06.51

03.28.14 07.09

Analysis Date

Analysis Date

Analysis Date

% Moisture:

% Moisture:

% Moisture:

of 112 Final 1.000





OEMAnalyst:

SW5030CPrep Method:

03.31.14 21.52 Date Prep:

OEMTech:


Parameter Result

20.0 0.500

1.50 0.500 0.500

1.00 5.00 5.00 2.00 2.50 1.50 2.50

0.500 0.500 0.500

4.00 0.500

5.00 1.50 2.00 1.50

0.500 2.00

0.500 0.500

1.50 1.50 1.50 2.00

0.500 0.500 0.500 0.500 0.500 0.500

1.00 0.500

1.00 1.00

Flag


Units

1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1

DilCas Number

67-64-171-43-2108-86-174-97-575-27-475-25-274-83-978-93-31634-04-4104-51-8135-98-898-06-675-15-056-23-5108-90-775-00-367-66-374-87-395-49-8106-43-499-87-6124-48-196-12-8106-93-474-95-395-50-1541-73-1106-46-775-71-875-34-3107-06-275-35-4156-59-2156-60-578-87-5142-28-9594-20-7563-58-610061-01-5

<20.0<0.500

<1.50<0.500<0.500

<1.00<5.00<5.00<2.00<2.50<1.50<2.50

<0.500<0.500<0.500

<4.00<0.500

<5.00<1.50<2.00<1.50

<0.500<2.00

<0.500<0.500

<1.50<1.50<1.50<2.00

<0.500<0.500<0.500<0.500<0.500<0.500

<1.00<0.500

<1.00<1.00

937532Seq Number:

RL

04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47

Analysis Date

% Moisture:

of 112 Final 1.000





OEMAnalyst:

SW5030CPrep Method:

03.31.14 21.52 Date Prep:

OEMTech:


Parameter Result

0.500 2.00 5.00 5.00 2.50 3.00 2.00 5.00 5.00 2.00 1.00

0.500 0.500 0.500

2.00 5.00 5.00

0.500 0.500 0.500

2.00 1.00 2.00 1.50 1.00 2.00 5.00

0.500 1.00

Flag


Units

1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1

DilCas Number

10061-02-6100-41-487-68-3591-78-698-82-875-09-274-88-4108-10-191-20-3103-65-1100-42-5630-20-679-34-5127-18-4108-88-387-61-6120-82-171-55-679-00-579-01-675-69-496-18-495-63-6108-67-895-47-6179601-23-1108-05-475-01-41330-20-7

<0.500<2.00<5.00<5.00<2.50<3.00<2.00<5.00<5.00<2.00<1.00

<0.500<0.500<0.500

<2.00<5.00<5.00

<0.500<0.500<0.500

<2.00<1.00<2.00<1.50<1.00<2.00<5.00

<0.500<1.00

937532Seq Number:

RL

04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47

Analysis Date

Surrogate

69-13366-13970-13070-135

%Recovery Flag

%%%%

95104

9893

04.01.14 07.47 04.01.14 07.47 04.01.14 07.47 04.01.14 07.47

Cas Number

1868-53-717060-07-02037-26-5460-00-4

Units Analysis Date


Limits

% Moisture:

of 112 Final 1.000



03.27.14 16.40 Date Received:03.27.14 10.35 Date Collected:482073-013Lab Sample Id:WaterMatrix: RID-111RSample Id:




Analytical Method:

Analytical Method:

Analytical Method:

MKO

MKO

TNL

Analyst:

Analyst:

Analyst:

SW3010A

SW3010A

Prep Method:

Prep Method:

04.03.14 10.10

04.07.14 11.00

Date Prep:

Date Prep:

MLI

MLI

RYR

Tech:

Tech:

Tech:

Chromium

Chromium


Parameter

Parameter

Parameter

Result

Result

Result

0.0100

0.0100

0.00500

Flag

Flag

Flag

mg/L

mg/L

mg/L

Units

Units

Units

1

1

1

Dil

Dil

Dil

Cas Number

Cas Number

Cas Number

7440-47-3

7440-47-3

18540-29-9

<0.0100

<0.0100

<0.00500

938379

938352

937261

Seq Number:

Seq Number:

Seq Number:

SUB: AZ0765

SUB: AZ0765

RL

RL

RL

04.11.14 13.37

04.11.14 06.57

03.28.14 07.09

Analysis Date

Analysis Date

Analysis Date

% Moisture:

% Moisture:

% Moisture:

of 112 Final 1.000





OEMAnalyst:

SW5030CPrep Method:

03.31.14 21.52 Date Prep:

OEMTech:


Parameter Result

20.0 0.500

1.50 0.500 0.500

1.00 5.00 5.00 2.00 2.50 1.50 2.50

0.500 0.500 0.500

4.00 0.500

5.00 1.50 2.00 1.50

0.500 2.00

0.500 0.500

1.50 1.50 1.50 2.00

0.500 0.500 0.500 0.500 0.500 0.500

1.00 0.500

1.00 1.00

Flag


Units

1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1

DilCas Number

67-64-171-43-2108-86-174-97-575-27-475-25-274-83-978-93-31634-04-4104-51-8135-98-898-06-675-15-056-23-5108-90-775-00-367-66-374-87-395-49-8106-43-499-87-6124-48-196-12-8106-93-474-95-395-50-1541-73-1106-46-775-71-875-34-3107-06-275-35-4156-59-2156-60-578-87-5142-28-9594-20-7563-58-610061-01-5

<20.0<0.500

<1.50<0.500<0.500

<1.00<5.00<5.00<2.00<2.50<1.50<2.50

<0.500<0.500<0.500

<4.004.10

<5.00<1.50<2.00<1.50

<0.500<2.00

<0.500<0.500

<1.50<1.50<1.50<2.00

<0.500<0.500<0.500<0.500<0.500<0.500

<1.00<0.500

<1.00<1.00

937532Seq Number:

RL

04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13

Analysis Date

% Moisture:

of 112 Final 1.000





OEMAnalyst:

SW5030CPrep Method:

03.31.14 21.52 Date Prep:

OEMTech:


Parameter Result

0.500 2.00 5.00 5.00 2.50 3.00 2.00 5.00 5.00 2.00 1.00

0.500 0.500 0.500

2.00 5.00 5.00

0.500 0.500 0.500

2.00 1.00 2.00 1.50 1.00 2.00 5.00

0.500 1.00

Flag


Units

1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1

DilCas Number

10061-02-6100-41-487-68-3591-78-698-82-875-09-274-88-4108-10-191-20-3103-65-1100-42-5630-20-679-34-5127-18-4108-88-387-61-6120-82-171-55-679-00-579-01-675-69-496-18-495-63-6108-67-895-47-6179601-23-1108-05-475-01-41330-20-7

<0.500<2.00<5.00<5.00<2.50<3.00<2.00<5.00<5.00<2.00<1.00

<0.500<0.500

1.53 <2.00<5.00<5.00

<0.500<0.500<0.500

<2.00<1.00<2.00<1.50<1.00<2.00<5.00

<0.500<1.00

937532Seq Number:

RL

04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13

Analysis Date

Surrogate

69-13366-13970-13070-135

%Recovery Flag

%%%%

99105100

95

04.01.14 08.13 04.01.14 08.13 04.01.14 08.13 04.01.14 08.13

Cas Number

1868-53-717060-07-02037-26-5460-00-4

Units Analysis Date


Limits

% Moisture:

of 112 Final 1.000







Analytical Method:

Analytical Method:

Analytical Method:

MKO

MKO

TNL

Analyst:

Analyst:

Analyst:

SW3010A

SW3010A

Prep Method:

Prep Method:

04.03.14 10.10

04.07.14 11.00

Date Prep:

Date Prep:

MLI

MLI

RYR

Tech:

Tech:

Tech:

Chromium

Chromium


Parameter

Parameter

Parameter

Result

Result

Result

0.0100

0.0100

0.00500

Flag

Flag

Flag

mg/L

mg/L

mg/L

Units

Units

Units

1

1

1

Dil

Dil

Dil

Cas Number

Cas Number

Cas Number

7440-47-3

7440-47-3

18540-29-9

<0.0100

<0.0100

<0.00500

938379

938352

937261

Seq Number:

Seq Number:

Seq Number:

SUB: AZ0765

SUB: AZ0765

RL

RL

RL

04.11.14 13.43

04.11.14 07.17

03.28.14 07.09

Analysis Date

Analysis Date

Analysis Date

% Moisture:

% Moisture:

% Moisture:

of 112 Final 1.000





OEMAnalyst:

SW5030CPrep Method:

03.31.14 21.52 Date Prep:

OEMTech:


Parameter Result

20.0 0.500

1.50 0.500 0.500

1.00 5.00 5.00 2.00 2.50 1.50 2.50

0.500 0.500 0.500

4.00 0.500

5.00 1.50 2.00 1.50

0.500 2.00

0.500 0.500

1.50 1.50 1.50 2.00

0.500 0.500 0.500 0.500 0.500 0.500

1.00 0.500

1.00 1.00

Flag


Units

1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1

DilCas Number

67-64-171-43-2108-86-174-97-575-27-475-25-274-83-978-93-31634-04-4104-51-8135-98-898-06-675-15-056-23-5108-90-775-00-367-66-374-87-395-49-8106-43-499-87-6124-48-196-12-8106-93-474-95-395-50-1541-73-1106-46-775-71-875-34-3107-06-275-35-4156-59-2156-60-578-87-5142-28-9594-20-7563-58-610061-01-5

<20.0<0.500

<1.50<0.500<0.500

<1.00<5.00<5.00<2.00<2.50<1.50<2.50

<0.500<0.500<0.500

<4.003.44

<5.00<1.50<2.00<1.50

<0.500<2.00

<0.500<0.500

<1.50<1.50<1.50<2.00

<0.500<0.5000.520

1.14 <0.500<0.500

<1.00<0.500

<1.00<1.00

937532Seq Number:

RL

04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40

Analysis Date

% Moisture:

of 112 Final 1.000





OEMAnalyst:

SW5030CPrep Method:

03.31.14 21.52 Date Prep:

OEMTech:


Parameter Result

0.500 2.00 5.00 5.00 2.50 3.00 2.00 5.00 5.00 2.00 1.00

0.500 0.500 0.500

2.00 5.00 5.00

0.500 0.500 0.500

2.00 1.00 2.00 1.50 1.00 2.00 5.00

0.500 1.00

Flag


Units

1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1

DilCas Number

10061-02-6100-41-487-68-3591-78-698-82-875-09-274-88-4108-10-191-20-3103-65-1100-42-5630-20-679-34-5127-18-4108-88-387-61-6120-82-171-55-679-00-579-01-675-69-496-18-495-63-6108-67-895-47-6179601-23-1108-05-475-01-41330-20-7

<0.500<2.00<5.00<5.00<2.50<3.00<2.00<5.00<5.00<2.00<1.00

<0.500<0.500

3.03 <2.00<5.00<5.00

<0.500<0.500

8.24 <2.00<1.00<2.00<1.50<1.00<2.00<5.00

<0.500<1.00

937532Seq Number:

RL

04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40

Analysis Date

Surrogate

69-13366-13970-13070-135

%Recovery Flag

%%%%

99104

9995

04.01.14 08.40 04.01.14 08.40 04.01.14 08.40 04.01.14 08.40

Cas Number

1868-53-717060-07-02037-26-5460-00-4

Units Analysis Date


Limits

% Moisture:

of 112 Final 1.000







Analytical Method:

Analytical Method:

Analytical Method:

MKO

MKO

TNL

Analyst:

Analyst:

Analyst:

SW3010A

SW3010A

Prep Method:

Prep Method:

04.03.14 10.10

04.07.14 11.00

Date Prep:

Date Prep:

MLI

MLI

RYR

Tech:

Tech:

Tech:

Chromium

Chromium


Parameter

Parameter

Parameter

Result

Result

Result

0.0100

0.0100

0.00500

Flag

Flag

Flag

mg/L

mg/L

mg/L

Units

Units

Units

1

1

1

Dil

Dil

Dil

Cas Number

Cas Number

Cas Number

7440-47-3

7440-47-3

18540-29-9

<0.0100

<0.0100

<0.00500

938379

938352

937261

Seq Number:

Seq Number:

Seq Number:

SUB: AZ0765

SUB: AZ0765

RL

RL

RL

04.11.14 13.50

04.11.14 07.23

03.28.14 07.09

Analysis Date

Analysis Date

Analysis Date

% Moisture:

% Moisture:

% Moisture:

of 112 Final 1.000





OEMAnalyst:

SW5030CPrep Method:

03.31.14 21.52 Date Prep:

OEMTech:


Parameter Result

20.0 0.500

1.50 0.500 0.500

1.00 5.00 5.00 2.00 2.50 1.50 2.50

0.500 0.500 0.500

4.00 0.500

5.00 1.50 2.00 1.50

0.500 2.00

0.500 0.500

1.50 1.50 1.50 2.00

0.500 0.500 0.500 0.500 0.500 0.500

1.00 0.500

1.00 1.00

Flag


Units

1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1

DilCas Number

67-64-171-43-2108-86-174-97-575-27-475-25-274-83-978-93-31634-04-4104-51-8135-98-898-06-675-15-056-23-5108-90-775-00-367-66-374-87-395-49-8106-43-499-87-6124-48-196-12-8106-93-474-95-395-50-1541-73-1106-46-775-71-875-34-3107-06-275-35-4156-59-2156-60-578-87-5142-28-9594-20-7563-58-610061-01-5

