o'donnell, david (deq) [mailto:odonnelld@michigan.gov ... · fw 413 hall street tables and...

Post on 15-Jul-2020

2 Views

Category:

Documents

0 Downloads

Preview:

Click to see full reader

TRANSCRIPT

FW 413 Hall Street Tables and Figures- - GR VI MDEQ DATA 2.htm[6/13/2016 12:08:53 PM]

From: O'Donnell, David (DEQ) [mailto:ODONNELLD@michigan.gov] Sent: Thursday, June 09, 2016 8:44 AMTo: Bandlow, David (DEQ) <BandlowD@michigan.gov>Cc: Hendershott, Abigail (DEQ) <HENDERSHOTTA@michigan.gov>; Nightingale, Elizabeth <nightingale.elizabeth@epa.gov>Subject: RE: 413 Hall Street, Tables and Figures

From: Bandlow, David (DEQ) Sent: Thursday, June 09, 2016 8:12 AMTo: O'Donnell, David (DEQ)Cc: Hendershott, Abigail (DEQ); Nightingale, Elizabeth; Schram, Tammy (DEQ)Subject: Fw: 413 Hall Street, Tables and FiguresImportance: High

David, Please see note below from Betsy. Can we provide her with all of the raw lab data that we have in the 413 Hall Street file today? Thanks, Dave

From: Nightingale, Elizabeth <nightingale.elizabeth@epa.gov>Sent: Wednesday, June 8, 2016 11:47:40 PMTo: Bandlow, David (DEQ)Subject: RE: 413 Hall Street, Tables and Figures Hi guys – I need to write an action memo ASAP to get more funding for this response, and I need to include your raw lab data in my record for the action memo. Could I possibly request the raw lab data associated with these figures ASAP? Thanks, Betsy Betsy NightingaleFederal On-Scene CoordinatorUnited States Environmental Protection Agency, Region 59311 Groh RoadGrosse Ile, MI 48138 office: 734-692-7665cell: 734-770-8402fax: 734-692-7677email: nightingale.elizabeth@epa.gov

Report spills to the National Response Center at:

FW 413 Hall Street Tables and Figures- - GR VI MDEQ DATA 2.htm[6/13/2016 12:08:53 PM]

-800-424-8802, or-www.nrc.uscg.mil.

From: Bandlow, David (DEQ) [mailto:BandlowD@michigan.gov] Sent: Tuesday, June 07, 2016 9:38 AMTo: Nightingale, Elizabeth <nightingale.elizabeth@epa.gov>Cc: Britchie@manniksmithgroup.comSubject: Fw: 413 Hall Street, Tables and Figures

From: Trevor Painter (Global) <tpainter@globaleei.com>Sent: Friday, May 27, 2016 1:11:07 PMTo: Bandlow, David (DEQ)Cc: Hendershott, Abigail (DEQ); Jill Auger; Andy GirardSubject: 413 Hall Street, Tables and Figures Dear Mr. Bandlow,

Global has compiled the requested tables and figures for the 413 Hall Street Site in Grand Rapids, MI. If you have any questions, don't not hesitate to contact me. Sincerely,

Trevor Painter

Trevor D. Painter

Staff Engineer

Global Environmental Engineering

O: (231) 264-3000; 302

M: (231) 631-3472

363 W. South Airport Road

Traverse City, MI 49686

www.globaleei.com

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

MDEQ-RRD-GRAND RAPIDS

RE: HALL STREET

Grand Rapids, MI 49503-2341

350 Ottawa Ave. NW, Unit 10

Abigail Hendershott

I certify that the analyses performed by the MDEQ Environmental Laboratory were conducted by methods

approved by the U.S. Environmental Protection Agency and other appropriate regulatory agencies .

Sincerely,

14 January 2016 Work Order: 1601031

Price: $690.00

George Krisztian

Laboratory Director

Lab Work Order # 1601031

Page 1 of 9Page 1 of 10

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

Project:

Project Manager:

Reported:

MDEQ-RRD-GRAND RAPIDS

350 Ottawa Ave. NW, Unit 10

Abigail Hendershott

HALL STREET

Grand Rapids MI, 49503-2341

Site Code: 4100112101/14/2016

Sample ID Laboratory ID Date SampledMatrix Date Received

Analytical Report for Samples

Qualifier

1601031-01 Water 01/11/2016GP 11 @25' 01/11/2016

1601031-02 Water 01/11/2016GP 11 @30' 01/11/2016

1601031-03 Water 01/11/2016GP 11 @35' 01/11/2016

Notes and Definitions

X Methods 8260 & 624 are used to analyze volatile organics that have boiling points below 200 ºC. 2-Methylnaphthalene & naphthalene

have boiling points above 200 ºC and are better suited to analysis by methods 8270 & 625 as semivolatile organics.

A03 Result(s) and reporting limit(s) are estimated due to low matrix spike recovery.

Reporting LimitRL

Indicates compound analyzed for but not detectedND

Not ApplicableNA

Lab Work Order # 1601031

Page 2 of 9Page 2 of 10

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1601031-01

RLCAS #

Client ID: GP 11 @25'

QC Batch

Organics-Volatiles

1.0 ug/L 1 82601,1,1,2-Tetrachloroethane630-20-6 01/11/16ND B6A1106

1.0 ug/L 1 82601,1,1-Trichloroethane71-55-6 01/11/16ND B6A1106

1.0 ug/L 1 82601,1,2,2-Tetrachloroethane79-34-5 01/11/16ND B6A1106

1.0 ug/L 1 82601,1,2-Trichloroethane79-00-5 01/11/16ND B6A1106

1.0 ug/L 1 82601,1-Dichloroethane75-34-3 01/11/16ND B6A1106

1.0 ug/L 1 82601,1-Dichloroethylene75-35-4 01/11/16ND B6A1106

5.0 ug/L 1 82601,2,3-Trichlorobenzene87-61-6 01/11/16ND B6A1106

1.0 ug/L 1 82601,2,3-Trichloropropane96-18-4 01/11/16ND B6A1106

1.0 ug/L 1 82601,2,3-Trimethylbenzene526-73-8 01/11/16ND B6A1106

5.0 ug/L 1 82601,2,4-Trichlorobenzene120-82-1 01/11/16ND B6A1106

1.0 ug/L 1 82601,2,4-Trimethylbenzene95-63-6 01/11/16ND B6A1106

5.0 ug/L 1 82601,2-Dibromo-3-chloropropane96-12-8 01/11/16ND B6A1106

1.0 ug/L 1 82601,2-Dibromoethane106-93-4 01/11/16ND B6A1106

1.0 ug/L 1 82601,2-Dichlorobenzene95-50-1 01/11/16ND B6A1106

1.0 ug/L 1 82601,2-Dichloroethane107-06-2 01/11/16ND B6A1106

1.0 ug/L 1 82601,2-Dichloropropane78-87-5 01/11/16ND B6A1106

1.0 ug/L 1 82601,3,5-Trimethylbenzene108-67-8 01/11/16ND B6A1106

1.0 ug/L 1 82601,3-Dichlorobenzene541-73-1 01/11/16ND B6A1106

1.0 ug/L 1 82601,4-Dichlorobenzene106-46-7 01/11/16ND B6A1106

5.0 ug/L 1 82602-Butanone (MEK)78-93-3 01/11/16ND B6A1106

5.0 ug/L 1 82602-Hexanone591-78-6 01/11/16ND B6A1106

5.0 Xug/L 1 82602-Methylnaphthalene91-57-6 01/11/16ND B6A1106

20 A03ug/L 1 82602-Propanone (acetone)67-64-1 01/11/1625 B6A1106

5.0 ug/L 1 82604-Methyl-2-pentanone (MIBK)108-10-1 01/11/16ND B6A1106

5.0 ug/L 1 8260Acrylonitrile107-13-1 01/11/16ND B6A1106

1.0 ug/L 1 8260Benzene71-43-2 01/11/16ND B6A1106

1.0 ug/L 1 8260Bromobenzene108-86-1 01/11/16ND B6A1106

1.0 ug/L 1 8260Bromochloromethane74-97-5 01/11/16ND B6A1106

1.0 ug/L 1 8260Bromodichloromethane75-27-4 01/11/16ND B6A1106

1.0 ug/L 1 8260Bromoform75-25-2 01/11/16ND B6A1106

5.0 ug/L 1 8260Bromomethane74-83-9 01/11/16ND B6A1106

1.0 ug/L 1 8260Carbon disulfide75-15-0 01/11/16ND B6A1106

1.0 ug/L 1 8260Carbon tetrachloride56-23-5 01/11/16ND B6A1106

1.0 ug/L 1 8260Chlorobenzene108-90-7 01/11/16ND B6A1106

5.0 ug/L 1 8260Chloroethane75-00-3 01/11/16ND B6A1106

1.0 ug/L 1 8260Chloroform67-66-3 01/11/161.4 B6A1106

5.0 ug/L 1 8260Chloromethane74-87-3 01/11/16ND B6A1106

1.0 ug/L 1 8260cis-1,2-Dichloroethylene156-59-2 01/11/16ND B6A1106

1.0 ug/L 1 8260cis-1,3-Dichloropropylene10061-01-5 01/11/16ND B6A1106

5.0 ug/L 1 8260Cyclohexane110-82-7 01/11/16ND B6A1106

1.0 ug/L 1 8260Dibromochloromethane124-48-1 01/11/16ND B6A1106

Lab Work Order # 1601031

Page 3 of 9Page 3 of 10

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1601031-01

RLCAS #

Client ID: GP 11 @25'

QC Batch

Organics-Volatiles

1.0 ug/L 1 8260Dibromomethane74-95-3 01/11/16ND B6A1106

5.0 ug/L 1 8260Dichlorodifluoromethane75-71-8 01/11/16ND B6A1106

5.0 ug/L 1 8260Diethyl ether60-29-7 01/11/16ND B6A1106

5.0 ug/L 1 8260Diisopropyl Ether108-20-3 01/11/16ND B6A1106

1.0 ug/L 1 8260Ethylbenzene100-41-4 01/11/16ND B6A1106

5.0 ug/L 1 8260Ethyltertiarybutylether637-92-3 01/11/16ND B6A1106

5.0 ug/L 1 8260Hexachloroethane67-72-1 01/11/16ND B6A1106

1.0 ug/L 1 8260Isopropylbenzene98-82-8 01/11/16ND B6A1106

2.0 ug/L 1 8260m & p - Xylene1330-20-7 01/11/16ND B6A1106

1.0 ug/L 1 8260Methyl iodide74-88-4 01/11/16ND B6A1106

5.0 ug/L 1 8260Methylene chloride75-09-2 01/11/16ND B6A1106

1.0 ug/L 1 8260Methyltertiarybutylether1634-04-4 01/11/16ND B6A1106

5.0 Xug/L 1 8260Naphthalene91-20-3 01/11/16ND B6A1106

1.0 ug/L 1 8260n-Butylbenzene104-51-8 01/11/16ND B6A1106

1.0 ug/L 1 8260n-Propylbenzene103-65-1 01/11/16ND B6A1106

1.0 ug/L 1 8260o-Xylene95-47-6 01/11/16ND B6A1106

1.0 ug/L 1 8260p-Isopropyl toluene99-87-6 01/11/16ND B6A1106

1.0 ug/L 1 8260sec-Butylbenzene135-98-8 01/11/16ND B6A1106

1.0 ug/L 1 8260Styrene100-42-5 01/11/16ND B6A1106

1.0 ug/L 1 8260tert-Butylbenzene98-06-6 01/11/16ND B6A1106

50 ug/L 1 8260tertiary Butyl Alcohol75-65-0 01/11/16ND B6A1106

5.0 ug/L 1 8260tertiaryAmylmethylether994-05-8 01/11/16ND B6A1106

1.0 ug/L 1 8260Tetrachloroethylene127-18-4 01/11/16ND B6A1106

5.0 ug/L 1 8260Tetrahydrofuran109-99-9 01/11/16ND B6A1106

1.0 ug/L 1 8260Toluene108-88-3 01/11/16ND B6A1106

1.0 ug/L 1 8260trans-1,2-Dichloroethylene156-60-5 01/11/16ND B6A1106

1.0 ug/L 1 8260trans-1,3-Dichloropropylene10061-02-6 01/11/16ND B6A1106

5.0 ug/L 1 8260trans-1,4-Dichloro-2-butene110-57-6 01/11/16ND B6A1106

1.0 ug/L 1 8260Trichloroethylene79-01-6 01/11/16ND B6A1106

1.0 ug/L 1 8260Trichlorofluoromethane75-69-4 01/11/16ND B6A1106

1.0 ug/L 1 8260Vinyl chloride75-01-4 01/11/16ND B6A1106

85-115101 %Surrogate: Bromofluorobenzene 826001/11/16 B6A1106

82.7-115101 %Surrogate: Dibromofluoromethane 826001/11/16 B6A1106

85-11599.9 %Surrogate: Toluene-d8 826001/11/16 B6A1106

Lab Work Order # 1601031

Page 4 of 9Page 4 of 10

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1601031-02

RLCAS #

Client ID: GP 11 @30'

QC Batch

Organics-Volatiles

1.0 ug/L 1 82601,1,1,2-Tetrachloroethane630-20-6 01/11/16ND B6A1106

1.0 ug/L 1 82601,1,1-Trichloroethane71-55-6 01/11/16ND B6A1106

1.0 ug/L 1 82601,1,2,2-Tetrachloroethane79-34-5 01/11/16ND B6A1106

1.0 ug/L 1 82601,1,2-Trichloroethane79-00-5 01/11/16ND B6A1106

1.0 ug/L 1 82601,1-Dichloroethane75-34-3 01/11/16ND B6A1106

1.0 ug/L 1 82601,1-Dichloroethylene75-35-4 01/11/16ND B6A1106

5.0 ug/L 1 82601,2,3-Trichlorobenzene87-61-6 01/11/16ND B6A1106

1.0 ug/L 1 82601,2,3-Trichloropropane96-18-4 01/11/16ND B6A1106

1.0 ug/L 1 82601,2,3-Trimethylbenzene526-73-8 01/11/16ND B6A1106

5.0 ug/L 1 82601,2,4-Trichlorobenzene120-82-1 01/11/16ND B6A1106

1.0 ug/L 1 82601,2,4-Trimethylbenzene95-63-6 01/11/16ND B6A1106

5.0 ug/L 1 82601,2-Dibromo-3-chloropropane96-12-8 01/11/16ND B6A1106

1.0 ug/L 1 82601,2-Dibromoethane106-93-4 01/11/16ND B6A1106

1.0 ug/L 1 82601,2-Dichlorobenzene95-50-1 01/11/16ND B6A1106

1.0 ug/L 1 82601,2-Dichloroethane107-06-2 01/11/16ND B6A1106

1.0 ug/L 1 82601,2-Dichloropropane78-87-5 01/11/16ND B6A1106

1.0 ug/L 1 82601,3,5-Trimethylbenzene108-67-8 01/11/16ND B6A1106

1.0 ug/L 1 82601,3-Dichlorobenzene541-73-1 01/11/16ND B6A1106

1.0 ug/L 1 82601,4-Dichlorobenzene106-46-7 01/11/16ND B6A1106

5.0 ug/L 1 82602-Butanone (MEK)78-93-3 01/11/16ND B6A1106

5.0 ug/L 1 82602-Hexanone591-78-6 01/11/16ND B6A1106

5.0 Xug/L 1 82602-Methylnaphthalene91-57-6 01/11/16ND B6A1106

20 ug/L 1 82602-Propanone (acetone)67-64-1 01/11/16ND B6A1106

5.0 ug/L 1 82604-Methyl-2-pentanone (MIBK)108-10-1 01/11/16ND B6A1106

5.0 ug/L 1 8260Acrylonitrile107-13-1 01/11/16ND B6A1106

1.0 ug/L 1 8260Benzene71-43-2 01/11/16ND B6A1106

1.0 ug/L 1 8260Bromobenzene108-86-1 01/11/16ND B6A1106

1.0 ug/L 1 8260Bromochloromethane74-97-5 01/11/16ND B6A1106

1.0 ug/L 1 8260Bromodichloromethane75-27-4 01/11/16ND B6A1106

1.0 ug/L 1 8260Bromoform75-25-2 01/11/16ND B6A1106

5.0 ug/L 1 8260Bromomethane74-83-9 01/11/16ND B6A1106

1.0 ug/L 1 8260Carbon disulfide75-15-0 01/11/16ND B6A1106

1.0 ug/L 1 8260Carbon tetrachloride56-23-5 01/11/16ND B6A1106

1.0 ug/L 1 8260Chlorobenzene108-90-7 01/11/16ND B6A1106

5.0 ug/L 1 8260Chloroethane75-00-3 01/11/16ND B6A1106

1.0 ug/L 1 8260Chloroform67-66-3 01/11/161.6 B6A1106

5.0 ug/L 1 8260Chloromethane74-87-3 01/11/16ND B6A1106

1.0 ug/L 1 8260cis-1,2-Dichloroethylene156-59-2 01/11/16ND B6A1106

1.0 ug/L 1 8260cis-1,3-Dichloropropylene10061-01-5 01/11/16ND B6A1106

5.0 ug/L 1 8260Cyclohexane110-82-7 01/11/16ND B6A1106

1.0 ug/L 1 8260Dibromochloromethane124-48-1 01/11/16ND B6A1106

Lab Work Order # 1601031

Page 5 of 9Page 5 of 10

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1601031-02

RLCAS #

Client ID: GP 11 @30'

QC Batch

Organics-Volatiles

1.0 ug/L 1 8260Dibromomethane74-95-3 01/11/16ND B6A1106

5.0 ug/L 1 8260Dichlorodifluoromethane75-71-8 01/11/16ND B6A1106

5.0 ug/L 1 8260Diethyl ether60-29-7 01/11/16ND B6A1106

5.0 ug/L 1 8260Diisopropyl Ether108-20-3 01/11/16ND B6A1106

1.0 ug/L 1 8260Ethylbenzene100-41-4 01/11/16ND B6A1106

5.0 ug/L 1 8260Ethyltertiarybutylether637-92-3 01/11/16ND B6A1106

5.0 ug/L 1 8260Hexachloroethane67-72-1 01/11/16ND B6A1106

1.0 ug/L 1 8260Isopropylbenzene98-82-8 01/11/16ND B6A1106

2.0 ug/L 1 8260m & p - Xylene1330-20-7 01/11/16ND B6A1106

1.0 ug/L 1 8260Methyl iodide74-88-4 01/11/16ND B6A1106

5.0 ug/L 1 8260Methylene chloride75-09-2 01/11/16ND B6A1106

1.0 ug/L 1 8260Methyltertiarybutylether1634-04-4 01/11/16ND B6A1106

5.0 Xug/L 1 8260Naphthalene91-20-3 01/11/16ND B6A1106

1.0 ug/L 1 8260n-Butylbenzene104-51-8 01/11/16ND B6A1106

1.0 ug/L 1 8260n-Propylbenzene103-65-1 01/11/16ND B6A1106

1.0 ug/L 1 8260o-Xylene95-47-6 01/11/16ND B6A1106

1.0 ug/L 1 8260p-Isopropyl toluene99-87-6 01/11/16ND B6A1106

1.0 ug/L 1 8260sec-Butylbenzene135-98-8 01/11/16ND B6A1106

1.0 ug/L 1 8260Styrene100-42-5 01/11/16ND B6A1106

1.0 ug/L 1 8260tert-Butylbenzene98-06-6 01/11/16ND B6A1106

50 ug/L 1 8260tertiary Butyl Alcohol75-65-0 01/11/16ND B6A1106

5.0 ug/L 1 8260tertiaryAmylmethylether994-05-8 01/11/16ND B6A1106

1.0 ug/L 1 8260Tetrachloroethylene127-18-4 01/11/16ND B6A1106

5.0 ug/L 1 8260Tetrahydrofuran109-99-9 01/11/16ND B6A1106

1.0 ug/L 1 8260Toluene108-88-3 01/11/16ND B6A1106

1.0 ug/L 1 8260trans-1,2-Dichloroethylene156-60-5 01/11/16ND B6A1106

1.0 ug/L 1 8260trans-1,3-Dichloropropylene10061-02-6 01/11/16ND B6A1106

5.0 ug/L 1 8260trans-1,4-Dichloro-2-butene110-57-6 01/11/16ND B6A1106

1.0 ug/L 1 8260Trichloroethylene79-01-6 01/11/16ND B6A1106

1.0 ug/L 1 8260Trichlorofluoromethane75-69-4 01/11/16ND B6A1106

1.0 ug/L 1 8260Vinyl chloride75-01-4 01/11/16ND B6A1106

85-115103 %Surrogate: Bromofluorobenzene 826001/11/16 B6A1106

82.7-11599.9 %Surrogate: Dibromofluoromethane 826001/11/16 B6A1106

85-115101 %Surrogate: Toluene-d8 826001/11/16 B6A1106

Lab Work Order # 1601031

Page 6 of 9Page 6 of 10

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1601031-03

RLCAS #

Client ID: GP 11 @35'

QC Batch

Organics-Volatiles

1.0 ug/L 1 82601,1,1,2-Tetrachloroethane630-20-6 01/11/16ND B6A1106

1.0 ug/L 1 82601,1,1-Trichloroethane71-55-6 01/11/16ND B6A1106

1.0 ug/L 1 82601,1,2,2-Tetrachloroethane79-34-5 01/11/16ND B6A1106

1.0 ug/L 1 82601,1,2-Trichloroethane79-00-5 01/11/16ND B6A1106

1.0 ug/L 1 82601,1-Dichloroethane75-34-3 01/11/16ND B6A1106

1.0 ug/L 1 82601,1-Dichloroethylene75-35-4 01/11/16ND B6A1106

5.0 ug/L 1 82601,2,3-Trichlorobenzene87-61-6 01/11/16ND B6A1106

1.0 ug/L 1 82601,2,3-Trichloropropane96-18-4 01/11/16ND B6A1106

1.0 ug/L 1 82601,2,3-Trimethylbenzene526-73-8 01/11/16ND B6A1106

5.0 ug/L 1 82601,2,4-Trichlorobenzene120-82-1 01/11/16ND B6A1106

1.0 ug/L 1 82601,2,4-Trimethylbenzene95-63-6 01/11/16ND B6A1106

5.0 ug/L 1 82601,2-Dibromo-3-chloropropane96-12-8 01/11/16ND B6A1106

1.0 ug/L 1 82601,2-Dibromoethane106-93-4 01/11/16ND B6A1106

1.0 ug/L 1 82601,2-Dichlorobenzene95-50-1 01/11/16ND B6A1106

1.0 ug/L 1 82601,2-Dichloroethane107-06-2 01/11/16ND B6A1106

1.0 ug/L 1 82601,2-Dichloropropane78-87-5 01/11/16ND B6A1106

1.0 ug/L 1 82601,3,5-Trimethylbenzene108-67-8 01/11/16ND B6A1106

1.0 ug/L 1 82601,3-Dichlorobenzene541-73-1 01/11/16ND B6A1106

1.0 ug/L 1 82601,4-Dichlorobenzene106-46-7 01/11/16ND B6A1106

5.0 ug/L 1 82602-Butanone (MEK)78-93-3 01/11/16ND B6A1106

5.0 ug/L 1 82602-Hexanone591-78-6 01/11/16ND B6A1106

5.0 Xug/L 1 82602-Methylnaphthalene91-57-6 01/11/16ND B6A1106

20 ug/L 1 82602-Propanone (acetone)67-64-1 01/11/16ND B6A1106

5.0 ug/L 1 82604-Methyl-2-pentanone (MIBK)108-10-1 01/11/16ND B6A1106

5.0 ug/L 1 8260Acrylonitrile107-13-1 01/11/16ND B6A1106

1.0 ug/L 1 8260Benzene71-43-2 01/11/16ND B6A1106

1.0 ug/L 1 8260Bromobenzene108-86-1 01/11/16ND B6A1106

1.0 ug/L 1 8260Bromochloromethane74-97-5 01/11/16ND B6A1106

1.0 ug/L 1 8260Bromodichloromethane75-27-4 01/11/16ND B6A1106

1.0 ug/L 1 8260Bromoform75-25-2 01/11/16ND B6A1106

5.0 ug/L 1 8260Bromomethane74-83-9 01/11/16ND B6A1106

1.0 ug/L 1 8260Carbon disulfide75-15-0 01/11/16ND B6A1106

1.0 ug/L 1 8260Carbon tetrachloride56-23-5 01/11/16ND B6A1106

1.0 ug/L 1 8260Chlorobenzene108-90-7 01/11/16ND B6A1106

5.0 ug/L 1 8260Chloroethane75-00-3 01/11/16ND B6A1106

1.0 ug/L 1 8260Chloroform67-66-3 01/11/161.8 B6A1106

5.0 ug/L 1 8260Chloromethane74-87-3 01/11/16ND B6A1106

1.0 ug/L 1 8260cis-1,2-Dichloroethylene156-59-2 01/11/16ND B6A1106

1.0 ug/L 1 8260cis-1,3-Dichloropropylene10061-01-5 01/11/16ND B6A1106

5.0 ug/L 1 8260Cyclohexane110-82-7 01/11/16ND B6A1106

1.0 ug/L 1 8260Dibromochloromethane124-48-1 01/11/16ND B6A1106

Lab Work Order # 1601031

Page 7 of 9Page 7 of 10

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1601031-03

RLCAS #

Client ID: GP 11 @35'

QC Batch

Organics-Volatiles

1.0 ug/L 1 8260Dibromomethane74-95-3 01/11/16ND B6A1106

5.0 ug/L 1 8260Dichlorodifluoromethane75-71-8 01/11/16ND B6A1106

5.0 ug/L 1 8260Diethyl ether60-29-7 01/11/16ND B6A1106

5.0 ug/L 1 8260Diisopropyl Ether108-20-3 01/11/16ND B6A1106

1.0 ug/L 1 8260Ethylbenzene100-41-4 01/11/16ND B6A1106

5.0 ug/L 1 8260Ethyltertiarybutylether637-92-3 01/11/16ND B6A1106

5.0 ug/L 1 8260Hexachloroethane67-72-1 01/11/16ND B6A1106

1.0 ug/L 1 8260Isopropylbenzene98-82-8 01/11/16ND B6A1106

2.0 ug/L 1 8260m & p - Xylene1330-20-7 01/11/16ND B6A1106

1.0 ug/L 1 8260Methyl iodide74-88-4 01/11/16ND B6A1106

5.0 ug/L 1 8260Methylene chloride75-09-2 01/11/16ND B6A1106

1.0 ug/L 1 8260Methyltertiarybutylether1634-04-4 01/11/16ND B6A1106

5.0 Xug/L 1 8260Naphthalene91-20-3 01/11/16ND B6A1106

1.0 ug/L 1 8260n-Butylbenzene104-51-8 01/11/16ND B6A1106

1.0 ug/L 1 8260n-Propylbenzene103-65-1 01/11/16ND B6A1106

1.0 ug/L 1 8260o-Xylene95-47-6 01/11/16ND B6A1106

1.0 ug/L 1 8260p-Isopropyl toluene99-87-6 01/11/16ND B6A1106

1.0 ug/L 1 8260sec-Butylbenzene135-98-8 01/11/16ND B6A1106

1.0 ug/L 1 8260Styrene100-42-5 01/11/16ND B6A1106

1.0 ug/L 1 8260tert-Butylbenzene98-06-6 01/11/16ND B6A1106

50 ug/L 1 8260tertiary Butyl Alcohol75-65-0 01/11/16ND B6A1106

5.0 ug/L 1 8260tertiaryAmylmethylether994-05-8 01/11/16ND B6A1106

1.0 ug/L 1 8260Tetrachloroethylene127-18-4 01/11/16ND B6A1106

5.0 ug/L 1 8260Tetrahydrofuran109-99-9 01/11/16ND B6A1106

1.0 ug/L 1 8260Toluene108-88-3 01/11/16ND B6A1106

1.0 ug/L 1 8260trans-1,2-Dichloroethylene156-60-5 01/11/16ND B6A1106

1.0 ug/L 1 8260trans-1,3-Dichloropropylene10061-02-6 01/11/16ND B6A1106

5.0 ug/L 1 8260trans-1,4-Dichloro-2-butene110-57-6 01/11/16ND B6A1106

1.0 ug/L 1 8260Trichloroethylene79-01-6 01/11/16ND B6A1106

1.0 ug/L 1 8260Trichlorofluoromethane75-69-4 01/11/16ND B6A1106

1.0 ug/L 1 8260Vinyl chloride75-01-4 01/11/16ND B6A1106

85-115104 %Surrogate: Bromofluorobenzene 826001/11/16 B6A1106

82.7-115100 %Surrogate: Dibromofluoromethane 826001/11/16 B6A1106

85-115100 %Surrogate: Toluene-d8 826001/11/16 B6A1106

Lab Work Order # 1601031

Page 8 of 9Page 8 of 10

Page 9 of 10

Page 10 of 10

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

MDEQ-RRD-GRAND RAPIDS

RE: HALL STREET

Grand Rapids, MI 49503-2341

350 Ottawa Ave. NW, Unit 10

Abigail Hendershott

I certify that the analyses performed by the MDEQ Environmental Laboratory were conducted by methods

approved by the U.S. Environmental Protection Agency and other appropriate regulatory agencies .

