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Analytical Chemistry is a peer-reviewed research journal that explores the latest concepts in analytical measurements and the best new ways to increase accuracy, selectivity, sensitivity, and reproducibility.

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Analytical ChemistryTable of ContentsVol. 78, No. 13: July 1, 2006

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EDITORIAL

Person to Person: Human Interaction and Scientific CreativityRoyce W. Murrayp 4237

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American Chemical Society: Analytical Chemistry Table of Contents

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American Chemical Society: Analytical Chemistry Table of Contents

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Analytical Currents: STED microscopy illuminates vesicle fate | Imaging of the oxidant peroxynitrite in living cells | Solid immersion lenses made from PDMS | Molecular sorting in microfluidic devices | DNA sequencing on a chip | Single-molecule binding assay in femtoliter arrays | Simple derivatization of glycopeptides for MALDI | Direct electrical detection of DNA synthesispp 4239 - 4242

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ACS Division of Analytical Chemistry teams up with PittconRajendrani Mukhopadhyayp 4243

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Research Profile: Decoding the chromosome core with top-down MSKaren R. Jonscherp 4244

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Research Profile: Multidimensional IMSBritt Ericksonp 4245

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BIO SPHERE

Detecting mucins in vivoLinda Sagep 4246

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LAB FAB

Microparticles of all shapes and chemistriesRajendrani Mukhopadhyayp 4247

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MATERIAL WORLD

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American Chemical Society: Analytical Chemistry Table of Contents

Vesicle making goes microfluidicRajendrani Mukhopadhyayp 4248

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FEATURES

Instrumental Analysis in the Undergraduate CurriculumAngela Fahey, Julian Tysonpp 4249 - 4254

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Devices to Drool ForRajendrani Mukhopadhyaypp 4255 - 4259

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Nanowire-Based BiosensorsFernando Patolsky, Gengfeng Zheng, Charles M. Lieberpp 4260 - 4269

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NEW PRODUCTS

New Productsp 4270

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ACCELERATED ARTICLES

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Quantitative Analysis of Modified Proteins and Their Positional Isomers by Tandem Mass Spectrometry: Human Histone H4James J. Pesavento, Craig A. Mizzen, and Neil L. Kelleherpp 4271 - 4280; (Accelerated Article) DOI: 10.1021/ac0600050

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ARTICLES

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American Chemical Society: Analytical Chemistry Table of Contents

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Probabilistic Quotient Normalization as Robust Method to Account for Dilution of Complex Biological Mixtures. Application in 1H NMR MetabonomicsFrank Dieterle, Alfred Ross, Götz Schlotterbeck, and Hans Sennpp 4281 - 4290; (Article) DOI: 10.1021/ac051632c

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Liver-Specific Functional Studies in a Microfluidic Array of Primary Mammalian HepatocytesBartholomew J. Kane, Michael J. Zinner, Martin L. Yarmush, and Mehmet Tonerpp 4291 - 4298; (Article) DOI: 10.1021/ac051856v

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Optimization of a Microfluidic Mixer for Studying Protein Folding KineticsDavid E. Hertzog, Benjamin Ivorra, Bijan Mohammadi, Olgica Bakajin, and Juan G. Santiagopp 4299 - 4306; (Article) DOI: 10.1021/ac051903j

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Impact of Analytical Bias in Metabonomic Studies of Human Blood Serum and PlasmaOrla Teahan, Simon Gamble, Elaine Holmes, Jonathan Waxman, Jeremy K. Nicholson, Charlotte Bevan, and Hector C. Keunpp 4307 - 4318; (Article) DOI: 10.1021/ac051972y

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Characterization of a Second-Generation Focal-Plane Camera Coupled to an Inductively Coupled Plasma Mattauch-Herzog Geometry Mass SpectrographGregory D. Schilling, Francisco J. Andrade, James H. Barnes, IV, Roger P. Sperline, M. Bonner Denton, Charles J. Barinaga, David W. Koppenaal, and Gary M. Hieftjepp 4319 - 4325; (Article) DOI: 10.1021/ac052026k