<20.0<0.500

<1.50<0.500<0.500

<1.00<5.00<5.00<2.00<2.50<1.50<2.50

<0.500<0.500<0.500

<4.002.39

<5.00<1.50<2.00<1.50

<0.500<2.00

<0.500<0.500

<1.50<1.50<1.50<2.002.12

<0.5003.01 7.48

<0.500<0.500

<1.00<0.500

<1.00<1.00

937532Seq Number:

RL

04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06

Analysis Date

% Moisture:

of 112 Final 1.000





OEMAnalyst:

SW5030CPrep Method:

03.31.14 21.52 Date Prep:

OEMTech:


Parameter Result

0.500 2.00 5.00 5.00 2.50 3.00 2.00 5.00 5.00 2.00 1.00

0.500 0.500 0.500

2.00 5.00 5.00

0.500 0.500 0.500

2.00 1.00 2.00 1.50 1.00 2.00 5.00

0.500 1.00

Flag


Units

1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1

DilCas Number

10061-02-6100-41-487-68-3591-78-698-82-875-09-274-88-4108-10-191-20-3103-65-1100-42-5630-20-679-34-5127-18-4108-88-387-61-6120-82-171-55-679-00-579-01-675-69-496-18-495-63-6108-67-895-47-6179601-23-1108-05-475-01-41330-20-7

<0.500<2.00<5.00<5.00<2.50<3.00<2.00<5.00<5.00<2.00<1.00

<0.500<0.500

2.86 <2.00<5.00<5.00

<0.500<0.500

45.6 <2.00<1.00<2.00<1.50<1.00<2.00<5.00

<0.500<1.00

937532Seq Number:

RL

04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06

Analysis Date

Surrogate

69-13366-13970-13070-135

%Recovery Flag

%%%%

99107

9794

04.01.14 09.06 04.01.14 09.06 04.01.14 09.06 04.01.14 09.06

Cas Number

1868-53-717060-07-02037-26-5460-00-4

Units Analysis Date


Limits

% Moisture:

of 112 Final 1.000







Analytical Method:

Analytical Method:

Analytical Method:

MKO

MKO

TNL

Analyst:

Analyst:

Analyst:

SW3010A

SW3010A

Prep Method:

Prep Method:

04.03.14 10.10

04.07.14 11.00

Date Prep:

Date Prep:

MLI

MLI

RYR

Tech:

Tech:

Tech:

Chromium

Chromium


Parameter

Parameter

Parameter

Result

Result

Result

0.0100

0.0100

0.00500

Flag

Flag

Flag

mg/L

mg/L

mg/L

Units

Units

Units

1

1

1

Dil

Dil

Dil

Cas Number

Cas Number

Cas Number

7440-47-3

7440-47-3

18540-29-9

<0.0100

<0.0100

<0.00500

938379

938352

937261

Seq Number:

Seq Number:

Seq Number:

SUB: AZ0765

SUB: AZ0765

RL

RL

RL

04.11.14 13.56

04.11.14 07.30

03.28.14 07.09

Analysis Date

Analysis Date

Analysis Date

% Moisture:

% Moisture:

% Moisture:

of 112 Final 1.000





OEMAnalyst:

SW5030CPrep Method:

04.04.14 00.34 Date Prep:

OEMTech:


Parameter Result

20.0 0.500

1.50 0.500 0.500

1.00 5.00 5.00 2.00 2.50 1.50 2.50

0.500 0.500 0.500

4.00 0.500

5.00 1.50 2.00 1.50

0.500 2.00

0.500 0.500

1.50 1.50 1.50 2.00

0.500 0.500 0.500 0.500 0.500 0.500

1.00 0.500

1.00 1.00

Flag


Units

1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1

DilCas Number

67-64-171-43-2108-86-174-97-575-27-475-25-274-83-978-93-31634-04-4104-51-8135-98-898-06-675-15-056-23-5108-90-775-00-367-66-374-87-395-49-8106-43-499-87-6124-48-196-12-8106-93-474-95-395-50-1541-73-1106-46-775-71-875-34-3107-06-275-35-4156-59-2156-60-578-87-5142-28-9594-20-7563-58-610061-01-5

<20.0<0.500

<1.50<0.500<0.500

<1.00<5.00<5.00<2.00<2.50<1.50<2.50

<0.500<0.500<0.500

<4.00<0.500

<5.00<1.50<2.00<1.50

<0.500<2.00

<0.500<0.500

<1.50<1.50<1.50<2.00

<0.500<0.500<0.500<0.500<0.500<0.500

<1.00<0.500

<1.00<1.00

937846Seq Number:

RL

04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09

Analysis Date

% Moisture:

of 112 Final 1.000





OEMAnalyst:

SW5030CPrep Method:

04.04.14 00.34 Date Prep:

OEMTech:


Parameter Result

0.500 2.00 5.00 5.00 2.50 3.00 2.00 5.00 5.00 2.00 1.00

0.500 0.500 0.500

2.00 5.00 5.00

0.500 0.500 0.500

2.00 1.00 2.00 1.50 1.00 2.00 5.00

0.500 1.00

Flag


Units

1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1

DilCas Number

10061-02-6100-41-487-68-3591-78-698-82-875-09-274-88-4108-10-191-20-3103-65-1100-42-5630-20-679-34-5127-18-4108-88-387-61-6120-82-171-55-679-00-579-01-675-69-496-18-495-63-6108-67-895-47-6179601-23-1108-05-475-01-41330-20-7

<0.500<2.00<5.00<5.00<2.50<3.00<2.00<5.00<5.00<2.00<1.00

<0.500<0.500

3.38 <2.00<5.00<5.00

<0.500<0.500<0.500

<2.00<1.00<2.00<1.50<1.00<2.00<5.00

<0.500<1.00

937846Seq Number:

RL

04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09

Analysis Date

Surrogate

69-13366-13970-13070-135

%Recovery Flag

%%%%

95959792

04.04.14 03.09 04.04.14 03.09 04.04.14 03.09 04.04.14 03.09

Cas Number

1868-53-717060-07-02037-26-5460-00-4

Units Analysis Date


Limits

% Moisture:

of 112 Final 1.000







Analytical Method:

Analytical Method:

Analytical Method:

MKO

MKO

TNL

Analyst:

Analyst:

Analyst:

SW3010A

SW3010A

Prep Method:

Prep Method:

04.03.14 10.10

04.07.14 11.00

Date Prep:

Date Prep:

MLI

MLI

RYR

Tech:

Tech:

Tech:

Chromium

Chromium


Parameter

Parameter

Parameter

Result

Result

Result

0.0100

0.0100

0.00500

Flag

Flag

Flag

mg/L

mg/L

mg/L

Units

Units

Units

1

1

1

Dil

Dil

Dil

Cas Number

Cas Number

Cas Number

7440-47-3

7440-47-3

18540-29-9

0.0161

0.0157

0.0130

938379

938352

937261

Seq Number:

Seq Number:

Seq Number:

SUB: AZ0765

SUB: AZ0765

RL

RL

RL

04.11.14 14.03

04.11.14 07.36

03.28.14 07.09

Analysis Date

Analysis Date

Analysis Date

% Moisture:

% Moisture:

% Moisture:

of 112 Final 1.000





OEMAnalyst:

SW5030CPrep Method:

04.04.14 00.34 Date Prep:

OEMTech:


Parameter Result

20.0 0.500

1.50 0.500 0.500

1.00 5.00 5.00 2.00 2.50 1.50 2.50

0.500 0.500 0.500

4.00 0.500

5.00 1.50 2.00 1.50

0.500 2.00

0.500 0.500

1.50 1.50 1.50 2.00

0.500 0.500 0.500 0.500 0.500 0.500

1.00 0.500

1.00 1.00

Flag


Units

1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1

DilCas Number

67-64-171-43-2108-86-174-97-575-27-475-25-274-83-978-93-31634-04-4104-51-8135-98-898-06-675-15-056-23-5108-90-775-00-367-66-374-87-395-49-8106-43-499-87-6124-48-196-12-8106-93-474-95-395-50-1541-73-1106-46-775-71-875-34-3107-06-275-35-4156-59-2156-60-578-87-5142-28-9594-20-7563-58-610061-01-5

<20.0<0.500

<1.50<0.500<0.500

<1.00<5.00<5.00<2.00<2.50<1.50<2.50

<0.500<0.500<0.500

<4.00<0.500

<5.00<1.50<2.00<1.50

<0.500<2.00

<0.500<0.500

<1.50<1.50<1.50<2.00

<0.500<0.500<0.500<0.500<0.500<0.500

<1.00<0.500

<1.00<1.00

937846Seq Number:

RL

04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28

Analysis Date

% Moisture:

of 112 Final 1.000





OEMAnalyst:

SW5030CPrep Method:

04.04.14 00.34 Date Prep:

OEMTech:


Parameter Result

0.500 2.00 5.00 5.00 2.50 3.00 2.00 5.00 5.00 2.00 1.00

0.500 0.500 0.500

2.00 5.00 5.00

0.500 0.500 0.500

2.00 1.00 2.00 1.50 1.00 2.00 5.00

0.500 1.00

Flag


Units

1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1

DilCas Number

10061-02-6100-41-487-68-3591-78-698-82-875-09-274-88-4108-10-191-20-3103-65-1100-42-5630-20-679-34-5127-18-4108-88-387-61-6120-82-171-55-679-00-579-01-675-69-496-18-495-63-6108-67-895-47-6179601-23-1108-05-475-01-41330-20-7

<0.500<2.00<5.00<5.00<2.50<3.00<2.00<5.00<5.00<2.00<1.00

<0.500<0.500

3.86 <2.00<5.00<5.00

<0.500<0.500<0.500

<2.00<1.00<2.00<1.50<1.00<2.00<5.00

<0.500<1.00

937846Seq Number:

RL

04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28

Analysis Date

Surrogate

69-13366-13970-13070-135

%Recovery Flag

%%%%

97999992

04.04.14 04.28 04.04.14 04.28 04.04.14 04.28 04.04.14 04.28

Cas Number

1868-53-717060-07-02037-26-5460-00-4

Units Analysis Date


Limits

% Moisture:

of 112 Final 1.000







Analytical Method:

Analytical Method:

Analytical Method:

MKO

MKO

TNL

Analyst:

Analyst:

Analyst:

SW3010A

SW3010A

Prep Method:

Prep Method:

04.03.14 10.10

04.07.14 11.00

Date Prep:

Date Prep:

MLI

MLI

RYR

Tech:

Tech:

Tech:

Chromium

Chromium


Parameter

Parameter

Parameter

Result

Result

Result

0.0100

0.0100

0.00500

Flag

Flag

Flag

mg/L

mg/L

mg/L

Units

Units

Units

1

1

1

Dil

Dil

Dil

Cas Number

Cas Number

Cas Number

7440-47-3

7440-47-3

18540-29-9

<0.0100

<0.0100

<0.00500

938379

938352

937261

Seq Number:

Seq Number:

Seq Number:

SUB: AZ0765

SUB: AZ0765

RL

RL

RL

04.11.14 14.09

04.11.14 07.43

03.28.14 07.09

Analysis Date

Analysis Date

Analysis Date

% Moisture:

% Moisture:

% Moisture:

of 112 Final 1.000





OEMAnalyst:

SW5030CPrep Method:

04.04.14 00.34 Date Prep:

OEMTech:


Parameter Result

20.0 0.500

1.50 0.500 0.500

1.00 5.00 5.00 2.00 2.50 1.50 2.50

0.500 0.500 0.500

4.00 0.500

5.00 1.50 2.00 1.50

0.500 2.00

0.500 0.500

1.50 1.50 1.50 2.00

0.500 0.500 0.500 0.500 0.500 0.500

1.00 0.500

1.00 1.00

Flag


Units

1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1

DilCas Number

67-64-171-43-2108-86-174-97-575-27-475-25-274-83-978-93-31634-04-4104-51-8135-98-898-06-675-15-056-23-5108-90-775-00-367-66-374-87-395-49-8106-43-499-87-6124-48-196-12-8106-93-474-95-395-50-1541-73-1106-46-775-71-875-34-3107-06-275-35-4156-59-2156-60-578-87-5142-28-9594-20-7563-58-610061-01-5

<20.0<0.500

<1.50<0.500<0.500

<1.00<5.00<5.00<2.00<2.50<1.50<2.50

<0.500<0.500<0.500

<4.00<0.500

<5.00<1.50<2.00<1.50

<0.500<2.00

<0.500<0.500

<1.50<1.50<1.50<2.00

<0.500<0.500<0.500<0.500<0.500<0.500

<1.00<0.500

<1.00<1.00

937846Seq Number:

RL

04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54

Analysis Date

% Moisture:

of 112 Final 1.000





OEMAnalyst:

SW5030CPrep Method:

04.04.14 00.34 Date Prep:

OEMTech:


Parameter Result

0.500 2.00 5.00 5.00 2.50 3.00 2.00 5.00 5.00 2.00 1.00

0.500 0.500 0.500

2.00 5.00 5.00

0.500 0.500 0.500

2.00 1.00 2.00 1.50 1.00 2.00 5.00

0.500 1.00

Flag


Units

1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1

DilCas Number

10061-02-6100-41-487-68-3591-78-698-82-875-09-274-88-4108-10-191-20-3103-65-1100-42-5630-20-679-34-5127-18-4108-88-387-61-6120-82-171-55-679-00-579-01-675-69-496-18-495-63-6108-67-895-47-6179601-23-1108-05-475-01-41330-20-7

<0.500<2.00<5.00<5.00<2.50<3.00<2.00<5.00<5.00<2.00<1.00

<0.500<0.500<0.500

<2.00<5.00<5.00

<0.500<0.500<0.500

<2.00<1.00<2.00<1.50<1.00<2.00<5.00

<0.500<1.00

937846Seq Number:

RL

04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54

Analysis Date

Surrogate

69-13366-13970-13070-135

%Recovery Flag

%%%%

97969893

04.04.14 04.54 04.04.14 04.54 04.04.14 04.54 04.04.14 04.54

Cas Number

1868-53-717060-07-02037-26-5460-00-4

Units Analysis Date


Limits

% Moisture:

of 112 Final 1.000







Analytical Method:

Analytical Method:

Analytical Method:

MKO

MKO

TNL

Analyst:

Analyst:

Analyst:

SW3010A

SW3010A

Prep Method:

Prep Method:

04.03.14 10.10

04.07.14 11.10

Date Prep:

Date Prep:

MLI

MLI

RYR

Tech:

Tech:

Tech:

Chromium

Chromium


Parameter

Parameter

Parameter

Result

Result

Result

0.0100

0.0100

0.00500

Flag

Flag

Flag

mg/L

mg/L

mg/L

Units

Units

Units

1

1

1

Dil

Dil

Dil

Cas Number

Cas Number

Cas Number

7440-47-3

7440-47-3

18540-29-9

<0.0100

<0.0100

<0.00500

938379

938492

937261

Seq Number:

Seq Number:

Seq Number:

SUB: AZ0765

SUB: AZ0765

RL

RL

RL

04.11.14 14.16

04.13.14 18.45

03.28.14 07.09

Analysis Date

Analysis Date

Analysis Date

% Moisture:

% Moisture:

% Moisture:

of 112 Final 1.000





OEMAnalyst:

SW5030CPrep Method:

04.04.14 00.34 Date Prep:

OEMTech:


Parameter Result

20.0 0.500

1.50 0.500 0.500

1.00 5.00 5.00 2.00 2.50 1.50 2.50

0.500 0.500 0.500

4.00 0.500

5.00 1.50 2.00 1.50

0.500 2.00

0.500 0.500

1.50 1.50 1.50 2.00

0.500 0.500 0.500 0.500 0.500 0.500

1.00 0.500

1.00 1.00

Flag


Units

1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1

DilCas Number

67-64-171-43-2108-86-174-97-575-27-475-25-274-83-978-93-31634-04-4104-51-8135-98-898-06-675-15-056-23-5108-90-775-00-367-66-374-87-395-49-8106-43-499-87-6124-48-196-12-8106-93-474-95-395-50-1541-73-1106-46-775-71-875-34-3107-06-275-35-4156-59-2156-60-578-87-5142-28-9594-20-7563-58-610061-01-5

<20.0<0.500

<1.50<0.500<0.500

<1.00<5.00<5.00<2.00<2.50<1.50<2.50

<0.500<0.500<0.500

<4.00<0.500

<5.00<1.50<2.00<1.50

<0.500<2.00

<0.500<0.500

<1.50<1.50<1.50<2.00

<0.500<0.500

1.14 <0.500<0.500<0.500

<1.00<0.500

<1.00<1.00

937846Seq Number:

RL

04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20

Analysis Date

% Moisture:

of 112 Final 1.000





OEMAnalyst:

SW5030CPrep Method:

04.04.14 00.34 Date Prep:

OEMTech:


Parameter Result

0.500 2.00 5.00 5.00 2.50 3.00 2.00 5.00 5.00 2.00 1.00

0.500 0.500 0.500

2.00 5.00 5.00

0.500 0.500 0.500

2.00 1.00 2.00 1.50 1.00 2.00 5.00

0.500 1.00

Flag


Units

1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1

DilCas Number

10061-02-6100-41-487-68-3591-78-698-82-875-09-274-88-4108-10-191-20-3103-65-1100-42-5630-20-679-34-5127-18-4108-88-387-61-6120-82-171-55-679-00-579-01-675-69-496-18-495-63-6108-67-895-47-6179601-23-1108-05-475-01-41330-20-7

<0.500<2.00<5.00<5.00<2.50<3.00<2.00<5.00<5.00<2.00<1.00

<0.500<0.500<0.500

<2.00<5.00<5.00

<0.500<0.500<0.500

<2.00<1.00<2.00<1.50<1.00<2.00<5.00

<0.500<1.00

937846Seq Number:

RL

04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20

Analysis Date

Surrogate

69-13366-13970-13070-135

%Recovery Flag

%%%%

99999994

04.04.14 05.20 04.04.14 05.20 04.04.14 05.20 04.04.14 05.20

Cas Number

1868-53-717060-07-02037-26-5460-00-4

Units Analysis Date


Limits

% Moisture:

of 112 Final 1.000







Analytical Method:

Analytical Method:

Analytical Method:

MKO

MKO

TNL

Analyst:

Analyst:

Analyst:

SW3010A

SW3010A

Prep Method:

Prep Method:

04.03.14 10.10

04.07.14 11.10

Date Prep:

Date Prep:

MLI

MLI

RYR

Tech:

Tech:

Tech:

Chromium

Chromium


Parameter

Parameter

Parameter

Result

Result

Result

0.0100

0.0100

0.00500

Flag

Flag

Flag

mg/L

mg/L

mg/L

Units

Units

Units

1

1

1

Dil

Dil

Dil

Cas Number

Cas Number

Cas Number

7440-47-3

7440-47-3

18540-29-9

<0.0100

<0.0100

<0.00500

938379

938492

937261

Seq Number:

Seq Number:

Seq Number:

SUB: AZ0765

SUB: AZ0765

RL

RL

RL

04.11.14 14.23

04.13.14 18.52

03.28.14 07.09

Analysis Date

Analysis Date

Analysis Date

% Moisture:

% Moisture:

% Moisture:

of 112 Final 1.000





OEMAnalyst:

SW5030CPrep Method:

04.04.14 00.34 Date Prep:

OEMTech:


Parameter Result

20.0 0.500

1.50 0.500 0.500

1.00 5.00 5.00 2.00 2.50 1.50 2.50

0.500 0.500 0.500

4.00 0.500

5.00 1.50 2.00 1.50

0.500 2.00

0.500 0.500

1.50 1.50 1.50 2.00

0.500 0.500 0.500 0.500 0.500 0.500

1.00 0.500

1.00 1.00

Flag


Units

1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1

DilCas Number

67-64-171-43-2108-86-174-97-575-27-475-25-274-83-978-93-31634-04-4104-51-8135-98-898-06-675-15-056-23-5108-90-775-00-367-66-374-87-395-49-8106-43-499-87-6124-48-196-12-8106-93-474-95-395-50-1541-73-1106-46-775-71-875-34-3107-06-275-35-4156-59-2156-60-578-87-5142-28-9594-20-7563-58-610061-01-5

<20.0<0.500

<1.50<0.500<0.500

<1.00<5.00<5.00<2.00<2.50<1.50<2.50

<0.500<0.500<0.500

<4.00<0.500

<5.00<1.50<2.00<1.50

<0.500<2.00

<0.500<0.500

<1.50<1.50<1.50<2.001.45

<0.5002.51 2.29

<0.500<0.500

<1.00<0.500

<1.00<1.00

937846Seq Number:

RL

04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46

Analysis Date

% Moisture:

of 112 Final 1.000





OEMAnalyst:

SW5030CPrep Method:

04.04.14 00.34 Date Prep:

OEMTech:


Parameter Result

0.500 2.00 5.00 5.00 2.50 3.00 2.00 5.00 5.00 2.00 1.00

0.500 0.500 0.500

2.00 5.00 5.00

0.500 0.500 0.500

2.00 1.00 2.00 1.50 1.00 2.00 5.00

0.500 1.00

Flag


Units

1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1

DilCas Number

10061-02-6100-41-487-68-3591-78-698-82-875-09-274-88-4108-10-191-20-3103-65-1100-42-5630-20-679-34-5127-18-4108-88-387-61-6120-82-171-55-679-00-579-01-675-69-496-18-495-63-6108-67-895-47-6179601-23-1108-05-475-01-41330-20-7

<0.500<2.00<5.00<5.00<2.50<3.00<2.00<5.00<5.00<2.00<1.00

<0.500<0.500

3.25 <2.00<5.00<5.00

<0.500<0.500

8.97 <2.00<1.00<2.00<1.50<1.00<2.00<5.00

<0.500<1.00

937846Seq Number:

RL

04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46

Analysis Date

Surrogate

69-13366-13970-13070-135

%Recovery Flag

%%%%

97969892

04.04.14 05.46 04.04.14 05.46 04.04.14 05.46 04.04.14 05.46

Cas Number

1868-53-717060-07-02037-26-5460-00-4

Units Analysis Date


Limits

% Moisture:

of 112 Final 1.000







Analytical Method:

Analytical Method:

Analytical Method:

MKO

MKO

TNL

Analyst:

Analyst:

Analyst:

SW3010A

SW3010A

Prep Method:

Prep Method:

04.07.14 11.10

04.09.14 11.10

Date Prep:

Date Prep:

MLI

MLI

RYR

Tech:

Tech:

Tech:

Chromium

Chromium


Parameter

Parameter

Parameter

Result

Result

Result

0.0100

0.0100

0.00500

Flag

Flag

Flag

mg/L

mg/L

mg/L

Units

Units

Units

1

1

1

Dil

Dil

Dil

Cas Number

Cas Number

Cas Number

7440-47-3

7440-47-3

18540-29-9

0.0481

0.0144

0.0430

938492

938532

937325

Seq Number:

Seq Number:

Seq Number:

SUB: AZ0765

SUB: AZ0765

RL

RL

RL

04.13.14 17.01

04.14.14 13.20

03.28.14 07.48

Analysis Date

Analysis Date

Analysis Date

% Moisture:

% Moisture:

% Moisture:

of 112 Final 1.000





OEMAnalyst:

SW5030CPrep Method:

04.04.14 00.34 Date Prep:

OEMTech:


Parameter Result

20.0 0.500

1.50 0.500 0.500

1.00 5.00 5.00 2.00 2.50 1.50 2.50

0.500 0.500 0.500

4.00 0.500

5.00 1.50 2.00 1.50

0.500 2.00

0.500 0.500

1.50 1.50 1.50 2.00

0.500 0.500 0.500 0.500 0.500 0.500

1.00 0.500

1.00 1.00

Flag


Units

1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1

DilCas Number

67-64-171-43-2108-86-174-97-575-27-475-25-274-83-978-93-31634-04-4104-51-8135-98-898-06-675-15-056-23-5108-90-775-00-367-66-374-87-395-49-8106-43-499-87-6124-48-196-12-8106-93-474-95-395-50-1541-73-1106-46-775-71-875-34-3107-06-275-35-4156-59-2156-60-578-87-5142-28-9594-20-7563-58-610061-01-5

<20.0<0.500

<1.50<0.500<0.500

<1.00<5.00<5.00<2.00<2.50<1.50<2.50

<0.500<0.500<0.500

<4.00<0.500

<5.00<1.50<2.00<1.50

<0.500<2.00

<0.500<0.500

<1.50<1.50<1.50<2.00

<0.500<0.5000.500

<0.500<0.500<0.500

<1.00<0.500

<1.00<1.00

937846Seq Number:

RL

04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11

Analysis Date

% Moisture:

of 112 Final 1.000





OEMAnalyst:

SW5030CPrep Method:

04.04.14 00.34 Date Prep:

OEMTech:


Parameter Result

0.500 2.00 5.00 5.00 2.50 3.00 2.00 5.00 5.00 2.00 1.00

0.500 0.500 0.500

2.00 5.00 5.00

0.500 0.500 0.500

2.00 1.00 2.00 1.50 1.00 2.00 5.00

0.500 1.00

Flag


Units

1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1

DilCas Number

10061-02-6100-41-487-68-3591-78-698-82-875-09-274-88-4108-10-191-20-3103-65-1100-42-5630-20-679-34-5127-18-4108-88-387-61-6120-82-171-55-679-00-579-01-675-69-496-18-495-63-6108-67-895-47-6179601-23-1108-05-475-01-41330-20-7

<0.500<2.00<5.00<5.00<2.50<3.00<2.00<5.00<5.00<2.00<1.00

<0.500<0.500

8.31 <2.00<5.00<5.00

<0.500<0.500<0.500

<2.00<1.00<2.00<1.50<1.00<2.00<5.00

<0.500<1.00

937846Seq Number:

RL

04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11

Analysis Date

Surrogate

69-13366-13970-13070-135

%Recovery Flag

%%%%

97969893

04.04.14 06.11 04.04.14 06.11 04.04.14 06.11 04.04.14 06.11

Cas Number

1868-53-717060-07-02037-26-5460-00-4

Units Analysis Date


Limits

% Moisture:

of 112 Final 1.000







Analytical Method:

Analytical Method:

Analytical Method:

MKO

MKO

TNL

Analyst:

Analyst:

Analyst:

SW3010A

SW3010A

Prep Method:

Prep Method:

04.07.14 11.10

04.09.14 11.10

Date Prep:

Date Prep:

MLI

MLI

RYR

Tech:

Tech:

Tech:

Chromium

Chromium


Parameter

Parameter

Parameter

Result

Result

Result

0.0100

0.0100

0.00500

Flag

Flag

Flag

mg/L

mg/L

mg/L

Units

Units

Units

1

1

1

Dil

Dil

Dil

Cas Number

Cas Number

Cas Number

7440-47-3

7440-47-3

18540-29-9

0.0483

0.0125

0.0430

938492

938532

937325

Seq Number:

Seq Number:

Seq Number:

SUB: AZ0765

SUB: AZ0765

RL

RL

RL

04.13.14 17.33

04.14.14 13.39

03.28.14 07.48

Analysis Date

Analysis Date

Analysis Date

% Moisture:

% Moisture:

% Moisture:

of 112 Final 1.000





OEMAnalyst:

SW5030CPrep Method:

04.04.14 00.34 Date Prep:

OEMTech:


Parameter Result

20.0 0.500

1.50 0.500 0.500

1.00 5.00 5.00 2.00 2.50 1.50 2.50

0.500 0.500 0.500

4.00 0.500

5.00 1.50 2.00 1.50

0.500 2.00

0.500 0.500

1.50 1.50 1.50 2.00

0.500 0.500 0.500 0.500 0.500 0.500

1.00 0.500

1.00 1.00

Flag


Units

1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1

DilCas Number

67-64-171-43-2108-86-174-97-575-27-475-25-274-83-978-93-31634-04-4104-51-8135-98-898-06-675-15-056-23-5108-90-775-00-367-66-374-87-395-49-8106-43-499-87-6124-48-196-12-8106-93-474-95-395-50-1541-73-1106-46-775-71-875-34-3107-06-275-35-4156-59-2156-60-578-87-5142-28-9594-20-7563-58-610061-01-5

<20.0<0.500

<1.50<0.500<0.500

<1.00<5.00<5.00<2.00<2.50<1.50<2.50

<0.500<0.500<0.500

<4.00<0.500

<5.00<1.50<2.00<1.50

<0.500<2.00

<0.500<0.500

<1.50<1.50<1.50<2.00

<0.500<0.5000.600

<0.500<0.500<0.500

<1.00<0.500

<1.00<1.00

937846Seq Number:

RL

04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37

Analysis Date

% Moisture:

of 112 Final 1.000





OEMAnalyst:

SW5030CPrep Method:

04.04.14 00.34 Date Prep:

OEMTech:


Parameter Result

0.500 2.00 5.00 5.00 2.50 3.00 2.00 5.00 5.00 2.00 1.00

0.500 0.500 0.500

2.00 5.00 5.00

0.500 0.500 0.500

2.00 1.00 2.00 1.50 1.00 2.00 5.00

0.500 1.00

Flag


Units

1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1

DilCas Number

10061-02-6100-41-487-68-3591-78-698-82-875-09-274-88-4108-10-191-20-3103-65-1100-42-5630-20-679-34-5127-18-4108-88-387-61-6120-82-171-55-679-00-579-01-675-69-496-18-495-63-6108-67-895-47-6179601-23-1108-05-475-01-41330-20-7

<0.500<2.00<5.00<5.00<2.50<3.00<2.00<5.00<5.00<2.00<1.00

<0.500<0.500

8.01 <2.00<5.00<5.00

<0.500<0.5000.630 <2.00<1.00<2.00<1.50<1.00<2.00<5.00

<0.500<1.00

937846Seq Number:

RL

04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37

Analysis Date

Surrogate

69-13366-13970-13070-135

%Recovery Flag

%%%%

9699

10093

04.04.14 06.37 04.04.14 06.37 04.04.14 06.37 04.04.14 06.37

Cas Number

1868-53-717060-07-02037-26-5460-00-4

Units Analysis Date


Limits

% Moisture:

of 112 Final 1.000







Analytical Method:

Analytical Method:

Analytical Method:

MKO

MKO

TNL

Analyst:

Analyst:

Analyst:

SW3010A

SW3010A

Prep Method:

Prep Method:

04.07.14 11.10

04.09.14 11.10

Date Prep:

Date Prep:

MLI

MLI

RYR

Tech:

Tech:

Tech:

Chromium

Chromium


Parameter

Parameter

Parameter

Result

Result

Result

0.0100

0.0100

0.00500

Flag

Flag

Flag

mg/L

mg/L

mg/L

Units

Units

Units

1

1

1

Dil

Dil

Dil

Cas Number

Cas Number

Cas Number

7440-47-3

7440-47-3

18540-29-9

<0.0100

<0.0100

0.00600

938492

938532

937325

Seq Number:

Seq Number:

Seq Number:

SUB: AZ0765

SUB: AZ0765

RL

RL

RL

04.13.14 17.40

04.14.14 13.46

03.28.14 07.48

Analysis Date

Analysis Date

Analysis Date

% Moisture:

% Moisture:

% Moisture:

of 112 Final 1.000





OEMAnalyst:

SW5030CPrep Method:

04.04.14 00.34 Date Prep:

OEMTech:


Parameter Result

20.0 0.500

1.50 0.500 0.500

1.00 5.00 5.00 2.00 2.50 1.50 2.50

0.500 0.500 0.500

4.00 0.500

5.00 1.50 2.00 1.50

0.500 2.00

0.500 0.500

1.50 1.50 1.50 2.00

0.500 0.500 0.500 0.500 0.500 0.500

1.00 0.500

1.00 1.00

Flag


Units

1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1

DilCas Number

67-64-171-43-2108-86-174-97-575-27-475-25-274-83-978-93-31634-04-4104-51-8135-98-898-06-675-15-056-23-5108-90-775-00-367-66-374-87-395-49-8106-43-499-87-6124-48-196-12-8106-93-474-95-395-50-1541-73-1106-46-775-71-875-34-3107-06-275-35-4156-59-2156-60-578-87-5142-28-9594-20-7563-58-610061-01-5

<20.0<0.500

<1.50<0.500<0.500

<1.00<5.00<5.00<2.00<2.50<1.50<2.50

<0.500<0.500<0.500

<4.00<0.500

<5.00<1.50<2.00<1.50

<0.500<2.00

<0.500<0.500

<1.50<1.50<1.50<2.003.48

<0.5006.18 7.86

<0.500<0.500

<1.00<0.500

<1.00<1.00

937846Seq Number:

RL

04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03

Analysis Date

% Moisture:

of 112 Final 1.000





OEMAnalyst:

SW5030CPrep Method:

04.04.14 00.34 Date Prep:

OEMTech:


Parameter Result

0.500 2.00 5.00 5.00 2.50 3.00 2.00 5.00 5.00 2.00 1.00

0.500 0.500 0.500

2.00 5.00 5.00

0.500 0.500 0.500

2.00 1.00 2.00 1.50 1.00 2.00 5.00

0.500 1.00

Flag


Units

1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1

DilCas Number

10061-02-6100-41-487-68-3591-78-698-82-875-09-274-88-4108-10-191-20-3103-65-1100-42-5630-20-679-34-5127-18-4108-88-387-61-6120-82-171-55-679-00-579-01-675-69-496-18-495-63-6108-67-895-47-6179601-23-1108-05-475-01-41330-20-7

<0.500<2.00<5.00<5.00<2.50<3.00<2.00<5.00<5.00<2.00<1.00

<0.500<0.500

2.99 <2.00<5.00<5.00

<0.500<0.500

44.0 <2.00<1.00<2.00<1.50<1.00<2.00<5.00

<0.500<1.00

937846Seq Number:

RL

04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03

Analysis Date

Surrogate

69-13366-13970-13070-135

%Recovery Flag

%%%%

98979893

04.04.14 07.03 04.04.14 07.03 04.04.14 07.03 04.04.14 07.03

Cas Number

1868-53-717060-07-02037-26-5460-00-4

Units Analysis Date


Limits

% Moisture:

of 112 Final 1.000







Analytical Method:

Analytical Method:

Analytical Method:

MKO

MKO

TNL

Analyst:

Analyst:

Analyst:

SW3010A

SW3010A

Prep Method:

Prep Method:

04.07.14 11.10

04.09.14 11.10

Date Prep:

Date Prep:

MLI

MLI

RYR

Tech:

Tech:

Tech:

Chromium

Chromium


Parameter

Parameter

Parameter

Result

Result

Result

0.0100

0.0100

0.00500

Flag

Flag

Flag

mg/L

mg/L

mg/L

Units

Units

Units

1

1

1

Dil

Dil

Dil

Cas Number

Cas Number

Cas Number

7440-47-3

7440-47-3

18540-29-9

<0.0100

<0.0100

<0.00500

938492

938532

937325

Seq Number:

Seq Number:

Seq Number:

SUB: AZ0765

SUB: AZ0765

RL

RL

RL

04.13.14 17.59

04.14.14 13.52

03.28.14 07.48

Analysis Date

Analysis Date

Analysis Date

% Moisture:

% Moisture:

% Moisture:

of 112 Final 1.000





OEMAnalyst:

SW5030CPrep Method:

04.04.14 00.34 Date Prep:

OEMTech:


Parameter Result

20.0 0.500

1.50 0.500 0.500

1.00 5.00 5.00 2.00 2.50 1.50 2.50

0.500 0.500 0.500

4.00 0.500

5.00 1.50 2.00 1.50

0.500 2.00

0.500 0.500

1.50 1.50 1.50 2.00

0.500 0.500 0.500 0.500 0.500 0.500

1.00 0.500

1.00 1.00

Flag


Units

1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1

DilCas Number

67-64-171-43-2108-86-174-97-575-27-475-25-274-83-978-93-31634-04-4104-51-8135-98-898-06-675-15-056-23-5108-90-775-00-367-66-374-87-395-49-8106-43-499-87-6124-48-196-12-8106-93-474-95-395-50-1541-73-1106-46-775-71-875-34-3107-06-275-35-4156-59-2156-60-578-87-5142-28-9594-20-7563-58-610061-01-5

<20.0<0.500

<1.50<0.500<0.500

<1.00<5.00<5.00<2.00<2.50<1.50<2.50

<0.500<0.500<0.500

<4.00<0.500

<5.00<1.50<2.00<1.50

<0.500<2.00

<0.500<0.500

<1.50<1.50<1.50<2.00

<0.500<0.500

1.03 <0.500<0.500<0.500

<1.00<0.500

<1.00<1.00

937846Seq Number:

RL

04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29

Analysis Date

% Moisture:

of 112 Final 1.000





OEMAnalyst:

SW5030CPrep Method:

04.04.14 00.34 Date Prep:

OEMTech:


Parameter Result

0.500 2.00 5.00 5.00 2.50 3.00 2.00 5.00 5.00 2.00 1.00

0.500 0.500 0.500

2.00 5.00 5.00

0.500 0.500 0.500

2.00 1.00 2.00 1.50 1.00 2.00 5.00

0.500 1.00

Flag


Units

1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1

DilCas Number

10061-02-6100-41-487-68-3591-78-698-82-875-09-274-88-4108-10-191-20-3103-65-1100-42-5630-20-679-34-5127-18-4108-88-387-61-6120-82-171-55-679-00-579-01-675-69-496-18-495-63-6108-67-895-47-6179601-23-1108-05-475-01-41330-20-7

<0.500<2.00<5.00<5.00<2.50<3.00<2.00<5.00<5.00<2.00<1.00

<0.500<0.500

1.34 <2.00<5.00<5.00

<0.500<0.5000.650 <2.00<1.00<2.00<1.50<1.00<2.00<5.00

<0.500<1.00

937846Seq Number:

RL

04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29

Analysis Date

Surrogate

69-13366-13970-13070-135

%Recovery Flag

%%%%

95949693

04.04.14 07.29 04.04.14 07.29 04.04.14 07.29 04.04.14 07.29

Cas Number

1868-53-717060-07-02037-26-5460-00-4

Units Analysis Date


Limits

% Moisture:

of 112 Final 1.000







Analytical Method:

Analytical Method:

Analytical Method:

MKO

MKO

TNL

Analyst:

Analyst:

Analyst:

SW3010A

SW3010A

Prep Method:

Prep Method:

04.07.14 11.10

04.09.14 11.10

Date Prep:

Date Prep:

MLI

MLI

RYR

Tech:

Tech:

Tech:

Chromium

Chromium


Parameter

Parameter

Parameter

Result

Result

Result

0.0100

0.0100

0.00500

Flag

Flag

Flag

mg/L

mg/L

mg/L

Units

Units

Units

1

1

1

Dil

Dil

Dil

Cas Number

Cas Number

Cas Number

7440-47-3

7440-47-3

18540-29-9

<0.0100

<0.0100

<0.00500

938492

938532

937325

Seq Number:

Seq Number:

Seq Number:

SUB: AZ0765

SUB: AZ0765

RL

RL

RL

04.13.14 18.06

04.14.14 13.59

03.28.14 07.48

Analysis Date

Analysis Date

Analysis Date

% Moisture:

% Moisture:

% Moisture:

of 112 Final 1.000





OEMAnalyst:

SW5030CPrep Method:

04.04.14 00.34 Date Prep:

OEMTech:


Parameter Result

20.0 0.500

1.50 0.500 0.500

1.00 5.00 5.00 2.00 2.50 1.50 2.50

0.500 0.500 0.500

4.00 0.500

5.00 1.50 2.00 1.50

0.500 2.00

0.500 0.500

1.50 1.50 1.50 2.00

0.500 0.500 0.500 0.500 0.500 0.500

1.00 0.500

1.00 1.00

Flag


Units

1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1

DilCas Number

67-64-171-43-2108-86-174-97-575-27-475-25-274-83-978-93-31634-04-4104-51-8135-98-898-06-675-15-056-23-5108-90-775-00-367-66-374-87-395-49-8106-43-499-87-6124-48-196-12-8106-93-474-95-395-50-1541-73-1106-46-775-71-875-34-3107-06-275-35-4156-59-2156-60-578-87-5142-28-9594-20-7563-58-610061-01-5

<20.0<0.500

<1.50<0.500<0.500

<1.00<5.00<5.00<2.00<2.50<1.50<2.50

<0.500<0.500<0.500

<4.00<0.500

<5.00<1.50<2.00<1.50

<0.500<2.00

<0.500<0.500

<1.50<1.50<1.50<2.00

<0.500<0.500<0.500<0.500<0.500<0.500

<1.00<0.500

<1.00<1.00

937846Seq Number:

RL

04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55

Analysis Date

% Moisture:

of 112 Final 1.000





OEMAnalyst:

SW5030CPrep Method:

04.04.14 00.34 Date Prep:

OEMTech:


Parameter Result

0.500 2.00 5.00 5.00 2.50 3.00 2.00 5.00 5.00 2.00 1.00

0.500 0.500 0.500

2.00 5.00 5.00

0.500 0.500 0.500

2.00 1.00 2.00 1.50 1.00 2.00 5.00

0.500 1.00

Flag


Units

1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1

DilCas Number

10061-02-6100-41-487-68-3591-78-698-82-875-09-274-88-4108-10-191-20-3103-65-1100-42-5630-20-679-34-5127-18-4108-88-387-61-6120-82-171-55-679-00-579-01-675-69-496-18-495-63-6108-67-895-47-6179601-23-1108-05-475-01-41330-20-7

<0.500<2.00<5.00<5.00<2.50<3.00<2.00<5.00<5.00<2.00<1.00

<0.500<0.5000.630 <2.00<5.00<5.00

<0.500<0.500

1.05 <2.00<1.00<2.00<1.50<1.00<2.00<5.00

<0.500<1.00

937846Seq Number:

RL

04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55

Analysis Date

Surrogate

69-13366-13970-13070-135

%Recovery Flag

%%%%

98989891

04.04.14 07.55 04.04.14 07.55 04.04.14 07.55 04.04.14 07.55

Cas Number

1868-53-717060-07-02037-26-5460-00-4

Units Analysis Date


Limits

% Moisture:

of 112 Final 1.000







Analytical Method:

Analytical Method:

Analytical Method:

MKO

MKO

TNL

Analyst:

Analyst:

Analyst:

SW3010A

SW3010A

Prep Method:

Prep Method:

04.07.14 11.10

04.09.14 11.10

Date Prep:

Date Prep:

MLI

MLI

RYR

Tech:

Tech:

Tech:

Chromium

Chromium


Parameter

Parameter

Parameter

Result

Result

Result

0.0100

0.0100

0.00500

Flag

Flag

Flag

mg/L

mg/L

mg/L

Units

Units

Units

1

1

1

Dil

Dil

Dil

Cas Number

Cas Number

Cas Number

7440-47-3

7440-47-3

18540-29-9

<0.0100

<0.0100

<0.00500

938492

938532

937325

Seq Number:

Seq Number:

Seq Number:

SUB: AZ0765

SUB: AZ0765

RL

RL

RL

04.13.14 18.13

04.14.14 14.21

03.28.14 07.48

Analysis Date

Analysis Date

Analysis Date

% Moisture:

% Moisture:

% Moisture:

of 112 Final 1.000





OEMAnalyst:

SW5030CPrep Method:

04.04.14 00.34 Date Prep:

OEMTech:


Parameter Result

20.0 0.500

1.50 0.500 0.500

1.00 5.00 5.00 2.00 2.50 1.50 2.50

0.500 0.500 0.500

4.00 0.500

5.00 1.50 2.00 1.50

0.500 2.00

0.500 0.500

1.50 1.50 1.50 2.00

0.500 0.500 0.500 0.500 0.500 0.500

1.00 0.500

1.00 1.00

Flag


Units

1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1

DilCas Number

67-64-171-43-2108-86-174-97-575-27-475-25-274-83-978-93-31634-04-4104-51-8135-98-898-06-675-15-056-23-5108-90-775-00-367-66-374-87-395-49-8106-43-499-87-6124-48-196-12-8106-93-474-95-395-50-1541-73-1106-46-775-71-875-34-3107-06-275-35-4156-59-2156-60-578-87-5142-28-9594-20-7563-58-610061-01-5

<20.0<0.500

<1.50<0.500<0.500

<1.00<5.00<5.00<2.00<2.50<1.50<2.50

<0.500<0.500<0.500

<4.00<0.500

<5.00<1.50<2.00<1.50

<0.500<2.00

<0.500<0.500

<1.50<1.50<1.50<2.00

<0.500<0.500<0.500<0.500<0.500<0.500

<1.00<0.500

<1.00<1.00

937846Seq Number:

RL

04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21

Analysis Date

% Moisture:

of 112 Final 1.000





OEMAnalyst:

SW5030CPrep Method:

04.04.14 00.34 Date Prep:

OEMTech:


Parameter Result

0.500 2.00 5.00 5.00 2.50 3.00 2.00 5.00 5.00 2.00 1.00

0.500 0.500 0.500

2.00 5.00 5.00

0.500 0.500 0.500

2.00 1.00 2.00 1.50 1.00 2.00 5.00

0.500 1.00

Flag


Units

1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1

DilCas Number

10061-02-6100-41-487-68-3591-78-698-82-875-09-274-88-4108-10-191-20-3103-65-1100-42-5630-20-679-34-5127-18-4108-88-387-61-6120-82-171-55-679-00-579-01-675-69-496-18-495-63-6108-67-895-47-6179601-23-1108-05-475-01-41330-20-7

<0.500<2.00<5.00<5.00<2.50<3.00<2.00<5.00<5.00<2.00<1.00

<0.500<0.500<0.500

<2.00<5.00<5.00

<0.500<0.500

1.11 <2.00<1.00<2.00<1.50<1.00<2.00<5.00

<0.500<1.00

937846Seq Number:

RL

04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21

Analysis Date

Surrogate

69-13366-13970-13070-135

%Recovery Flag

%%%%

96959894

04.04.14 08.21 04.04.14 08.21 04.04.14 08.21 04.04.14 08.21

Cas Number

1868-53-717060-07-02037-26-5460-00-4

Units Analysis Date


Limits

% Moisture:

of 112 Final 1.000







Analytical Method:

Analytical Method:

Analytical Method:

MKO

MKO

TNL

Analyst:

Analyst:

Analyst:

SW3010A

SW3010A

Prep Method:

Prep Method:

04.07.14 11.10

04.09.14 11.10

Date Prep:

Date Prep:

MLI

MLI

RYR

Tech:

Tech:

Tech:

Chromium

Chromium


Parameter

Parameter

Parameter

Result

Result

Result

0.0100

0.0100

0.00500

Flag

Flag

Flag

mg/L

mg/L

mg/L

Units

Units

Units

1

1

1

Dil

Dil

Dil

Cas Number

Cas Number

Cas Number

7440-47-3

7440-47-3

18540-29-9

<0.0100

<0.0100

<0.00500

938492

938532

937325

Seq Number:

Seq Number:

Seq Number:

SUB: AZ0765

SUB: AZ0765

RL

RL

RL

04.13.14 18.19

04.14.14 14.27

03.28.14 07.48

Analysis Date

Analysis Date

Analysis Date

% Moisture:

% Moisture:

% Moisture:

of 112 Final 1.000





OEMAnalyst:

SW5030CPrep Method:

04.04.14 00.34 Date Prep:

OEMTech:


Parameter Result

20.0 0.500

1.50 0.500 0.500

1.00 5.00 5.00 2.00 2.50 1.50 2.50

0.500 0.500 0.500

4.00 0.500

5.00 1.50 2.00 1.50

0.500 2.00

0.500 0.500

1.50 1.50 1.50 2.00

0.500 0.500 0.500 0.500 0.500 0.500

1.00 0.500

1.00 1.00

Flag


Units

1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1

DilCas Number

67-64-171-43-2108-86-174-97-575-27-475-25-274-83-978-93-31634-04-4104-51-8135-98-898-06-675-15-056-23-5108-90-775-00-367-66-374-87-395-49-8106-43-499-87-6124-48-196-12-8106-93-474-95-395-50-1541-73-1106-46-775-71-875-34-3107-06-275-35-4156-59-2156-60-578-87-5142-28-9594-20-7563-58-610061-01-5

<20.0<0.500

<1.50<0.500<0.500

<1.00<5.00<5.00<2.00<2.50<1.50<2.50

<0.500<0.500<0.500

<4.003.07

<5.00<1.50<2.00<1.50

<0.500<2.00

<0.500<0.500

<1.50<1.50<1.50<2.001.92

<0.5004.84 7.77

<0.500<0.500

<1.00<0.500

<1.00<1.00

937846Seq Number:

RL

04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48

Analysis Date

% Moisture:

of 112 Final 1.000





OEMAnalyst:

SW5030CPrep Method:

04.04.14 00.34 Date Prep:

OEMTech:


Parameter Result

0.500 2.00 5.00 5.00 2.50 3.00 2.00 5.00 5.00 2.00 1.00

0.500 0.500 0.500

2.00 5.00 5.00

0.500 0.500 0.500

2.00 1.00 2.00 1.50 1.00 2.00 5.00

0.500 1.00

Flag


Units

1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1

DilCas Number

10061-02-6100-41-487-68-3591-78-698-82-875-09-274-88-4108-10-191-20-3103-65-1100-42-5630-20-679-34-5127-18-4108-88-387-61-6120-82-171-55-679-00-579-01-675-69-496-18-495-63-6108-67-895-47-6179601-23-1108-05-475-01-41330-20-7

<0.500<2.00<5.00<5.00<2.50<3.00<2.00<5.00<5.00<2.00<1.00

<0.500<0.500

13.5 <2.00<5.00<5.00

<0.500<0.500

76.2 <2.00<1.00<2.00<1.50<1.00<2.00<5.00

<0.500<1.00

937846Seq Number:

RL

04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48

Analysis Date

Surrogate

69-13366-13970-13070-135

%Recovery Flag

%%%%

96969992

04.04.14 08.48 04.04.14 08.48 04.04.14 08.48 04.04.14 08.48

Cas Number

1868-53-717060-07-02037-26-5460-00-4

Units Analysis Date


Limits

% Moisture:

of 112 Final 1.000







Analytical Method:

Analytical Method:

Analytical Method:

MKO

MKO

TNL

Analyst:

Analyst:

Analyst:

SW3010A

SW3010A

Prep Method:

Prep Method:

04.07.14 11.10

04.09.14 11.10

Date Prep:

Date Prep:

MLI

MLI

RYR

Tech:

Tech:

Tech:

Chromium

Chromium


Parameter

Parameter

Parameter

Result

Result

Result

0.0100

0.0100

0.00500

Flag

Flag

Flag

mg/L

mg/L

mg/L

Units

Units

Units

1

1

1

Dil

Dil

Dil

Cas Number

Cas Number

Cas Number

7440-47-3

7440-47-3

18540-29-9

<0.0100

<0.0100

<0.00500

938492

938532

937325

Seq Number:

Seq Number:

Seq Number:

SUB: AZ0765

SUB: AZ0765

RL

RL

RL

04.13.14 18.26

04.14.14 14.34

03.28.14 07.48

Analysis Date

Analysis Date

Analysis Date

% Moisture:

% Moisture:

% Moisture:

of 112 Final 1.000





OEMAnalyst:

SW5030CPrep Method:

04.04.14 00.34 Date Prep:

OEMTech:


Parameter Result

20.0 0.500

1.50 0.500 0.500

1.00 5.00 5.00 2.00 2.50 1.50 2.50

0.500 0.500 0.500

4.00 0.500

5.00 1.50 2.00 1.50

0.500 2.00

0.500 0.500

1.50 1.50 1.50 2.00

0.500 0.500 0.500 0.500 0.500 0.500

1.00 0.500

1.00 1.00

Flag


Units

1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1

DilCas Number

67-64-171-43-2108-86-174-97-575-27-475-25-274-83-978-93-31634-04-4104-51-8135-98-898-06-675-15-056-23-5108-90-775-00-367-66-374-87-395-49-8106-43-499-87-6124-48-196-12-8106-93-474-95-395-50-1541-73-1106-46-775-71-875-34-3107-06-275-35-4156-59-2156-60-578-87-5142-28-9594-20-7563-58-610061-01-5

<20.0<0.500

<1.50<0.500<0.500

<1.00<5.00<5.00<2.00<2.50<1.50<2.50

<0.500<0.500<0.500

<4.00<0.500

<5.00<1.50<2.00<1.50

<0.500<2.00

<0.500<0.500

<1.50<1.50<1.50<2.00

<0.500<0.500<0.500<0.500<0.500<0.500

<1.00<0.500

<1.00<1.00

937846Seq Number:

RL

04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14

Analysis Date

% Moisture:

of 112 Final 1.000





OEMAnalyst:

SW5030CPrep Method:

04.04.14 00.34 Date Prep:

OEMTech:


Parameter Result

0.500 2.00 5.00 5.00 2.50 3.00 2.00 5.00 5.00 2.00 1.00

0.500 0.500 0.500

2.00 5.00 5.00

0.500 0.500 0.500

2.00 1.00 2.00 1.50 1.00 2.00 5.00

0.500 1.00

Flag


Units

1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1

DilCas Number

10061-02-6100-41-487-68-3591-78-698-82-875-09-274-88-4108-10-191-20-3103-65-1100-42-5630-20-679-34-5127-18-4108-88-387-61-6120-82-171-55-679-00-579-01-675-69-496-18-495-63-6108-67-895-47-6179601-23-1108-05-475-01-41330-20-7

<0.500<2.00<5.00<5.00<2.50<3.00<2.00<5.00<5.00<2.00<1.00

<0.500<0.500<0.500

<2.00<5.00<5.00

<0.500<0.5000.630 <2.00<1.00<2.00<1.50<1.00<2.00<5.00

<0.500<1.00

937846Seq Number:

RL

04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14

Analysis Date

Surrogate

69-13366-13970-13070-135

%Recovery Flag

%%%%

98959793

04.04.14 09.14 04.04.14 09.14 04.04.14 09.14 04.04.14 09.14

Cas Number

1868-53-717060-07-02037-26-5460-00-4

Units Analysis Date


Limits

% Moisture:

of 112 Final 1.000







Analytical Method:

Analytical Method:

Analytical Method:

MKO

MKO

TNL

Analyst:

Analyst:

Analyst:

SW3010A

SW3010A

Prep Method:

Prep Method:

04.07.14 11.10

04.09.14 11.10

Date Prep:

Date Prep:

MLI

MLI

RYR

Tech:

Tech:

Tech:

Chromium

Chromium


Parameter

Parameter

Parameter

Result

Result

Result

0.0100

0.0100

0.00500

Flag

Flag

Flag

mg/L

mg/L

mg/L

Units

Units

Units

1

1

1

Dil

Dil

Dil

Cas Number

Cas Number

Cas Number

7440-47-3

7440-47-3

18540-29-9

<0.0100

<0.0100

<0.00500

938492

938532

937325

Seq Number:

Seq Number:

Seq Number:

SUB: AZ0765

SUB: AZ0765

RL

RL

RL

04.13.14 18.32

04.14.14 14.40

03.28.14 07.48

Analysis Date

Analysis Date

Analysis Date

% Moisture:

% Moisture:

% Moisture:

of 112 Final 1.000





OEMAnalyst:

SW5030CPrep Method:

04.04.14 00.34 Date Prep:

OEMTech:


Parameter Result

20.0 0.500

1.50 0.500 0.500

1.00 5.00 5.00 2.00 2.50 1.50 2.50

0.500 0.500 0.500

4.00 0.500

5.00 1.50 2.00 1.50

0.500 2.00

0.500 0.500

1.50 1.50 1.50 2.00

0.500 0.500 0.500 0.500 0.500 0.500

1.00 0.500

1.00 1.00

Flag


Units

1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1

DilCas Number

67-64-171-43-2108-86-174-97-575-27-475-25-274-83-978-93-31634-04-4104-51-8135-98-898-06-675-15-056-23-5108-90-775-00-367-66-374-87-395-49-8106-43-499-87-6124-48-196-12-8106-93-474-95-395-50-1541-73-1106-46-775-71-875-34-3107-06-275-35-4156-59-2156-60-578-87-5142-28-9594-20-7563-58-610061-01-5

<20.0<0.500

<1.50<0.500<0.500

<1.00<5.00<5.00<2.00<2.50<1.50<2.50

<0.500<0.500<0.500

<4.003.53

<5.00<1.50<2.00<1.50

<0.500<2.00

<0.500<0.500

<1.50<1.50<1.50<2.001.09

<0.5002.84 3.06

<0.500<0.500

<1.00<0.500

<1.00<1.00

937846Seq Number:

RL

04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40

Analysis Date

% Moisture:

of 112 Final 1.000





OEMAnalyst:

SW5030CPrep Method:

04.04.14 00.34 Date Prep:

OEMTech:


Parameter Result

0.500 2.00 5.00 5.00 2.50 3.00 2.00 5.00 5.00 2.00 1.00

0.500 0.500 0.500

2.00 5.00 5.00

0.500 0.500 0.500

2.00 1.00 2.00 1.50 1.00 2.00 5.00

0.500 1.00

Flag


Units

1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1

DilCas Number

10061-02-6100-41-487-68-3591-78-698-82-875-09-274-88-4108-10-191-20-3103-65-1100-42-5630-20-679-34-5127-18-4108-88-387-61-6120-82-171-55-679-00-579-01-675-69-496-18-495-63-6108-67-895-47-6179601-23-1108-05-475-01-41330-20-7

<0.500<2.00<5.00<5.00<2.50<3.00<2.00<5.00<5.00<2.00<1.00

<0.500<0.500

10.3 <2.00<5.00<5.00

<0.500<0.500

35.5 <2.00<1.00<2.00<1.50<1.00<2.00<5.00

<0.500<1.00

937846Seq Number:

RL

04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40

Analysis Date

Surrogate

69-13366-13970-13070-135

%Recovery Flag

%%%%

100989893

04.04.14 09.40 04.04.14 09.40 04.04.14 09.40 04.04.14 09.40

Cas Number

1868-53-717060-07-02037-26-5460-00-4

Units Analysis Date


Limits

% Moisture:

of 112 Final 1.000







Analytical Method:

Analytical Method:

Analytical Method:

MKO

MKO

TNL

Analyst:

Analyst:

Analyst:

SW3010A

SW3010A

Prep Method:

Prep Method:

04.07.14 11.10

04.09.14 11.10

Date Prep:

Date Prep:

MLI

MLI

RYR

Tech:

Tech:

Tech:

Chromium

Chromium


Parameter

Parameter

Parameter

Result

Result

Result

0.0100

0.0100

0.00500

Flag

Flag

Flag

mg/L

mg/L

mg/L

Units

Units

Units

1

1

1

Dil

Dil

Dil

Cas Number

Cas Number

Cas Number

7440-47-3

7440-47-3

18540-29-9

<0.0100

<0.0100

<0.00500

938492

938532

937325

Seq Number:

Seq Number:

Seq Number:

SUB: AZ0765

SUB: AZ0765

RL

RL

RL

04.13.14 18.39

04.14.14 14.47

03.28.14 07.48

Analysis Date

Analysis Date

Analysis Date

% Moisture:

% Moisture:

% Moisture:

of 112 Final 1.000





OEMAnalyst:

SW5030CPrep Method:

04.04.14 00.34 Date Prep:

OEMTech:


Parameter Result

20.0 0.500

1.50 0.500 0.500

1.00 5.00 5.00 2.00 2.50 1.50 2.50

0.500 0.500 0.500

4.00 0.500

5.00 1.50 2.00 1.50

0.500 2.00

0.500 0.500

1.50 1.50 1.50 2.00

0.500 0.500 0.500 0.500 0.500 0.500

1.00 0.500

1.00 1.00

Flag


Units

1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1

DilCas Number

67-64-171-43-2108-86-174-97-575-27-475-25-274-83-978-93-31634-04-4104-51-8135-98-898-06-675-15-056-23-5108-90-775-00-367-66-374-87-395-49-8106-43-499-87-6124-48-196-12-8106-93-474-95-395-50-1541-73-1106-46-775-71-875-34-3107-06-275-35-4156-59-2156-60-578-87-5142-28-9594-20-7563-58-610061-01-5

<20.0<0.500

<1.50<0.500<0.500

<1.00<5.00<5.00<2.00<2.50<1.50<2.50

<0.500<0.500<0.500

<4.00<0.500

<5.00<1.50<2.00<1.50

<0.500<2.00

<0.500<0.500

<1.50<1.50<1.50<2.00

<0.500<0.500<0.500<0.500<0.500<0.500

<1.00<0.500

<1.00<1.00

937846Seq Number:

RL

04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06

Analysis Date

% Moisture:

of 112 Final 1.000





OEMAnalyst:

SW5030CPrep Method:

04.04.14 00.34 Date Prep:

OEMTech:


Parameter Result

0.500 2.00 5.00 5.00 2.50 3.00 2.00 5.00 5.00 2.00 1.00

0.500 0.500 0.500

2.00 5.00 5.00

0.500 0.500 0.500

2.00 1.00 2.00 1.50 1.00 2.00 5.00

0.500 1.00

Flag


Units

1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1

DilCas Number

10061-02-6100-41-487-68-3591-78-698-82-875-09-274-88-4108-10-191-20-3103-65-1100-42-5630-20-679-34-5127-18-4108-88-387-61-6120-82-171-55-679-00-579-01-675-69-496-18-495-63-6108-67-895-47-6179601-23-1108-05-475-01-41330-20-7

<0.500<2.00<5.00<5.00<2.50<3.00<2.00<5.00<5.00<2.00<1.00

<0.500<0.500<0.500

<2.00<5.00<5.00

<0.500<0.500<0.500

<2.00<1.00<2.00<1.50<1.00<2.00<5.00

<0.500<1.00

937846Seq Number:

RL

04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06

Analysis Date

Surrogate

69-13366-13970-13070-135

%Recovery Flag

%%%%

97969792

04.04.14 10.06 04.04.14 10.06 04.04.14 10.06 04.04.14 10.06

Cas Number

1868-53-717060-07-02037-26-5460-00-4

Units Analysis Date


Limits

% Moisture:

of 112 Final 1.000



03.27.14 16.40 Date Received:03.27.14 07.27 Date Collected:482073-031Lab Sample Id:WaterMatrix: Trip BlankSample Id:


OEMAnalyst:

SW5030CPrep Method:

04.04.14 00.34 Date Prep:

OEMTech:


Parameter Result

20.0 0.500

1.50 0.500 0.500

1.00 5.00 5.00 2.00 2.50 1.50 2.50

0.500 0.500 0.500

4.00 0.500

5.00 1.50 2.00 1.50

0.500 2.00

0.500 0.500

1.50 1.50 1.50 2.00

0.500 0.500 0.500 0.500 0.500 0.500

1.00 0.500

1.00 1.00

Flag


Units

1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1

DilCas Number

67-64-171-43-2108-86-174-97-575-27-475-25-274-83-978-93-31634-04-4104-51-8135-98-898-06-675-15-056-23-5108-90-775-00-367-66-374-87-395-49-8106-43-499-87-6124-48-196-12-8106-93-474-95-395-50-1541-73-1106-46-775-71-875-34-3107-06-275-35-4156-59-2156-60-578-87-5142-28-9594-20-7563-58-610061-01-5

<20.0<0.500

<1.50<0.500<0.500

<1.00<5.00<5.00<2.00<2.50<1.50<2.50

<0.500<0.500<0.500

<4.00<0.500

<5.00<1.50<2.00<1.50

<0.500<2.00

<0.500<0.500

<1.50<1.50<1.50<2.00

<0.500<0.500<0.500<0.500<0.500<0.500

<1.00<0.500

<1.00<1.00

937846Seq Number:

RL

04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32

Analysis Date

% Moisture:

of 112 Final 1.000



03.27.14 16.40 Date Received:03.27.14 07.27 Date Collected:482073-031Lab Sample Id:WaterMatrix: Trip BlankSample Id:


OEMAnalyst:

SW5030CPrep Method:

04.04.14 00.34 Date Prep:

OEMTech:


Parameter Result

0.500 2.00 5.00 5.00 2.50 3.00 2.00 5.00 5.00 2.00 1.00

0.500 0.500 0.500

2.00 5.00 5.00

0.500 0.500 0.500

2.00 1.00 2.00 1.50 1.00 2.00 5.00

0.500 1.00

Flag


Units

1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1

DilCas Number

10061-02-6100-41-487-68-3591-78-698-82-875-09-274-88-4108-10-191-20-3103-65-1100-42-5630-20-679-34-5127-18-4108-88-387-61-6120-82-171-55-679-00-579-01-675-69-496-18-495-63-6108-67-895-47-6179601-23-1108-05-475-01-41330-20-7

<0.500<2.00<5.00<5.00<2.50<3.00<2.00<5.00<5.00<2.00<1.00

<0.500<0.500<0.500

<2.00<5.00<5.00

<0.500<0.500<0.500

<2.00<1.00<2.00<1.50<1.00<2.00<5.00

<0.500<1.00

937846Seq Number:

RL

04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32

Analysis Date

Surrogate

69-13366-13970-13070-135

%Recovery Flag

%%%%

94949791

04.04.14 10.32 04.04.14 10.32 04.04.14 10.32 04.04.14 10.32

Cas Number

1868-53-717060-07-02037-26-5460-00-4

Units Analysis Date


Limits

% Moisture:

of 112 Final 1.000

QC Summary 482073

TerranextWVBA

653451-1-BLK

653576-1-BLK

482073-001

482073-021

653575-1-BLK

653697-1-BLK

MB Sample Id:

MB Sample Id:

Parent Sample Id:

Parent Sample Id:

MB Sample Id:

MB Sample Id:

Water

Water

Water

Water

Water

Water

Matrix:

Matrix:

Matrix:

Matrix:

Matrix:

Matrix:







Analytical Method:

Analytical Method:

Analytical Method:

Analytical Method:

Analytical Method:

Analytical Method:

SW3010A

SW3010A

SW3010A

SW3010A

SW3010A

SW3010A

Prep Method:

Prep Method:

Prep Method:

Prep Method:

Prep Method:

Prep Method:

04.03.14

04.07.14

04.03.14

04.07.14

04.07.14

04.09.14

Date Prep:

Date Prep:

Date Prep:

Date Prep:

Date Prep:

Date Prep:

Chromium

Chromium

Chromium

Chromium

Chromium

Chromium

Parameter

Parameter

Parameter

Parameter

Parameter

Parameter

%RPD

%RPD

%RPD

%RPD

%RPD

%RPD

Flag

Flag

Flag

Flag

Flag

Flag

20

20

20

20

20

20

RPDLimit

RPDLimit

RPDLimit

RPDLimit

RPDLimit

RPDLimit

1

4

1

2

1

2

938379

938492

938379

938492

938352

938532

Seq Number:

Seq Number:

Seq Number:

Seq Number:

Seq Number:

Seq Number:

04.11.14 11:13

04.13.14 16:48

04.11.14 11:33

04.13.14 17:08

04.11.14 04:44

04.14.14 13:07

Analysis Date

Analysis Date

Analysis Date

Analysis Date

Analysis Date

Analysis Date

Limits

Limits

Limits

Limits

Limits

Limits

80-120

80-120

75-125

75-125

80-120

80-120

LCSD %Rec

LCSD %Rec

MSD %Rec

MSD %Rec

LCSD %Rec

LCSD %Rec

108

106

108

107

106

104

LCSD Result

LCSD Result

MSD Result

MSD Result

LCSD Result

LCSD Result

1.08

1.06

1.08

1.12

1.06

1.04

LCS %Rec

LCS %Rec

MS %Rec

MS %Rec

LCS %Rec

LCS %Rec

109

110

107

105

107

102

1.09

1.10

1.07

1.10

1.07

1.02

Spike Amount

Spike Amount

Spike Amount

Spike Amount

Spike Amount

Spike Amount

1.00

1.00

1.00

1.00

1.00

1.00

MB Result

MB Result

Parent Result

Parent Result

MB Result

MB Result

<0.0100

<0.0100

<0.0100

0.0481

<0.0100

<0.0100

653451-1-BKS

653576-1-BKS

482073-001 S

482073-021 S

653575-1-BKS

653697-1-BKS

LCS Sample Id:

LCS Sample Id:

MS Sample Id:

MS Sample Id:

LCS Sample Id:

LCS Sample Id:

653451-1-BSD

653576-1-BSD

482073-001 SD

482073-021 SD

653575-1-BSD

653697-1-BSD

LCSD Sample Id:

LCSD Sample Id:

MSD Sample Id:

MSD Sample Id:

LCSD Sample Id:

LCSD Sample Id:

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

Units

Units

Units

Units

Units

Units

LCS Result

LCS Result

MS Result

MS Result

LCS Result

LCS Result

of 112 Final 1.000

QC Summary 482073

TerranextWVBA

482073-001

482073-021

937261-1-BLK

937325-1-BLK

482073-001

482073-020

Parent Sample Id:

Parent Sample Id:

MB Sample Id:

MB Sample Id:

Parent Sample Id:

Parent Sample Id:

Water

Water

Water

Water

Water

Water

Matrix:

Matrix:

Matrix:

Matrix:

Matrix:

Matrix:







Analytical Method:

Analytical Method:

Analytical Method:

Analytical Method:

Analytical Method:

Analytical Method:

SW3010A

SW3010A

Prep Method:

Prep Method:

04.07.14

04.09.14

Date Prep:

Date Prep:

Chromium

Chromium





Parameter

Parameter

Parameter

Parameter

Parameter

Parameter

%RPD

%RPD

%RPD

%RPD

%RPD

%RPD

Flag

Flag

Flag

Flag

Flag

Flag

20

20

20

20

20

20

RPDLimit

RPDLimit

RPDLimit

RPDLimit

RPDLimit

RPDLimit

0

3

1

2

0

0

938352

938532

937261

937325

937261

937261

Seq Number:

Seq Number:

Seq Number:

Seq Number:

Seq Number:

Seq Number:

04.11.14 05:07

04.14.14 13:27

03.28.14 07:09

03.28.14 07:48

03.28.14 07:09

03.28.14 07:09

Analysis Date

Analysis Date

Analysis Date

Analysis Date

Analysis Date

Analysis Date

Limits

Limits

Limits

Limits

Limits

Limits

75-125

75-125

81-119

81-119

36-153

36-153

MSD %Rec

MSD %Rec

LCSD %Rec

LCSD %Rec

MSD %Rec

MSD %Rec

106

107

99

98

97

96

MSD Result

MSD Result

LCSD Result

LCSD Result

MSD Result

MSD Result

1.06

1.08

0.0990

0.0980

0.102

0.0960

MS %Rec

MS %Rec

LCS %Rec

LCS %Rec

MS %Rec

MS %Rec

106

104

100

96

97

96

1.06

1.05

0.100

0.0960

0.102

0.0960

Spike Amount

Spike Amount

Spike Amount

Spike Amount

Spike Amount

Spike Amount

1.00

1.00

0.100

0.100

0.100

0.100

Parent Result

Parent Result

MB Result

MB Result

Parent Result

Parent Result

<0.0100

0.0144

<0.00500

<0.00500

0.00500

<0.00500

482073-001 S

482073-021 S

937261-1-BKS

937325-1-BKS

482073-001 S

482073-020 S

MS Sample Id:

MS Sample Id:

LCS Sample Id:

LCS Sample Id:

MS Sample Id:

MS Sample Id:

482073-001 SD

482073-021 SD

937261-1-BSD

937325-1-BSD

482073-001 SD

482073-020 SD

MSD Sample Id:

MSD Sample Id:

LCSD Sample Id:

LCSD Sample Id:

MSD Sample Id:

MSD Sample Id:

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

Units

Units

Units

Units

Units

Units

MS Result

MS Result

LCS Result

LCS Result

MS Result

MS Result

of 112 Final 1.000

QC Summary 482073

TerranextWVBA

482073-022Parent Sample Id:WaterMatrix:

Chromium Hexavalent by SM 3500 Cr-DAnalytical Method:


Parameter %RPD Flag

20

RPDLimit

1

937325Seq Number:

03.28.14 07:48

Analysis Date

Limits

36-153

MSD %Rec

98

MSD Result

0.141

MS %Rec

990.142

Spike Amount

0.100

Parent Result

0.0430

482073-022 SMS Sample Id: 482073-022 SDMSD Sample Id:

mg/L

UnitsMS Result

of 112 Final 1.000

QC Summary 482073

TerranextWVBA

653270-1-BLKMB Sample Id:WaterMatrix:

VOCs by EPA 8260B Analytical Method: SW5030CPrep Method: 03.31.14Date Prep:

AcetoneBenzeneBromobenzeneBromochloromethaneBromodichloromethaneBromoformBromomethane2-ButanoneMTBEn-ButylbenzeneSec-Butylbenzenetert-ButylbenzeneCarbon DisulfideCarbon TetrachlorideChlorobenzeneChloroethaneChloroformChloromethane2-Chlorotoluene4-Chlorotoluenep-Cymene (p-Isopropyltoluene)Dibromochloromethane1,2-Dibromo-3-Chloropropane1,2-DibromoethaneDibromomethane1,2-Dichlorobenzene1,3-Dichlorobenzene1,4-DichlorobenzeneDichlorodifluoromethane1,1-Dichloroethane1,2-Dichloroethane1,1-Dichloroethenecis-1,2-Dichloroethenetrans-1,2-dichloroethene1,2-Dichloropropane1,3-Dichloropropane2,2-Dichloropropane1,1-Dichloropropenecis-1,3-Dichloropropenetrans-1,3-dichloropropeneEthylbenzeneHexachlorobutadiene2-HexanoneisopropylbenzeneMethylene ChlorideIodomethane (Methyl Iodide)4-Methyl-2-PentanoneNaphthalenen-PropylbenzeneStyrene1,1,1,2-Tetrachloroethane1,1,2,2-Tetrachloroethane

Parameter %RPD Flag

28202024202025272120202022212024242620282020212023202020272020212421202024202020202220202022212720202020

RPDLimit

8020102173210121141303101001035103051380231106020562012

937532Seq Number:

03.31.14 23:09

03.31.14 23:0903.31.14 23:0903.31.14 23:0903.31.14 23:0903.31.14 23:0903.31.14 23:0903.31.14 23:09

03.31.14 23:0903.31.14 23:0903.31.14 23:0903.31.14 23:0903.31.14 23:0903.31.14 23:0903.31.14 23:09

03.31.14 23:0903.31.14 23:0903.31.14 23:0903.31.14 23:0903.31.14 23:0903.31.14 23:09

03.31.14 23:0903.31.14 23:0903.31.14 23:0903.31.14 23:0903.31.14 23:0903.31.14 23:0903.31.14 23:09

03.31.14 23:0903.31.14 23:0903.31.14 23:0903.31.14 23:0903.31.14 23:0903.31.14 23:09

03.31.14 23:0903.31.14 23:0903.31.14 23:0903.31.14 23:0903.31.14 23:0903.31.14 23:0903.31.14 23:09

03.31.14 23:0903.31.14 23:0903.31.14 23:0903.31.14 23:0903.31.14 23:0903.31.14 23:0903.31.14 23:09

03.31.14 23:0903.31.14 23:0903.31.14 23:0903.31.14 23:09

Analysis Date

Limits

55-16570-13070-13067-12570-13069-13058-13858-14670-13058-12861-13365-12859-13857-14070-13060-14666-12847-14470-13070-13067-13570-13060-12870-13070-13070-13070-13070-1309-13466-13270-13058-14467-12963-13770-13070-13060-14164-13570-13070-13070-13054-14565-12970-13061-12768-12867-13164-13365-12870-13070-13070-130

LCSD %Rec

123108

99106109104

91118115105101

98108106102

99108

98102101101105109107107105102107106107108110109109107100105110107105109

99116106105104119112104105100116

LCSD Result

49.121.519.721.121.820.718.247.222.920.920.219.621.621.120.319.721.519.520.320.220.221.021.821.321.420.920.321.321.121.321.621.921.821.821.419.920.922.021.421.021.719.746.521.121.020.847.522.420.720.920.023.1

LCS %Rec

11310897

10511110411311011110310098

11010810011310910010198

10010699

10710910510510210710711111010411011110810511211110710899

110105103104113106102105102114

45.121.619.421.022.120.722.543.922.220.519.919.621.921.520.022.621.820.020.219.619.921.119.821.321.721.021.020.321.321.322.221.920.722.022.121.520.922.422.121.321.519.743.921.020.520.745.021.120.321.020.322.7

Spike Amount

40.020.020.020.020.020.020.040.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.040.020.020.020.040.020.020.020.020.020.0

MB Result

<20.0<0.500

<1.50<0.500<0.500

<1.00<5.00<5.00<2.00<2.50<1.50<2.50

<0.500<0.500<0.500

<4.00<0.500

<5.00<1.50<2.00<1.50

<0.500<2.00

<0.500<0.500

<1.50<1.50<1.50<2.00

<0.500<0.500<0.500<0.500<0.500<0.500

<1.00<0.500

<1.00<1.00

<0.500<2.00<5.00<5.00<2.50<3.00<2.00<5.00<5.00<2.00<1.00

<0.500<0.500

653270-1-BKSLCS Sample Id: 653270-1-BSDLCSD Sample Id:

ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L

UnitsLCS Result

of 112 Final 1.000

QC Summary 482073

TerranextWVBA



TetrachloroethyleneToluene1,2,3-Trichlorobenzene1,2,4-Trichlorobenzene1,1,1-Trichloroethane1,1,2-TrichloroethaneTrichloroetheneTrichlorofluoromethane1,2,3-Trichloropropane1,2,4-Trimethylbenzene1,3,5-Trimethylbenzeneo-Xylenem,p-XylenesVinyl AcetateVinyl Chloride

Parameter %RPD Flag

202027202020202220202020202225

RPDLimit

509500196130037

937532Seq Number:

03.31.14 23:09

03.31.14 23:0903.31.14 23:0903.31.14 23:0903.31.14 23:0903.31.14 23:0903.31.14 23:0903.31.14 23:09

03.31.14 23:0903.31.14 23:0903.31.14 23:0903.31.14 23:0903.31.14 23:0903.31.14 23:0903.31.14 23:09

Analysis Date

Limits

63-12770-13066-13169-12762-13370-13070-13045-15170-13070-13070-13070-13070-13052-14243-120

LCSD %Rec

110105100102107105105106108100102105105120

94

LCSD Result

21.920.920.020.421.421.020.921.221.620.020.420.941.823.918.7

LCS %Rec

1051049197

10710510397

1029999

105104116101

20.920.818.219.421.421.020.619.420.419.819.721.041.723.220.1

Spike Amount

20.020.020.020.020.020.020.020.020.020.020.020.040.020.020.0

MB Result

<0.500<2.00<5.00<5.00

<0.500<0.500<0.500

<2.00<1.00<2.00<1.50<1.00<2.00<5.00

<0.500


ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L

UnitsLCS Result

Dibromofluoromethane1,2-Dichloroethane-D4Toluene-D84-Bromofluorobenzene

Surrogate LCSD Flag

03.31.14 23:0903.31.14 23:0903.31.14 23:0903.31.14 23:09

Analysis Date

Limits

69-13366-13970-13070-135

LCSD %Rec

9810199103

LCS %Rec

100105101103

MB %Rec

9810310397

%%%%

UnitsLCSFlag

MBFlag

of 112 Final 1.000

QC Summary 482073

TerranextWVBA




Parameter %RPD Flag

28202024202025272120202022212024242620282020212023202020272020212421202024202020202220202022212720202020

RPDLimit

15022148211212012182312530112111212141133211131492227

937846Seq Number:

04.04.14 01:52

04.04.14 01:5204.04.14 01:5204.04.14 01:5204.04.14 01:5204.04.14 01:5204.04.14 01:5204.04.14 01:52

04.04.14 01:5204.04.14 01:5204.04.14 01:5204.04.14 01:5204.04.14 01:5204.04.14 01:5204.04.14 01:52

04.04.14 01:5204.04.14 01:5204.04.14 01:5204.04.14 01:5204.04.14 01:5204.04.14 01:52

04.04.14 01:5204.04.14 01:5204.04.14 01:5204.04.14 01:5204.04.14 01:5204.04.14 01:5204.04.14 01:52

04.04.14 01:5204.04.14 01:5204.04.14 01:5204.04.14 01:5204.04.14 01:5204.04.14 01:52

04.04.14 01:5204.04.14 01:5204.04.14 01:5204.04.14 01:5204.04.14 01:5204.04.14 01:5204.04.14 01:52

04.04.14 01:5204.04.14 01:5204.04.14 01:5204.04.14 01:5204.04.14 01:5204.04.14 01:5204.04.14 01:52