Sincerely,

15 January 2016 Work Order: 1601052

Price: $920.00

George Krisztian

Laboratory Director

Lab Work Order # 1601052

Page 1 of 19Page 1 of 20

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

Project:

Project Manager:

Reported:

MDEQ-RRD-GRAND RAPIDS

350 Ottawa Ave. NW, Unit 10

Abigail Hendershott

HALL STREET

Grand Rapids MI, 49503-2341

Site Code: 4100112101/15/2016

Sample ID Laboratory ID Date SampledMatrix Date Received

Analytical Report for Samples

Qualifier

1601052-01 Water 01/13/2016GP13@25' 01/12/2016

1601052-02 Water 01/13/2016GP13@30' 01/12/2016

1601052-03 Water 01/13/2016GP13@35' 01/12/2016

1601052-04 Water 01/13/2016GP13@40' 01/12/2016

1601052-05 Water 01/13/2016GP14@25' 01/13/2016

1601052-06 Water 01/13/2016GP14@30' 01/13/2016

1601052-07 Water 01/13/2016GP14@35' 01/13/2016

1601052-08 Water 01/13/2016GP14@40' 01/13/2016

Notes and Definitions

X Methods 8260 & 624 are used to analyze volatile organics that have boiling points below 200 ºC. 2-Methylnaphthalene & naphthalene

have boiling points above 200 ºC and are better suited to analysis by methods 8270 & 625 as semivolatile organics.

A11 Result is estimated due to high initial verification standard criteria failure.

A09 Result is estimated due to high recovery of batch quality control.

A06 Result is estimated due to high continuing calibration standard criteria failure.

Reporting LimitRL

Indicates compound analyzed for but not detectedND

Not ApplicableNA

Lab Work Order # 1601052

Page 2 of 19Page 2 of 20

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1601052-01

RLCAS #

Client ID: GP13@25'

QC Batch

Organics-Volatiles

1.0 ug/L 1 82601,1,1,2-Tetrachloroethane630-20-6 01/13/16ND B6A1304

1.0 ug/L 1 82601,1,1-Trichloroethane71-55-6 01/13/16ND B6A1304

1.0 ug/L 1 82601,1,2,2-Tetrachloroethane79-34-5 01/13/16ND B6A1304

1.0 ug/L 1 82601,1,2-Trichloroethane79-00-5 01/13/16ND B6A1304

1.0 ug/L 1 82601,1-Dichloroethane75-34-3 01/13/16ND B6A1304

1.0 ug/L 1 82601,1-Dichloroethylene75-35-4 01/13/16ND B6A1304

5.0 ug/L 1 82601,2,3-Trichlorobenzene87-61-6 01/13/16ND B6A1304

1.0 ug/L 1 82601,2,3-Trichloropropane96-18-4 01/13/16ND B6A1304

1.0 ug/L 1 82601,2,3-Trimethylbenzene526-73-8 01/13/16ND B6A1304

5.0 ug/L 1 82601,2,4-Trichlorobenzene120-82-1 01/13/16ND B6A1304

1.0 ug/L 1 82601,2,4-Trimethylbenzene95-63-6 01/13/16ND B6A1304

5.0 ug/L 1 82601,2-Dibromo-3-chloropropane96-12-8 01/13/16ND B6A1304

1.0 ug/L 1 82601,2-Dibromoethane106-93-4 01/13/16ND B6A1304

1.0 ug/L 1 82601,2-Dichlorobenzene95-50-1 01/13/16ND B6A1304

1.0 ug/L 1 82601,2-Dichloroethane107-06-2 01/13/16ND B6A1304

1.0 ug/L 1 82601,2-Dichloropropane78-87-5 01/13/16ND B6A1304

1.0 ug/L 1 82601,3,5-Trimethylbenzene108-67-8 01/13/16ND B6A1304

1.0 ug/L 1 82601,3-Dichlorobenzene541-73-1 01/13/16ND B6A1304

1.0 ug/L 1 82601,4-Dichlorobenzene106-46-7 01/13/16ND B6A1304

5.0 ug/L 1 82602-Butanone (MEK)78-93-3 01/13/16ND B6A1304

5.0 ug/L 1 82602-Hexanone591-78-6 01/13/16ND B6A1304

5.0 Xug/L 1 82602-Methylnaphthalene91-57-6 01/13/16ND B6A1304

20 ug/L 1 82602-Propanone (acetone)67-64-1 01/13/16ND B6A1304

5.0 ug/L 1 82604-Methyl-2-pentanone (MIBK)108-10-1 01/13/16ND B6A1304

5.0 ug/L 1 8260Acrylonitrile107-13-1 01/13/16ND B6A1304

1.0 ug/L 1 8260Benzene71-43-2 01/13/16ND B6A1304

1.0 ug/L 1 8260Bromobenzene108-86-1 01/13/16ND B6A1304

1.0 ug/L 1 8260Bromochloromethane74-97-5 01/13/16ND B6A1304

1.0 ug/L 1 8260Bromodichloromethane75-27-4 01/13/16ND B6A1304

1.0 ug/L 1 8260Bromoform75-25-2 01/13/16ND B6A1304

5.0 ug/L 1 8260Bromomethane74-83-9 01/13/16ND B6A1304

1.0 ug/L 1 8260Carbon disulfide75-15-0 01/13/16ND B6A1304

1.0 ug/L 1 8260Carbon tetrachloride56-23-5 01/13/16ND B6A1304

1.0 ug/L 1 8260Chlorobenzene108-90-7 01/13/16ND B6A1304

5.0 ug/L 1 8260Chloroethane75-00-3 01/13/16ND B6A1304

1.0 ug/L 1 8260Chloroform67-66-3 01/13/161.0 B6A1304

5.0 ug/L 1 8260Chloromethane74-87-3 01/13/16ND B6A1304

1.0 ug/L 1 8260cis-1,2-Dichloroethylene156-59-2 01/13/1621 B6A1304

1.0 ug/L 1 8260cis-1,3-Dichloropropylene10061-01-5 01/13/16ND B6A1304

5.0 ug/L 1 8260Cyclohexane110-82-7 01/13/16ND B6A1304

1.0 ug/L 1 8260Dibromochloromethane124-48-1 01/13/16ND B6A1304

Lab Work Order # 1601052

Page 3 of 19Page 3 of 20

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1601052-01

RLCAS #

Client ID: GP13@25'

QC Batch

Organics-Volatiles

1.0 ug/L 1 8260Dibromomethane74-95-3 01/13/16ND B6A1304

5.0 ug/L 1 8260Dichlorodifluoromethane75-71-8 01/13/16ND B6A1304

5.0 ug/L 1 8260Diethyl ether60-29-7 01/13/16ND B6A1304

5.0 ug/L 1 8260Diisopropyl Ether108-20-3 01/13/16ND B6A1304

1.0 ug/L 1 8260Ethylbenzene100-41-4 01/13/16ND B6A1304

5.0 ug/L 1 8260Ethyltertiarybutylether637-92-3 01/13/16ND B6A1304

5.0 ug/L 1 8260Hexachloroethane67-72-1 01/13/16ND B6A1304

1.0 ug/L 1 8260Isopropylbenzene98-82-8 01/13/16ND B6A1304

2.0 ug/L 1 8260m & p - Xylene1330-20-7 01/13/16ND B6A1304

1.0 ug/L 1 8260Methyl iodide74-88-4 01/13/16ND B6A1304

5.0 ug/L 1 8260Methylene chloride75-09-2 01/13/16ND B6A1304

1.0 ug/L 1 8260Methyltertiarybutylether1634-04-4 01/13/16ND B6A1304

5.0 Xug/L 1 8260Naphthalene91-20-3 01/13/16ND B6A1304

1.0 ug/L 1 8260n-Butylbenzene104-51-8 01/13/16ND B6A1304

1.0 ug/L 1 8260n-Propylbenzene103-65-1 01/13/16ND B6A1304

1.0 ug/L 1 8260o-Xylene95-47-6 01/13/16ND B6A1304

1.0 ug/L 1 8260p-Isopropyl toluene99-87-6 01/13/16ND B6A1304

1.0 ug/L 1 8260sec-Butylbenzene135-98-8 01/13/16ND B6A1304

1.0 ug/L 1 8260Styrene100-42-5 01/13/16ND B6A1304

1.0 ug/L 1 8260tert-Butylbenzene98-06-6 01/13/16ND B6A1304

50 ug/L 1 8260tertiary Butyl Alcohol75-65-0 01/13/16ND B6A1304

5.0 ug/L 1 8260tertiaryAmylmethylether994-05-8 01/13/16ND B6A1304

10 ug/L 10 8260Tetrachloroethylene127-18-4 01/14/16560 B6A1304

5.0 ug/L 1 8260Tetrahydrofuran109-99-9 01/13/16ND B6A1304

1.0 ug/L 1 8260Toluene108-88-3 01/13/16ND B6A1304

1.0 ug/L 1 8260trans-1,2-Dichloroethylene156-60-5 01/13/16ND B6A1304

1.0 ug/L 1 8260trans-1,3-Dichloropropylene10061-02-6 01/13/16ND B6A1304

5.0 ug/L 1 8260trans-1,4-Dichloro-2-butene110-57-6 01/13/16ND B6A1304

1.0 ug/L 1 8260Trichloroethylene79-01-6 01/13/1610 B6A1304

1.0 ug/L 1 8260Trichlorofluoromethane75-69-4 01/13/16ND B6A1304

1.0 ug/L 1 8260Vinyl chloride75-01-4 01/13/16ND B6A1304

85-11595.7 %Surrogate: Bromofluorobenzene 826001/13/16 B6A1304

82.7-115102 %Surrogate: Dibromofluoromethane 826001/13/16 B6A1304

85-115104 %Surrogate: Toluene-d8 826001/13/16 B6A1304

Lab Work Order # 1601052

Page 4 of 19Page 4 of 20

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1601052-02

RLCAS #

Client ID: GP13@30'

QC Batch

Organics-Volatiles

1.0 ug/L 1 82601,1,1,2-Tetrachloroethane630-20-6 01/13/16ND B6A1304

1.0 ug/L 1 82601,1,1-Trichloroethane71-55-6 01/13/16ND B6A1304

1.0 ug/L 1 82601,1,2,2-Tetrachloroethane79-34-5 01/13/16ND B6A1304

1.0 ug/L 1 82601,1,2-Trichloroethane79-00-5 01/13/16ND B6A1304

1.0 ug/L 1 82601,1-Dichloroethane75-34-3 01/13/16ND B6A1304

1.0 ug/L 1 82601,1-Dichloroethylene75-35-4 01/13/16ND B6A1304

5.0 ug/L 1 82601,2,3-Trichlorobenzene87-61-6 01/13/16ND B6A1304

1.0 ug/L 1 82601,2,3-Trichloropropane96-18-4 01/13/16ND B6A1304

1.0 ug/L 1 82601,2,3-Trimethylbenzene526-73-8 01/13/16ND B6A1304

5.0 ug/L 1 82601,2,4-Trichlorobenzene120-82-1 01/13/16ND B6A1304

1.0 ug/L 1 82601,2,4-Trimethylbenzene95-63-6 01/13/16ND B6A1304

5.0 ug/L 1 82601,2-Dibromo-3-chloropropane96-12-8 01/13/16ND B6A1304

1.0 ug/L 1 82601,2-Dibromoethane106-93-4 01/13/16ND B6A1304

1.0 ug/L 1 82601,2-Dichlorobenzene95-50-1 01/13/16ND B6A1304

1.0 ug/L 1 82601,2-Dichloroethane107-06-2 01/13/16ND B6A1304

1.0 ug/L 1 82601,2-Dichloropropane78-87-5 01/13/16ND B6A1304

1.0 ug/L 1 82601,3,5-Trimethylbenzene108-67-8 01/13/16ND B6A1304

1.0 ug/L 1 82601,3-Dichlorobenzene541-73-1 01/13/16ND B6A1304

1.0 ug/L 1 82601,4-Dichlorobenzene106-46-7 01/13/16ND B6A1304

5.0 ug/L 1 82602-Butanone (MEK)78-93-3 01/13/16ND B6A1304

5.0 ug/L 1 82602-Hexanone591-78-6 01/13/16ND B6A1304

5.0 Xug/L 1 82602-Methylnaphthalene91-57-6 01/13/16ND B6A1304

20 ug/L 1 82602-Propanone (acetone)67-64-1 01/13/16ND B6A1304

5.0 ug/L 1 82604-Methyl-2-pentanone (MIBK)108-10-1 01/13/16ND B6A1304

5.0 ug/L 1 8260Acrylonitrile107-13-1 01/13/16ND B6A1304

1.0 ug/L 1 8260Benzene71-43-2 01/13/16ND B6A1304

1.0 ug/L 1 8260Bromobenzene108-86-1 01/13/16ND B6A1304

1.0 ug/L 1 8260Bromochloromethane74-97-5 01/13/16ND B6A1304

1.0 ug/L 1 8260Bromodichloromethane75-27-4 01/13/16ND B6A1304

1.0 ug/L 1 8260Bromoform75-25-2 01/13/16ND B6A1304

5.0 ug/L 1 8260Bromomethane74-83-9 01/13/16ND B6A1304

1.0 ug/L 1 8260Carbon disulfide75-15-0 01/13/16ND B6A1304

1.0 ug/L 1 8260Carbon tetrachloride56-23-5 01/13/16ND B6A1304

1.0 ug/L 1 8260Chlorobenzene108-90-7 01/13/16ND B6A1304

5.0 ug/L 1 8260Chloroethane75-00-3 01/13/16ND B6A1304

1.0 ug/L 1 8260Chloroform67-66-3 01/13/16ND B6A1304

5.0 ug/L 1 8260Chloromethane74-87-3 01/13/16ND B6A1304

1.0 ug/L 1 8260cis-1,2-Dichloroethylene156-59-2 01/13/168.6 B6A1304

1.0 ug/L 1 8260cis-1,3-Dichloropropylene10061-01-5 01/13/16ND B6A1304

5.0 ug/L 1 8260Cyclohexane110-82-7 01/13/16ND B6A1304

1.0 ug/L 1 8260Dibromochloromethane124-48-1 01/13/16ND B6A1304

Lab Work Order # 1601052

Page 5 of 19Page 5 of 20

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1601052-02

RLCAS #

Client ID: GP13@30'

QC Batch

Organics-Volatiles

1.0 ug/L 1 8260Dibromomethane74-95-3 01/13/16ND B6A1304

5.0 ug/L 1 8260Dichlorodifluoromethane75-71-8 01/13/16ND B6A1304

5.0 ug/L 1 8260Diethyl ether60-29-7 01/13/16ND B6A1304

5.0 ug/L 1 8260Diisopropyl Ether108-20-3 01/13/16ND B6A1304

1.0 ug/L 1 8260Ethylbenzene100-41-4 01/13/16ND B6A1304

5.0 ug/L 1 8260Ethyltertiarybutylether637-92-3 01/13/16ND B6A1304

5.0 ug/L 1 8260Hexachloroethane67-72-1 01/13/16ND B6A1304

1.0 ug/L 1 8260Isopropylbenzene98-82-8 01/13/16ND B6A1304

2.0 ug/L 1 8260m & p - Xylene1330-20-7 01/13/16ND B6A1304

1.0 ug/L 1 8260Methyl iodide74-88-4 01/13/16ND B6A1304

5.0 ug/L 1 8260Methylene chloride75-09-2 01/13/16ND B6A1304

1.0 ug/L 1 8260Methyltertiarybutylether1634-04-4 01/13/16ND B6A1304

5.0 Xug/L 1 8260Naphthalene91-20-3 01/13/16ND B6A1304

1.0 ug/L 1 8260n-Butylbenzene104-51-8 01/13/16ND B6A1304

1.0 ug/L 1 8260n-Propylbenzene103-65-1 01/13/16ND B6A1304

1.0 ug/L 1 8260o-Xylene95-47-6 01/13/16ND B6A1304

1.0 ug/L 1 8260p-Isopropyl toluene99-87-6 01/13/16ND B6A1304

1.0 ug/L 1 8260sec-Butylbenzene135-98-8 01/13/16ND B6A1304

1.0 ug/L 1 8260Styrene100-42-5 01/13/16ND B6A1304

1.0 ug/L 1 8260tert-Butylbenzene98-06-6 01/13/16ND B6A1304

50 ug/L 1 8260tertiary Butyl Alcohol75-65-0 01/13/16ND B6A1304

5.0 ug/L 1 8260tertiaryAmylmethylether994-05-8 01/13/16ND B6A1304

1.0 ug/L 1 8260Tetrachloroethylene127-18-4 01/13/16140 B6A1304

5.0 ug/L 1 8260Tetrahydrofuran109-99-9 01/13/16ND B6A1304

1.0 ug/L 1 8260Toluene108-88-3 01/13/16ND B6A1304

1.0 ug/L 1 8260trans-1,2-Dichloroethylene156-60-5 01/13/16ND B6A1304

1.0 ug/L 1 8260trans-1,3-Dichloropropylene10061-02-6 01/13/16ND B6A1304

5.0 ug/L 1 8260trans-1,4-Dichloro-2-butene110-57-6 01/13/16ND B6A1304

1.0 ug/L 1 8260Trichloroethylene79-01-6 01/13/163.0 B6A1304

1.0 ug/L 1 8260Trichlorofluoromethane75-69-4 01/13/16ND B6A1304

1.0 ug/L 1 8260Vinyl chloride75-01-4 01/13/16ND B6A1304

85-11595.3 %Surrogate: Bromofluorobenzene 826001/13/16 B6A1304

82.7-115101 %Surrogate: Dibromofluoromethane 826001/13/16 B6A1304

85-115102 %Surrogate: Toluene-d8 826001/13/16 B6A1304

Lab Work Order # 1601052

Page 6 of 19Page 6 of 20

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1601052-03

RLCAS #

Client ID: GP13@35'

QC Batch

Organics-Volatiles

1.0 ug/L 1 82601,1,1,2-Tetrachloroethane630-20-6 01/13/16ND B6A1304

1.0 ug/L 1 82601,1,1-Trichloroethane71-55-6 01/13/16ND B6A1304

1.0 ug/L 1 82601,1,2,2-Tetrachloroethane79-34-5 01/13/16ND B6A1304

1.0 ug/L 1 82601,1,2-Trichloroethane79-00-5 01/13/16ND B6A1304

1.0 ug/L 1 82601,1-Dichloroethane75-34-3 01/13/16ND B6A1304

1.0 ug/L 1 82601,1-Dichloroethylene75-35-4 01/13/16ND B6A1304

5.0 ug/L 1 82601,2,3-Trichlorobenzene87-61-6 01/13/16ND B6A1304

1.0 ug/L 1 82601,2,3-Trichloropropane96-18-4 01/13/16ND B6A1304

1.0 ug/L 1 82601,2,3-Trimethylbenzene526-73-8 01/13/16ND B6A1304

5.0 ug/L 1 82601,2,4-Trichlorobenzene120-82-1 01/13/16ND B6A1304

1.0 ug/L 1 82601,2,4-Trimethylbenzene95-63-6 01/13/16ND B6A1304

5.0 ug/L 1 82601,2-Dibromo-3-chloropropane96-12-8 01/13/16ND B6A1304

1.0 ug/L 1 82601,2-Dibromoethane106-93-4 01/13/16ND B6A1304

1.0 ug/L 1 82601,2-Dichlorobenzene95-50-1 01/13/16ND B6A1304

1.0 ug/L 1 82601,2-Dichloroethane107-06-2 01/13/16ND B6A1304

1.0 ug/L 1 82601,2-Dichloropropane78-87-5 01/13/16ND B6A1304

1.0 ug/L 1 82601,3,5-Trimethylbenzene108-67-8 01/13/16ND B6A1304

1.0 ug/L 1 82601,3-Dichlorobenzene541-73-1 01/13/16ND B6A1304

1.0 ug/L 1 82601,4-Dichlorobenzene106-46-7 01/13/16ND B6A1304

5.0 ug/L 1 82602-Butanone (MEK)78-93-3 01/13/16ND B6A1304

5.0 ug/L 1 82602-Hexanone591-78-6 01/13/16ND B6A1304

5.0 Xug/L 1 82602-Methylnaphthalene91-57-6 01/13/16ND B6A1304

20 ug/L 1 82602-Propanone (acetone)67-64-1 01/13/16ND B6A1304

5.0 ug/L 1 82604-Methyl-2-pentanone (MIBK)108-10-1 01/13/16ND B6A1304

5.0 ug/L 1 8260Acrylonitrile107-13-1 01/13/16ND B6A1304

1.0 ug/L 1 8260Benzene71-43-2 01/13/16ND B6A1304

1.0 ug/L 1 8260Bromobenzene108-86-1 01/13/16ND B6A1304

1.0 ug/L 1 8260Bromochloromethane74-97-5 01/13/16ND B6A1304

1.0 ug/L 1 8260Bromodichloromethane75-27-4 01/13/16ND B6A1304

1.0 ug/L 1 8260Bromoform75-25-2 01/13/16ND B6A1304

5.0 ug/L 1 8260Bromomethane74-83-9 01/13/16ND B6A1304

1.0 ug/L 1 8260Carbon disulfide75-15-0 01/13/16ND B6A1304

1.0 ug/L 1 8260Carbon tetrachloride56-23-5 01/13/16ND B6A1304

1.0 ug/L 1 8260Chlorobenzene108-90-7 01/13/16ND B6A1304

5.0 ug/L 1 8260Chloroethane75-00-3 01/13/16ND B6A1304

1.0 ug/L 1 8260Chloroform67-66-3 01/13/16ND B6A1304

5.0 ug/L 1 8260Chloromethane74-87-3 01/13/16ND B6A1304

1.0 ug/L 1 8260cis-1,2-Dichloroethylene156-59-2 01/13/163.4 B6A1304

1.0 ug/L 1 8260cis-1,3-Dichloropropylene10061-01-5 01/13/16ND B6A1304

5.0 ug/L 1 8260Cyclohexane110-82-7 01/13/16ND B6A1304

1.0 ug/L 1 8260Dibromochloromethane124-48-1 01/13/16ND B6A1304

Lab Work Order # 1601052

Page 7 of 19Page 7 of 20

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1601052-03

RLCAS #

Client ID: GP13@35'

QC Batch

Organics-Volatiles

1.0 ug/L 1 8260Dibromomethane74-95-3 01/13/16ND B6A1304

5.0 ug/L 1 8260Dichlorodifluoromethane75-71-8 01/13/16ND B6A1304

5.0 ug/L 1 8260Diethyl ether60-29-7 01/13/16ND B6A1304

5.0 ug/L 1 8260Diisopropyl Ether108-20-3 01/13/16ND B6A1304

1.0 ug/L 1 8260Ethylbenzene100-41-4 01/13/16ND B6A1304

5.0 ug/L 1 8260Ethyltertiarybutylether637-92-3 01/13/16ND B6A1304

5.0 ug/L 1 8260Hexachloroethane67-72-1 01/13/16ND B6A1304

1.0 ug/L 1 8260Isopropylbenzene98-82-8 01/13/16ND B6A1304

2.0 ug/L 1 8260m & p - Xylene1330-20-7 01/13/16ND B6A1304

1.0 ug/L 1 8260Methyl iodide74-88-4 01/13/16ND B6A1304

5.0 ug/L 1 8260Methylene chloride75-09-2 01/13/16ND B6A1304

1.0 ug/L 1 8260Methyltertiarybutylether1634-04-4 01/13/16ND B6A1304

5.0 Xug/L 1 8260Naphthalene91-20-3 01/13/16ND B6A1304

1.0 ug/L 1 8260n-Butylbenzene104-51-8 01/13/16ND B6A1304

1.0 ug/L 1 8260n-Propylbenzene103-65-1 01/13/16ND B6A1304

1.0 ug/L 1 8260o-Xylene95-47-6 01/13/16ND B6A1304

1.0 ug/L 1 8260p-Isopropyl toluene99-87-6 01/13/16ND B6A1304

1.0 ug/L 1 8260sec-Butylbenzene135-98-8 01/13/16ND B6A1304

1.0 ug/L 1 8260Styrene100-42-5 01/13/16ND B6A1304

1.0 ug/L 1 8260tert-Butylbenzene98-06-6 01/13/16ND B6A1304

50 ug/L 1 8260tertiary Butyl Alcohol75-65-0 01/13/16ND B6A1304

5.0 ug/L 1 8260tertiaryAmylmethylether994-05-8 01/13/16ND B6A1304

1.0 ug/L 1 8260Tetrachloroethylene127-18-4 01/13/16100 B6A1304

5.0 ug/L 1 8260Tetrahydrofuran109-99-9 01/13/16ND B6A1304

1.0 ug/L 1 8260Toluene108-88-3 01/13/16ND B6A1304

1.0 ug/L 1 8260trans-1,2-Dichloroethylene156-60-5 01/13/16ND B6A1304

1.0 ug/L 1 8260trans-1,3-Dichloropropylene10061-02-6 01/13/16ND B6A1304

5.0 ug/L 1 8260trans-1,4-Dichloro-2-butene110-57-6 01/13/16ND B6A1304

1.0 ug/L 1 8260Trichloroethylene79-01-6 01/13/161.4 B6A1304

1.0 ug/L 1 8260Trichlorofluoromethane75-69-4 01/13/16ND B6A1304

1.0 ug/L 1 8260Vinyl chloride75-01-4 01/13/16ND B6A1304

85-11594.8 %Surrogate: Bromofluorobenzene 826001/13/16 B6A1304

82.7-115101 %Surrogate: Dibromofluoromethane 826001/13/16 B6A1304

85-115102 %Surrogate: Toluene-d8 826001/13/16 B6A1304

Lab Work Order # 1601052

Page 8 of 19Page 8 of 20

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1601052-04

RLCAS #

Client ID: GP13@40'