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ESI-MS Compatible Permanent Coating of Glass Surfaces Using Poly(ethylene glycol)-Terminated Alkoxysilanes for Capillary Zone Electrophoretic Protein SeparationsTrust T. Razunguzwa, Manoj Warrier, and Aaron T. Timpermanpp 4326 - 4333; (Article) DOI: 10.1021/ac052121t

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MET-IDEA: Data Extraction Tool for Mass Spectrometry-Based MetabolomicsCorey D. Broeckling, Indira R. Reddy, Anthony L. Duran, Xuechun Zhao, and Lloyd W. Sumnerpp 4334 - 4341; (Article) DOI: 10.1021/ac0521596

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Identification and Quantification of Neuropeptides in Brain Tissue by Capillary Liquid Chromatography Coupled Off-Line to MALDI-TOF and MALDI-TOF/TOF-MSHui Wei, Kerstin Nolkrantz, Mark C. Parkin, Claire N. Chisolm, James P. O'Callaghan, and Robert T. Kennedypp 4342 - 4351; (Article) DOI: 10.1021/ac052196x

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American Chemical Society: Analytical Chemistry Table of Contents

Ozone in Ambient Air as a Source of Adventitious Oxidation. A Mass Spectrometric StudySteven L. Cohenpp 4352 - 4362; (Article) DOI: 10.1021/ac052263n

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Automated Analysis of Electrospray Ionization Fourier Transform Ion Cyclotron Resonance Mass Spectra of Natural Organic MatterElizabeth B. Kujawinski and Mark D. Behnpp 4363 - 4373; (Article) DOI: 10.1021/ac0600306

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Probabilistic Enrichment of Phosphopeptides by Their Mass DefectCan Bruce, Mark A. Shifman, Perry Miller, and Erol E. Gulcicekpp 4374 - 4382; (Article) DOI: 10.1021/ac060046w

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Characterization of ac Voltammetric Reaction-Diffusion Dynamics: From Patterns to Physical ParametersCostas A. Anastassiou, Nicolas Ducros, Kim H. Parker, and Danny O'Harepp 4383 - 4389; (Article) DOI: 10.1021/ac060122v

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American Chemical Society: Analytical Chemistry Table of Contents

Tubulin-Binding Drug Screening by MALDI-TOFMSPaul Hannewald, Benoît Maunit, and Jean-François Mullerpp 4390 - 4397; (Article) DOI: 10.1021/ac0601462

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Statistical Search Space Reduction and Two-Dimensional Data Display Approaches for UPLC-MS in Biomarker Discovery and Pathway AnalysisDerek J. Crockford, John C. Lindon, Olivier Cloarec, Robert S. Plumb, Stephen J. Bruce, Severine Zirah, Paul Rainville, Chris L. Stumpf, Kelly Johnson, Elaine Holmes, and Jeremy K. Nicholsonpp 4398 - 4408; (Article) DOI: 10.1021/ac060168o

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Self-Associating Block Copolymer Networks for Microchip Electrophoresis Provide Enhanced DNA Separation via "Inchworm" Chain DynamicsThomas N. Chiesl, Karl W. Putz, Meena Babu, Patrick Mathias, Kashan A. Shaikh, Edgar D. Goluch, Chang Liu, and Annelise E. Barronpp 4409 - 4415; (Article) DOI: 10.1021/ac060193u

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Improving the Instrumental Resolution of Sensors Based on Localized Surface Plasmon ResonanceAndreas B. Dahlin, Jonas O. Tegenfeldt, and Fredrik Höökpp 4416 - 4423; (Article) DOI: 10.1021/ac0601967

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American Chemical Society: Analytical Chemistry Table of Contents

Studies on Stress-Induced Changes at the Subcellular Level by Raman Microspectroscopic MappingChristoph Krafft, Thomas Knetschke, Richard H. W. Funk, and Reiner Salzerpp 4424 - 4429; (Article) DOI: 10.1021/ac060205b

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Targeted Profiling: Quantitative Analysis of 1H NMR Metabolomics DataAalim M. Weljie, Jack Newton, Pascal Mercier, Erin Carlson, and Carolyn. M. Slupskypp 4430 - 4442; (Article) DOI: 10.1021/ac060209g

