matrix: derivative certificate of analysis
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This report shall not be reproduced, unless in its entirety, without written approval from Kaycha Labs. This report isan Kaycha Labs certification. The results relate only to the material or product analyzed. Test results areconfidential unless explicitly waived otherwise. Void after 1 year from test end date. Cannabinoid content of batchmaterial may vary depending on sampling error. IC=In-control QC parameter, NC=Non-controlled QC parameter,ND=Not Detected, NA=Not Analyzed, ppm=Parts Per Million, ppb=Parts Per Billion. Limit of Detection (LoD) andLimit Of Quantitation (LoQ) are terms used to describe the smallest concentration that can be reliably measured byan analytical procedure. RPD=Reproducibility of two measurements. Action Levels are State determined thresholdsfor human safety for consumption and/or inhalation. The result >99% are variable based on uncertainty ofmeasurement (UM) for the analyte. The UM error is available from the lab upon request.The "Decision Rule" for thepass/fail does not include the UM. The limits are based on F.S. Rule 64-4.310.
Jorge SegredoLab Director
State License # CMTL-0002ISO Accreditation # ISO/IEC17025:2017 Accreditation
PJLA-Testing 97164
___________________Signature
04/20/2021
___________________Signed On
4131 SW 47th AVENUE SUITE 1408DAVIE, FL, 33314, US
Kaycha LabsMíami Vibes Drops 11,25g
Miami VibesMatrix: Derivative
Certificateof Analysis
Sample:DA10414006-005Harvest/Lot ID: 6858 3748 8454 2841
Cultivation Facility: Tampa CultivationProcessing Facility : Tampa Processing
Seed to Sale #6858 3748 8454 2841Batch Date :02/03/21
Batch#: 9564 8680 8642 3515Sample Size Received: 6 units
Total Weight/Volume: 1426 unitsRetail Product Size: 11.25 gram
Ordered : 04/13/21sampled : 04/13/21
Completed: 04/20/21Sampling Method: SOP.T.20.010
Apr 20, 2021 | FLUENT82 NE 26th streetMiami, FL, 33137, US
PASSEDPage 1 of 5
PRODUCT IMAGE SAFETY RESULTS MISC.
PesticidesPASSED
Heavy MetalsPASSED
MicrobialsPASSED
MycotoxinsPASSED
ResidualsSolventsPASSED
FilthPASSED
Water ActivityPASSED
MoistureNOT TESTED
TerpenesTESTED
CANNABINOID RESULTS
Total THC
4.119%TOTAL THC/Container :463.421mg
Total CBD
0.269%TOTAL CBD/Container :30.263 mg
Total Cannabinoids
4.664%Total Cannabinoids/Container:524.700 mg
CBDV CBDA CBGA CBG CBD THCV CBN D9-THC D8-THC CBC THCA
% ND <0.010 0.015 0.119 0.269 0.026 0.043 4.100 ND 0.070 0.022
mg/g ND <0.010 0.150 1.190 2.690 0.260 0.430 41.000 ND 0.700 0.220
LOD 0.001 0.001 0.001 0.001 0.0001 0.001 0.001 0.0001 0.001 0.001 0.001
% % % % % % % % % % %
Cannabinoid Profile TestAnalyzed by Weight Extraction date : Extracted By :450 3.0031g 04/14/21 01:04:42 2198Analysis Method -SOP.T.40.020, SOP.T.30.050 Reviewed On - 04/15/21 11:24:55 Batch Date : 04/14/21 09:50:30Analytical Batch -DA025002POT Instrument Used : DA-LC-002
Reagent Dilution Consums. ID
041421.R12 400 287035261021121.36 76262-590041421.R02 914C4-914AK
929C6-929HFull spectrum cannabinoid analysis utilizing High Performance Liquid Chromatography with UV detection (HPLC-UV). (Method: SOP.T.30.050 for sample prep andShimadzu High Sensitivity Method SOP.T.40.020 for analysis. LOQ for all cannabinoids is 1 mg/L).
Filth PASSEDAnalyzed By Weight Extraction date Extracted By457 NA NA NAAnalyte LOD ResultFilth and Foreign Material 0.1 NDAnalysis Method -SOP.T.40.013 Batch Date : 04/14/21 12:45:29Analytical Batch -DA025037FIL Reviewed On - 04/14/21 14:33:25Instrument Used : Filth/Foreign Material Microscope
This includes but is not limited to hair, insects, feces, packaging contaminants, and manufacturing wasteand by-products. An SH-2B/T Stereo Microscope is use for inspection.
Water Activity PASSEDAnalyte Analyzed by Weight Ext. date LOD A.L ResultWATER ACTIVITY 457 NA NA 0.01 aw 0.85aw 0.418aWAnalysis Method -Water ActivitySOP.T.40.010 Batch Date : 04/14/21 12:38:36Analytical Batch -DA025036WAT Reviewed On - 04/14/21 16:12:10Instrument Used : DA-028 Rotronic Hygropalm
This report shall not be reproduced, unless in its entirety, without written approval from Kaycha Labs. This report isan Kaycha Labs certification. The results relate only to the material or product analyzed. Test results areconfidential unless explicitly waived otherwise. Void after 1 year from test end date. Cannabinoid content of batchmaterial may vary depending on sampling error. IC=In-control QC parameter, NC=Non-controlled QC parameter,ND=Not Detected, NA=Not Analyzed, ppm=Parts Per Million, ppb=Parts Per Billion. Limit of Detection (LoD) andLimit Of Quantitation (LoQ) are terms used to describe the smallest concentration that can be reliably measured byan analytical procedure. RPD=Reproducibility of two measurements. Action Levels are State determined thresholdsfor human safety for consumption and/or inhalation. The result >99% are variable based on uncertainty ofmeasurement (UM) for the analyte. The UM error is available from the lab upon request.The "Decision Rule" for thepass/fail does not include the UM. The limits are based on F.S. Rule 64-4.310.