QC Batch

Organics-Volatiles

1.0 ug/L 1 82601,1,1,2-Tetrachloroethane630-20-6 01/13/16ND B6A1304

1.0 ug/L 1 82601,1,1-Trichloroethane71-55-6 01/13/16ND B6A1304

1.0 ug/L 1 82601,1,2,2-Tetrachloroethane79-34-5 01/13/16ND B6A1304

1.0 ug/L 1 82601,1,2-Trichloroethane79-00-5 01/13/16ND B6A1304

1.0 ug/L 1 82601,1-Dichloroethane75-34-3 01/13/16ND B6A1304

1.0 ug/L 1 82601,1-Dichloroethylene75-35-4 01/13/16ND B6A1304

5.0 ug/L 1 82601,2,3-Trichlorobenzene87-61-6 01/13/16ND B6A1304

1.0 ug/L 1 82601,2,3-Trichloropropane96-18-4 01/13/16ND B6A1304

1.0 ug/L 1 82601,2,3-Trimethylbenzene526-73-8 01/13/16ND B6A1304

5.0 ug/L 1 82601,2,4-Trichlorobenzene120-82-1 01/13/16ND B6A1304

1.0 ug/L 1 82601,2,4-Trimethylbenzene95-63-6 01/13/16ND B6A1304

5.0 ug/L 1 82601,2-Dibromo-3-chloropropane96-12-8 01/13/16ND B6A1304

1.0 ug/L 1 82601,2-Dibromoethane106-93-4 01/13/16ND B6A1304

1.0 ug/L 1 82601,2-Dichlorobenzene95-50-1 01/13/16ND B6A1304

1.0 ug/L 1 82601,2-Dichloroethane107-06-2 01/13/16ND B6A1304

1.0 ug/L 1 82601,2-Dichloropropane78-87-5 01/13/16ND B6A1304

1.0 ug/L 1 82601,3,5-Trimethylbenzene108-67-8 01/13/16ND B6A1304

1.0 ug/L 1 82601,3-Dichlorobenzene541-73-1 01/13/16ND B6A1304

1.0 ug/L 1 82601,4-Dichlorobenzene106-46-7 01/13/16ND B6A1304

5.0 ug/L 1 82602-Butanone (MEK)78-93-3 01/13/16ND B6A1304

5.0 ug/L 1 82602-Hexanone591-78-6 01/13/16ND B6A1304

5.0 Xug/L 1 82602-Methylnaphthalene91-57-6 01/13/16ND B6A1304

20 ug/L 1 82602-Propanone (acetone)67-64-1 01/13/16ND B6A1304

5.0 ug/L 1 82604-Methyl-2-pentanone (MIBK)108-10-1 01/13/16ND B6A1304

5.0 ug/L 1 8260Acrylonitrile107-13-1 01/13/16ND B6A1304

1.0 ug/L 1 8260Benzene71-43-2 01/13/16ND B6A1304

1.0 ug/L 1 8260Bromobenzene108-86-1 01/13/16ND B6A1304

1.0 ug/L 1 8260Bromochloromethane74-97-5 01/13/16ND B6A1304

1.0 ug/L 1 8260Bromodichloromethane75-27-4 01/13/16ND B6A1304

1.0 ug/L 1 8260Bromoform75-25-2 01/13/16ND B6A1304

5.0 ug/L 1 8260Bromomethane74-83-9 01/13/16ND B6A1304

1.0 ug/L 1 8260Carbon disulfide75-15-0 01/13/16ND B6A1304

1.0 ug/L 1 8260Carbon tetrachloride56-23-5 01/13/16ND B6A1304

1.0 ug/L 1 8260Chlorobenzene108-90-7 01/13/16ND B6A1304

5.0 ug/L 1 8260Chloroethane75-00-3 01/13/16ND B6A1304

1.0 ug/L 1 8260Chloroform67-66-3 01/13/16ND B6A1304

5.0 ug/L 1 8260Chloromethane74-87-3 01/13/16ND B6A1304

1.0 ug/L 1 8260cis-1,2-Dichloroethylene156-59-2 01/13/16ND B6A1304

1.0 ug/L 1 8260cis-1,3-Dichloropropylene10061-01-5 01/13/16ND B6A1304

5.0 ug/L 1 8260Cyclohexane110-82-7 01/13/16ND B6A1304

1.0 ug/L 1 8260Dibromochloromethane124-48-1 01/13/16ND B6A1304

Lab Work Order # 1601052

Page 9 of 19Page 9 of 20

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1601052-04

RLCAS #

Client ID: GP13@40'

QC Batch

Organics-Volatiles

1.0 ug/L 1 8260Dibromomethane74-95-3 01/13/16ND B6A1304

5.0 ug/L 1 8260Dichlorodifluoromethane75-71-8 01/13/16ND B6A1304

5.0 ug/L 1 8260Diethyl ether60-29-7 01/13/16ND B6A1304

5.0 ug/L 1 8260Diisopropyl Ether108-20-3 01/13/16ND B6A1304

1.0 ug/L 1 8260Ethylbenzene100-41-4 01/13/16ND B6A1304

5.0 ug/L 1 8260Ethyltertiarybutylether637-92-3 01/13/16ND B6A1304

5.0 ug/L 1 8260Hexachloroethane67-72-1 01/13/16ND B6A1304

1.0 ug/L 1 8260Isopropylbenzene98-82-8 01/13/16ND B6A1304

2.0 ug/L 1 8260m & p - Xylene1330-20-7 01/13/16ND B6A1304

1.0 ug/L 1 8260Methyl iodide74-88-4 01/13/16ND B6A1304

5.0 ug/L 1 8260Methylene chloride75-09-2 01/13/16ND B6A1304

1.0 ug/L 1 8260Methyltertiarybutylether1634-04-4 01/13/16ND B6A1304

5.0 Xug/L 1 8260Naphthalene91-20-3 01/13/16ND B6A1304

1.0 ug/L 1 8260n-Butylbenzene104-51-8 01/13/16ND B6A1304

1.0 ug/L 1 8260n-Propylbenzene103-65-1 01/13/16ND B6A1304

1.0 ug/L 1 8260o-Xylene95-47-6 01/13/16ND B6A1304

1.0 ug/L 1 8260p-Isopropyl toluene99-87-6 01/13/16ND B6A1304

1.0 ug/L 1 8260sec-Butylbenzene135-98-8 01/13/16ND B6A1304

1.0 ug/L 1 8260Styrene100-42-5 01/13/16ND B6A1304

1.0 ug/L 1 8260tert-Butylbenzene98-06-6 01/13/16ND B6A1304

50 ug/L 1 8260tertiary Butyl Alcohol75-65-0 01/13/16ND B6A1304

5.0 ug/L 1 8260tertiaryAmylmethylether994-05-8 01/13/16ND B6A1304

1.0 ug/L 1 8260Tetrachloroethylene127-18-4 01/13/1646 B6A1304

5.0 ug/L 1 8260Tetrahydrofuran109-99-9 01/13/16ND B6A1304

1.0 ug/L 1 8260Toluene108-88-3 01/13/16ND B6A1304

1.0 ug/L 1 8260trans-1,2-Dichloroethylene156-60-5 01/13/16ND B6A1304

1.0 ug/L 1 8260trans-1,3-Dichloropropylene10061-02-6 01/13/16ND B6A1304

5.0 ug/L 1 8260trans-1,4-Dichloro-2-butene110-57-6 01/13/16ND B6A1304

1.0 ug/L 1 8260Trichloroethylene79-01-6 01/13/161.1 B6A1304

1.0 ug/L 1 8260Trichlorofluoromethane75-69-4 01/13/16ND B6A1304

1.0 ug/L 1 8260Vinyl chloride75-01-4 01/13/16ND B6A1304

85-11598.5 %Surrogate: Bromofluorobenzene 826001/13/16 B6A1304

82.7-115103 %Surrogate: Dibromofluoromethane 826001/13/16 B6A1304

85-11599.7 %Surrogate: Toluene-d8 826001/13/16 B6A1304

Lab Work Order # 1601052

Page 10 of 19Page 10 of 20

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1601052-05

RLCAS #

Client ID: GP14@25'

QC Batch

Organics-Volatiles

1.0 ug/L 1 82601,1,1,2-Tetrachloroethane630-20-6 01/13/16ND B6A1304

1.0 ug/L 1 82601,1,1-Trichloroethane71-55-6 01/13/16ND B6A1304

1.0 ug/L 1 82601,1,2,2-Tetrachloroethane79-34-5 01/13/16ND B6A1304

1.0 ug/L 1 82601,1,2-Trichloroethane79-00-5 01/13/16ND B6A1304

1.0 ug/L 1 82601,1-Dichloroethane75-34-3 01/13/16ND B6A1304

1.0 ug/L 1 82601,1-Dichloroethylene75-35-4 01/13/16ND B6A1304

5.0 ug/L 1 82601,2,3-Trichlorobenzene87-61-6 01/13/16ND B6A1304

1.0 ug/L 1 82601,2,3-Trichloropropane96-18-4 01/13/16ND B6A1304

1.0 ug/L 1 82601,2,3-Trimethylbenzene526-73-8 01/13/16ND B6A1304

5.0 ug/L 1 82601,2,4-Trichlorobenzene120-82-1 01/13/16ND B6A1304

1.0 ug/L 1 82601,2,4-Trimethylbenzene95-63-6 01/13/16ND B6A1304

5.0 ug/L 1 82601,2-Dibromo-3-chloropropane96-12-8 01/13/16ND B6A1304

1.0 ug/L 1 82601,2-Dibromoethane106-93-4 01/13/16ND B6A1304

1.0 ug/L 1 82601,2-Dichlorobenzene95-50-1 01/13/16ND B6A1304

1.0 ug/L 1 82601,2-Dichloroethane107-06-2 01/13/16ND B6A1304

1.0 ug/L 1 82601,2-Dichloropropane78-87-5 01/13/16ND B6A1304

1.0 ug/L 1 82601,3,5-Trimethylbenzene108-67-8 01/13/16ND B6A1304

1.0 ug/L 1 82601,3-Dichlorobenzene541-73-1 01/13/16ND B6A1304

1.0 ug/L 1 82601,4-Dichlorobenzene106-46-7 01/13/16ND B6A1304

5.0 ug/L 1 82602-Butanone (MEK)78-93-3 01/13/16ND B6A1304

5.0 ug/L 1 82602-Hexanone591-78-6 01/13/16ND B6A1304

5.0 Xug/L 1 82602-Methylnaphthalene91-57-6 01/13/16ND B6A1304

20 ug/L 1 82602-Propanone (acetone)67-64-1 01/13/16ND B6A1304

5.0 ug/L 1 82604-Methyl-2-pentanone (MIBK)108-10-1 01/13/16ND B6A1304

5.0 ug/L 1 8260Acrylonitrile107-13-1 01/13/16ND B6A1304

1.0 ug/L 1 8260Benzene71-43-2 01/13/16ND B6A1304

1.0 ug/L 1 8260Bromobenzene108-86-1 01/13/16ND B6A1304

1.0 ug/L 1 8260Bromochloromethane74-97-5 01/13/16ND B6A1304

1.0 ug/L 1 8260Bromodichloromethane75-27-4 01/13/16ND B6A1304

1.0 ug/L 1 8260Bromoform75-25-2 01/13/16ND B6A1304

5.0 ug/L 1 8260Bromomethane74-83-9 01/13/16ND B6A1304

1.0 ug/L 1 8260Carbon disulfide75-15-0 01/13/16ND B6A1304

1.0 ug/L 1 8260Carbon tetrachloride56-23-5 01/13/16ND B6A1304

1.0 ug/L 1 8260Chlorobenzene108-90-7 01/13/16ND B6A1304

5.0 ug/L 1 8260Chloroethane75-00-3 01/13/16ND B6A1304

1.0 ug/L 1 8260Chloroform67-66-3 01/13/16ND B6A1304

5.0 ug/L 1 8260Chloromethane74-87-3 01/13/16ND B6A1304

1.0 ug/L 1 8260cis-1,2-Dichloroethylene156-59-2 01/13/16ND B6A1304

1.0 ug/L 1 8260cis-1,3-Dichloropropylene10061-01-5 01/13/16ND B6A1304

5.0 ug/L 1 8260Cyclohexane110-82-7 01/13/16ND B6A1304

1.0 ug/L 1 8260Dibromochloromethane124-48-1 01/13/16ND B6A1304

Lab Work Order # 1601052

Page 11 of 19Page 11 of 20

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1601052-05

RLCAS #

Client ID: GP14@25'

QC Batch

Organics-Volatiles

1.0 ug/L 1 8260Dibromomethane74-95-3 01/13/16ND B6A1304

5.0 ug/L 1 8260Dichlorodifluoromethane75-71-8 01/13/16ND B6A1304

5.0 ug/L 1 8260Diethyl ether60-29-7 01/13/16ND B6A1304

5.0 ug/L 1 8260Diisopropyl Ether108-20-3 01/13/16ND B6A1304

1.0 ug/L 1 8260Ethylbenzene100-41-4 01/13/16ND B6A1304

5.0 ug/L 1 8260Ethyltertiarybutylether637-92-3 01/13/16ND B6A1304

5.0 ug/L 1 8260Hexachloroethane67-72-1 01/13/16ND B6A1304

1.0 ug/L 1 8260Isopropylbenzene98-82-8 01/13/16ND B6A1304

2.0 ug/L 1 8260m & p - Xylene1330-20-7 01/13/16ND B6A1304

1.0 ug/L 1 8260Methyl iodide74-88-4 01/13/16ND B6A1304

5.0 ug/L 1 8260Methylene chloride75-09-2 01/13/16ND B6A1304

1.0 ug/L 1 8260Methyltertiarybutylether1634-04-4 01/13/16ND B6A1304

5.0 Xug/L 1 8260Naphthalene91-20-3 01/13/16ND B6A1304

1.0 ug/L 1 8260n-Butylbenzene104-51-8 01/13/16ND B6A1304

1.0 ug/L 1 8260n-Propylbenzene103-65-1 01/13/16ND B6A1304

1.0 ug/L 1 8260o-Xylene95-47-6 01/13/16ND B6A1304

1.0 ug/L 1 8260p-Isopropyl toluene99-87-6 01/13/16ND B6A1304

1.0 ug/L 1 8260sec-Butylbenzene135-98-8 01/13/16ND B6A1304

1.0 ug/L 1 8260Styrene100-42-5 01/13/16ND B6A1304

1.0 ug/L 1 8260tert-Butylbenzene98-06-6 01/13/16ND B6A1304

50 ug/L 1 8260tertiary Butyl Alcohol75-65-0 01/13/16ND B6A1304

5.0 ug/L 1 8260tertiaryAmylmethylether994-05-8 01/13/16ND B6A1304

1.0 ug/L 1 8260Tetrachloroethylene127-18-4 01/13/1662 B6A1304

5.0 ug/L 1 8260Tetrahydrofuran109-99-9 01/13/16ND B6A1304

1.0 ug/L 1 8260Toluene108-88-3 01/13/16ND B6A1304

1.0 ug/L 1 8260trans-1,2-Dichloroethylene156-60-5 01/13/16ND B6A1304

1.0 ug/L 1 8260trans-1,3-Dichloropropylene10061-02-6 01/13/16ND B6A1304

5.0 ug/L 1 8260trans-1,4-Dichloro-2-butene110-57-6 01/13/16ND B6A1304

1.0 ug/L 1 8260Trichloroethylene79-01-6 01/13/16ND B6A1304

1.0 ug/L 1 8260Trichlorofluoromethane75-69-4 01/13/16ND B6A1304

1.0 ug/L 1 8260Vinyl chloride75-01-4 01/13/16ND B6A1304

85-11597.1 %Surrogate: Bromofluorobenzene 826001/13/16 B6A1304

82.7-115103 %Surrogate: Dibromofluoromethane 826001/13/16 B6A1304

85-115102 %Surrogate: Toluene-d8 826001/13/16 B6A1304

Lab Work Order # 1601052

Page 12 of 19Page 12 of 20

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1601052-06

RLCAS #

Client ID: GP14@30'

QC Batch

Organics-Volatiles

1.0 ug/L 1 82601,1,1,2-Tetrachloroethane630-20-6 01/13/16ND B6A1304

1.0 ug/L 1 82601,1,1-Trichloroethane71-55-6 01/13/16ND B6A1304

1.0 ug/L 1 82601,1,2,2-Tetrachloroethane79-34-5 01/13/16ND B6A1304

1.0 ug/L 1 82601,1,2-Trichloroethane79-00-5 01/13/16ND B6A1304

1.0 ug/L 1 82601,1-Dichloroethane75-34-3 01/13/16ND B6A1304

1.0 ug/L 1 82601,1-Dichloroethylene75-35-4 01/13/16ND B6A1304

5.0 ug/L 1 82601,2,3-Trichlorobenzene87-61-6 01/13/16ND B6A1304

1.0 ug/L 1 82601,2,3-Trichloropropane96-18-4 01/13/16ND B6A1304

1.0 ug/L 1 82601,2,3-Trimethylbenzene526-73-8 01/13/16ND B6A1304

5.0 ug/L 1 82601,2,4-Trichlorobenzene120-82-1 01/13/16ND B6A1304

1.0 ug/L 1 82601,2,4-Trimethylbenzene95-63-6 01/13/16ND B6A1304

5.0 ug/L 1 82601,2-Dibromo-3-chloropropane96-12-8 01/13/16ND B6A1304

1.0 ug/L 1 82601,2-Dibromoethane106-93-4 01/13/16ND B6A1304

1.0 ug/L 1 82601,2-Dichlorobenzene95-50-1 01/13/16ND B6A1304

1.0 ug/L 1 82601,2-Dichloroethane107-06-2 01/13/16ND B6A1304

1.0 ug/L 1 82601,2-Dichloropropane78-87-5 01/13/16ND B6A1304

1.0 ug/L 1 82601,3,5-Trimethylbenzene108-67-8 01/13/16ND B6A1304

1.0 ug/L 1 82601,3-Dichlorobenzene541-73-1 01/13/16ND B6A1304

1.0 ug/L 1 82601,4-Dichlorobenzene106-46-7 01/13/16ND B6A1304

5.0 ug/L 1 82602-Butanone (MEK)78-93-3 01/13/16ND B6A1304

5.0 ug/L 1 82602-Hexanone591-78-6 01/13/16ND B6A1304

5.0 Xug/L 1 82602-Methylnaphthalene91-57-6 01/13/16ND B6A1304

20 ug/L 1 82602-Propanone (acetone)67-64-1 01/13/16ND B6A1304

5.0 ug/L 1 82604-Methyl-2-pentanone (MIBK)108-10-1 01/13/16ND B6A1304

5.0 ug/L 1 8260Acrylonitrile107-13-1 01/13/16ND B6A1304

1.0 ug/L 1 8260Benzene71-43-2 01/13/16ND B6A1304

1.0 ug/L 1 8260Bromobenzene108-86-1 01/13/16ND B6A1304

1.0 ug/L 1 8260Bromochloromethane74-97-5 01/13/16ND B6A1304

1.0 ug/L 1 8260Bromodichloromethane75-27-4 01/13/16ND B6A1304

1.0 ug/L 1 8260Bromoform75-25-2 01/13/16ND B6A1304

5.0 ug/L 1 8260Bromomethane74-83-9 01/13/16ND B6A1304

1.0 ug/L 1 8260Carbon disulfide75-15-0 01/13/16ND B6A1304

1.0 ug/L 1 8260Carbon tetrachloride56-23-5 01/13/16ND B6A1304

1.0 ug/L 1 8260Chlorobenzene108-90-7 01/13/16ND B6A1304

5.0 ug/L 1 8260Chloroethane75-00-3 01/13/16ND B6A1304

1.0 ug/L 1 8260Chloroform67-66-3 01/13/16ND B6A1304

5.0 ug/L 1 8260Chloromethane74-87-3 01/13/16ND B6A1304

1.0 ug/L 1 8260cis-1,2-Dichloroethylene156-59-2 01/13/16ND B6A1304

1.0 ug/L 1 8260cis-1,3-Dichloropropylene10061-01-5 01/13/16ND B6A1304

5.0 ug/L 1 8260Cyclohexane110-82-7 01/13/16ND B6A1304

1.0 ug/L 1 8260Dibromochloromethane124-48-1 01/13/16ND B6A1304

Lab Work Order # 1601052

Page 13 of 19Page 13 of 20

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1601052-06

RLCAS #

Client ID: GP14@30'

QC Batch

Organics-Volatiles

1.0 ug/L 1 8260Dibromomethane74-95-3 01/13/16ND B6A1304

5.0 ug/L 1 8260Dichlorodifluoromethane75-71-8 01/13/16ND B6A1304

5.0 ug/L 1 8260Diethyl ether60-29-7 01/13/16ND B6A1304

5.0 ug/L 1 8260Diisopropyl Ether108-20-3 01/13/16ND B6A1304

1.0 ug/L 1 8260Ethylbenzene100-41-4 01/13/16ND B6A1304

5.0 ug/L 1 8260Ethyltertiarybutylether637-92-3 01/13/16ND B6A1304

5.0 ug/L 1 8260Hexachloroethane67-72-1 01/13/16ND B6A1304

1.0 ug/L 1 8260Isopropylbenzene98-82-8 01/13/16ND B6A1304

2.0 ug/L 1 8260m & p - Xylene1330-20-7 01/13/16ND B6A1304

1.0 ug/L 1 8260Methyl iodide74-88-4 01/13/16ND B6A1304

5.0 ug/L 1 8260Methylene chloride75-09-2 01/13/16ND B6A1304

1.0 ug/L 1 8260Methyltertiarybutylether1634-04-4 01/13/16ND B6A1304

5.0 Xug/L 1 8260Naphthalene91-20-3 01/13/16ND B6A1304

1.0 ug/L 1 8260n-Butylbenzene104-51-8 01/13/16ND B6A1304

1.0 ug/L 1 8260n-Propylbenzene103-65-1 01/13/16ND B6A1304

1.0 ug/L 1 8260o-Xylene95-47-6 01/13/16ND B6A1304

1.0 ug/L 1 8260p-Isopropyl toluene99-87-6 01/13/16ND B6A1304

1.0 ug/L 1 8260sec-Butylbenzene135-98-8 01/13/16ND B6A1304

1.0 ug/L 1 8260Styrene100-42-5 01/13/16ND B6A1304

1.0 ug/L 1 8260tert-Butylbenzene98-06-6 01/13/16ND B6A1304

50 ug/L 1 8260tertiary Butyl Alcohol75-65-0 01/13/16ND B6A1304

5.0 ug/L 1 8260tertiaryAmylmethylether994-05-8 01/13/16ND B6A1304

1.0 ug/L 1 8260Tetrachloroethylene127-18-4 01/14/163.3 B6A1304

5.0 ug/L 1 8260Tetrahydrofuran109-99-9 01/13/16ND B6A1304

1.0 ug/L 1 8260Toluene108-88-3 01/13/16ND B6A1304

1.0 ug/L 1 8260trans-1,2-Dichloroethylene156-60-5 01/13/16ND B6A1304

1.0 ug/L 1 8260trans-1,3-Dichloropropylene10061-02-6 01/13/16ND B6A1304

5.0 ug/L 1 8260trans-1,4-Dichloro-2-butene110-57-6 01/13/16ND B6A1304

1.0 ug/L 1 8260Trichloroethylene79-01-6 01/13/16ND B6A1304

1.0 ug/L 1 8260Trichlorofluoromethane75-69-4 01/13/16ND B6A1304

1.0 ug/L 1 8260Vinyl chloride75-01-4 01/13/16ND B6A1304

85-11598.4 %Surrogate: Bromofluorobenzene 826001/13/16 B6A1304

82.7-115101 %Surrogate: Dibromofluoromethane 826001/13/16 B6A1304

85-115101 %Surrogate: Toluene-d8 826001/13/16 B6A1304

Lab Work Order # 1601052

Page 14 of 19Page 14 of 20

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1601052-07

RLCAS #

Client ID: GP14@35'

QC Batch

Organics-Volatiles

1.0 ug/L 1 82601,1,1,2-Tetrachloroethane630-20-6 01/13/16ND B6A1304

1.0 ug/L 1 82601,1,1-Trichloroethane71-55-6 01/13/16ND B6A1304

1.0 ug/L 1 82601,1,2,2-Tetrachloroethane79-34-5 01/13/16ND B6A1304

1.0 ug/L 1 82601,1,2-Trichloroethane79-00-5 01/13/16ND B6A1304

1.0 ug/L 1 82601,1-Dichloroethane75-34-3 01/13/16ND B6A1304

1.0 ug/L 1 82601,1-Dichloroethylene75-35-4 01/13/16ND B6A1304

5.0 ug/L 1 82601,2,3-Trichlorobenzene87-61-6 01/13/16ND B6A1304

1.0 ug/L 1 82601,2,3-Trichloropropane96-18-4 01/13/16ND B6A1304

1.0 ug/L 1 82601,2,3-Trimethylbenzene526-73-8 01/13/16ND B6A1304

5.0 ug/L 1 82601,2,4-Trichlorobenzene120-82-1 01/13/16ND B6A1304

1.0 ug/L 1 82601,2,4-Trimethylbenzene95-63-6 01/13/16ND B6A1304

5.0 ug/L 1 82601,2-Dibromo-3-chloropropane96-12-8 01/13/16ND B6A1304

1.0 ug/L 1 82601,2-Dibromoethane106-93-4 01/13/16ND B6A1304

1.0 ug/L 1 82601,2-Dichlorobenzene95-50-1 01/13/16ND B6A1304

1.0 ug/L 1 82601,2-Dichloroethane107-06-2 01/13/16ND B6A1304

1.0 ug/L 1 82601,2-Dichloropropane78-87-5 01/13/16ND B6A1304

1.0 ug/L 1 82601,3,5-Trimethylbenzene108-67-8 01/13/16ND B6A1304

1.0 ug/L 1 82601,3-Dichlorobenzene541-73-1 01/13/16ND B6A1304

1.0 ug/L 1 82601,4-Dichlorobenzene106-46-7 01/13/16ND B6A1304

5.0 ug/L 1 82602-Butanone (MEK)78-93-3 01/13/16ND B6A1304

5.0 ug/L 1 82602-Hexanone591-78-6 01/13/16ND B6A1304

5.0 Xug/L 1 82602-Methylnaphthalene91-57-6 01/13/16ND B6A1304

20 ug/L 1 82602-Propanone (acetone)67-64-1 01/13/16ND B6A1304

5.0 ug/L 1 82604-Methyl-2-pentanone (MIBK)108-10-1 01/13/16ND B6A1304

5.0 ug/L 1 8260Acrylonitrile107-13-1 01/13/16ND B6A1304

1.0 ug/L 1 8260Benzene71-43-2 01/13/16ND B6A1304

1.0 ug/L 1 8260Bromobenzene108-86-1 01/13/16ND B6A1304

1.0 ug/L 1 8260Bromochloromethane74-97-5 01/13/16ND B6A1304

1.0 ug/L 1 8260Bromodichloromethane75-27-4 01/13/16ND B6A1304

1.0 ug/L 1 8260Bromoform75-25-2 01/13/16ND B6A1304

5.0 ug/L 1 8260Bromomethane74-83-9 01/13/16ND B6A1304

1.0 ug/L 1 8260Carbon disulfide75-15-0 01/13/16ND B6A1304

1.0 ug/L 1 8260Carbon tetrachloride56-23-5 01/13/16ND B6A1304

1.0 ug/L 1 8260Chlorobenzene108-90-7 01/13/16ND B6A1304

5.0 ug/L 1 8260Chloroethane75-00-3 01/13/16ND B6A1304

1.0 ug/L 1 8260Chloroform67-66-3 01/13/16ND B6A1304

5.0 ug/L 1 8260Chloromethane74-87-3 01/13/16ND B6A1304

1.0 ug/L 1 8260cis-1,2-Dichloroethylene156-59-2 01/13/16ND B6A1304

1.0 ug/L 1 8260cis-1,3-Dichloropropylene10061-01-5 01/13/16ND B6A1304

5.0 ug/L 1 8260Cyclohexane110-82-7 01/13/16ND B6A1304

1.0 ug/L 1 8260Dibromochloromethane124-48-1 01/13/16ND B6A1304

Lab Work Order # 1601052

Page 15 of 19Page 15 of 20

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1601052-07

RLCAS #

Client ID: GP14@35'