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Correlation between Protein Binding Strength on Immobilized Metal Affinity Chromatography and the Histidine-Related Protein Surface StructureLakshmi P. Pathange, David R. Bevan, Timothy J. Larson, and Chenming Zhangpp 4443 - 4449; (Article) DOI: 10.1021/ac060217x

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Magnetically-Assisted Transport Evanescent Field FluoroimmunoassayAmber D. Wellman and Michael J. Sepaniakpp 4450 - 4456; (Article) DOI: 10.1021/ac060330n

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American Chemical Society: Analytical Chemistry Table of Contents

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Achieving Uniform Mixing in a Microfluidic Device: Hydrodynamic Focusing Prior to MixingHye Yoon Park, Xiangyun Qiu, Elizabeth Rhoades, Jonas Korlach, Lisa W. Kwok, Warren R. Zipfel, Watt W. Webb, and Lois Pollackpp 4465 - 4473; (Article) DOI: 10.1021/ac060572n

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Hadamard Transform Ion Mobility SpectrometryAndrew W. Szumlas, Steven J. Ray, and Gary M. Hieftjepp 4474 - 4481; (Article) DOI: 10.1021/ac051743b

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Enzyme System for Improving the Detection Limit in PyrosequencingGuohua Zhou, Tomoharu Kajiyama, Mari Gotou, Akihiko Kishimoto, Shigeya Suzuki, and Hideki Kambarapp 4482 - 4489; (Article) DOI: 10.1021/ac051927q

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Combined GC/MS Analytical Procedure for the Characterization of Glycerolipid, Waxy, Resinous, and Proteinaceous Materials in a Unique Paint MicrosampleAlessia Andreotti, Ilaria Bonaduce, Maria Perla Colombini, Gwénaëlle Gautier, Francesca Modugno, and Erika Ribechinipp 4490 - 4500; (Article) DOI: 10.1021/ac0519615

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Isolation and Characterization of a Thermally Stable Recombinant Anti-Caffeine Heavy-Chain Antibody FragmentRuth C.Ladenson, Dan L. Crimmins, Yvonne Landt, and Jack H. Ladensonpp 4501 - 4508; (Article) DOI: 10.1021/ac058044j

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Analysis of the Gas Phase of Cigarette Smoke by Gas Chromatography Coupled with UV-Diode Array DetectionDimitris G. Hatzinikolaou, Verner Lagesson, Anastasia J. Stavridou, Aristea E. Pouli, Ludmila Lagesson-Andrasko, and John C. Stavridespp 4509 - 4516; (Article) DOI: 10.1021/ac052004y

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Isothermal Calorimetry as a Tool To Investigate Slow Conformational Changes in Proteins and PeptidesJörg Fanghänel, Stephan Wawra, Christian Lücke, Dirk Wildemann, and Gunter Fischerpp 4517 - 4523; (Article) DOI: 10.1021/ac052040x

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American Chemical Society: Analytical Chemistry Table of Contents

Binding of Small Mono- and Oligomeric Integrin Ligands to Membrane-Embedded Integrins Monitored by Surface Plasmon-Enhanced Fluorescence SpectroscopyDaniela Lössner, Horst Kessler, Georgette Thumshirn, Claudia Dahmen, Birgit Wiltschi, Motomu Tanaka, Wolfgang Knoll, Eva-Kathrin Sinner, and Ute Reuningpp 4524 - 4533; (Article) DOI: 10.1021/ac052078+

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Characterization of Sulfated Oligosaccharides in Mucopolysaccharidosis Type IIIA by Electrospray Ionization Mass SpectrometryKerryn E. Mason, Peter J. Meikle, John J. Hopwood, and Maria Fullerpp 4534 - 4542; (Article) DOI: 10.1021/ac052083d

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Utility of Cleavable Isotope-Coded Affinity-Tagged Reagents for Quantification of Low-Copy Proteins Induced by Methylprednisolone Using Liquid Chromatography/Tandem Mass SpectrometryJun Qu, William J. Jusko, and Robert M. Straubingerpp 4543 - 4552; (Article) DOI: 10.1021/ac0521697