04.04.14 01:5204.04.14 01:5204.04.14 01:5204.04.14 01:52

Analysis Date

Limits

55-16570-13070-13067-12570-13069-13058-13858-14670-13058-12861-13365-12859-13857-14070-13060-14666-12847-14470-13070-13067-13570-13060-12870-13070-13070-13070-13070-1309-13466-13270-13058-14467-12963-13770-13070-13060-14164-13570-13070-13070-13054-14565-12970-13061-12768-12867-13164-13365-12870-13070-13070-130

LCSD %Rec

1019498969797

1089995

10096

10195

1029595

100969895

1009694949499

101101

9495969599979696989796

100989897

101999299

10196

104103102

LCSD Result

40.218.819.619.219.319.421.539.618.919.919.220.119.020.319.018.919.919.219.519.020.019.218.718.818.819.820.220.218.818.919.119.019.819.419.119.219.519.419.120.019.619.538.620.219.818.339.420.119.120.820.620.3

LCS %Rec

8794

100989693

10097949998

10294

1029496

100899698

10295899294

1001009995959597

10096979299979398979996

1009791949297

10210195

34.718.820.019.519.218.619.938.818.719.819.520.318.720.418.819.220.017.819.219.520.318.917.818.318.819.919.919.819.019.019.019.319.919.119.318.419.719.318.619.519.319.738.320.019.318.137.718.419.420.420.218.9

Spike Amount

40.020.020.020.020.020.020.040.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.040.020.020.020.040.020.020.020.020.020.0

MB Result

<20.0<0.500

<1.50<0.500<0.500

<1.00<5.00<5.00<2.00<2.50<1.50<2.50

<0.500<0.500<0.500

<4.00<0.500

<5.00<1.50<2.00<1.50

<0.500<2.00

<0.500<0.500

<1.50<1.50<1.50<2.00

<0.500<0.500<0.500<0.500<0.500<0.500

<1.00<0.500

<1.00<1.00

<0.500<2.00<5.00<5.00<2.50<3.00<2.00<5.00<5.00<2.00<1.00

<0.500<0.500



UnitsLCS Result

of 112 Final 1.000

QC Summary 482073

TerranextWVBA




Parameter %RPD Flag

202027202020202220202020202225

RPDLimit

416323204113311

937846Seq Number:

04.04.14 01:52

04.04.14 01:5204.04.14 01:5204.04.14 01:5204.04.14 01:5204.04.14 01:5204.04.14 01:5204.04.14 01:52

04.04.14 01:5204.04.14 01:5204.04.14 01:5204.04.14 01:5204.04.14 01:5204.04.14 01:5204.04.14 01:52

Analysis Date

Limits

63-12770-13066-13169-12762-13370-13070-13045-15170-13070-13070-13070-13070-13052-14243-120

LCSD %Rec

9598

101100

95101

97101

97100100105105

9591

LCSD Result

19.019.520.220.018.920.119.420.219.420.019.920.942.119.018.2

LCS %Rec

92979697939899

10294

1011011011029491

18.319.419.119.418.619.519.820.318.720.220.120.240.718.818.1

Spike Amount

20.020.020.020.020.020.020.020.020.020.020.020.040.020.020.0

MB Result

<0.500<2.00<5.00<5.00

<0.500<0.500<0.500

<2.00<1.00<2.00<1.50<1.00<2.00<5.00

<0.500



UnitsLCS Result


Surrogate LCSD Flag

04.04.14 01:5204.04.14 01:5204.04.14 01:5204.04.14 01:52

Analysis Date

Limits

69-13366-13970-13070-135

LCSD %Rec

979897100

LCS %Rec

96999998

MB %Rec

97979892

%%%%

UnitsLCSFlag

MBFlag

of 112 Final 1.000

QC Summary 482073

TerranextWVBA




Parameter %RPD Flag

20202022202022222020202028202020222220202020222020202020332020202020202020202020202033202020202620372020

RPDLimit

33200042131203032621011111420100211112011120101071102

937532Seq Number:

04.01.14 03:27

04.01.14 03:2704.01.14 03:2704.01.14 03:2704.01.14 03:2704.01.14 03:2704.01.14 03:2704.01.14 03:27

04.01.14 03:2704.01.14 03:2704.01.14 03:2704.01.14 03:2704.01.14 03:2704.01.14 03:2704.01.14 03:27

04.01.14 03:2704.01.14 03:2704.01.14 03:2704.01.14 03:2704.01.14 03:2704.01.14 03:27

04.01.14 03:2704.01.14 03:2704.01.14 03:2704.01.14 03:2704.01.14 03:2704.01.14 03:2704.01.14 03:27

04.01.14 03:2704.01.14 03:2704.01.14 03:2704.01.14 03:2704.01.14 03:2704.01.14 03:27

04.01.14 03:2704.01.14 03:2704.01.14 03:2704.01.14 03:2704.01.14 03:2704.01.14 03:2704.01.14 03:27

04.01.14 03:2704.01.14 03:2704.01.14 03:2704.01.14 03:2704.01.14 03:2704.01.14 03:2704.01.14 03:27

04.01.14 03:2704.01.14 03:2704.01.14 03:2704.01.14 03:27

Analysis Date

Limits

35-16069-13070-13063-11970-13057-12153-14146-13665-12765-12770-13070-13058-14560-15270-13059-15365-12347-14870-13070-13070-13070-13050-11767-11766-11570-13070-13070-13016-15166-12964-12665-15266-12666-13570-13067-11562-14572-14067-12270-13070-13068-14352-12270-13059-12166-12753-12554-12969-12649-14270-13064-122

MSD %Rec

116110100107113106104115114106102100108111102105108

98105102101108109107111107106105112105110110109110108108106113110107109

97116106103108118108106

98103118

MSD Result

46.221.920.021.322.621.120.746.022.821.120.320.021.522.120.421.022.619.521.020.420.121.521.821.422.121.421.220.922.421.822.023.024.521.921.621.621.122.522.021.421.819.446.521.120.621.547.021.521.119.520.523.6

MS %Rec

11910799

10711410510011711310310199

10710710310811010410310110110710810811010610210711210711110910710811011010511011110911110911610710310711811610597

103116

47.721.319.721.422.721.019.946.722.620.520.119.721.421.420.521.623.120.720.520.220.121.321.521.621.921.220.321.322.422.122.122.924.121.621.921.920.922.022.121.722.121.846.421.320.521.347.223.120.919.320.623.1

Spike Amount

40.020.020.020.020.020.020.040.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.040.020.020.020.040.020.020.020.020.020.0

Parent Result

<20.0<0.500

<1.50<0.500<0.500

<1.00<5.00<5.00<2.00<2.50<1.50<2.50

<0.500<0.500<0.500

<4.001.04

<5.00<1.50<2.00<1.50

<0.500<2.00

<0.500<0.500

<1.50<1.50<1.50<2.000.730

<0.5001.072.66

<0.500<0.500

<1.00<0.500

<1.00<1.00

<0.500<2.00<5.00<5.00<2.50<3.00<2.00<5.00<5.00<2.00<1.00

<0.500<0.500



UnitsMS Result

of 112 Final 1.000

QC Summary 482073

TerranextWVBA




Parameter %RPD Flag

202024202020202020222020202321

RPDLimit

1062002114202137

937532Seq Number:

04.01.14 03:27

04.01.14 03:2704.01.14 03:2704.01.14 03:2704.01.14 03:2704.01.14 03:2704.01.14 03:2704.01.14 03:27

04.01.14 03:2704.01.14 03:2704.01.14 03:2704.01.14 03:2704.01.14 03:2704.01.14 03:2704.01.14 03:27

Analysis Date

Limits

69-13070-13061-12664-12368-13665-11270-13053-17158-11667-12870-13070-13070-13043-13346-132

MSD %Rec

105106

95102109105109107110102103107106101

97

MSD Result

27.221.218.920.421.821.027.721.322.020.320.521.442.220.219.3

MS %Rec

10610610110510910610696

10699

103105104104104

27.421.220.120.921.821.127.119.121.219.820.521.041.720.820.8

Spike Amount

20.020.020.020.020.020.020.020.020.020.020.020.040.020.020.0

Parent Result

6.26<2.00<5.00<5.00

<0.500<0.500

5.99<2.00<1.00<2.00<1.50<1.00<2.00<5.00

<0.500



UnitsMS Result


Surrogate MSD Flag

04.01.14 03:2704.01.14 03:2704.01.14 03:2704.01.14 03:27

Analysis Date

Limits

69-13366-13970-13070-135

MSD %Rec

98103100102

MS %Rec

98103101100

%%%%

UnitsMSFlag

of 112 Final 1.000

QC Summary 482073

TerranextWVBA




Parameter %RPD

R5

Flag

20202022202022222020202028202020222220202020222020202020332020202020202020202020202033202020202620372020

RPDLimit

33215241110521120252512225310151313213321141814043781003

937846Seq Number:

04.04.14 03:35

04.04.14 03:3504.04.14 03:3504.04.14 03:3504.04.14 03:3504.04.14 03:3504.04.14 03:3504.04.14 03:35

04.04.14 03:3504.04.14 03:3504.04.14 03:3504.04.14 03:3504.04.14 03:3504.04.14 03:3504.04.14 03:35

04.04.14 03:3504.04.14 03:3504.04.14 03:3504.04.14 03:3504.04.14 03:3504.04.14 03:35

04.04.14 03:3504.04.14 03:3504.04.14 03:3504.04.14 03:3504.04.14 03:3504.04.14 03:3504.04.14 03:35

04.04.14 03:3504.04.14 03:3504.04.14 03:3504.04.14 03:3504.04.14 03:3504.04.14 03:35

04.04.14 03:3504.04.14 03:3504.04.14 03:3504.04.14 03:3504.04.14 03:3504.04.14 03:3504.04.14 03:35

04.04.14 03:3504.04.14 03:3504.04.14 03:3504.04.14 03:3504.04.14 03:3504.04.14 03:3504.04.14 03:35

04.04.14 03:3504.04.14 03:3504.04.14 03:3504.04.14 03:35

Analysis Date

Limits

35-16069-13070-13063-11970-13057-12153-14146-13665-12765-12770-13070-13058-14560-15270-13059-15365-12347-14870-13070-13070-13070-13050-11767-11766-11570-13070-13070-13016-15166-12964-12665-15266-12666-13570-13067-11562-14572-14067-12270-13070-13068-14352-12270-13059-12166-12753-12554-12969-12649-14270-13064-122

MSD %Rec

11594

100101

9496

103107

989995

10094

1019796

1059898959897989795

101100104

96979697

102979597969594

1009995

103101101

93101107

9798

104103

MSD Result

45.918.819.920.218.719.220.642.619.519.819.019.918.820.219.319.221.019.519.518.919.619.419.519.318.920.220.020.819.219.419.119.420.419.319.019.319.218.918.720.019.718.941.320.220.118.640.321.319.319.520.720.6

MS %Rec

8396

101969592

1159693

10196

10092

1019591

1031039797

10095939496

1011029996949594

1009698949496959798

10390

101979194999898

103100

33.019.120.219.219.018.422.938.518.620.119.220.018.420.118.918.220.620.619.419.320.019.018.518.719.120.220.319.819.118.819.018.820.019.219.518.718.819.118.919.319.620.536.020.219.318.137.619.719.519.520.619.9

Spike Amount

40.020.020.020.020.020.020.040.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.020.040.020.020.020.040.020.020.020.020.020.0

Parent Result

<20.0<0.500

<1.50<0.500<0.500

<1.00<5.00<5.00<2.00<2.50<1.50<2.50

<0.500<0.500<0.500

<4.00<0.500

<5.00<1.50<2.00<1.50

<0.500<2.00

<0.500<0.500

<1.50<1.50<1.50<2.00

<0.500<0.500<0.500<0.500<0.500<0.500

<1.00<0.500

<1.00<1.00

<0.500<2.00<5.00<5.00<2.50<3.00<2.00<5.00<5.00<2.00<1.00

<0.500<0.500



UnitsMS Result

of 112 Final 1.000

QC Summary 482073

TerranextWVBA




Parameter %RPD

R5

Flag

202024202020202020222020202321

RPDLimit

13302302810011151

937846Seq Number:

04.04.14 03:35

04.04.14 03:3504.04.14 03:3504.04.14 03:3504.04.14 03:3504.04.14 03:3504.04.14 03:3504.04.14 03:35

04.04.14 03:3504.04.14 03:3504.04.14 03:3504.04.14 03:3504.04.14 03:3504.04.14 03:3504.04.14 03:35

Analysis Date

Limits

69-13070-13061-12664-12368-13665-11270-13053-17158-11667-12870-13070-13070-13043-13346-132

MSD %Rec

94100104100

94103

9798

104101

99104104

8796

MSD Result

22.219.920.720.018.820.619.419.620.720.119.820.841.517.419.2

MS %Rec

9397

10110093

100977494

1011001031038397

22.019.420.120.018.519.919.414.818.820.119.920.641.016.619.3

Spike Amount

20.020.020.020.020.020.020.020.020.020.020.020.040.020.020.0

Parent Result

3.38<2.00<5.00<5.00

<0.500<0.500<0.500

<2.00<1.00<2.00<1.50<1.00<2.00<5.00

<0.500



UnitsMS Result


Surrogate MSD Flag

04.04.14 03:3504.04.14 03:3504.04.14 03:3504.04.14 03:35

Analysis Date

Limits

69-13366-13970-13070-135

MSD %Rec

98989899

MS %Rec

97979698

%%%%

UnitsMSFlag

of 112 Final 1.000

of 112 Final 1.000

analytical report 482073 - azdeq.gov · · 2014-04-16analytical report 482073 for terranext...

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