QC Batch

Organics-Volatiles

1.0 ug/L 1 8260Dibromomethane74-95-3 01/13/16ND B6A1304

5.0 ug/L 1 8260Dichlorodifluoromethane75-71-8 01/13/16ND B6A1304

5.0 ug/L 1 8260Diethyl ether60-29-7 01/13/16ND B6A1304

5.0 ug/L 1 8260Diisopropyl Ether108-20-3 01/13/16ND B6A1304

1.0 ug/L 1 8260Ethylbenzene100-41-4 01/13/16ND B6A1304

5.0 ug/L 1 8260Ethyltertiarybutylether637-92-3 01/13/16ND B6A1304

5.0 ug/L 1 8260Hexachloroethane67-72-1 01/13/16ND B6A1304

1.0 ug/L 1 8260Isopropylbenzene98-82-8 01/13/16ND B6A1304

2.0 ug/L 1 8260m & p - Xylene1330-20-7 01/13/16ND B6A1304

1.0 ug/L 1 8260Methyl iodide74-88-4 01/13/16ND B6A1304

5.0 ug/L 1 8260Methylene chloride75-09-2 01/13/16ND B6A1304

1.0 ug/L 1 8260Methyltertiarybutylether1634-04-4 01/13/16ND B6A1304

5.0 Xug/L 1 8260Naphthalene91-20-3 01/13/16ND B6A1304

1.0 ug/L 1 8260n-Butylbenzene104-51-8 01/13/16ND B6A1304

1.0 ug/L 1 8260n-Propylbenzene103-65-1 01/13/16ND B6A1304

1.0 ug/L 1 8260o-Xylene95-47-6 01/13/16ND B6A1304

1.0 ug/L 1 8260p-Isopropyl toluene99-87-6 01/13/16ND B6A1304

1.0 ug/L 1 8260sec-Butylbenzene135-98-8 01/13/16ND B6A1304

1.0 ug/L 1 8260Styrene100-42-5 01/13/16ND B6A1304

1.0 ug/L 1 8260tert-Butylbenzene98-06-6 01/13/16ND B6A1304

50 ug/L 1 8260tertiary Butyl Alcohol75-65-0 01/13/16ND B6A1304

5.0 ug/L 1 8260tertiaryAmylmethylether994-05-8 01/13/16ND B6A1304

1.0 ug/L 1 8260Tetrachloroethylene127-18-4 01/14/164.7 B6A1304

5.0 ug/L 1 8260Tetrahydrofuran109-99-9 01/13/16ND B6A1304

1.0 ug/L 1 8260Toluene108-88-3 01/13/16ND B6A1304

1.0 ug/L 1 8260trans-1,2-Dichloroethylene156-60-5 01/13/16ND B6A1304

1.0 ug/L 1 8260trans-1,3-Dichloropropylene10061-02-6 01/13/16ND B6A1304

5.0 ug/L 1 8260trans-1,4-Dichloro-2-butene110-57-6 01/13/16ND B6A1304

1.0 ug/L 1 8260Trichloroethylene79-01-6 01/13/16ND B6A1304

1.0 ug/L 1 8260Trichlorofluoromethane75-69-4 01/13/16ND B6A1304

1.0 ug/L 1 8260Vinyl chloride75-01-4 01/13/16ND B6A1304

85-11598.3 %Surrogate: Bromofluorobenzene 826001/13/16 B6A1304

82.7-115103 %Surrogate: Dibromofluoromethane 826001/13/16 B6A1304

85-115102 %Surrogate: Toluene-d8 826001/13/16 B6A1304

Lab Work Order # 1601052

Page 16 of 19Page 16 of 20

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1601052-08

RLCAS #

Client ID: GP14@40'

QC Batch

Organics-Volatiles

1.0 ug/L 1 82601,1,1,2-Tetrachloroethane630-20-6 01/13/16ND B6A1304

1.0 ug/L 1 82601,1,1-Trichloroethane71-55-6 01/13/16ND B6A1304

1.0 ug/L 1 82601,1,2,2-Tetrachloroethane79-34-5 01/13/16ND B6A1304

1.0 ug/L 1 82601,1,2-Trichloroethane79-00-5 01/13/16ND B6A1304

1.0 ug/L 1 82601,1-Dichloroethane75-34-3 01/13/16ND B6A1304

1.0 ug/L 1 82601,1-Dichloroethylene75-35-4 01/13/16ND B6A1304

5.0 ug/L 1 82601,2,3-Trichlorobenzene87-61-6 01/13/16ND B6A1304

1.0 ug/L 1 82601,2,3-Trichloropropane96-18-4 01/13/16ND B6A1304

1.0 ug/L 1 82601,2,3-Trimethylbenzene526-73-8 01/13/16ND B6A1304

5.0 ug/L 1 82601,2,4-Trichlorobenzene120-82-1 01/13/16ND B6A1304

1.0 ug/L 1 82601,2,4-Trimethylbenzene95-63-6 01/13/16ND B6A1304

5.0 ug/L 1 82601,2-Dibromo-3-chloropropane96-12-8 01/13/16ND B6A1304

1.0 ug/L 1 82601,2-Dibromoethane106-93-4 01/13/16ND B6A1304

1.0 ug/L 1 82601,2-Dichlorobenzene95-50-1 01/13/16ND B6A1304

1.0 ug/L 1 82601,2-Dichloroethane107-06-2 01/13/16ND B6A1304

1.0 ug/L 1 82601,2-Dichloropropane78-87-5 01/13/16ND B6A1304

1.0 ug/L 1 82601,3,5-Trimethylbenzene108-67-8 01/13/16ND B6A1304

1.0 ug/L 1 82601,3-Dichlorobenzene541-73-1 01/13/16ND B6A1304

1.0 ug/L 1 82601,4-Dichlorobenzene106-46-7 01/13/16ND B6A1304

5.0 ug/L 1 82602-Butanone (MEK)78-93-3 01/13/16ND B6A1304

5.0 ug/L 1 82602-Hexanone591-78-6 01/13/16ND B6A1304

5.0 Xug/L 1 82602-Methylnaphthalene91-57-6 01/13/16ND B6A1304

20 ug/L 1 82602-Propanone (acetone)67-64-1 01/13/16ND B6A1304

5.0 ug/L 1 82604-Methyl-2-pentanone (MIBK)108-10-1 01/13/16ND B6A1304

5.0 ug/L 1 8260Acrylonitrile107-13-1 01/13/16ND B6A1304

1.0 ug/L 1 8260Benzene71-43-2 01/13/16ND B6A1304

1.0 ug/L 1 8260Bromobenzene108-86-1 01/13/16ND B6A1304

1.0 ug/L 1 8260Bromochloromethane74-97-5 01/13/16ND B6A1304

1.0 ug/L 1 8260Bromodichloromethane75-27-4 01/13/16ND B6A1304

1.0 ug/L 1 8260Bromoform75-25-2 01/13/16ND B6A1304

5.0 ug/L 1 8260Bromomethane74-83-9 01/13/16ND B6A1304

1.0 ug/L 1 8260Carbon disulfide75-15-0 01/13/16ND B6A1304

1.0 ug/L 1 8260Carbon tetrachloride56-23-5 01/13/16ND B6A1304

1.0 ug/L 1 8260Chlorobenzene108-90-7 01/13/16ND B6A1304

5.0 ug/L 1 8260Chloroethane75-00-3 01/13/16ND B6A1304

1.0 ug/L 1 8260Chloroform67-66-3 01/13/16ND B6A1304

5.0 ug/L 1 8260Chloromethane74-87-3 01/13/16ND B6A1304

1.0 ug/L 1 8260cis-1,2-Dichloroethylene156-59-2 01/13/16ND B6A1304

1.0 ug/L 1 8260cis-1,3-Dichloropropylene10061-01-5 01/13/16ND B6A1304

5.0 ug/L 1 8260Cyclohexane110-82-7 01/13/16ND B6A1304

1.0 ug/L 1 8260Dibromochloromethane124-48-1 01/13/16ND B6A1304

Lab Work Order # 1601052

Page 17 of 19Page 17 of 20

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1601052-08

RLCAS #

Client ID: GP14@40'

QC Batch

Organics-Volatiles

1.0 ug/L 1 8260Dibromomethane74-95-3 01/13/16ND B6A1304

5.0 ug/L 1 8260Dichlorodifluoromethane75-71-8 01/13/16ND B6A1304

5.0 ug/L 1 8260Diethyl ether60-29-7 01/13/16ND B6A1304

5.0 ug/L 1 8260Diisopropyl Ether108-20-3 01/13/16ND B6A1304

1.0 ug/L 1 8260Ethylbenzene100-41-4 01/13/16ND B6A1304

5.0 ug/L 1 8260Ethyltertiarybutylether637-92-3 01/13/16ND B6A1304

5.0 ug/L 1 8260Hexachloroethane67-72-1 01/13/16ND B6A1304

1.0 ug/L 1 8260Isopropylbenzene98-82-8 01/13/16ND B6A1304

2.0 ug/L 1 8260m & p - Xylene1330-20-7 01/13/16ND B6A1304

1.0 ug/L 1 8260Methyl iodide74-88-4 01/13/16ND B6A1304

5.0 ug/L 1 8260Methylene chloride75-09-2 01/13/16ND B6A1304

1.0 ug/L 1 8260Methyltertiarybutylether1634-04-4 01/13/16ND B6A1304

5.0 Xug/L 1 8260Naphthalene91-20-3 01/13/16ND B6A1304

1.0 ug/L 1 8260n-Butylbenzene104-51-8 01/13/16ND B6A1304

1.0 ug/L 1 8260n-Propylbenzene103-65-1 01/13/16ND B6A1304

1.0 ug/L 1 8260o-Xylene95-47-6 01/13/16ND B6A1304

1.0 ug/L 1 8260p-Isopropyl toluene99-87-6 01/13/16ND B6A1304

1.0 ug/L 1 8260sec-Butylbenzene135-98-8 01/13/16ND B6A1304

1.0 ug/L 1 8260Styrene100-42-5 01/13/16ND B6A1304

1.0 ug/L 1 8260tert-Butylbenzene98-06-6 01/13/16ND B6A1304

50 ug/L 1 8260tertiary Butyl Alcohol75-65-0 01/13/16ND B6A1304

5.0 ug/L 1 8260tertiaryAmylmethylether994-05-8 01/13/16ND B6A1304

1.0 ug/L 1 8260Tetrachloroethylene127-18-4 01/14/164.4 B6A1304

5.0 ug/L 1 8260Tetrahydrofuran109-99-9 01/13/16ND B6A1304

1.0 ug/L 1 8260Toluene108-88-3 01/13/16ND B6A1304

1.0 ug/L 1 8260trans-1,2-Dichloroethylene156-60-5 01/13/16ND B6A1304

1.0 ug/L 1 8260trans-1,3-Dichloropropylene10061-02-6 01/13/16ND B6A1304

5.0 ug/L 1 8260trans-1,4-Dichloro-2-butene110-57-6 01/13/16ND B6A1304

1.0 ug/L 1 8260Trichloroethylene79-01-6 01/13/16ND B6A1304

1.0 ug/L 1 8260Trichlorofluoromethane75-69-4 01/13/16ND B6A1304

1.0 ug/L 1 8260Vinyl chloride75-01-4 01/13/16ND B6A1304

85-11596.3 %Surrogate: Bromofluorobenzene 826001/13/16 B6A1304

82.7-115105 %Surrogate: Dibromofluoromethane 826001/13/16 B6A1304

85-115102 %Surrogate: Toluene-d8 826001/13/16 B6A1304

Lab Work Order # 1601052

Page 18 of 19Page 18 of 20

Page 19 of 20

Page 20 of 20

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

MDEQ-RRD-GRAND RAPIDS

RE: HALL STREET

Grand Rapids, MI 49503-2341

350 Ottawa Ave. NW, Unit 10

Abigail Hendershott

I certify that the analyses performed by the MDEQ Environmental Laboratory were conducted by methods

approved by the U.S. Environmental Protection Agency and other appropriate regulatory agencies .

Sincerely,

20 January 2016 Work Order: 1601033

Price: $1,840.00

George Krisztian

Laboratory Director

Lab Work Order # 1601033

Page 1 of 19Page 1 of 20

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

Project:

Project Manager:

Reported:

MDEQ-RRD-GRAND RAPIDS

350 Ottawa Ave. NW, Unit 10

Abigail Hendershott

HALL STREET

Grand Rapids MI, 49503-2341

Site Code: 4100112101/20/2016

Sample ID Laboratory ID Date SampledMatrix Date Received

Analytical Report for Samples

Qualifier

1601033-01 Water 01/12/2016GP11@40' 01/11/2016

1601033-02 Water 01/12/2016GP11@45' 01/11/2016

1601033-03 Water 01/12/2016GP11@50' 01/11/2016

1601033-04 Water 01/12/2016GP11@55' 01/11/2016

1601033-05 Water 01/12/2016GP12@25' 01/12/2016

1601033-06 Water 01/12/2016GP12@30' 01/12/2016

1601033-07 Water 01/12/2016GP12@35' 01/12/2016

1601033-08 Water 01/12/2016GP12@40' 01/12/2016

Notes and Definitions

X Methods 8260 & 624 are used to analyze volatile organics that have boiling points below 200 ºC. 2-Methylnaphthalene & naphthalene

have boiling points above 200 ºC and are better suited to analysis by methods 8270 & 625 as semivolatile organics.

T Reported value is less than the reporting limit (RL). Result is estimated.

A07 Result(s) and reporting limit(s) are estimated due to poor precision.

A06 Result is estimated due to high continuing calibration standard criteria failure.

A04 Result is estimated due to high matrix spike recovery.

Reporting LimitRL

Indicates compound analyzed for but not detectedND

Not ApplicableNA

Case Narrative

Priority Samples

Lab Work Order # 1601033

Page 2 of 19Page 2 of 20

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1601033-01

RLCAS #

Client ID: GP11@40'

QC Batch

Organics-Volatiles

1.0 ug/L 1 82601,1,1,2-Tetrachloroethane630-20-6 01/12/16ND B6A1205

1.0 ug/L 1 82601,1,1-Trichloroethane71-55-6 01/12/16ND B6A1205

1.0 ug/L 1 82601,1,2,2-Tetrachloroethane79-34-5 01/12/16ND B6A1205

1.0 ug/L 1 82601,1,2-Trichloroethane79-00-5 01/12/16ND B6A1205

1.0 ug/L 1 82601,1-Dichloroethane75-34-3 01/12/16ND B6A1205

1.0 ug/L 1 82601,1-Dichloroethylene75-35-4 01/12/16ND B6A1205

5.0 ug/L 1 82601,2,3-Trichlorobenzene87-61-6 01/12/16ND B6A1205

1.0 ug/L 1 82601,2,3-Trichloropropane96-18-4 01/12/16ND B6A1205

1.0 ug/L 1 82601,2,3-Trimethylbenzene526-73-8 01/12/16ND B6A1205

5.0 ug/L 1 82601,2,4-Trichlorobenzene120-82-1 01/12/16ND B6A1205

1.0 ug/L 1 82601,2,4-Trimethylbenzene95-63-6 01/12/16ND B6A1205

5.0 ug/L 1 82601,2-Dibromo-3-chloropropane96-12-8 01/12/16ND B6A1205

1.0 ug/L 1 82601,2-Dibromoethane106-93-4 01/12/16ND B6A1205

1.0 ug/L 1 82601,2-Dichlorobenzene95-50-1 01/12/16ND B6A1205

1.0 ug/L 1 82601,2-Dichloroethane107-06-2 01/12/16ND B6A1205

1.0 ug/L 1 82601,2-Dichloropropane78-87-5 01/12/16ND B6A1205

1.0 ug/L 1 82601,3,5-Trimethylbenzene108-67-8 01/12/16ND B6A1205

1.0 ug/L 1 82601,3-Dichlorobenzene541-73-1 01/12/16ND B6A1205

1.0 ug/L 1 82601,4-Dichlorobenzene106-46-7 01/12/16ND B6A1205

5.0 ug/L 1 82602-Butanone (MEK)78-93-3 01/12/16ND B6A1205

5.0 ug/L 1 82602-Hexanone591-78-6 01/12/16ND B6A1205

5.0 Xug/L 1 82602-Methylnaphthalene91-57-6 01/12/16ND B6A1205

20 ug/L 1 82602-Propanone (acetone)67-64-1 01/12/16ND B6A1205

5.0 ug/L 1 82604-Methyl-2-pentanone (MIBK)108-10-1 01/12/16ND B6A1205

5.0 ug/L 1 8260Acrylonitrile107-13-1 01/12/16ND B6A1205

1.0 ug/L 1 8260Benzene71-43-2 01/12/16ND B6A1205

1.0 ug/L 1 8260Bromobenzene108-86-1 01/12/16ND B6A1205

1.0 ug/L 1 8260Bromochloromethane74-97-5 01/12/16ND B6A1205

1.0 ug/L 1 8260Bromodichloromethane75-27-4 01/12/16ND B6A1205

1.0 ug/L 1 8260Bromoform75-25-2 01/12/16ND B6A1205

5.0 ug/L 1 8260Bromomethane74-83-9 01/12/16ND B6A1205

1.0 ug/L 1 8260Carbon disulfide75-15-0 01/12/16ND B6A1205

1.0 ug/L 1 8260Carbon tetrachloride56-23-5 01/12/16ND B6A1205

1.0 ug/L 1 8260Chlorobenzene108-90-7 01/12/16ND B6A1205

5.0 ug/L 1 8260Chloroethane75-00-3 01/12/16ND B6A1205

1.0 ug/L 1 8260Chloroform67-66-3 01/12/162.0 B6A1205

5.0 ug/L 1 8260Chloromethane74-87-3 01/12/16ND B6A1205

1.0 ug/L 1 8260cis-1,2-Dichloroethylene156-59-2 01/12/16ND B6A1205

1.0 ug/L 1 8260cis-1,3-Dichloropropylene10061-01-5 01/12/16ND B6A1205

5.0 ug/L 1 8260Cyclohexane110-82-7 01/12/16ND B6A1205

1.0 ug/L 1 8260Dibromochloromethane124-48-1 01/12/16ND B6A1205

Lab Work Order # 1601033

Page 3 of 19Page 3 of 20

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1601033-01

RLCAS #

Client ID: GP11@40'

QC Batch

Organics-Volatiles

1.0 ug/L 1 8260Dibromomethane74-95-3 01/12/16ND B6A1205

5.0 ug/L 1 8260Dichlorodifluoromethane75-71-8 01/12/16ND B6A1205

5.0 ug/L 1 8260Diethyl ether60-29-7 01/12/16ND B6A1205

5.0 ug/L 1 8260Diisopropyl Ether108-20-3 01/12/16ND B6A1205

1.0 ug/L 1 8260Ethylbenzene100-41-4 01/12/16ND B6A1205

5.0 ug/L 1 8260Ethyltertiarybutylether637-92-3 01/12/16ND B6A1205

5.0 ug/L 1 8260Hexachloroethane67-72-1 01/12/16ND B6A1205

1.0 ug/L 1 8260Isopropylbenzene98-82-8 01/12/16ND B6A1205

2.0 ug/L 1 8260m & p - Xylene1330-20-7 01/12/16ND B6A1205

1.0 ug/L 1 8260Methyl iodide74-88-4 01/12/16ND B6A1205

5.0 ug/L 1 8260Methylene chloride75-09-2 01/12/16ND B6A1205

1.0 ug/L 1 8260Methyltertiarybutylether1634-04-4 01/12/16ND B6A1205

5.0 Xug/L 1 8260Naphthalene91-20-3 01/12/16ND B6A1205

1.0 ug/L 1 8260n-Butylbenzene104-51-8 01/12/16ND B6A1205

1.0 ug/L 1 8260n-Propylbenzene103-65-1 01/12/16ND B6A1205

1.0 ug/L 1 8260o-Xylene95-47-6 01/12/16ND B6A1205

1.0 ug/L 1 8260p-Isopropyl toluene99-87-6 01/12/16ND B6A1205

1.0 ug/L 1 8260sec-Butylbenzene135-98-8 01/12/16ND B6A1205

1.0 ug/L 1 8260Styrene100-42-5 01/12/16ND B6A1205

1.0 ug/L 1 8260tert-Butylbenzene98-06-6 01/12/16ND B6A1205

50 ug/L 1 8260tertiary Butyl Alcohol75-65-0 01/12/16ND B6A1205

5.0 ug/L 1 8260tertiaryAmylmethylether994-05-8 01/12/16ND B6A1205

1.0 ug/L 1 8260Tetrachloroethylene127-18-4 01/12/16ND B6A1205

5.0 ug/L 1 8260Tetrahydrofuran109-99-9 01/12/16ND B6A1205

1.0 ug/L 1 8260Toluene108-88-3 01/12/16ND B6A1205

1.0 ug/L 1 8260trans-1,2-Dichloroethylene156-60-5 01/12/16ND B6A1205

1.0 ug/L 1 8260trans-1,3-Dichloropropylene10061-02-6 01/12/16ND B6A1205

5.0 ug/L 1 8260trans-1,4-Dichloro-2-butene110-57-6 01/12/16ND B6A1205

1.0 ug/L 1 8260Trichloroethylene79-01-6 01/12/16ND B6A1205

1.0 ug/L 1 8260Trichlorofluoromethane75-69-4 01/12/16ND B6A1205

1.0 ug/L 1 8260Vinyl chloride75-01-4 01/12/16ND B6A1205

85-115102 %Surrogate: Bromofluorobenzene 826001/12/16 B6A1205

82.7-115101 %Surrogate: Dibromofluoromethane 826001/12/16 B6A1205

85-115101 %Surrogate: Toluene-d8 826001/12/16 B6A1205

Lab Work Order # 1601033

Page 4 of 19Page 4 of 20

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1601033-02

RLCAS #

Client ID: GP11@45'

QC Batch

Organics-Volatiles

1.0 ug/L 1 82601,1,1,2-Tetrachloroethane630-20-6 01/12/16ND B6A1205

1.0 ug/L 1 82601,1,1-Trichloroethane71-55-6 01/12/16ND B6A1205

1.0 ug/L 1 82601,1,2,2-Tetrachloroethane79-34-5 01/12/16ND B6A1205

1.0 ug/L 1 82601,1,2-Trichloroethane79-00-5 01/12/16ND B6A1205

1.0 ug/L 1 82601,1-Dichloroethane75-34-3 01/12/16ND B6A1205

1.0 ug/L 1 82601,1-Dichloroethylene75-35-4 01/12/16ND B6A1205

5.0 ug/L 1 82601,2,3-Trichlorobenzene87-61-6 01/12/16ND B6A1205

1.0 ug/L 1 82601,2,3-Trichloropropane96-18-4 01/12/16ND B6A1205

1.0 ug/L 1 82601,2,3-Trimethylbenzene526-73-8 01/12/16ND B6A1205

5.0 ug/L 1 82601,2,4-Trichlorobenzene120-82-1 01/12/16ND B6A1205

1.0 ug/L 1 82601,2,4-Trimethylbenzene95-63-6 01/12/16ND B6A1205

5.0 ug/L 1 82601,2-Dibromo-3-chloropropane96-12-8 01/12/16ND B6A1205

1.0 ug/L 1 82601,2-Dibromoethane106-93-4 01/12/16ND B6A1205

1.0 ug/L 1 82601,2-Dichlorobenzene95-50-1 01/12/16ND B6A1205

1.0 ug/L 1 82601,2-Dichloroethane107-06-2 01/12/16ND B6A1205

1.0 ug/L 1 82601,2-Dichloropropane78-87-5 01/12/16ND B6A1205

1.0 ug/L 1 82601,3,5-Trimethylbenzene108-67-8 01/12/16ND B6A1205

1.0 ug/L 1 82601,3-Dichlorobenzene541-73-1 01/12/16ND B6A1205

1.0 ug/L 1 82601,4-Dichlorobenzene106-46-7 01/12/16ND B6A1205

5.0 ug/L 1 82602-Butanone (MEK)78-93-3 01/12/16ND B6A1205

5.0 ug/L 1 82602-Hexanone591-78-6 01/12/16ND B6A1205

5.0 Xug/L 1 82602-Methylnaphthalene91-57-6 01/12/16ND B6A1205

20 ug/L 1 82602-Propanone (acetone)67-64-1 01/12/16ND B6A1205

5.0 ug/L 1 82604-Methyl-2-pentanone (MIBK)108-10-1 01/12/16ND B6A1205

5.0 ug/L 1 8260Acrylonitrile107-13-1 01/12/16ND B6A1205

1.0 ug/L 1 8260Benzene71-43-2 01/12/16ND B6A1205

1.0 ug/L 1 8260Bromobenzene108-86-1 01/12/16ND B6A1205

1.0 ug/L 1 8260Bromochloromethane74-97-5 01/12/16ND B6A1205

1.0 ug/L 1 8260Bromodichloromethane75-27-4 01/12/16ND B6A1205

1.0 ug/L 1 8260Bromoform75-25-2 01/12/16ND B6A1205

5.0 ug/L 1 8260Bromomethane74-83-9 01/12/16ND B6A1205

1.0 ug/L 1 8260Carbon disulfide75-15-0 01/12/16ND B6A1205

1.0 ug/L 1 8260Carbon tetrachloride56-23-5 01/12/16ND B6A1205

1.0 ug/L 1 8260Chlorobenzene108-90-7 01/12/16ND B6A1205

5.0 ug/L 1 8260Chloroethane75-00-3 01/12/16ND B6A1205

1.0 ug/L 1 8260Chloroform67-66-3 01/12/161.8 B6A1205

5.0 ug/L 1 8260Chloromethane74-87-3 01/12/16ND B6A1205

1.0 ug/L 1 8260cis-1,2-Dichloroethylene156-59-2 01/12/16ND B6A1205

1.0 ug/L 1 8260cis-1,3-Dichloropropylene10061-01-5 01/12/16ND B6A1205

5.0 ug/L 1 8260Cyclohexane110-82-7 01/12/16ND B6A1205

1.0 ug/L 1 8260Dibromochloromethane124-48-1 01/12/16ND B6A1205

Lab Work Order # 1601033

Page 5 of 19Page 5 of 20

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1601033-02

RLCAS #

Client ID: GP11@45'

QC Batch

Organics-Volatiles

1.0 ug/L 1 8260Dibromomethane74-95-3 01/12/16ND B6A1205

5.0 ug/L 1 8260Dichlorodifluoromethane75-71-8 01/12/16ND B6A1205

5.0 ug/L 1 8260Diethyl ether60-29-7 01/12/16ND B6A1205

5.0 ug/L 1 8260Diisopropyl Ether108-20-3 01/12/16ND B6A1205

1.0 ug/L 1 8260Ethylbenzene100-41-4 01/12/16ND B6A1205

5.0 ug/L 1 8260Ethyltertiarybutylether637-92-3 01/12/16ND B6A1205

5.0 ug/L 1 8260Hexachloroethane67-72-1 01/12/16ND B6A1205

1.0 ug/L 1 8260Isopropylbenzene98-82-8 01/12/16ND B6A1205

2.0 ug/L 1 8260m & p - Xylene1330-20-7 01/12/16ND B6A1205

1.0 ug/L 1 8260Methyl iodide74-88-4 01/12/16ND B6A1205

5.0 ug/L 1 8260Methylene chloride75-09-2 01/12/16ND B6A1205

1.0 ug/L 1 8260Methyltertiarybutylether1634-04-4 01/12/16ND B6A1205

5.0 Xug/L 1 8260Naphthalene91-20-3 01/12/16ND B6A1205

1.0 ug/L 1 8260n-Butylbenzene104-51-8 01/12/16ND B6A1205

1.0 ug/L 1 8260n-Propylbenzene103-65-1 01/12/16ND B6A1205

1.0 ug/L 1 8260o-Xylene95-47-6 01/12/16ND B6A1205

1.0 ug/L 1 8260p-Isopropyl toluene99-87-6 01/12/16ND B6A1205

1.0 ug/L 1 8260sec-Butylbenzene135-98-8 01/12/16ND B6A1205

1.0 ug/L 1 8260Styrene100-42-5 01/12/16ND B6A1205

1.0 ug/L 1 8260tert-Butylbenzene98-06-6 01/12/16ND B6A1205

50 ug/L 1 8260tertiary Butyl Alcohol75-65-0 01/12/16ND B6A1205

5.0 ug/L 1 8260tertiaryAmylmethylether994-05-8 01/12/16ND B6A1205

1.0 ug/L 1 8260Tetrachloroethylene127-18-4 01/12/16ND B6A1205

5.0 ug/L 1 8260Tetrahydrofuran109-99-9 01/12/16ND B6A1205

1.0 ug/L 1 8260Toluene108-88-3 01/12/16ND B6A1205

1.0 ug/L 1 8260trans-1,2-Dichloroethylene156-60-5 01/12/16ND B6A1205

1.0 ug/L 1 8260trans-1,3-Dichloropropylene10061-02-6 01/12/16ND B6A1205

5.0 ug/L 1 8260trans-1,4-Dichloro-2-butene110-57-6 01/12/16ND B6A1205

1.0 ug/L 1 8260Trichloroethylene79-01-6 01/12/16ND B6A1205

1.0 ug/L 1 8260Trichlorofluoromethane75-69-4 01/12/16ND B6A1205

1.0 ug/L 1 8260Vinyl chloride75-01-4 01/12/16ND B6A1205

85-11599.4 %Surrogate: Bromofluorobenzene 826001/12/16 B6A1205

82.7-115102 %Surrogate: Dibromofluoromethane 826001/12/16 B6A1205

85-115100 %Surrogate: Toluene-d8 826001/12/16 B6A1205

Lab Work Order # 1601033

Page 6 of 19Page 6 of 20

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1601033-03

RLCAS #

Client ID: GP11@50'