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Miniature Differential Mobility Spectrometry Using Atmospheric Pressure PhotoionizationErkinjon G. Nazarov, Raanan A. Miller, Gary A. Eiceman, and John A. Stonepp 4553 - 4563; (Article) DOI: 10.1021/ac052213i

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Metabolic Profiling of Glucuronides in Human Urine by LC-MS/MS and Partial Least-Squares Discriminant Analysis for Classification and Prediction of GenderUrsula Lutz, Roman W. Lutz, and Werner K. Lutzpp 4564 - 4571; (Article) DOI: 10.1021/ac0522299

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Infrared Multiphoton Dissociation in Quadrupole Time-of-Flight Mass Spectrometry: Top-Down Characterization of ProteinsSerguei A. Raspopov, Ayman El-Faramawy, Bruce A. Thomson, and K. W. Michael Siupp 4572 - 4577; (Article) DOI: 10.1021/ac052248i

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Modulation Ratio in Comprehensive Two-dimensional Gas ChromatographyWeeraya Khummueng, James Harynuk, and Philip J. Marriottpp 4578 - 4587; (Article) DOI: 10.1021/ac052270b

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Controlling Electroosmotic Flow in Poly(dimethylsiloxane) Separation Channels by Means of Prepolymer AdditivesYiqi Luo, Bo Huang, Hongkai Wu, and Richard N. Zarepp 4588 - 4592; (Article) DOI: 10.1021/ac052274g

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Establishment of Long-Term Preservation for Dimethyl Sulfide by the Solid-Phase Microextraction MethodAi Sakamoto, Takushi Niki, and Yutaka W. Watanabepp 4593 - 4597; (Article) DOI: 10.1021/ac052294i

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Automatic Selection of Optimal Savitzky-Golay SmoothingGabriel Vivó-Truyols and Peter J. Schoenmakerspp 4598 - 4608; (Article) DOI: 10.1021/ac0600196

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Thermally Assisted Collision-Induced Dissociation in a Quadrupole Ion Trap Mass SpectrometerAlawee H. Racine, Anne H. Payne, Philip M. Remes, and Gary L. Glishpp 4609 - 4614; (Article) DOI: 10.1021/ac060082v

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Validation of the Tracer-Pulse Method for Multicomponent Liquid Chromatography, A Classical Paradox RevisitedRobert Arnell and Torgny Fornstedtpp 4615 - 4623; (Article) DOI: 10.1021/ac0601260

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American Chemical Society: Analytical Chemistry Table of Contents

LC-MS/MS Screen for Penitrem A and Roquefortine C in Serum and Urine SamplesElizabeth R. Tor, Birgit Puschner, Michael S. Filigenzi, Asheesh K. Tiwary, and Robert H. Poppengapp 4624 - 4629; (Article) DOI: 10.1021/ac0601617

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Use of Elemental Analysis To Determine Comparative Performance of Established DNA Quantification MethodsClaire A. English, Sheila Merson, and Jacquie T. Keerpp 4630 - 4633; (Article) DOI: 10.1021/ac060174k

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Chemical Characterization of Diaspirin Cross-Linked Hemoglobin Polymerized with Poly(ethylene glycol)Paul W. Buehler, Robert A. Boykins, Scott Norris, and Abdu I. Alayashpp 4634 - 4641; (Article) DOI: 10.1021/ac060188q

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Adsorption Mechanisms and Effect of Temperature in Reversed-Phase Liquid Chromatography. Meaning of the Classical Van't Hoff Plot in ChromatographyFabrice Gritti and Georges Guiochonpp 4642 - 4653; (Article) DOI: 10.1021/ac0602017

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American Chemical Society: Analytical Chemistry Table of Contents

Fabrication of Conductive Membrane in a Polymeric Electric Field Gradient Focusing MicrodeviceJikun Liu, Xuefei Sun, Paul B. Farnsworth, and Milton L. Leepp 4654 - 4662; (Article) DOI: 10.1021/ac060204j