QC Batch

Organics-Volatiles

1.0 ug/L 1 82601,1,1,2-Tetrachloroethane630-20-6 01/12/16ND B6A1205

1.0 ug/L 1 82601,1,1-Trichloroethane71-55-6 01/12/16ND B6A1205

1.0 ug/L 1 82601,1,2,2-Tetrachloroethane79-34-5 01/12/16ND B6A1205

1.0 ug/L 1 82601,1,2-Trichloroethane79-00-5 01/12/16ND B6A1205

1.0 ug/L 1 82601,1-Dichloroethane75-34-3 01/12/16ND B6A1205

1.0 ug/L 1 82601,1-Dichloroethylene75-35-4 01/12/16ND B6A1205

5.0 ug/L 1 82601,2,3-Trichlorobenzene87-61-6 01/12/16ND B6A1205

1.0 ug/L 1 82601,2,3-Trichloropropane96-18-4 01/12/16ND B6A1205

1.0 ug/L 1 82601,2,3-Trimethylbenzene526-73-8 01/12/16ND B6A1205

5.0 ug/L 1 82601,2,4-Trichlorobenzene120-82-1 01/12/16ND B6A1205

1.0 ug/L 1 82601,2,4-Trimethylbenzene95-63-6 01/12/16ND B6A1205

5.0 ug/L 1 82601,2-Dibromo-3-chloropropane96-12-8 01/12/16ND B6A1205

1.0 ug/L 1 82601,2-Dibromoethane106-93-4 01/12/16ND B6A1205

1.0 ug/L 1 82601,2-Dichlorobenzene95-50-1 01/12/16ND B6A1205

1.0 ug/L 1 82601,2-Dichloroethane107-06-2 01/12/16ND B6A1205

1.0 ug/L 1 82601,2-Dichloropropane78-87-5 01/12/16ND B6A1205

1.0 ug/L 1 82601,3,5-Trimethylbenzene108-67-8 01/12/16ND B6A1205

1.0 ug/L 1 82601,3-Dichlorobenzene541-73-1 01/12/16ND B6A1205

1.0 ug/L 1 82601,4-Dichlorobenzene106-46-7 01/12/16ND B6A1205

5.0 ug/L 1 82602-Butanone (MEK)78-93-3 01/12/16ND B6A1205

5.0 ug/L 1 82602-Hexanone591-78-6 01/12/16ND B6A1205

5.0 Xug/L 1 82602-Methylnaphthalene91-57-6 01/12/16ND B6A1205

20 ug/L 1 82602-Propanone (acetone)67-64-1 01/12/16ND B6A1205

5.0 ug/L 1 82604-Methyl-2-pentanone (MIBK)108-10-1 01/12/16ND B6A1205

5.0 ug/L 1 8260Acrylonitrile107-13-1 01/12/16ND B6A1205

1.0 ug/L 1 8260Benzene71-43-2 01/12/16ND B6A1205

1.0 ug/L 1 8260Bromobenzene108-86-1 01/12/16ND B6A1205

1.0 ug/L 1 8260Bromochloromethane74-97-5 01/12/16ND B6A1205

1.0 ug/L 1 8260Bromodichloromethane75-27-4 01/12/16ND B6A1205

1.0 ug/L 1 8260Bromoform75-25-2 01/12/16ND B6A1205

5.0 ug/L 1 8260Bromomethane74-83-9 01/12/16ND B6A1205

1.0 ug/L 1 8260Carbon disulfide75-15-0 01/12/16ND B6A1205

1.0 ug/L 1 8260Carbon tetrachloride56-23-5 01/12/16ND B6A1205

1.0 ug/L 1 8260Chlorobenzene108-90-7 01/12/16ND B6A1205

5.0 ug/L 1 8260Chloroethane75-00-3 01/12/16ND B6A1205

1.0 ug/L 1 8260Chloroform67-66-3 01/12/162.0 B6A1205

5.0 ug/L 1 8260Chloromethane74-87-3 01/12/16ND B6A1205

1.0 ug/L 1 8260cis-1,2-Dichloroethylene156-59-2 01/12/16ND B6A1205

1.0 ug/L 1 8260cis-1,3-Dichloropropylene10061-01-5 01/12/16ND B6A1205

5.0 ug/L 1 8260Cyclohexane110-82-7 01/12/16ND B6A1205

1.0 ug/L 1 8260Dibromochloromethane124-48-1 01/12/16ND B6A1205

Lab Work Order # 1601033

Page 7 of 19Page 7 of 20

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1601033-03

RLCAS #

Client ID: GP11@50'

QC Batch

Organics-Volatiles

1.0 ug/L 1 8260Dibromomethane74-95-3 01/12/16ND B6A1205

5.0 ug/L 1 8260Dichlorodifluoromethane75-71-8 01/12/16ND B6A1205

5.0 ug/L 1 8260Diethyl ether60-29-7 01/12/16ND B6A1205

5.0 ug/L 1 8260Diisopropyl Ether108-20-3 01/12/16ND B6A1205

1.0 ug/L 1 8260Ethylbenzene100-41-4 01/12/16ND B6A1205

5.0 ug/L 1 8260Ethyltertiarybutylether637-92-3 01/12/16ND B6A1205

5.0 ug/L 1 8260Hexachloroethane67-72-1 01/12/16ND B6A1205

1.0 ug/L 1 8260Isopropylbenzene98-82-8 01/12/16ND B6A1205

2.0 ug/L 1 8260m & p - Xylene1330-20-7 01/12/16ND B6A1205

1.0 ug/L 1 8260Methyl iodide74-88-4 01/12/16ND B6A1205

5.0 ug/L 1 8260Methylene chloride75-09-2 01/12/16ND B6A1205

1.0 ug/L 1 8260Methyltertiarybutylether1634-04-4 01/12/16ND B6A1205

5.0 Xug/L 1 8260Naphthalene91-20-3 01/12/16ND B6A1205

1.0 ug/L 1 8260n-Butylbenzene104-51-8 01/12/16ND B6A1205

1.0 ug/L 1 8260n-Propylbenzene103-65-1 01/12/16ND B6A1205

1.0 ug/L 1 8260o-Xylene95-47-6 01/12/16ND B6A1205

1.0 ug/L 1 8260p-Isopropyl toluene99-87-6 01/12/16ND B6A1205

1.0 ug/L 1 8260sec-Butylbenzene135-98-8 01/12/16ND B6A1205

1.0 ug/L 1 8260Styrene100-42-5 01/12/16ND B6A1205

1.0 ug/L 1 8260tert-Butylbenzene98-06-6 01/12/16ND B6A1205

50 ug/L 1 8260tertiary Butyl Alcohol75-65-0 01/12/16ND B6A1205

5.0 ug/L 1 8260tertiaryAmylmethylether994-05-8 01/12/16ND B6A1205

1.0 ug/L 1 8260Tetrachloroethylene127-18-4 01/12/16ND B6A1205

5.0 ug/L 1 8260Tetrahydrofuran109-99-9 01/12/16ND B6A1205

1.0 ug/L 1 8260Toluene108-88-3 01/12/16ND B6A1205

1.0 ug/L 1 8260trans-1,2-Dichloroethylene156-60-5 01/12/16ND B6A1205

1.0 ug/L 1 8260trans-1,3-Dichloropropylene10061-02-6 01/12/16ND B6A1205

5.0 ug/L 1 8260trans-1,4-Dichloro-2-butene110-57-6 01/12/16ND B6A1205

1.0 ug/L 1 8260Trichloroethylene79-01-6 01/12/16ND B6A1205

1.0 ug/L 1 8260Trichlorofluoromethane75-69-4 01/12/16ND B6A1205

1.0 ug/L 1 8260Vinyl chloride75-01-4 01/12/16ND B6A1205

85-115103 %Surrogate: Bromofluorobenzene 826001/12/16 B6A1205

82.7-11599.2 %Surrogate: Dibromofluoromethane 826001/12/16 B6A1205

85-115101 %Surrogate: Toluene-d8 826001/12/16 B6A1205

Lab Work Order # 1601033

Page 8 of 19Page 8 of 20

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1601033-04

RLCAS #

Client ID: GP11@55'

QC Batch

Organics-Volatiles

1.0 ug/L 1 82601,1,1,2-Tetrachloroethane630-20-6 01/12/16ND B6A1205

1.0 ug/L 1 82601,1,1-Trichloroethane71-55-6 01/12/16ND B6A1205

1.0 ug/L 1 82601,1,2,2-Tetrachloroethane79-34-5 01/12/16ND B6A1205

1.0 ug/L 1 82601,1,2-Trichloroethane79-00-5 01/12/16ND B6A1205

1.0 ug/L 1 82601,1-Dichloroethane75-34-3 01/12/16ND B6A1205

1.0 ug/L 1 82601,1-Dichloroethylene75-35-4 01/12/16ND B6A1205

5.0 ug/L 1 82601,2,3-Trichlorobenzene87-61-6 01/12/16ND B6A1205

1.0 ug/L 1 82601,2,3-Trichloropropane96-18-4 01/12/16ND B6A1205

1.0 ug/L 1 82601,2,3-Trimethylbenzene526-73-8 01/12/16ND B6A1205

5.0 ug/L 1 82601,2,4-Trichlorobenzene120-82-1 01/12/16ND B6A1205

1.0 ug/L 1 82601,2,4-Trimethylbenzene95-63-6 01/12/16ND B6A1205

5.0 ug/L 1 82601,2-Dibromo-3-chloropropane96-12-8 01/12/16ND B6A1205

1.0 ug/L 1 82601,2-Dibromoethane106-93-4 01/12/16ND B6A1205

1.0 ug/L 1 82601,2-Dichlorobenzene95-50-1 01/12/16ND B6A1205

1.0 ug/L 1 82601,2-Dichloroethane107-06-2 01/12/16ND B6A1205

1.0 ug/L 1 82601,2-Dichloropropane78-87-5 01/12/16ND B6A1205

1.0 ug/L 1 82601,3,5-Trimethylbenzene108-67-8 01/12/16ND B6A1205

1.0 ug/L 1 82601,3-Dichlorobenzene541-73-1 01/12/16ND B6A1205

1.0 ug/L 1 82601,4-Dichlorobenzene106-46-7 01/12/16ND B6A1205

5.0 ug/L 1 82602-Butanone (MEK)78-93-3 01/12/16ND B6A1205

5.0 ug/L 1 82602-Hexanone591-78-6 01/12/16ND B6A1205

5.0 Xug/L 1 82602-Methylnaphthalene91-57-6 01/12/16ND B6A1205

20 ug/L 1 82602-Propanone (acetone)67-64-1 01/12/16ND B6A1205

5.0 ug/L 1 82604-Methyl-2-pentanone (MIBK)108-10-1 01/12/16ND B6A1205

5.0 ug/L 1 8260Acrylonitrile107-13-1 01/12/16ND B6A1205

1.0 ug/L 1 8260Benzene71-43-2 01/12/16ND B6A1205

1.0 ug/L 1 8260Bromobenzene108-86-1 01/12/16ND B6A1205

1.0 ug/L 1 8260Bromochloromethane74-97-5 01/12/16ND B6A1205

1.0 ug/L 1 8260Bromodichloromethane75-27-4 01/12/16ND B6A1205

1.0 ug/L 1 8260Bromoform75-25-2 01/12/16ND B6A1205

5.0 ug/L 1 8260Bromomethane74-83-9 01/12/16ND B6A1205

1.0 ug/L 1 8260Carbon disulfide75-15-0 01/12/16ND B6A1205

1.0 ug/L 1 8260Carbon tetrachloride56-23-5 01/12/16ND B6A1205

1.0 ug/L 1 8260Chlorobenzene108-90-7 01/12/16ND B6A1205

5.0 ug/L 1 8260Chloroethane75-00-3 01/12/16ND B6A1205

1.0 ug/L 1 8260Chloroform67-66-3 01/12/161.2 B6A1205

5.0 ug/L 1 8260Chloromethane74-87-3 01/12/16ND B6A1205

1.0 ug/L 1 8260cis-1,2-Dichloroethylene156-59-2 01/12/16ND B6A1205

1.0 ug/L 1 8260cis-1,3-Dichloropropylene10061-01-5 01/12/16ND B6A1205

5.0 ug/L 1 8260Cyclohexane110-82-7 01/12/16ND B6A1205

1.0 ug/L 1 8260Dibromochloromethane124-48-1 01/12/16ND B6A1205

Lab Work Order # 1601033

Page 9 of 19Page 9 of 20

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1601033-04

RLCAS #

Client ID: GP11@55'

QC Batch

Organics-Volatiles

1.0 ug/L 1 8260Dibromomethane74-95-3 01/12/16ND B6A1205

5.0 ug/L 1 8260Dichlorodifluoromethane75-71-8 01/12/16ND B6A1205

5.0 ug/L 1 8260Diethyl ether60-29-7 01/12/16ND B6A1205

5.0 ug/L 1 8260Diisopropyl Ether108-20-3 01/12/16ND B6A1205

1.0 ug/L 1 8260Ethylbenzene100-41-4 01/12/16ND B6A1205

5.0 ug/L 1 8260Ethyltertiarybutylether637-92-3 01/12/16ND B6A1205

5.0 ug/L 1 8260Hexachloroethane67-72-1 01/12/16ND B6A1205

1.0 ug/L 1 8260Isopropylbenzene98-82-8 01/12/16ND B6A1205

2.0 ug/L 1 8260m & p - Xylene1330-20-7 01/12/16ND B6A1205

1.0 ug/L 1 8260Methyl iodide74-88-4 01/12/16ND B6A1205

5.0 ug/L 1 8260Methylene chloride75-09-2 01/12/16ND B6A1205

1.0 ug/L 1 8260Methyltertiarybutylether1634-04-4 01/12/16ND B6A1205

5.0 Xug/L 1 8260Naphthalene91-20-3 01/12/16ND B6A1205

1.0 ug/L 1 8260n-Butylbenzene104-51-8 01/12/16ND B6A1205

1.0 ug/L 1 8260n-Propylbenzene103-65-1 01/12/16ND B6A1205

1.0 ug/L 1 8260o-Xylene95-47-6 01/12/16ND B6A1205

1.0 ug/L 1 8260p-Isopropyl toluene99-87-6 01/12/16ND B6A1205

1.0 ug/L 1 8260sec-Butylbenzene135-98-8 01/12/16ND B6A1205

1.0 ug/L 1 8260Styrene100-42-5 01/12/16ND B6A1205

1.0 ug/L 1 8260tert-Butylbenzene98-06-6 01/12/16ND B6A1205

50 ug/L 1 8260tertiary Butyl Alcohol75-65-0 01/12/16ND B6A1205

5.0 ug/L 1 8260tertiaryAmylmethylether994-05-8 01/12/16ND B6A1205

1.0 ug/L 1 8260Tetrachloroethylene127-18-4 01/12/16ND B6A1205

5.0 ug/L 1 8260Tetrahydrofuran109-99-9 01/12/16ND B6A1205

1.0 ug/L 1 8260Toluene108-88-3 01/12/16ND B6A1205

1.0 ug/L 1 8260trans-1,2-Dichloroethylene156-60-5 01/12/16ND B6A1205

1.0 ug/L 1 8260trans-1,3-Dichloropropylene10061-02-6 01/12/16ND B6A1205

5.0 ug/L 1 8260trans-1,4-Dichloro-2-butene110-57-6 01/12/16ND B6A1205

1.0 ug/L 1 8260Trichloroethylene79-01-6 01/12/16ND B6A1205

1.0 ug/L 1 8260Trichlorofluoromethane75-69-4 01/12/16ND B6A1205

1.0 ug/L 1 8260Vinyl chloride75-01-4 01/12/16ND B6A1205

85-115101 %Surrogate: Bromofluorobenzene 826001/12/16 B6A1205

82.7-115101 %Surrogate: Dibromofluoromethane 826001/12/16 B6A1205

85-115100 %Surrogate: Toluene-d8 826001/12/16 B6A1205

Lab Work Order # 1601033

Page 10 of 19Page 10 of 20

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1601033-05

RLCAS #

Client ID: GP12@25'

QC Batch

Organics-Volatiles

20 ug/L 20 82601,1,1,2-Tetrachloroethane630-20-6 01/13/16ND B6A1302

20 ug/L 20 82601,1,1-Trichloroethane71-55-6 01/13/16ND B6A1302

20 ug/L 20 82601,1,2,2-Tetrachloroethane79-34-5 01/13/16ND B6A1302

20 ug/L 20 82601,1,2-Trichloroethane79-00-5 01/13/16ND B6A1302

20 ug/L 20 82601,1-Dichloroethane75-34-3 01/13/16ND B6A1302

20 ug/L 20 82601,1-Dichloroethylene75-35-4 01/13/16ND B6A1302

100 ug/L 20 82601,2,3-Trichlorobenzene87-61-6 01/13/16ND B6A1302

20 ug/L 20 82601,2,3-Trichloropropane96-18-4 01/13/16ND B6A1302

20 ug/L 20 82601,2,3-Trimethylbenzene526-73-8 01/13/16ND B6A1302

100 ug/L 20 82601,2,4-Trichlorobenzene120-82-1 01/13/16ND B6A1302

20 ug/L 20 82601,2,4-Trimethylbenzene95-63-6 01/13/16ND B6A1302

100 ug/L 20 82601,2-Dibromo-3-chloropropane96-12-8 01/13/16ND B6A1302

20 ug/L 20 82601,2-Dibromoethane106-93-4 01/13/16ND B6A1302

20 ug/L 20 82601,2-Dichlorobenzene95-50-1 01/13/16ND B6A1302

20 ug/L 20 82601,2-Dichloroethane107-06-2 01/13/16ND B6A1302

20 ug/L 20 82601,2-Dichloropropane78-87-5 01/13/16ND B6A1302

20 ug/L 20 82601,3,5-Trimethylbenzene108-67-8 01/13/16ND B6A1302

20 ug/L 20 82601,3-Dichlorobenzene541-73-1 01/13/16ND B6A1302

20 ug/L 20 82601,4-Dichlorobenzene106-46-7 01/13/16ND B6A1302

100 ug/L 20 82602-Butanone (MEK)78-93-3 01/13/16ND B6A1302

100 ug/L 20 82602-Hexanone591-78-6 01/13/16ND B6A1302

100 A07, Xug/L 20 82602-Methylnaphthalene91-57-6 01/13/16ND B6A1302

400 ug/L 20 82602-Propanone (acetone)67-64-1 01/13/16ND B6A1302

100 ug/L 20 82604-Methyl-2-pentanone (MIBK)108-10-1 01/13/16ND B6A1302

100 ug/L 20 8260Acrylonitrile107-13-1 01/13/16ND B6A1302

20 ug/L 20 8260Benzene71-43-2 01/13/16ND B6A1302

20 ug/L 20 8260Bromobenzene108-86-1 01/13/16ND B6A1302

20 ug/L 20 8260Bromochloromethane74-97-5 01/13/16ND B6A1302

20 ug/L 20 8260Bromodichloromethane75-27-4 01/13/16ND B6A1302

20 ug/L 20 8260Bromoform75-25-2 01/13/16ND B6A1302

100 ug/L 20 8260Bromomethane74-83-9 01/13/16ND B6A1302

20 ug/L 20 8260Carbon disulfide75-15-0 01/13/16ND B6A1302

20 ug/L 20 8260Carbon tetrachloride56-23-5 01/13/16ND B6A1302

20 ug/L 20 8260Chlorobenzene108-90-7 01/13/16ND B6A1302

100 ug/L 20 8260Chloroethane75-00-3 01/13/16ND B6A1302

20 ug/L 20 8260Chloroform67-66-3 01/13/16ND B6A1302

100 ug/L 20 8260Chloromethane74-87-3 01/13/16ND B6A1302

20 ug/L 20 8260cis-1,2-Dichloroethylene156-59-2 01/13/1661 B6A1302

20 ug/L 20 8260cis-1,3-Dichloropropylene10061-01-5 01/13/16ND B6A1302

100 ug/L 20 8260Cyclohexane110-82-7 01/13/16ND B6A1302

20 ug/L 20 8260Dibromochloromethane124-48-1 01/13/16ND B6A1302

Lab Work Order # 1601033

Page 11 of 19Page 11 of 20

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1601033-05

RLCAS #

Client ID: GP12@25'

QC Batch

Organics-Volatiles

20 ug/L 20 8260Dibromomethane74-95-3 01/13/16ND B6A1302

100 ug/L 20 8260Dichlorodifluoromethane75-71-8 01/13/16ND B6A1302

100 ug/L 20 8260Diethyl ether60-29-7 01/13/16ND B6A1302

100 ug/L 20 8260Diisopropyl Ether108-20-3 01/13/16ND B6A1302

20 ug/L 20 8260Ethylbenzene100-41-4 01/13/16ND B6A1302

100 ug/L 20 8260Ethyltertiarybutylether637-92-3 01/13/16ND B6A1302

100 ug/L 20 8260Hexachloroethane67-72-1 01/13/16ND B6A1302

20 ug/L 20 8260Isopropylbenzene98-82-8 01/13/16ND B6A1302

40 ug/L 20 8260m & p - Xylene1330-20-7 01/13/16ND B6A1302

20 ug/L 20 8260Methyl iodide74-88-4 01/13/16ND B6A1302

100 ug/L 20 8260Methylene chloride75-09-2 01/13/16ND B6A1302

20 ug/L 20 8260Methyltertiarybutylether1634-04-4 01/13/16ND B6A1302

100 Xug/L 20 8260Naphthalene91-20-3 01/13/16ND B6A1302

20 ug/L 20 8260n-Butylbenzene104-51-8 01/13/16ND B6A1302

20 ug/L 20 8260n-Propylbenzene103-65-1 01/13/16ND B6A1302

20 ug/L 20 8260o-Xylene95-47-6 01/13/16ND B6A1302

20 ug/L 20 8260p-Isopropyl toluene99-87-6 01/13/16ND B6A1302

20 ug/L 20 8260sec-Butylbenzene135-98-8 01/13/16ND B6A1302

20 ug/L 20 8260Styrene100-42-5 01/13/16ND B6A1302

20 ug/L 20 8260tert-Butylbenzene98-06-6 01/13/16ND B6A1302

1000 ug/L 20 8260tertiary Butyl Alcohol75-65-0 01/13/16ND B6A1302

100 ug/L 20 8260tertiaryAmylmethylether994-05-8 01/13/16ND B6A1302

20 ug/L 20 8260Tetrachloroethylene127-18-4 01/13/161400 B6A1302

100 ug/L 20 8260Tetrahydrofuran109-99-9 01/13/16ND B6A1302

20 ug/L 20 8260Toluene108-88-3 01/13/16ND B6A1302

20 ug/L 20 8260trans-1,2-Dichloroethylene156-60-5 01/13/16ND B6A1302

20 ug/L 20 8260trans-1,3-Dichloropropylene10061-02-6 01/13/16ND B6A1302

100 ug/L 20 8260trans-1,4-Dichloro-2-butene110-57-6 01/13/16ND B6A1302

20 ug/L 20 8260Trichloroethylene79-01-6 01/13/1626 B6A1302

20 ug/L 20 8260Trichlorofluoromethane75-69-4 01/13/16ND B6A1302

20 ug/L 20 8260Vinyl chloride75-01-4 01/13/16ND B6A1302

85-115104 %Surrogate: Bromofluorobenzene 826001/13/16 B6A1302

82.7-115100 %Surrogate: Dibromofluoromethane 826001/13/16 B6A1302

85-115100 %Surrogate: Toluene-d8 826001/13/16 B6A1302

Lab Work Order # 1601033

Page 12 of 19Page 12 of 20

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1601033-06

RLCAS #

Client ID: GP12@30'

QC Batch

Organics-Volatiles

1.0 ug/L 1 82601,1,1,2-Tetrachloroethane630-20-6 01/13/16ND B6A1302

1.0 ug/L 1 82601,1,1-Trichloroethane71-55-6 01/13/16ND B6A1302

1.0 ug/L 1 82601,1,2,2-Tetrachloroethane79-34-5 01/13/16ND B6A1302

1.0 ug/L 1 82601,1,2-Trichloroethane79-00-5 01/13/16ND B6A1302

1.0 ug/L 1 82601,1-Dichloroethane75-34-3 01/13/16ND B6A1302

1.0 ug/L 1 82601,1-Dichloroethylene75-35-4 01/13/16ND B6A1302

5.0 ug/L 1 82601,2,3-Trichlorobenzene87-61-6 01/13/16ND B6A1302

1.0 ug/L 1 82601,2,3-Trichloropropane96-18-4 01/13/16ND B6A1302

1.0 ug/L 1 82601,2,3-Trimethylbenzene526-73-8 01/13/16ND B6A1302

5.0 ug/L 1 82601,2,4-Trichlorobenzene120-82-1 01/13/16ND B6A1302

1.0 ug/L 1 82601,2,4-Trimethylbenzene95-63-6 01/13/16ND B6A1302

5.0 ug/L 1 82601,2-Dibromo-3-chloropropane96-12-8 01/13/16ND B6A1302

1.0 ug/L 1 82601,2-Dibromoethane106-93-4 01/13/16ND B6A1302

1.0 ug/L 1 82601,2-Dichlorobenzene95-50-1 01/13/16ND B6A1302

1.0 ug/L 1 82601,2-Dichloroethane107-06-2 01/13/16ND B6A1302

1.0 ug/L 1 82601,2-Dichloropropane78-87-5 01/13/16ND B6A1302

1.0 ug/L 1 82601,3,5-Trimethylbenzene108-67-8 01/13/16ND B6A1302

1.0 ug/L 1 82601,3-Dichlorobenzene541-73-1 01/13/16ND B6A1302

1.0 ug/L 1 82601,4-Dichlorobenzene106-46-7 01/13/16ND B6A1302

5.0 ug/L 1 82602-Butanone (MEK)78-93-3 01/13/16ND B6A1302

5.0 ug/L 1 82602-Hexanone591-78-6 01/13/16ND B6A1302

5.0 A07, Xug/L 1 82602-Methylnaphthalene91-57-6 01/13/16ND B6A1302

20 ug/L 1 82602-Propanone (acetone)67-64-1 01/13/16ND B6A1302

5.0 ug/L 1 82604-Methyl-2-pentanone (MIBK)108-10-1 01/13/16ND B6A1302

5.0 ug/L 1 8260Acrylonitrile107-13-1 01/13/16ND B6A1302

1.0 ug/L 1 8260Benzene71-43-2 01/13/16ND B6A1302

1.0 ug/L 1 8260Bromobenzene108-86-1 01/13/16ND B6A1302

1.0 ug/L 1 8260Bromochloromethane74-97-5 01/13/16ND B6A1302

1.0 ug/L 1 8260Bromodichloromethane75-27-4 01/13/16ND B6A1302

1.0 ug/L 1 8260Bromoform75-25-2 01/13/16ND B6A1302

5.0 ug/L 1 8260Bromomethane74-83-9 01/13/16ND B6A1302

1.0 ug/L 1 8260Carbon disulfide75-15-0 01/13/16ND B6A1302

1.0 ug/L 1 8260Carbon tetrachloride56-23-5 01/13/16ND B6A1302

1.0 ug/L 1 8260Chlorobenzene108-90-7 01/13/16ND B6A1302

5.0 ug/L 1 8260Chloroethane75-00-3 01/13/16ND B6A1302

1.0 ug/L 1 8260Chloroform67-66-3 01/13/16ND B6A1302

5.0 ug/L 1 8260Chloromethane74-87-3 01/13/16ND B6A1302

1.0 ug/L 1 8260cis-1,2-Dichloroethylene156-59-2 01/13/16ND B6A1302

1.0 ug/L 1 8260cis-1,3-Dichloropropylene10061-01-5 01/13/16ND B6A1302

5.0 ug/L 1 8260Cyclohexane110-82-7 01/13/16ND B6A1302

1.0 ug/L 1 8260Dibromochloromethane124-48-1 01/13/16ND B6A1302

Lab Work Order # 1601033

Page 13 of 19Page 13 of 20

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1601033-06

RLCAS #

Client ID: GP12@30'

QC Batch

Organics-Volatiles

1.0 ug/L 1 8260Dibromomethane74-95-3 01/13/16ND B6A1302

5.0 ug/L 1 8260Dichlorodifluoromethane75-71-8 01/13/16ND B6A1302

5.0 ug/L 1 8260Diethyl ether60-29-7 01/13/16ND B6A1302

5.0 ug/L 1 8260Diisopropyl Ether108-20-3 01/13/16ND B6A1302

1.0 ug/L 1 8260Ethylbenzene100-41-4 01/13/16ND B6A1302

5.0 ug/L 1 8260Ethyltertiarybutylether637-92-3 01/13/16ND B6A1302

5.0 ug/L 1 8260Hexachloroethane67-72-1 01/13/16ND B6A1302

1.0 ug/L 1 8260Isopropylbenzene98-82-8 01/13/16ND B6A1302

2.0 ug/L 1 8260m & p - Xylene1330-20-7 01/13/16ND B6A1302

1.0 ug/L 1 8260Methyl iodide74-88-4 01/13/16ND B6A1302

5.0 ug/L 1 8260Methylene chloride75-09-2 01/13/16ND B6A1302

1.0 ug/L 1 8260Methyltertiarybutylether1634-04-4 01/13/16ND B6A1302

5.0 Xug/L 1 8260Naphthalene91-20-3 01/13/16ND B6A1302

1.0 ug/L 1 8260n-Butylbenzene104-51-8 01/13/16ND B6A1302

1.0 ug/L 1 8260n-Propylbenzene103-65-1 01/13/16ND B6A1302

1.0 ug/L 1 8260o-Xylene95-47-6 01/13/16ND B6A1302

1.0 ug/L 1 8260p-Isopropyl toluene99-87-6 01/13/16ND B6A1302

1.0 ug/L 1 8260sec-Butylbenzene135-98-8 01/13/16ND B6A1302

1.0 ug/L 1 8260Styrene100-42-5 01/13/16ND B6A1302

1.0 ug/L 1 8260tert-Butylbenzene98-06-6 01/13/16ND B6A1302

50 ug/L 1 8260tertiary Butyl Alcohol75-65-0 01/13/16ND B6A1302

5.0 ug/L 1 8260tertiaryAmylmethylether994-05-8 01/13/16ND B6A1302

1.0 ug/L 1 8260Tetrachloroethylene127-18-4 01/13/163.0 B6A1302

5.0 ug/L 1 8260Tetrahydrofuran109-99-9 01/13/16ND B6A1302

1.0 ug/L 1 8260Toluene108-88-3 01/13/16ND B6A1302

1.0 ug/L 1 8260trans-1,2-Dichloroethylene156-60-5 01/13/16ND B6A1302

1.0 ug/L 1 8260trans-1,3-Dichloropropylene10061-02-6 01/13/16ND B6A1302

5.0 ug/L 1 8260trans-1,4-Dichloro-2-butene110-57-6 01/13/16ND B6A1302

1.0 ug/L 1 8260Trichloroethylene79-01-6 01/13/16ND B6A1302

1.0 ug/L 1 8260Trichlorofluoromethane75-69-4 01/13/16ND B6A1302

1.0 ug/L 1 8260Vinyl chloride75-01-4 01/13/16ND B6A1302

85-115105 %Surrogate: Bromofluorobenzene 826001/13/16 B6A1302

82.7-11599.9 %Surrogate: Dibromofluoromethane 826001/13/16 B6A1302

85-115100 %Surrogate: Toluene-d8 826001/13/16 B6A1302

Lab Work Order # 1601033

Page 14 of 19Page 14 of 20

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1601033-07

RLCAS #

Client ID: GP12@35'

QC Batch

Organics-Volatiles

1.0 ug/L 1 82601,1,1,2-Tetrachloroethane630-20-6 01/13/16ND B6A1302

1.0 ug/L 1 82601,1,1-Trichloroethane71-55-6 01/13/16ND B6A1302

1.0 ug/L 1 82601,1,2,2-Tetrachloroethane79-34-5 01/13/16ND B6A1302

1.0 ug/L 1 82601,1,2-Trichloroethane79-00-5 01/13/16ND B6A1302

1.0 ug/L 1 82601,1-Dichloroethane75-34-3 01/13/16ND B6A1302

1.0 ug/L 1 82601,1-Dichloroethylene75-35-4 01/13/16ND B6A1302

5.0 ug/L 1 82601,2,3-Trichlorobenzene87-61-6 01/13/16ND B6A1302

1.0 ug/L 1 82601,2,3-Trichloropropane96-18-4 01/13/16ND B6A1302

1.0 ug/L 1 82601,2,3-Trimethylbenzene526-73-8 01/13/16ND B6A1302

5.0 ug/L 1 82601,2,4-Trichlorobenzene120-82-1 01/13/16ND B6A1302

1.0 ug/L 1 82601,2,4-Trimethylbenzene95-63-6 01/13/16ND B6A1302

5.0 ug/L 1 82601,2-Dibromo-3-chloropropane96-12-8 01/13/16ND B6A1302

1.0 ug/L 1 82601,2-Dibromoethane106-93-4 01/13/16ND B6A1302

1.0 ug/L 1 82601,2-Dichlorobenzene95-50-1 01/13/16ND B6A1302

1.0 ug/L 1 82601,2-Dichloroethane107-06-2 01/13/16ND B6A1302

1.0 ug/L 1 82601,2-Dichloropropane78-87-5 01/13/16ND B6A1302

1.0 ug/L 1 82601,3,5-Trimethylbenzene108-67-8 01/13/16ND B6A1302

1.0 ug/L 1 82601,3-Dichlorobenzene541-73-1 01/13/16ND B6A1302

1.0 ug/L 1 82601,4-Dichlorobenzene106-46-7 01/13/16ND B6A1302

5.0 ug/L 1 82602-Butanone (MEK)78-93-3 01/13/16ND B6A1302

5.0 ug/L 1 82602-Hexanone591-78-6 01/13/16ND B6A1302

5.0 A07, Xug/L 1 82602-Methylnaphthalene91-57-6 01/13/16ND B6A1302

20 ug/L 1 82602-Propanone (acetone)67-64-1 01/13/16ND B6A1302

5.0 ug/L 1 82604-Methyl-2-pentanone (MIBK)108-10-1 01/13/16ND B6A1302

5.0 ug/L 1 8260Acrylonitrile107-13-1 01/13/16ND B6A1302

1.0 ug/L 1 8260Benzene71-43-2 01/13/16ND B6A1302

1.0 ug/L 1 8260Bromobenzene108-86-1 01/13/16ND B6A1302

1.0 ug/L 1 8260Bromochloromethane74-97-5 01/13/16ND B6A1302

1.0 ug/L 1 8260Bromodichloromethane75-27-4 01/13/16ND B6A1302

1.0 ug/L 1 8260Bromoform75-25-2 01/13/16ND B6A1302

5.0 ug/L 1 8260Bromomethane74-83-9 01/13/16ND B6A1302

1.0 ug/L 1 8260Carbon disulfide75-15-0 01/13/16ND B6A1302

1.0 ug/L 1 8260Carbon tetrachloride56-23-5 01/13/16ND B6A1302

1.0 ug/L 1 8260Chlorobenzene108-90-7 01/13/16ND B6A1302

5.0 ug/L 1 8260Chloroethane75-00-3 01/13/16ND B6A1302

1.0 Tug/L 1 8260Chloroform67-66-3 01/13/160.95 B6A1302

5.0 ug/L 1 8260Chloromethane74-87-3 01/13/16ND B6A1302

1.0 ug/L 1 8260cis-1,2-Dichloroethylene156-59-2 01/13/16ND B6A1302

1.0 ug/L 1 8260cis-1,3-Dichloropropylene10061-01-5 01/13/16ND B6A1302

5.0 ug/L 1 8260Cyclohexane110-82-7 01/13/16ND B6A1302

1.0 ug/L 1 8260Dibromochloromethane124-48-1 01/13/16ND B6A1302

Lab Work Order # 1601033

Page 15 of 19Page 15 of 20

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1601033-07

RLCAS #

Client ID: GP12@35'

QC Batch

Organics-Volatiles

1.0 ug/L 1 8260Dibromomethane74-95-3 01/13/16ND B6A1302

5.0 ug/L 1 8260Dichlorodifluoromethane75-71-8 01/13/16ND B6A1302

5.0 ug/L 1 8260Diethyl ether60-29-7 01/13/16ND B6A1302

5.0 ug/L 1 8260Diisopropyl Ether108-20-3 01/13/16ND B6A1302

1.0 ug/L 1 8260Ethylbenzene100-41-4 01/13/16ND B6A1302

5.0 ug/L 1 8260Ethyltertiarybutylether637-92-3 01/13/16ND B6A1302

5.0 ug/L 1 8260Hexachloroethane67-72-1 01/13/16ND B6A1302

1.0 ug/L 1 8260Isopropylbenzene98-82-8 01/13/16ND B6A1302

2.0 ug/L 1 8260m & p - Xylene1330-20-7 01/13/16ND B6A1302

1.0 ug/L 1 8260Methyl iodide74-88-4 01/13/16ND B6A1302

5.0 ug/L 1 8260Methylene chloride75-09-2 01/13/16ND B6A1302

1.0 ug/L 1 8260Methyltertiarybutylether1634-04-4 01/13/16ND B6A1302

5.0 Xug/L 1 8260Naphthalene91-20-3 01/13/16ND B6A1302

1.0 ug/L 1 8260n-Butylbenzene104-51-8 01/13/16ND B6A1302

1.0 ug/L 1 8260n-Propylbenzene103-65-1 01/13/16ND B6A1302

1.0 ug/L 1 8260o-Xylene95-47-6 01/13/16ND B6A1302

1.0 ug/L 1 8260p-Isopropyl toluene99-87-6 01/13/16ND B6A1302

1.0 ug/L 1 8260sec-Butylbenzene135-98-8 01/13/16ND B6A1302

1.0 ug/L 1 8260Styrene100-42-5 01/13/16ND B6A1302

1.0 ug/L 1 8260tert-Butylbenzene98-06-6 01/13/16ND B6A1302

50 ug/L 1 8260tertiary Butyl Alcohol75-65-0 01/13/16ND B6A1302

5.0 ug/L 1 8260tertiaryAmylmethylether994-05-8 01/13/16ND B6A1302

1.0 ug/L 1 8260Tetrachloroethylene127-18-4 01/13/162.2 B6A1302

5.0 ug/L 1 8260Tetrahydrofuran109-99-9 01/13/16ND B6A1302

1.0 ug/L 1 8260Toluene108-88-3 01/13/16ND B6A1302

1.0 ug/L 1 8260trans-1,2-Dichloroethylene156-60-5 01/13/16ND B6A1302

1.0 ug/L 1 8260trans-1,3-Dichloropropylene10061-02-6 01/13/16ND B6A1302

5.0 ug/L 1 8260trans-1,4-Dichloro-2-butene110-57-6 01/13/16ND B6A1302

1.0 ug/L 1 8260Trichloroethylene79-01-6 01/13/16ND B6A1302

1.0 ug/L 1 8260Trichlorofluoromethane75-69-4 01/13/16ND B6A1302

1.0 ug/L 1 8260Vinyl chloride75-01-4 01/13/16ND B6A1302

85-115103 %Surrogate: Bromofluorobenzene 826001/13/16 B6A1302

82.7-115102 %Surrogate: Dibromofluoromethane 826001/13/16 B6A1302

85-11598.9 %Surrogate: Toluene-d8 826001/13/16 B6A1302

Lab Work Order # 1601033

Page 16 of 19Page 16 of 20

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1601033-08

RLCAS #

Client ID: GP12@40'

QC Batch

Organics-Volatiles

1.0 ug/L 1 82601,1,1,2-Tetrachloroethane630-20-6 01/13/16ND B6A1302

1.0 ug/L 1 82601,1,1-Trichloroethane71-55-6 01/13/16ND B6A1302

1.0 ug/L 1 82601,1,2,2-Tetrachloroethane79-34-5 01/13/16ND B6A1302

1.0 ug/L 1 82601,1,2-Trichloroethane79-00-5 01/13/16ND B6A1302

1.0 ug/L 1 82601,1-Dichloroethane75-34-3 01/13/16ND B6A1302

1.0 ug/L 1 82601,1-Dichloroethylene75-35-4 01/13/16ND B6A1302

5.0 ug/L 1 82601,2,3-Trichlorobenzene87-61-6 01/13/16ND B6A1302

1.0 ug/L 1 82601,2,3-Trichloropropane96-18-4 01/13/16ND B6A1302

1.0 ug/L 1 82601,2,3-Trimethylbenzene526-73-8 01/13/16ND B6A1302

5.0 ug/L 1 82601,2,4-Trichlorobenzene120-82-1 01/13/16ND B6A1302

1.0 ug/L 1 82601,2,4-Trimethylbenzene95-63-6 01/13/16ND B6A1302

5.0 ug/L 1 82601,2-Dibromo-3-chloropropane96-12-8 01/13/16ND B6A1302

1.0 ug/L 1 82601,2-Dibromoethane106-93-4 01/13/16ND B6A1302

1.0 ug/L 1 82601,2-Dichlorobenzene95-50-1 01/13/16ND B6A1302

1.0 ug/L 1 82601,2-Dichloroethane107-06-2 01/13/16ND B6A1302

1.0 ug/L 1 82601,2-Dichloropropane78-87-5 01/13/16ND B6A1302

1.0 ug/L 1 82601,3,5-Trimethylbenzene108-67-8 01/13/16ND B6A1302

1.0 ug/L 1 82601,3-Dichlorobenzene541-73-1 01/13/16ND B6A1302

1.0 ug/L 1 82601,4-Dichlorobenzene106-46-7 01/13/16ND B6A1302

5.0 ug/L 1 82602-Butanone (MEK)78-93-3 01/13/16ND B6A1302

5.0 ug/L 1 82602-Hexanone591-78-6 01/13/16ND B6A1302

5.0 A07, Xug/L 1 82602-Methylnaphthalene91-57-6 01/13/16ND B6A1302

20 ug/L 1 82602-Propanone (acetone)67-64-1 01/13/16ND B6A1302

5.0 ug/L 1 82604-Methyl-2-pentanone (MIBK)108-10-1 01/13/16ND B6A1302

5.0 ug/L 1 8260Acrylonitrile107-13-1 01/13/16ND B6A1302

1.0 ug/L 1 8260Benzene71-43-2 01/13/16ND B6A1302

1.0 ug/L 1 8260Bromobenzene108-86-1 01/13/16ND B6A1302

1.0 ug/L 1 8260Bromochloromethane74-97-5 01/13/16ND B6A1302

1.0 ug/L 1 8260Bromodichloromethane75-27-4 01/13/16ND B6A1302

1.0 ug/L 1 8260Bromoform75-25-2 01/13/16ND B6A1302

5.0 ug/L 1 8260Bromomethane74-83-9 01/13/16ND B6A1302

1.0 ug/L 1 8260Carbon disulfide75-15-0 01/13/16ND B6A1302

1.0 ug/L 1 8260Carbon tetrachloride56-23-5 01/13/16ND B6A1302

1.0 ug/L 1 8260Chlorobenzene108-90-7 01/13/16ND B6A1302

5.0 ug/L 1 8260Chloroethane75-00-3 01/13/16ND B6A1302

1.0 Tug/L 1 8260Chloroform67-66-3 01/13/160.94 B6A1302

5.0 ug/L 1 8260Chloromethane74-87-3 01/13/16ND B6A1302

1.0 ug/L 1 8260cis-1,2-Dichloroethylene156-59-2 01/13/16ND B6A1302

1.0 ug/L 1 8260cis-1,3-Dichloropropylene10061-01-5 01/13/16ND B6A1302

5.0 ug/L 1 8260Cyclohexane110-82-7 01/13/16ND B6A1302

1.0 ug/L 1 8260Dibromochloromethane124-48-1 01/13/16ND B6A1302

Lab Work Order # 1601033

Page 17 of 19Page 17 of 20

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1601033-08

RLCAS #

Client ID: GP12@40'

QC Batch

Organics-Volatiles

1.0 ug/L 1 8260Dibromomethane74-95-3 01/13/16ND B6A1302

5.0 ug/L 1 8260Dichlorodifluoromethane75-71-8 01/13/16ND B6A1302

5.0 ug/L 1 8260Diethyl ether60-29-7 01/13/16ND B6A1302

5.0 ug/L 1 8260Diisopropyl Ether108-20-3 01/13/16ND B6A1302

1.0 ug/L 1 8260Ethylbenzene100-41-4 01/13/16ND B6A1302

5.0 ug/L 1 8260Ethyltertiarybutylether637-92-3 01/13/16ND B6A1302

5.0 ug/L 1 8260Hexachloroethane67-72-1 01/13/16ND B6A1302

1.0 ug/L 1 8260Isopropylbenzene98-82-8 01/13/16ND B6A1302

2.0 ug/L 1 8260m & p - Xylene1330-20-7 01/13/16ND B6A1302

1.0 ug/L 1 8260Methyl iodide74-88-4 01/13/16ND B6A1302

5.0 ug/L 1 8260Methylene chloride75-09-2 01/13/16ND B6A1302

1.0 ug/L 1 8260Methyltertiarybutylether1634-04-4 01/13/16ND B6A1302

5.0 Xug/L 1 8260Naphthalene91-20-3 01/13/16ND B6A1302

1.0 ug/L 1 8260n-Butylbenzene104-51-8 01/13/16ND B6A1302

1.0 ug/L 1 8260n-Propylbenzene103-65-1 01/13/16ND B6A1302

1.0 ug/L 1 8260o-Xylene95-47-6 01/13/16ND B6A1302

1.0 ug/L 1 8260p-Isopropyl toluene99-87-6 01/13/16ND B6A1302

1.0 ug/L 1 8260sec-Butylbenzene135-98-8 01/13/16ND B6A1302

1.0 ug/L 1 8260Styrene100-42-5 01/13/16ND B6A1302

1.0 ug/L 1 8260tert-Butylbenzene98-06-6 01/13/16ND B6A1302

50 ug/L 1 8260tertiary Butyl Alcohol75-65-0 01/13/16ND B6A1302

5.0 ug/L 1 8260tertiaryAmylmethylether994-05-8 01/13/16ND B6A1302

1.0 ug/L 1 8260Tetrachloroethylene127-18-4 01/13/163.1 B6A1302

5.0 ug/L 1 8260Tetrahydrofuran109-99-9 01/13/16ND B6A1302

1.0 ug/L 1 8260Toluene108-88-3 01/13/16ND B6A1302

1.0 ug/L 1 8260trans-1,2-Dichloroethylene156-60-5 01/13/16ND B6A1302

1.0 ug/L 1 8260trans-1,3-Dichloropropylene10061-02-6 01/13/16ND B6A1302

5.0 ug/L 1 8260trans-1,4-Dichloro-2-butene110-57-6 01/13/16ND B6A1302

1.0 ug/L 1 8260Trichloroethylene79-01-6 01/13/16ND B6A1302

1.0 ug/L 1 8260Trichlorofluoromethane75-69-4 01/13/16ND B6A1302

1.0 ug/L 1 8260Vinyl chloride75-01-4 01/13/16ND B6A1302

85-115101 %Surrogate: Bromofluorobenzene 826001/13/16 B6A1302

82.7-115101 %Surrogate: Dibromofluoromethane 826001/13/16 B6A1302

85-115100 %Surrogate: Toluene-d8 826001/13/16 B6A1302

Lab Work Order # 1601033

Page 18 of 19Page 18 of 20

Page 19 of 20

Page 20 of 20

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

MDEQ-RRD-GRAND RAPIDS

RE: HALL STREET

Grand Rapids, MI 49503-2341

350 Ottawa Ave. NW, Unit 10

Abigail Hendershott

I certify that the analyses performed by the MDEQ Environmental Laboratory were conducted by methods

approved by the U.S. Environmental Protection Agency and other appropriate regulatory agencies .

Sincerely,

20 January 2016 Work Order: 1601058

Price: $1,840.00

George Krisztian

Laboratory Director

Lab Work Order # 1601058

Page 1 of 19Page 1 of 19

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

Project:

Project Manager:

Reported:

MDEQ-RRD-GRAND RAPIDS

350 Ottawa Ave. NW, Unit 10

Abigail Hendershott

HALL STREET

Grand Rapids MI, 49503-2341

Site Code: 4100112101/20/2016

Sample ID Laboratory ID Date SampledMatrix Date Received

Analytical Report for Samples

Qualifier

1601058-01 Water 01/14/2016GP15@25' 01/13/2016

1601058-02 Water 01/14/2016GP15@30' 01/13/2016

1601058-03 Water 01/14/2016GP15@35' 01/13/2016

1601058-04 Water 01/14/2016GP15@40' 01/13/2016

1601058-05 Water 01/14/2016GP16@25' 01/14/2016

1601058-06 Water 01/14/2016GP16@30 01/14/2016

1601058-07 Water 01/14/2016GP16@35 01/14/2016

1601058-08 Water 01/14/2016GP16@40 01/14/2016

Notes and Definitions

X Methods 8260 & 624 are used to analyze volatile organics that have boiling points below 200 ºC. 2-Methylnaphthalene & naphthalene

have boiling points above 200 ºC and are better suited to analysis by methods 8270 & 625 as semivolatile organics.

T Reported value is less than the reporting limit (RL). Result is estimated.

A05 Result and reporting limit are estimated due to low continuing calibration standard criteria failure.

Reporting LimitRL

Indicates compound analyzed for but not detectedND

Not ApplicableNA

Case Narrative

Priority Samples

Lab Work Order # 1601058

Page 2 of 19Page 2 of 19

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1601058-01

RLCAS #

Client ID: GP15@25'

QC Batch

Organics-Volatiles

1.0 ug/L 1 82601,1,1,2-Tetrachloroethane630-20-6 01/14/16ND B6A1403

1.0 ug/L 1 82601,1,1-Trichloroethane71-55-6 01/14/16ND B6A1403

1.0 ug/L 1 82601,1,2,2-Tetrachloroethane79-34-5 01/14/16ND B6A1403

1.0 ug/L 1 82601,1,2-Trichloroethane79-00-5 01/14/16ND B6A1403

1.0 ug/L 1 82601,1-Dichloroethane75-34-3 01/14/16ND B6A1403

1.0 ug/L 1 82601,1-Dichloroethylene75-35-4 01/14/16ND B6A1403

5.0 ug/L 1 82601,2,3-Trichlorobenzene87-61-6 01/14/16ND B6A1403

1.0 ug/L 1 82601,2,3-Trichloropropane96-18-4 01/14/16ND B6A1403

1.0 ug/L 1 82601,2,3-Trimethylbenzene526-73-8 01/14/16ND B6A1403

5.0 ug/L 1 82601,2,4-Trichlorobenzene120-82-1 01/14/16ND B6A1403

1.0 ug/L 1 82601,2,4-Trimethylbenzene95-63-6 01/14/16ND B6A1403

5.0 ug/L 1 82601,2-Dibromo-3-chloropropane96-12-8 01/14/16ND B6A1403

1.0 ug/L 1 82601,2-Dibromoethane106-93-4 01/14/16ND B6A1403

1.0 ug/L 1 82601,2-Dichlorobenzene95-50-1 01/14/16ND B6A1403

1.0 ug/L 1 82601,2-Dichloroethane107-06-2 01/14/16ND B6A1403

1.0 ug/L 1 82601,2-Dichloropropane78-87-5 01/14/16ND B6A1403

1.0 ug/L 1 82601,3,5-Trimethylbenzene108-67-8 01/14/16ND B6A1403

1.0 ug/L 1 82601,3-Dichlorobenzene541-73-1 01/14/16ND B6A1403

1.0 ug/L 1 82601,4-Dichlorobenzene106-46-7 01/14/16ND B6A1403

5.0 ug/L 1 82602-Butanone (MEK)78-93-3 01/14/16ND B6A1403

5.0 ug/L 1 82602-Hexanone591-78-6 01/14/16ND B6A1403

5.0 Xug/L 1 82602-Methylnaphthalene91-57-6 01/14/16ND B6A1403

20 ug/L 1 82602-Propanone (acetone)67-64-1 01/14/16ND B6A1403

5.0 ug/L 1 82604-Methyl-2-pentanone (MIBK)108-10-1 01/14/16ND B6A1403

5.0 ug/L 1 8260Acrylonitrile107-13-1 01/14/16ND B6A1403

1.0 ug/L 1 8260Benzene71-43-2 01/14/16ND B6A1403

1.0 ug/L 1 8260Bromobenzene108-86-1 01/14/16ND B6A1403

1.0 ug/L 1 8260Bromochloromethane74-97-5 01/14/16ND B6A1403

1.0 ug/L 1 8260Bromodichloromethane75-27-4 01/14/16ND B6A1403

1.0 ug/L 1 8260Bromoform75-25-2 01/14/16ND B6A1403

5.0 ug/L 1 8260Bromomethane74-83-9 01/14/16ND B6A1403

1.0 ug/L 1 8260Carbon disulfide75-15-0 01/14/16ND B6A1403

1.0 ug/L 1 8260Carbon tetrachloride56-23-5 01/14/16ND B6A1403

1.0 ug/L 1 8260Chlorobenzene108-90-7 01/14/16ND B6A1403

5.0 ug/L 1 8260Chloroethane75-00-3 01/14/16ND B6A1403

1.0 ug/L 1 8260Chloroform67-66-3 01/14/161.0 B6A1403

5.0 ug/L 1 8260Chloromethane74-87-3 01/14/16ND B6A1403

1.0 ug/L 1 8260cis-1,2-Dichloroethylene156-59-2 01/14/16ND B6A1403

1.0 ug/L 1 8260cis-1,3-Dichloropropylene10061-01-5 01/14/16ND B6A1403

5.0 ug/L 1 8260Cyclohexane110-82-7 01/14/16ND B6A1403

1.0 ug/L 1 8260Dibromochloromethane124-48-1 01/14/16ND B6A1403

Lab Work Order # 1601058

Page 3 of 19Page 3 of 19

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1601058-01

RLCAS #

Client ID: GP15@25'

QC Batch

Organics-Volatiles

1.0 ug/L 1 8260Dibromomethane74-95-3 01/14/16ND B6A1403

5.0 ug/L 1 8260Dichlorodifluoromethane75-71-8 01/14/16ND B6A1403

5.0 ug/L 1 8260Diethyl ether60-29-7 01/14/16ND B6A1403

5.0 ug/L 1 8260Diisopropyl Ether108-20-3 01/14/16ND B6A1403

1.0 ug/L 1 8260Ethylbenzene100-41-4 01/14/16ND B6A1403

5.0 ug/L 1 8260Ethyltertiarybutylether637-92-3 01/14/16ND B6A1403

5.0 ug/L 1 8260Hexachloroethane67-72-1 01/14/16ND B6A1403

1.0 ug/L 1 8260Isopropylbenzene98-82-8 01/14/16ND B6A1403

2.0 ug/L 1 8260m & p - Xylene1330-20-7 01/14/16ND B6A1403

1.0 ug/L 1 8260Methyl iodide74-88-4 01/14/16ND B6A1403

5.0 ug/L 1 8260Methylene chloride75-09-2 01/14/16ND B6A1403

1.0 ug/L 1 8260Methyltertiarybutylether1634-04-4 01/14/16ND B6A1403

5.0 Xug/L 1 8260Naphthalene91-20-3 01/14/16ND B6A1403

1.0 ug/L 1 8260n-Butylbenzene104-51-8 01/14/16ND B6A1403

1.0 ug/L 1 8260n-Propylbenzene103-65-1 01/14/16ND B6A1403

1.0 ug/L 1 8260o-Xylene95-47-6 01/14/16ND B6A1403

1.0 ug/L 1 8260p-Isopropyl toluene99-87-6 01/14/16ND B6A1403

1.0 ug/L 1 8260sec-Butylbenzene135-98-8 01/14/16ND B6A1403

1.0 ug/L 1 8260Styrene100-42-5 01/14/16ND B6A1403

1.0 ug/L 1 8260tert-Butylbenzene98-06-6 01/14/16ND B6A1403

50 ug/L 1 8260tertiary Butyl Alcohol75-65-0 01/14/16ND B6A1403

5.0 ug/L 1 8260tertiaryAmylmethylether994-05-8 01/14/16ND B6A1403

1.0 ug/L 1 8260Tetrachloroethylene127-18-4 01/14/1699 B6A1403

5.0 ug/L 1 8260Tetrahydrofuran109-99-9 01/14/16ND B6A1403

1.0 ug/L 1 8260Toluene108-88-3 01/14/16ND B6A1403

1.0 ug/L 1 8260trans-1,2-Dichloroethylene156-60-5 01/14/16ND B6A1403

1.0 ug/L 1 8260trans-1,3-Dichloropropylene10061-02-6 01/14/16ND B6A1403

5.0 ug/L 1 8260trans-1,4-Dichloro-2-butene110-57-6 01/14/16ND B6A1403

1.0 ug/L 1 8260Trichloroethylene79-01-6 01/14/16ND B6A1403

1.0 ug/L 1 8260Trichlorofluoromethane75-69-4 01/14/16ND B6A1403

1.0 ug/L 1 8260Vinyl chloride75-01-4 01/14/16ND B6A1403

85-115103 %Surrogate: Bromofluorobenzene 826001/14/16 B6A1403

82.7-115101 %Surrogate: Dibromofluoromethane 826001/14/16 B6A1403

85-11598.8 %Surrogate: Toluene-d8 826001/14/16 B6A1403

Lab Work Order # 1601058

Page 4 of 19Page 4 of 19

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1601058-02

RLCAS #

Client ID: GP15@30'