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GC/Multiple Collector-ICPMS Method for Chlorine Stable Isotope Analysis of Chlorinated Aliphatic HydrocarbonsMarc R. M. D. Van Acker, Anat Shahar, Edward D. Young, and Max L. Colemanpp 4663 - 4667; (Article) DOI: 10.1021/ac0602120

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Specific Affinity Extraction Method for Small Molecule-Binding ProteinsNariyasu Mano, Koichi Sato, and Junichi Gotopp 4668 - 4675; (Article) DOI: 10.1021/ac060213s

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Ozone Monitoring Based on a Biosensor Concept Utilizing a Reagentless Alcohol Oxidase ElectrodeDimitrios V. Stergiou, Mamas I. Prodromidis, Panayotis G. Veltsistas, and Nicholaos P. Evmiridispp 4676 - 4682; (Article) DOI: 10.1021/ac060230h

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Investigation of Sodium Sulfate Phase Transitions in a Porous Material Using Humidity- and Temperature-Controlled X-ray DiffractionKirsten Linnow, Anke Zeunert, and Michael Steigerpp 4683 - 4689; (Article) DOI: 10.1021/ac0603936

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Upconversion Fluorescence Resonance Energy Transfer in a Homogeneous Immunoassay for EstradiolKatri Kuningas, Telle Ukonaho, Henna Päkkilä, Terhi Rantanen, Jaana Rosenberg, Timo Lövgren, and Tero Soukkapp 4690 - 4696; (Article) DOI: 10.1021/ac0603983

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TECHNICAL NOTES

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Screening of Nerve Agent Degradation Products by MALDI-TOFMSYou-Ren Shu, An-Kai Su, Ju-Tsung Liu, and Cheng-Huang Linpp 4697 - 4701; (Technical Note) DOI: 10.1021/ac060007k

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Enhancement of Amino Acid Detection and Quantification by Electrospray Ionization Mass SpectrometryWen-Chu Yang, Hamid Mirzaei, Xiuping Liu, and Fred E. Regnierpp 4702 - 4708; (Technical Note) DOI: 10.1021/ac0600510

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American Chemical Society: Analytical Chemistry Table of Contents

Kinetic Monitoring of Electrophoretically Induced Solute Reaction by Axial Absorption Detection with Liquid-Core WaveguideAkira Wada, Makoto Harada, and Tetsuo Okadapp 4709 - 4712; (Technical Note) DOI: 10.1021/ac060175c

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Apparatus for Pressurized Planar Electrochromatography in a Completely Closed SystemTadeusz H. Dzido, Pawe W. P ocharz, and Piotr l zak

pp 4713 - 4721; (Technical Note) DOI: 10.1021/ac060044b

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CORRESPONDENCE

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Selective Photoelectrochemical Detection of DNA with High-Affinity Metallointercalator and Tin Oxide Nanoparticle ElectrodeShili Liu, Chao Li, Jing Cheng, and Yuxiang Zhoupp 4722 - 4726; (Small Correspondence) DOI: 10.1021/ac052022f

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Label-Free Electrochemical Detection of Protein Based on a Ferrocene-Bearing Cationic Polythiophene and AptamerFabien Le Floch, Hoang A. Ho, and Mario Leclercpp 4727 - 4731; (Small Correspondence) DOI: 10.1021/ac0521955

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Improving Nanoprobes Using Surface-Enhanced Raman Scattering from 30-nm Hollow Gold ParticlesAdam M. Schwartzberg, Tammy Y. Oshiro, Jin Z. Zhang, Thomas Huser, and Chad E. Talleypp 4732 - 4736; (Small Correspondence) DOI: 10.1021/ac060220g

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Direct On-Line Method To Monitor the Dynamic Structure of Noncovalent Titanium Complexes in Solution by Using Cold-Spray Ionization Time-of-Flight Mass SpectrometryJiuming He, Zeper Abliz, Ruiping Zhang, Yuxue Liang, and Kuiling Dingpp 4737 - 4740; (Small Correspondence) DOI: 10.1021/ac0603476

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American Chemical Society: Analytical Chemistry Table of Contents

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