QC Batch

Organics-Volatiles

1.0 ug/L 1 82601,1,1,2-Tetrachloroethane630-20-6 01/14/16ND B6A1403

1.0 ug/L 1 82601,1,1-Trichloroethane71-55-6 01/14/16ND B6A1403

1.0 ug/L 1 82601,1,2,2-Tetrachloroethane79-34-5 01/14/16ND B6A1403

1.0 ug/L 1 82601,1,2-Trichloroethane79-00-5 01/14/16ND B6A1403

1.0 ug/L 1 82601,1-Dichloroethane75-34-3 01/14/16ND B6A1403

1.0 ug/L 1 82601,1-Dichloroethylene75-35-4 01/14/16ND B6A1403

5.0 ug/L 1 82601,2,3-Trichlorobenzene87-61-6 01/14/16ND B6A1403

1.0 ug/L 1 82601,2,3-Trichloropropane96-18-4 01/14/16ND B6A1403

1.0 ug/L 1 82601,2,3-Trimethylbenzene526-73-8 01/14/16ND B6A1403

5.0 ug/L 1 82601,2,4-Trichlorobenzene120-82-1 01/14/16ND B6A1403

1.0 ug/L 1 82601,2,4-Trimethylbenzene95-63-6 01/14/16ND B6A1403

5.0 ug/L 1 82601,2-Dibromo-3-chloropropane96-12-8 01/14/16ND B6A1403

1.0 ug/L 1 82601,2-Dibromoethane106-93-4 01/14/16ND B6A1403

1.0 ug/L 1 82601,2-Dichlorobenzene95-50-1 01/14/16ND B6A1403

1.0 ug/L 1 82601,2-Dichloroethane107-06-2 01/14/16ND B6A1403

1.0 ug/L 1 82601,2-Dichloropropane78-87-5 01/14/16ND B6A1403

1.0 ug/L 1 82601,3,5-Trimethylbenzene108-67-8 01/14/16ND B6A1403

1.0 ug/L 1 82601,3-Dichlorobenzene541-73-1 01/14/16ND B6A1403

1.0 ug/L 1 82601,4-Dichlorobenzene106-46-7 01/14/16ND B6A1403

5.0 ug/L 1 82602-Butanone (MEK)78-93-3 01/14/16ND B6A1403

5.0 ug/L 1 82602-Hexanone591-78-6 01/14/16ND B6A1403

5.0 Xug/L 1 82602-Methylnaphthalene91-57-6 01/14/16ND B6A1403

20 ug/L 1 82602-Propanone (acetone)67-64-1 01/14/16ND B6A1403

5.0 ug/L 1 82604-Methyl-2-pentanone (MIBK)108-10-1 01/14/16ND B6A1403

5.0 ug/L 1 8260Acrylonitrile107-13-1 01/14/16ND B6A1403

1.0 ug/L 1 8260Benzene71-43-2 01/14/16ND B6A1403

1.0 ug/L 1 8260Bromobenzene108-86-1 01/14/16ND B6A1403

1.0 ug/L 1 8260Bromochloromethane74-97-5 01/14/16ND B6A1403

1.0 ug/L 1 8260Bromodichloromethane75-27-4 01/14/16ND B6A1403

1.0 ug/L 1 8260Bromoform75-25-2 01/14/16ND B6A1403

5.0 ug/L 1 8260Bromomethane74-83-9 01/14/16ND B6A1403

1.0 ug/L 1 8260Carbon disulfide75-15-0 01/14/16ND B6A1403

1.0 ug/L 1 8260Carbon tetrachloride56-23-5 01/14/16ND B6A1403

1.0 ug/L 1 8260Chlorobenzene108-90-7 01/14/16ND B6A1403

5.0 ug/L 1 8260Chloroethane75-00-3 01/14/16ND B6A1403

1.0 ug/L 1 8260Chloroform67-66-3 01/14/161.0 B6A1403

5.0 ug/L 1 8260Chloromethane74-87-3 01/14/16ND B6A1403

1.0 ug/L 1 8260cis-1,2-Dichloroethylene156-59-2 01/14/16ND B6A1403

1.0 ug/L 1 8260cis-1,3-Dichloropropylene10061-01-5 01/14/16ND B6A1403

5.0 ug/L 1 8260Cyclohexane110-82-7 01/14/16ND B6A1403

1.0 ug/L 1 8260Dibromochloromethane124-48-1 01/14/16ND B6A1403

Lab Work Order # 1601058

Page 5 of 19Page 5 of 19

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1601058-02

RLCAS #

Client ID: GP15@30'

QC Batch

Organics-Volatiles

1.0 ug/L 1 8260Dibromomethane74-95-3 01/14/16ND B6A1403

5.0 ug/L 1 8260Dichlorodifluoromethane75-71-8 01/14/16ND B6A1403

5.0 ug/L 1 8260Diethyl ether60-29-7 01/14/16ND B6A1403

5.0 ug/L 1 8260Diisopropyl Ether108-20-3 01/14/16ND B6A1403

1.0 ug/L 1 8260Ethylbenzene100-41-4 01/14/16ND B6A1403

5.0 ug/L 1 8260Ethyltertiarybutylether637-92-3 01/14/16ND B6A1403

5.0 ug/L 1 8260Hexachloroethane67-72-1 01/14/16ND B6A1403

1.0 ug/L 1 8260Isopropylbenzene98-82-8 01/14/16ND B6A1403

2.0 ug/L 1 8260m & p - Xylene1330-20-7 01/14/16ND B6A1403

1.0 ug/L 1 8260Methyl iodide74-88-4 01/14/16ND B6A1403

5.0 ug/L 1 8260Methylene chloride75-09-2 01/14/16ND B6A1403

1.0 ug/L 1 8260Methyltertiarybutylether1634-04-4 01/14/16ND B6A1403

5.0 Xug/L 1 8260Naphthalene91-20-3 01/14/16ND B6A1403

1.0 ug/L 1 8260n-Butylbenzene104-51-8 01/14/16ND B6A1403

1.0 ug/L 1 8260n-Propylbenzene103-65-1 01/14/16ND B6A1403

1.0 ug/L 1 8260o-Xylene95-47-6 01/14/16ND B6A1403

1.0 ug/L 1 8260p-Isopropyl toluene99-87-6 01/14/16ND B6A1403

1.0 ug/L 1 8260sec-Butylbenzene135-98-8 01/14/16ND B6A1403

1.0 ug/L 1 8260Styrene100-42-5 01/14/16ND B6A1403

1.0 ug/L 1 8260tert-Butylbenzene98-06-6 01/14/16ND B6A1403

50 ug/L 1 8260tertiary Butyl Alcohol75-65-0 01/14/16ND B6A1403

5.0 ug/L 1 8260tertiaryAmylmethylether994-05-8 01/14/16ND B6A1403

1.0 ug/L 1 8260Tetrachloroethylene127-18-4 01/14/1612 B6A1403

5.0 ug/L 1 8260Tetrahydrofuran109-99-9 01/14/16ND B6A1403

1.0 ug/L 1 8260Toluene108-88-3 01/14/16ND B6A1403

1.0 ug/L 1 8260trans-1,2-Dichloroethylene156-60-5 01/14/16ND B6A1403

1.0 ug/L 1 8260trans-1,3-Dichloropropylene10061-02-6 01/14/16ND B6A1403

5.0 ug/L 1 8260trans-1,4-Dichloro-2-butene110-57-6 01/14/16ND B6A1403

1.0 ug/L 1 8260Trichloroethylene79-01-6 01/14/16ND B6A1403

1.0 ug/L 1 8260Trichlorofluoromethane75-69-4 01/14/16ND B6A1403

1.0 ug/L 1 8260Vinyl chloride75-01-4 01/14/16ND B6A1403

85-115101 %Surrogate: Bromofluorobenzene 826001/14/16 B6A1403

82.7-115103 %Surrogate: Dibromofluoromethane 826001/14/16 B6A1403

85-11597.5 %Surrogate: Toluene-d8 826001/14/16 B6A1403

Lab Work Order # 1601058

Page 6 of 19Page 6 of 19

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1601058-03

RLCAS #

Client ID: GP15@35'

QC Batch

Organics-Volatiles

1.0 ug/L 1 82601,1,1,2-Tetrachloroethane630-20-6 01/14/16ND B6A1403

1.0 ug/L 1 82601,1,1-Trichloroethane71-55-6 01/14/16ND B6A1403

1.0 ug/L 1 82601,1,2,2-Tetrachloroethane79-34-5 01/14/16ND B6A1403

1.0 ug/L 1 82601,1,2-Trichloroethane79-00-5 01/14/16ND B6A1403

1.0 ug/L 1 82601,1-Dichloroethane75-34-3 01/14/16ND B6A1403

1.0 ug/L 1 82601,1-Dichloroethylene75-35-4 01/14/16ND B6A1403

5.0 ug/L 1 82601,2,3-Trichlorobenzene87-61-6 01/14/16ND B6A1403

1.0 ug/L 1 82601,2,3-Trichloropropane96-18-4 01/14/16ND B6A1403

1.0 ug/L 1 82601,2,3-Trimethylbenzene526-73-8 01/14/16ND B6A1403

5.0 ug/L 1 82601,2,4-Trichlorobenzene120-82-1 01/14/16ND B6A1403

1.0 ug/L 1 82601,2,4-Trimethylbenzene95-63-6 01/14/16ND B6A1403

5.0 ug/L 1 82601,2-Dibromo-3-chloropropane96-12-8 01/14/16ND B6A1403

1.0 ug/L 1 82601,2-Dibromoethane106-93-4 01/14/16ND B6A1403

1.0 ug/L 1 82601,2-Dichlorobenzene95-50-1 01/14/16ND B6A1403

1.0 ug/L 1 82601,2-Dichloroethane107-06-2 01/14/16ND B6A1403

1.0 ug/L 1 82601,2-Dichloropropane78-87-5 01/14/16ND B6A1403

1.0 ug/L 1 82601,3,5-Trimethylbenzene108-67-8 01/14/16ND B6A1403

1.0 ug/L 1 82601,3-Dichlorobenzene541-73-1 01/14/16ND B6A1403

1.0 ug/L 1 82601,4-Dichlorobenzene106-46-7 01/14/16ND B6A1403

5.0 ug/L 1 82602-Butanone (MEK)78-93-3 01/14/16ND B6A1403

5.0 ug/L 1 82602-Hexanone591-78-6 01/14/16ND B6A1403

5.0 Xug/L 1 82602-Methylnaphthalene91-57-6 01/14/16ND B6A1403

20 ug/L 1 82602-Propanone (acetone)67-64-1 01/14/16ND B6A1403

5.0 ug/L 1 82604-Methyl-2-pentanone (MIBK)108-10-1 01/14/16ND B6A1403

5.0 ug/L 1 8260Acrylonitrile107-13-1 01/14/16ND B6A1403

1.0 ug/L 1 8260Benzene71-43-2 01/14/16ND B6A1403

1.0 ug/L 1 8260Bromobenzene108-86-1 01/14/16ND B6A1403

1.0 ug/L 1 8260Bromochloromethane74-97-5 01/14/16ND B6A1403

1.0 ug/L 1 8260Bromodichloromethane75-27-4 01/14/16ND B6A1403

1.0 ug/L 1 8260Bromoform75-25-2 01/14/16ND B6A1403

5.0 ug/L 1 8260Bromomethane74-83-9 01/14/16ND B6A1403

1.0 ug/L 1 8260Carbon disulfide75-15-0 01/14/16ND B6A1403

1.0 ug/L 1 8260Carbon tetrachloride56-23-5 01/14/16ND B6A1403

1.0 ug/L 1 8260Chlorobenzene108-90-7 01/14/16ND B6A1403

5.0 ug/L 1 8260Chloroethane75-00-3 01/14/16ND B6A1403

1.0 ug/L 1 8260Chloroform67-66-3 01/14/161.0 B6A1403

5.0 ug/L 1 8260Chloromethane74-87-3 01/14/16ND B6A1403

1.0 ug/L 1 8260cis-1,2-Dichloroethylene156-59-2 01/14/16ND B6A1403

1.0 ug/L 1 8260cis-1,3-Dichloropropylene10061-01-5 01/14/16ND B6A1403

5.0 ug/L 1 8260Cyclohexane110-82-7 01/14/16ND B6A1403

1.0 ug/L 1 8260Dibromochloromethane124-48-1 01/14/16ND B6A1403

Lab Work Order # 1601058

Page 7 of 19Page 7 of 19

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1601058-03

RLCAS #

Client ID: GP15@35'

QC Batch

Organics-Volatiles

1.0 ug/L 1 8260Dibromomethane74-95-3 01/14/16ND B6A1403

5.0 ug/L 1 8260Dichlorodifluoromethane75-71-8 01/14/16ND B6A1403

5.0 ug/L 1 8260Diethyl ether60-29-7 01/14/16ND B6A1403

5.0 ug/L 1 8260Diisopropyl Ether108-20-3 01/14/16ND B6A1403

1.0 ug/L 1 8260Ethylbenzene100-41-4 01/14/16ND B6A1403

5.0 ug/L 1 8260Ethyltertiarybutylether637-92-3 01/14/16ND B6A1403

5.0 ug/L 1 8260Hexachloroethane67-72-1 01/14/16ND B6A1403

1.0 ug/L 1 8260Isopropylbenzene98-82-8 01/14/16ND B6A1403

2.0 ug/L 1 8260m & p - Xylene1330-20-7 01/14/16ND B6A1403

1.0 ug/L 1 8260Methyl iodide74-88-4 01/14/16ND B6A1403

5.0 ug/L 1 8260Methylene chloride75-09-2 01/14/16ND B6A1403

1.0 ug/L 1 8260Methyltertiarybutylether1634-04-4 01/14/16ND B6A1403

5.0 Xug/L 1 8260Naphthalene91-20-3 01/14/16ND B6A1403

1.0 ug/L 1 8260n-Butylbenzene104-51-8 01/14/16ND B6A1403

1.0 ug/L 1 8260n-Propylbenzene103-65-1 01/14/16ND B6A1403

1.0 ug/L 1 8260o-Xylene95-47-6 01/14/16ND B6A1403

1.0 ug/L 1 8260p-Isopropyl toluene99-87-6 01/14/16ND B6A1403

1.0 ug/L 1 8260sec-Butylbenzene135-98-8 01/14/16ND B6A1403

1.0 ug/L 1 8260Styrene100-42-5 01/14/16ND B6A1403

1.0 ug/L 1 8260tert-Butylbenzene98-06-6 01/14/16ND B6A1403

50 ug/L 1 8260tertiary Butyl Alcohol75-65-0 01/14/16ND B6A1403

5.0 ug/L 1 8260tertiaryAmylmethylether994-05-8 01/14/16ND B6A1403

1.0 ug/L 1 8260Tetrachloroethylene127-18-4 01/14/169.5 B6A1403

5.0 ug/L 1 8260Tetrahydrofuran109-99-9 01/14/16ND B6A1403

1.0 ug/L 1 8260Toluene108-88-3 01/14/16ND B6A1403

1.0 ug/L 1 8260trans-1,2-Dichloroethylene156-60-5 01/14/16ND B6A1403

1.0 ug/L 1 8260trans-1,3-Dichloropropylene10061-02-6 01/14/16ND B6A1403

5.0 ug/L 1 8260trans-1,4-Dichloro-2-butene110-57-6 01/14/16ND B6A1403

1.0 ug/L 1 8260Trichloroethylene79-01-6 01/14/16ND B6A1403

1.0 ug/L 1 8260Trichlorofluoromethane75-69-4 01/14/16ND B6A1403

1.0 ug/L 1 8260Vinyl chloride75-01-4 01/14/16ND B6A1403

85-115101 %Surrogate: Bromofluorobenzene 826001/14/16 B6A1403

82.7-115101 %Surrogate: Dibromofluoromethane 826001/14/16 B6A1403

85-11598.1 %Surrogate: Toluene-d8 826001/14/16 B6A1403

Lab Work Order # 1601058

Page 8 of 19Page 8 of 19

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1601058-04

RLCAS #

Client ID: GP15@40'

QC Batch

Organics-Volatiles

1.0 ug/L 1 82601,1,1,2-Tetrachloroethane630-20-6 01/14/16ND B6A1403

1.0 ug/L 1 82601,1,1-Trichloroethane71-55-6 01/14/16ND B6A1403

1.0 ug/L 1 82601,1,2,2-Tetrachloroethane79-34-5 01/14/16ND B6A1403

1.0 ug/L 1 82601,1,2-Trichloroethane79-00-5 01/14/16ND B6A1403

1.0 ug/L 1 82601,1-Dichloroethane75-34-3 01/14/16ND B6A1403

1.0 ug/L 1 82601,1-Dichloroethylene75-35-4 01/14/16ND B6A1403

5.0 ug/L 1 82601,2,3-Trichlorobenzene87-61-6 01/14/16ND B6A1403

1.0 ug/L 1 82601,2,3-Trichloropropane96-18-4 01/14/16ND B6A1403

1.0 ug/L 1 82601,2,3-Trimethylbenzene526-73-8 01/14/16ND B6A1403

5.0 ug/L 1 82601,2,4-Trichlorobenzene120-82-1 01/14/16ND B6A1403

1.0 ug/L 1 82601,2,4-Trimethylbenzene95-63-6 01/14/16ND B6A1403

5.0 ug/L 1 82601,2-Dibromo-3-chloropropane96-12-8 01/14/16ND B6A1403

1.0 ug/L 1 82601,2-Dibromoethane106-93-4 01/14/16ND B6A1403

1.0 ug/L 1 82601,2-Dichlorobenzene95-50-1 01/14/16ND B6A1403

1.0 ug/L 1 82601,2-Dichloroethane107-06-2 01/14/16ND B6A1403

1.0 ug/L 1 82601,2-Dichloropropane78-87-5 01/14/16ND B6A1403

1.0 ug/L 1 82601,3,5-Trimethylbenzene108-67-8 01/14/16ND B6A1403

1.0 ug/L 1 82601,3-Dichlorobenzene541-73-1 01/14/16ND B6A1403

1.0 ug/L 1 82601,4-Dichlorobenzene106-46-7 01/14/16ND B6A1403

5.0 ug/L 1 82602-Butanone (MEK)78-93-3 01/14/16ND B6A1403

5.0 ug/L 1 82602-Hexanone591-78-6 01/14/16ND B6A1403

5.0 Xug/L 1 82602-Methylnaphthalene91-57-6 01/14/16ND B6A1403

20 ug/L 1 82602-Propanone (acetone)67-64-1 01/14/16ND B6A1403

5.0 ug/L 1 82604-Methyl-2-pentanone (MIBK)108-10-1 01/14/16ND B6A1403

5.0 ug/L 1 8260Acrylonitrile107-13-1 01/14/16ND B6A1403

1.0 ug/L 1 8260Benzene71-43-2 01/14/16ND B6A1403

1.0 ug/L 1 8260Bromobenzene108-86-1 01/14/16ND B6A1403

1.0 ug/L 1 8260Bromochloromethane74-97-5 01/14/16ND B6A1403

1.0 ug/L 1 8260Bromodichloromethane75-27-4 01/14/16ND B6A1403

1.0 ug/L 1 8260Bromoform75-25-2 01/14/16ND B6A1403

5.0 ug/L 1 8260Bromomethane74-83-9 01/14/16ND B6A1403

1.0 ug/L 1 8260Carbon disulfide75-15-0 01/14/16ND B6A1403

1.0 ug/L 1 8260Carbon tetrachloride56-23-5 01/14/16ND B6A1403

1.0 ug/L 1 8260Chlorobenzene108-90-7 01/14/16ND B6A1403

5.0 ug/L 1 8260Chloroethane75-00-3 01/14/16ND B6A1403

1.0 Tug/L 1 8260Chloroform67-66-3 01/14/160.99 B6A1403

5.0 ug/L 1 8260Chloromethane74-87-3 01/14/16ND B6A1403

1.0 ug/L 1 8260cis-1,2-Dichloroethylene156-59-2 01/14/16ND B6A1403

1.0 ug/L 1 8260cis-1,3-Dichloropropylene10061-01-5 01/14/16ND B6A1403

5.0 ug/L 1 8260Cyclohexane110-82-7 01/14/16ND B6A1403

1.0 ug/L 1 8260Dibromochloromethane124-48-1 01/14/16ND B6A1403

Lab Work Order # 1601058

Page 9 of 19Page 9 of 19

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1601058-04

RLCAS #

Client ID: GP15@40'

QC Batch

Organics-Volatiles

1.0 ug/L 1 8260Dibromomethane74-95-3 01/14/16ND B6A1403

5.0 ug/L 1 8260Dichlorodifluoromethane75-71-8 01/14/16ND B6A1403

5.0 ug/L 1 8260Diethyl ether60-29-7 01/14/16ND B6A1403

5.0 ug/L 1 8260Diisopropyl Ether108-20-3 01/14/16ND B6A1403

1.0 ug/L 1 8260Ethylbenzene100-41-4 01/14/16ND B6A1403

5.0 ug/L 1 8260Ethyltertiarybutylether637-92-3 01/14/16ND B6A1403

5.0 ug/L 1 8260Hexachloroethane67-72-1 01/14/16ND B6A1403

1.0 ug/L 1 8260Isopropylbenzene98-82-8 01/14/16ND B6A1403

2.0 ug/L 1 8260m & p - Xylene1330-20-7 01/14/16ND B6A1403

1.0 ug/L 1 8260Methyl iodide74-88-4 01/14/16ND B6A1403

5.0 ug/L 1 8260Methylene chloride75-09-2 01/14/16ND B6A1403

1.0 ug/L 1 8260Methyltertiarybutylether1634-04-4 01/14/16ND B6A1403

5.0 Xug/L 1 8260Naphthalene91-20-3 01/14/16ND B6A1403

1.0 ug/L 1 8260n-Butylbenzene104-51-8 01/14/16ND B6A1403

1.0 ug/L 1 8260n-Propylbenzene103-65-1 01/14/16ND B6A1403

1.0 ug/L 1 8260o-Xylene95-47-6 01/14/16ND B6A1403

1.0 ug/L 1 8260p-Isopropyl toluene99-87-6 01/14/16ND B6A1403

1.0 ug/L 1 8260sec-Butylbenzene135-98-8 01/14/16ND B6A1403

1.0 ug/L 1 8260Styrene100-42-5 01/14/16ND B6A1403

1.0 ug/L 1 8260tert-Butylbenzene98-06-6 01/14/16ND B6A1403

50 ug/L 1 8260tertiary Butyl Alcohol75-65-0 01/14/16ND B6A1403

5.0 ug/L 1 8260tertiaryAmylmethylether994-05-8 01/14/16ND B6A1403

1.0 ug/L 1 8260Tetrachloroethylene127-18-4 01/14/169.5 B6A1403

5.0 ug/L 1 8260Tetrahydrofuran109-99-9 01/14/16ND B6A1403

1.0 ug/L 1 8260Toluene108-88-3 01/14/16ND B6A1403

1.0 ug/L 1 8260trans-1,2-Dichloroethylene156-60-5 01/14/16ND B6A1403

1.0 ug/L 1 8260trans-1,3-Dichloropropylene10061-02-6 01/14/16ND B6A1403

5.0 ug/L 1 8260trans-1,4-Dichloro-2-butene110-57-6 01/14/16ND B6A1403

1.0 ug/L 1 8260Trichloroethylene79-01-6 01/14/16ND B6A1403

1.0 ug/L 1 8260Trichlorofluoromethane75-69-4 01/14/16ND B6A1403

1.0 ug/L 1 8260Vinyl chloride75-01-4 01/14/16ND B6A1403

85-115104 %Surrogate: Bromofluorobenzene 826001/14/16 B6A1403

82.7-11598.6 %Surrogate: Dibromofluoromethane 826001/14/16 B6A1403

85-11597.7 %Surrogate: Toluene-d8 826001/14/16 B6A1403

Lab Work Order # 1601058

Page 10 of 19Page 10 of 19

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1601058-05

RLCAS #

Client ID: GP16@25'

QC Batch

Organics-Volatiles

20 ug/L 20 82601,1,1,2-Tetrachloroethane630-20-6 01/14/16ND B6A1403

20 ug/L 20 82601,1,1-Trichloroethane71-55-6 01/14/16ND B6A1403

20 ug/L 20 82601,1,2,2-Tetrachloroethane79-34-5 01/14/16ND B6A1403

20 ug/L 20 82601,1,2-Trichloroethane79-00-5 01/14/16ND B6A1403

20 ug/L 20 82601,1-Dichloroethane75-34-3 01/14/16ND B6A1403

20 ug/L 20 82601,1-Dichloroethylene75-35-4 01/14/16ND B6A1403

100 ug/L 20 82601,2,3-Trichlorobenzene87-61-6 01/14/16ND B6A1403

20 ug/L 20 82601,2,3-Trichloropropane96-18-4 01/14/16ND B6A1403

20 ug/L 20 82601,2,3-Trimethylbenzene526-73-8 01/14/16ND B6A1403

100 ug/L 20 82601,2,4-Trichlorobenzene120-82-1 01/14/16ND B6A1403

20 ug/L 20 82601,2,4-Trimethylbenzene95-63-6 01/14/16ND B6A1403

100 ug/L 20 82601,2-Dibromo-3-chloropropane96-12-8 01/14/16ND B6A1403

20 ug/L 20 82601,2-Dibromoethane106-93-4 01/14/16ND B6A1403

20 ug/L 20 82601,2-Dichlorobenzene95-50-1 01/14/16ND B6A1403

20 ug/L 20 82601,2-Dichloroethane107-06-2 01/14/16ND B6A1403

20 ug/L 20 82601,2-Dichloropropane78-87-5 01/14/16ND B6A1403

20 ug/L 20 82601,3,5-Trimethylbenzene108-67-8 01/14/16ND B6A1403

20 ug/L 20 82601,3-Dichlorobenzene541-73-1 01/14/16ND B6A1403

20 ug/L 20 82601,4-Dichlorobenzene106-46-7 01/14/16ND B6A1403

100 ug/L 20 82602-Butanone (MEK)78-93-3 01/14/16ND B6A1403

100 ug/L 20 82602-Hexanone591-78-6 01/14/16ND B6A1403

100 Xug/L 20 82602-Methylnaphthalene91-57-6 01/14/16ND B6A1403

400 ug/L 20 82602-Propanone (acetone)67-64-1 01/14/16ND B6A1403

100 ug/L 20 82604-Methyl-2-pentanone (MIBK)108-10-1 01/14/16ND B6A1403

100 ug/L 20 8260Acrylonitrile107-13-1 01/14/16ND B6A1403

20 ug/L 20 8260Benzene71-43-2 01/14/16ND B6A1403

20 ug/L 20 8260Bromobenzene108-86-1 01/14/16ND B6A1403

20 ug/L 20 8260Bromochloromethane74-97-5 01/14/16ND B6A1403

20 ug/L 20 8260Bromodichloromethane75-27-4 01/14/16ND B6A1403

20 ug/L 20 8260Bromoform75-25-2 01/14/16ND B6A1403

100 ug/L 20 8260Bromomethane74-83-9 01/14/16ND B6A1403

20 ug/L 20 8260Carbon disulfide75-15-0 01/14/16ND B6A1403

20 ug/L 20 8260Carbon tetrachloride56-23-5 01/14/16ND B6A1403

20 ug/L 20 8260Chlorobenzene108-90-7 01/14/16ND B6A1403

100 ug/L 20 8260Chloroethane75-00-3 01/14/16ND B6A1403

20 ug/L 20 8260Chloroform67-66-3 01/14/16ND B6A1403

100 ug/L 20 8260Chloromethane74-87-3 01/14/16ND B6A1403

20 ug/L 20 8260cis-1,2-Dichloroethylene156-59-2 01/14/16ND B6A1403

20 ug/L 20 8260cis-1,3-Dichloropropylene10061-01-5 01/14/16ND B6A1403

100 ug/L 20 8260Cyclohexane110-82-7 01/14/16ND B6A1403

20 ug/L 20 8260Dibromochloromethane124-48-1 01/14/16ND B6A1403

Lab Work Order # 1601058

Page 11 of 19Page 11 of 19

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1601058-05

RLCAS #

Client ID: GP16@25'

QC Batch

Organics-Volatiles

20 ug/L 20 8260Dibromomethane74-95-3 01/14/16ND B6A1403

100 ug/L 20 8260Dichlorodifluoromethane75-71-8 01/14/16ND B6A1403

100 ug/L 20 8260Diethyl ether60-29-7 01/14/16ND B6A1403

100 ug/L 20 8260Diisopropyl Ether108-20-3 01/14/16ND B6A1403

20 ug/L 20 8260Ethylbenzene100-41-4 01/14/16ND B6A1403

100 ug/L 20 8260Ethyltertiarybutylether637-92-3 01/14/16ND B6A1403

100 ug/L 20 8260Hexachloroethane67-72-1 01/14/16ND B6A1403

20 ug/L 20 8260Isopropylbenzene98-82-8 01/14/16ND B6A1403

40 ug/L 20 8260m & p - Xylene1330-20-7 01/14/16ND B6A1403

20 ug/L 20 8260Methyl iodide74-88-4 01/14/16ND B6A1403

100 ug/L 20 8260Methylene chloride75-09-2 01/14/16ND B6A1403

20 ug/L 20 8260Methyltertiarybutylether1634-04-4 01/14/16ND B6A1403

100 Xug/L 20 8260Naphthalene91-20-3 01/14/16ND B6A1403

20 ug/L 20 8260n-Butylbenzene104-51-8 01/14/16ND B6A1403

20 ug/L 20 8260n-Propylbenzene103-65-1 01/14/16ND B6A1403

20 ug/L 20 8260o-Xylene95-47-6 01/14/16ND B6A1403

20 ug/L 20 8260p-Isopropyl toluene99-87-6 01/14/16ND B6A1403

20 ug/L 20 8260sec-Butylbenzene135-98-8 01/14/16ND B6A1403

20 ug/L 20 8260Styrene100-42-5 01/14/16ND B6A1403

20 ug/L 20 8260tert-Butylbenzene98-06-6 01/14/16ND B6A1403

1000 ug/L 20 8260tertiary Butyl Alcohol75-65-0 01/14/16ND B6A1403

100 ug/L 20 8260tertiaryAmylmethylether994-05-8 01/14/16ND B6A1403

20 ug/L 20 8260Tetrachloroethylene127-18-4 01/14/16820 B6A1403

100 ug/L 20 8260Tetrahydrofuran109-99-9 01/14/16ND B6A1403

20 ug/L 20 8260Toluene108-88-3 01/14/16ND B6A1403

20 ug/L 20 8260trans-1,2-Dichloroethylene156-60-5 01/14/16ND B6A1403

20 ug/L 20 8260trans-1,3-Dichloropropylene10061-02-6 01/14/16ND B6A1403

100 ug/L 20 8260trans-1,4-Dichloro-2-butene110-57-6 01/14/16ND B6A1403

20 ug/L 20 8260Trichloroethylene79-01-6 01/14/16ND B6A1403

20 ug/L 20 8260Trichlorofluoromethane75-69-4 01/14/16ND B6A1403

20 ug/L 20 8260Vinyl chloride75-01-4 01/14/16ND B6A1403

85-115102 %Surrogate: Bromofluorobenzene 826001/14/16 B6A1403

82.7-115101 %Surrogate: Dibromofluoromethane 826001/14/16 B6A1403

85-11599.8 %Surrogate: Toluene-d8 826001/14/16 B6A1403

Lab Work Order # 1601058

Page 12 of 19Page 12 of 19

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1601058-06

RLCAS #

Client ID: GP16@30

QC Batch

Organics-Volatiles

1.0 ug/L 1 82601,1,1,2-Tetrachloroethane630-20-6 01/15/16ND B6A1502

1.0 ug/L 1 82601,1,1-Trichloroethane71-55-6 01/15/16ND B6A1502

1.0 ug/L 1 82601,1,2,2-Tetrachloroethane79-34-5 01/15/16ND B6A1502

1.0 ug/L 1 82601,1,2-Trichloroethane79-00-5 01/15/16ND B6A1502

1.0 ug/L 1 82601,1-Dichloroethane75-34-3 01/15/16ND B6A1502

1.0 ug/L 1 82601,1-Dichloroethylene75-35-4 01/15/16ND B6A1502

5.0 ug/L 1 82601,2,3-Trichlorobenzene87-61-6 01/15/16ND B6A1502

1.0 ug/L 1 82601,2,3-Trichloropropane96-18-4 01/15/16ND B6A1502

1.0 ug/L 1 82601,2,3-Trimethylbenzene526-73-8 01/15/16ND B6A1502

5.0 ug/L 1 82601,2,4-Trichlorobenzene120-82-1 01/15/16ND B6A1502

1.0 ug/L 1 82601,2,4-Trimethylbenzene95-63-6 01/15/16ND B6A1502

5.0 ug/L 1 82601,2-Dibromo-3-chloropropane96-12-8 01/15/16ND B6A1502

1.0 ug/L 1 82601,2-Dibromoethane106-93-4 01/15/16ND B6A1502

1.0 ug/L 1 82601,2-Dichlorobenzene95-50-1 01/15/16ND B6A1502

1.0 ug/L 1 82601,2-Dichloroethane107-06-2 01/15/16ND B6A1502

1.0 ug/L 1 82601,2-Dichloropropane78-87-5 01/15/16ND B6A1502

1.0 ug/L 1 82601,3,5-Trimethylbenzene108-67-8 01/15/16ND B6A1502

1.0 ug/L 1 82601,3-Dichlorobenzene541-73-1 01/15/16ND B6A1502

1.0 ug/L 1 82601,4-Dichlorobenzene106-46-7 01/15/16ND B6A1502

5.0 ug/L 1 82602-Butanone (MEK)78-93-3 01/15/16ND B6A1502

5.0 ug/L 1 82602-Hexanone591-78-6 01/15/16ND B6A1502

5.0 Xug/L 1 82602-Methylnaphthalene91-57-6 01/15/16ND B6A1502

20 ug/L 1 82602-Propanone (acetone)67-64-1 01/15/16ND B6A1502

5.0 ug/L 1 82604-Methyl-2-pentanone (MIBK)108-10-1 01/15/16ND B6A1502

5.0 ug/L 1 8260Acrylonitrile107-13-1 01/15/16ND B6A1502

1.0 ug/L 1 8260Benzene71-43-2 01/15/16ND B6A1502

1.0 ug/L 1 8260Bromobenzene108-86-1 01/15/16ND B6A1502

1.0 ug/L 1 8260Bromochloromethane74-97-5 01/15/16ND B6A1502

1.0 ug/L 1 8260Bromodichloromethane75-27-4 01/15/16ND B6A1502

1.0 ug/L 1 8260Bromoform75-25-2 01/15/16ND B6A1502

5.0 ug/L 1 8260Bromomethane74-83-9 01/15/16ND B6A1502

1.0 ug/L 1 8260Carbon disulfide75-15-0 01/15/16ND B6A1502

1.0 ug/L 1 8260Carbon tetrachloride56-23-5 01/15/16ND B6A1502

1.0 ug/L 1 8260Chlorobenzene108-90-7 01/15/16ND B6A1502

5.0 ug/L 1 8260Chloroethane75-00-3 01/15/16ND B6A1502

1.0 ug/L 1 8260Chloroform67-66-3 01/15/16ND B6A1502

5.0 ug/L 1 8260Chloromethane74-87-3 01/15/16ND B6A1502

1.0 ug/L 1 8260cis-1,2-Dichloroethylene156-59-2 01/15/16ND B6A1502

1.0 ug/L 1 8260cis-1,3-Dichloropropylene10061-01-5 01/15/16ND B6A1502

5.0 ug/L 1 8260Cyclohexane110-82-7 01/15/16ND B6A1502

1.0 ug/L 1 8260Dibromochloromethane124-48-1 01/15/16ND B6A1502

Lab Work Order # 1601058

Page 13 of 19Page 13 of 19

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1601058-06

RLCAS #

Client ID: GP16@30

QC Batch

Organics-Volatiles

1.0 ug/L 1 8260Dibromomethane74-95-3 01/15/16ND B6A1502

5.0 A05ug/L 1 8260Dichlorodifluoromethane75-71-8 01/15/16ND B6A1502

5.0 ug/L 1 8260Diethyl ether60-29-7 01/15/16ND B6A1502

5.0 ug/L 1 8260Diisopropyl Ether108-20-3 01/15/16ND B6A1502

1.0 ug/L 1 8260Ethylbenzene100-41-4 01/15/16ND B6A1502

5.0 ug/L 1 8260Ethyltertiarybutylether637-92-3 01/15/16ND B6A1502

5.0 ug/L 1 8260Hexachloroethane67-72-1 01/15/16ND B6A1502

1.0 ug/L 1 8260Isopropylbenzene98-82-8 01/15/16ND B6A1502

2.0 ug/L 1 8260m & p - Xylene1330-20-7 01/15/16ND B6A1502

1.0 ug/L 1 8260Methyl iodide74-88-4 01/15/16ND B6A1502

5.0 ug/L 1 8260Methylene chloride75-09-2 01/15/16ND B6A1502

1.0 ug/L 1 8260Methyltertiarybutylether1634-04-4 01/15/16ND B6A1502

5.0 Xug/L 1 8260Naphthalene91-20-3 01/15/16ND B6A1502

1.0 ug/L 1 8260n-Butylbenzene104-51-8 01/15/16ND B6A1502

1.0 ug/L 1 8260n-Propylbenzene103-65-1 01/15/16ND B6A1502

1.0 ug/L 1 8260o-Xylene95-47-6 01/15/16ND B6A1502

1.0 ug/L 1 8260p-Isopropyl toluene99-87-6 01/15/16ND B6A1502

1.0 ug/L 1 8260sec-Butylbenzene135-98-8 01/15/16ND B6A1502

1.0 ug/L 1 8260Styrene100-42-5 01/15/16ND B6A1502

1.0 ug/L 1 8260tert-Butylbenzene98-06-6 01/15/16ND B6A1502

50 ug/L 1 8260tertiary Butyl Alcohol75-65-0 01/15/16ND B6A1502

5.0 ug/L 1 8260tertiaryAmylmethylether994-05-8 01/15/16ND B6A1502

1.0 ug/L 1 8260Tetrachloroethylene127-18-4 01/15/1611 B6A1502

5.0 ug/L 1 8260Tetrahydrofuran109-99-9 01/15/16ND B6A1502

1.0 ug/L 1 8260Toluene108-88-3 01/15/16ND B6A1502

1.0 ug/L 1 8260trans-1,2-Dichloroethylene156-60-5 01/15/16ND B6A1502

1.0 ug/L 1 8260trans-1,3-Dichloropropylene10061-02-6 01/15/16ND B6A1502

5.0 ug/L 1 8260trans-1,4-Dichloro-2-butene110-57-6 01/15/16ND B6A1502

1.0 ug/L 1 8260Trichloroethylene79-01-6 01/15/16ND B6A1502

1.0 ug/L 1 8260Trichlorofluoromethane75-69-4 01/15/16ND B6A1502

1.0 ug/L 1 8260Vinyl chloride75-01-4 01/15/16ND B6A1502

85-115102 %Surrogate: Bromofluorobenzene 826001/15/16 B6A1502

82.7-115101 %Surrogate: Dibromofluoromethane 826001/15/16 B6A1502

85-115100 %Surrogate: Toluene-d8 826001/15/16 B6A1502

Lab Work Order # 1601058

Page 14 of 19Page 14 of 19

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1601058-07

RLCAS #

Client ID: GP16@35

QC Batch

Organics-Volatiles

1.0 ug/L 1 82601,1,1,2-Tetrachloroethane630-20-6 01/15/16ND B6A1502

1.0 ug/L 1 82601,1,1-Trichloroethane71-55-6 01/15/16ND B6A1502

1.0 ug/L 1 82601,1,2,2-Tetrachloroethane79-34-5 01/15/16ND B6A1502

1.0 ug/L 1 82601,1,2-Trichloroethane79-00-5 01/15/16ND B6A1502

1.0 ug/L 1 82601,1-Dichloroethane75-34-3 01/15/16ND B6A1502

1.0 ug/L 1 82601,1-Dichloroethylene75-35-4 01/15/16ND B6A1502

5.0 ug/L 1 82601,2,3-Trichlorobenzene87-61-6 01/15/16ND B6A1502

1.0 ug/L 1 82601,2,3-Trichloropropane96-18-4 01/15/16ND B6A1502

1.0 ug/L 1 82601,2,3-Trimethylbenzene526-73-8 01/15/16ND B6A1502

5.0 ug/L 1 82601,2,4-Trichlorobenzene120-82-1 01/15/16ND B6A1502

1.0 ug/L 1 82601,2,4-Trimethylbenzene95-63-6 01/15/16ND B6A1502

5.0 ug/L 1 82601,2-Dibromo-3-chloropropane96-12-8 01/15/16ND B6A1502

1.0 ug/L 1 82601,2-Dibromoethane106-93-4 01/15/16ND B6A1502

1.0 ug/L 1 82601,2-Dichlorobenzene95-50-1 01/15/16ND B6A1502

1.0 ug/L 1 82601,2-Dichloroethane107-06-2 01/15/16ND B6A1502

1.0 ug/L 1 82601,2-Dichloropropane78-87-5 01/15/16ND B6A1502

1.0 ug/L 1 82601,3,5-Trimethylbenzene108-67-8 01/15/16ND B6A1502

1.0 ug/L 1 82601,3-Dichlorobenzene541-73-1 01/15/16ND B6A1502

1.0 ug/L 1 82601,4-Dichlorobenzene106-46-7 01/15/16ND B6A1502

5.0 ug/L 1 82602-Butanone (MEK)78-93-3 01/15/16ND B6A1502

5.0 ug/L 1 82602-Hexanone591-78-6 01/15/16ND B6A1502

5.0 Xug/L 1 82602-Methylnaphthalene91-57-6 01/15/16ND B6A1502

20 ug/L 1 82602-Propanone (acetone)67-64-1 01/15/16ND B6A1502

5.0 ug/L 1 82604-Methyl-2-pentanone (MIBK)108-10-1 01/15/16ND B6A1502

5.0 ug/L 1 8260Acrylonitrile107-13-1 01/15/16ND B6A1502

1.0 ug/L 1 8260Benzene71-43-2 01/15/16ND B6A1502

1.0 ug/L 1 8260Bromobenzene108-86-1 01/15/16ND B6A1502

1.0 ug/L 1 8260Bromochloromethane74-97-5 01/15/16ND B6A1502

1.0 ug/L 1 8260Bromodichloromethane75-27-4 01/15/16ND B6A1502

1.0 ug/L 1 8260Bromoform75-25-2 01/15/16ND B6A1502

5.0 ug/L 1 8260Bromomethane74-83-9 01/15/16ND B6A1502

1.0 ug/L 1 8260Carbon disulfide75-15-0 01/15/16ND B6A1502

1.0 ug/L 1 8260Carbon tetrachloride56-23-5 01/15/16ND B6A1502

1.0 ug/L 1 8260Chlorobenzene108-90-7 01/15/16ND B6A1502

5.0 ug/L 1 8260Chloroethane75-00-3 01/15/16ND B6A1502

1.0 ug/L 1 8260Chloroform67-66-3 01/15/16ND B6A1502

5.0 ug/L 1 8260Chloromethane74-87-3 01/15/16ND B6A1502

1.0 ug/L 1 8260cis-1,2-Dichloroethylene156-59-2 01/15/16ND B6A1502

1.0 ug/L 1 8260cis-1,3-Dichloropropylene10061-01-5 01/15/16ND B6A1502

5.0 ug/L 1 8260Cyclohexane110-82-7 01/15/16ND B6A1502

1.0 ug/L 1 8260Dibromochloromethane124-48-1 01/15/16ND B6A1502

Lab Work Order # 1601058

Page 15 of 19Page 15 of 19

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1601058-07

RLCAS #

Client ID: GP16@35

QC Batch

Organics-Volatiles

1.0 ug/L 1 8260Dibromomethane74-95-3 01/15/16ND B6A1502

5.0 A05ug/L 1 8260Dichlorodifluoromethane75-71-8 01/15/16ND B6A1502

5.0 ug/L 1 8260Diethyl ether60-29-7 01/15/16ND B6A1502

5.0 ug/L 1 8260Diisopropyl Ether108-20-3 01/15/16ND B6A1502

1.0 ug/L 1 8260Ethylbenzene100-41-4 01/15/16ND B6A1502

5.0 ug/L 1 8260Ethyltertiarybutylether637-92-3 01/15/16ND B6A1502

5.0 ug/L 1 8260Hexachloroethane67-72-1 01/15/16ND B6A1502

1.0 ug/L 1 8260Isopropylbenzene98-82-8 01/15/16ND B6A1502

2.0 ug/L 1 8260m & p - Xylene1330-20-7 01/15/16ND B6A1502

1.0 ug/L 1 8260Methyl iodide74-88-4 01/15/16ND B6A1502

5.0 ug/L 1 8260Methylene chloride75-09-2 01/15/16ND B6A1502

1.0 ug/L 1 8260Methyltertiarybutylether1634-04-4 01/15/16ND B6A1502

5.0 Xug/L 1 8260Naphthalene91-20-3 01/15/16ND B6A1502

1.0 ug/L 1 8260n-Butylbenzene104-51-8 01/15/16ND B6A1502

1.0 ug/L 1 8260n-Propylbenzene103-65-1 01/15/16ND B6A1502

1.0 ug/L 1 8260o-Xylene95-47-6 01/15/16ND B6A1502

1.0 ug/L 1 8260p-Isopropyl toluene99-87-6 01/15/16ND B6A1502

1.0 ug/L 1 8260sec-Butylbenzene135-98-8 01/15/16ND B6A1502

1.0 ug/L 1 8260Styrene100-42-5 01/15/16ND B6A1502

1.0 ug/L 1 8260tert-Butylbenzene98-06-6 01/15/16ND B6A1502

50 ug/L 1 8260tertiary Butyl Alcohol75-65-0 01/15/16ND B6A1502

5.0 ug/L 1 8260tertiaryAmylmethylether994-05-8 01/15/16ND B6A1502

1.0 ug/L 1 8260Tetrachloroethylene127-18-4 01/15/163.3 B6A1502

5.0 ug/L 1 8260Tetrahydrofuran109-99-9 01/15/16ND B6A1502

1.0 ug/L 1 8260Toluene108-88-3 01/15/16ND B6A1502

1.0 ug/L 1 8260trans-1,2-Dichloroethylene156-60-5 01/15/16ND B6A1502

1.0 ug/L 1 8260trans-1,3-Dichloropropylene10061-02-6 01/15/16ND B6A1502

5.0 ug/L 1 8260trans-1,4-Dichloro-2-butene110-57-6 01/15/16ND B6A1502

1.0 ug/L 1 8260Trichloroethylene79-01-6 01/15/16ND B6A1502

1.0 ug/L 1 8260Trichlorofluoromethane75-69-4 01/15/16ND B6A1502

1.0 ug/L 1 8260Vinyl chloride75-01-4 01/15/16ND B6A1502

85-115102 %Surrogate: Bromofluorobenzene 826001/15/16 B6A1502

82.7-11599.3 %Surrogate: Dibromofluoromethane 826001/15/16 B6A1502

85-11599.5 %Surrogate: Toluene-d8 826001/15/16 B6A1502

Lab Work Order # 1601058

Page 16 of 19Page 16 of 19

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1601058-08

RLCAS #

Client ID: GP16@40

QC Batch

Organics-Volatiles

1.0 ug/L 1 82601,1,1,2-Tetrachloroethane630-20-6 01/15/16ND B6A1502

1.0 ug/L 1 82601,1,1-Trichloroethane71-55-6 01/15/16ND B6A1502

1.0 ug/L 1 82601,1,2,2-Tetrachloroethane79-34-5 01/15/16ND B6A1502

1.0 ug/L 1 82601,1,2-Trichloroethane79-00-5 01/15/16ND B6A1502

1.0 ug/L 1 82601,1-Dichloroethane75-34-3 01/15/16ND B6A1502

1.0 ug/L 1 82601,1-Dichloroethylene75-35-4 01/15/16ND B6A1502

5.0 ug/L 1 82601,2,3-Trichlorobenzene87-61-6 01/15/16ND B6A1502

1.0 ug/L 1 82601,2,3-Trichloropropane96-18-4 01/15/16ND B6A1502

1.0 ug/L 1 82601,2,3-Trimethylbenzene526-73-8 01/15/16ND B6A1502

5.0 ug/L 1 82601,2,4-Trichlorobenzene120-82-1 01/15/16ND B6A1502

1.0 ug/L 1 82601,2,4-Trimethylbenzene95-63-6 01/15/16ND B6A1502

5.0 ug/L 1 82601,2-Dibromo-3-chloropropane96-12-8 01/15/16ND B6A1502

1.0 ug/L 1 82601,2-Dibromoethane106-93-4 01/15/16ND B6A1502

1.0 ug/L 1 82601,2-Dichlorobenzene95-50-1 01/15/16ND B6A1502

1.0 ug/L 1 82601,2-Dichloroethane107-06-2 01/15/16ND B6A1502

1.0 ug/L 1 82601,2-Dichloropropane78-87-5 01/15/16ND B6A1502

1.0 ug/L 1 82601,3,5-Trimethylbenzene108-67-8 01/15/16ND B6A1502

1.0 ug/L 1 82601,3-Dichlorobenzene541-73-1 01/15/16ND B6A1502

1.0 ug/L 1 82601,4-Dichlorobenzene106-46-7 01/15/16ND B6A1502

5.0 ug/L 1 82602-Butanone (MEK)78-93-3 01/15/16ND B6A1502

5.0 ug/L 1 82602-Hexanone591-78-6 01/15/16ND B6A1502

5.0 Xug/L 1 82602-Methylnaphthalene91-57-6 01/15/16ND B6A1502

20 ug/L 1 82602-Propanone (acetone)67-64-1 01/15/16ND B6A1502

5.0 ug/L 1 82604-Methyl-2-pentanone (MIBK)108-10-1 01/15/16ND B6A1502

5.0 ug/L 1 8260Acrylonitrile107-13-1 01/15/16ND B6A1502

1.0 ug/L 1 8260Benzene71-43-2 01/15/16ND B6A1502

1.0 ug/L 1 8260Bromobenzene108-86-1 01/15/16ND B6A1502

1.0 ug/L 1 8260Bromochloromethane74-97-5 01/15/16ND B6A1502

1.0 ug/L 1 8260Bromodichloromethane75-27-4 01/15/16ND B6A1502

1.0 ug/L 1 8260Bromoform75-25-2 01/15/16ND B6A1502

5.0 ug/L 1 8260Bromomethane74-83-9 01/15/16ND B6A1502

1.0 ug/L 1 8260Carbon disulfide75-15-0 01/15/16ND B6A1502

1.0 ug/L 1 8260Carbon tetrachloride56-23-5 01/15/16ND B6A1502

1.0 ug/L 1 8260Chlorobenzene108-90-7 01/15/16ND B6A1502

5.0 ug/L 1 8260Chloroethane75-00-3 01/15/16ND B6A1502

1.0 Tug/L 1 8260Chloroform67-66-3 01/15/160.99 B6A1502

5.0 ug/L 1 8260Chloromethane74-87-3 01/15/16ND B6A1502

1.0 ug/L 1 8260cis-1,2-Dichloroethylene156-59-2 01/15/16ND B6A1502

1.0 ug/L 1 8260cis-1,3-Dichloropropylene10061-01-5 01/15/16ND B6A1502

5.0 ug/L 1 8260Cyclohexane110-82-7 01/15/16ND B6A1502

1.0 ug/L 1 8260Dibromochloromethane124-48-1 01/15/16ND B6A1502

Lab Work Order # 1601058

Page 17 of 19Page 17 of 19

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1601058-08

RLCAS #

Client ID: GP16@40

QC Batch

Organics-Volatiles

1.0 ug/L 1 8260Dibromomethane74-95-3 01/15/16ND B6A1502

5.0 A05ug/L 1 8260Dichlorodifluoromethane75-71-8 01/15/16ND B6A1502

5.0 ug/L 1 8260Diethyl ether60-29-7 01/15/16ND B6A1502

5.0 ug/L 1 8260Diisopropyl Ether108-20-3 01/15/16ND B6A1502

1.0 ug/L 1 8260Ethylbenzene100-41-4 01/15/16ND B6A1502

5.0 ug/L 1 8260Ethyltertiarybutylether637-92-3 01/15/16ND B6A1502

5.0 ug/L 1 8260Hexachloroethane67-72-1 01/15/16ND B6A1502

1.0 ug/L 1 8260Isopropylbenzene98-82-8 01/15/16ND B6A1502

2.0 ug/L 1 8260m & p - Xylene1330-20-7 01/15/16ND B6A1502

1.0 ug/L 1 8260Methyl iodide74-88-4 01/15/16ND B6A1502

5.0 ug/L 1 8260Methylene chloride75-09-2 01/15/16ND B6A1502

1.0 ug/L 1 8260Methyltertiarybutylether1634-04-4 01/15/16ND B6A1502

5.0 Xug/L 1 8260Naphthalene91-20-3 01/15/16ND B6A1502

1.0 ug/L 1 8260n-Butylbenzene104-51-8 01/15/16ND B6A1502

1.0 ug/L 1 8260n-Propylbenzene103-65-1 01/15/16ND B6A1502

1.0 ug/L 1 8260o-Xylene95-47-6 01/15/16ND B6A1502

1.0 ug/L 1 8260p-Isopropyl toluene99-87-6 01/15/16ND B6A1502

1.0 ug/L 1 8260sec-Butylbenzene135-98-8 01/15/16ND B6A1502

1.0 ug/L 1 8260Styrene100-42-5 01/15/16ND B6A1502

1.0 ug/L 1 8260tert-Butylbenzene98-06-6 01/15/16ND B6A1502

50 ug/L 1 8260tertiary Butyl Alcohol75-65-0 01/15/16ND B6A1502

5.0 ug/L 1 8260tertiaryAmylmethylether994-05-8 01/15/16ND B6A1502

1.0 ug/L 1 8260Tetrachloroethylene127-18-4 01/15/167.5 B6A1502

5.0 ug/L 1 8260Tetrahydrofuran109-99-9 01/15/16ND B6A1502

1.0 ug/L 1 8260Toluene108-88-3 01/15/16ND B6A1502

1.0 ug/L 1 8260trans-1,2-Dichloroethylene156-60-5 01/15/16ND B6A1502

1.0 ug/L 1 8260trans-1,3-Dichloropropylene10061-02-6 01/15/16ND B6A1502

5.0 ug/L 1 8260trans-1,4-Dichloro-2-butene110-57-6 01/15/16ND B6A1502

1.0 ug/L 1 8260Trichloroethylene79-01-6 01/15/16ND B6A1502

1.0 ug/L 1 8260Trichlorofluoromethane75-69-4 01/15/16ND B6A1502

1.0 ug/L 1 8260Vinyl chloride75-01-4 01/15/16ND B6A1502

85-115102 %Surrogate: Bromofluorobenzene 826001/15/16 B6A1502

82.7-115101 %Surrogate: Dibromofluoromethane 826001/15/16 B6A1502

85-11597.3 %Surrogate: Toluene-d8 826001/15/16 B6A1502

Lab Work Order # 1601058

Page 18 of 19Page 18 of 19

Page 19 of 19

top related