Jorge SegredoLab Director
State License # CMTL-0002ISO Accreditation # ISO/IEC17025:2017 Accreditation
PJLA-Testing 97164
___________________Signature
04/20/2021
___________________Signed On
4131 SW 47th AVENUE SUITE 1408DAVIE, FL, 33314, US
Kaycha LabsMíami Vibes Drops 11,25g
Miami VibesMatrix : Derivative
Certificate of Analysis PASSEDFLUENT
82 NE 26th streetMiami, FL, 33137, USTelephone: (305) 900-6266Email: Sam@getfluent.com
Sample : DA10414006-005Harvest/LOT ID: 6858 3748 8454 2841Batch# : 9564 86808642 3515Sampled : 04/13/21Ordered : 04/13/21
Sample Size Received : 6 unitsTotal Weight/Volume : 1426 unitsCompleted : 04/20/21Expires: 04/20/22Sample Method : SOP.T.20.010
Page 2 of 5
Terpenes TESTEDTerpenes LOD(%) mg/g % Result (%)
CAMPHENE 0.007 ND NDBETA-MYRCENE 0.007 0.936 0.093ALPHA-PHELLANDRENE
0.007 0.073 0.007
3-CARENE 0.007 < 0.2 < 0.020OCIMENE 0.007 ND NDEUCALYPTOL 0.007 ND NDLINALOOL 0.007 < 0.2 < 0.020FENCHONE 0.007 ND NDISOPULEGOL 0.007 ND NDISOBORNEOL 0.007 ND NDHEXAHYDROTHYMOL
0.007 < 0.2 < 0.020
NEROL 0.007 ND NDGERANYL ACETATE 0.007 ND NDBETA-CARYOPHYLLENE
0.007 0.393 0.039
VALENCENE 0.007 < 0.2 < 0.020CIS-NEROLIDOL 0.007 ND NDCARYOPHYLLENEOXIDE
0.007 ND ND
CEDROL 0.007 ND NDFARNESENE 0.007 < 0.2 < 0.020ALPHA-BISABOLOL 0.007 < 0.2 < 0.020ALPHA-PINENE 0.007 < 0.2 < 0.020SABINENE 0.007 ND NDBETA-PINENE 0.007 0.208 0.020ALPHA-TERPINENE 0.007 < 0.2 < 0.020LIMONENE 0.007 0.582 0.058GAMMA-TERPINENE
0.007 ND ND
TERPINOLENE 0.007 3.446 0.344SABINENEHYDRATE
0.007 ND ND
FENCHYL ALCOHOL 0.007 ND NDCAMPHOR 0.013 ND NDBORNEOL 0.013 ND ND
Terpenes LOD(%) mg/g % Result (%)
TERPINEOL 0.007 ND NDGERANIOL 0.007 ND NDPULEGONE 0.007 ND NDALPHA-CEDRENE 0.007 ND NDALPHA-HUMULENE 0.007 < 0.2 < 0.020TRANS-NEROLIDOL 0.007 ND NDGUAIOL 0.007 0.079 0.007
Terpenes TESTED
Analyzed by Weight Extraction date Extracted By574 1.0138g 04/15/21 12:04:41 2651
Analysis Method -SOP.T.40.090Analytical Batch -DA024996TER Reviewed On - 04/19/21 17:56:09Instrument Used : DA-GCMS-004Running On : 04/16/21 17:53:09Batch Date : 04/14/21 09:09:08
Reagent Dilution Consums. ID
032521.R01 10 CE0123R1AB59720
Terpenoid profile screening is performed using GC-MS with Liquid Injection(Gas Chromatography – Mass Spectrometer) which can screen 38 terpenesusing Method SOP.T.40.091 Terpenoid Analysis Via GC/MS.
Total (%) 0.556
This report shall not be reproduced, unless in its entirety, without written approval from Kaycha Labs. This report isan Kaycha Labs certification. The results relate only to the material or product analyzed. Test results areconfidential unless explicitly waived otherwise. Void after 1 year from test end date. Cannabinoid content of batchmaterial may vary depending on sampling error. IC=In-control QC parameter, NC=Non-controlled QC parameter,ND=Not Detected, NA=Not Analyzed, ppm=Parts Per Million, ppb=Parts Per Billion. Limit of Detection (LoD) andLimit Of Quantitation (LoQ) are terms used to describe the smallest concentration that can be reliably measured byan analytical procedure. RPD=Reproducibility of two measurements. Action Levels are State determined thresholdsfor human safety for consumption and/or inhalation. The result >99% are variable based on uncertainty ofmeasurement (UM) for the analyte. The UM error is available from the lab upon request.The "Decision Rule" for thepass/fail does not include the UM. The limits are based on F.S. Rule 64-4.310.
Jorge SegredoLab Director
State License # CMTL-0002ISO Accreditation # ISO/IEC17025:2017 Accreditation
PJLA-Testing 97164
___________________Signature
04/20/2021
___________________Signed On
4131 SW 47th AVENUE SUITE 1408DAVIE, FL, 33314, US
Kaycha LabsMíami Vibes Drops 11,25g
Miami VibesMatrix : Derivative
Certificate of Analysis PASSEDFLUENT
82 NE 26th streetMiami, FL, 33137, USTelephone: (305) 900-6266Email: Sam@getfluent.com
Sample : DA10414006-005Harvest/LOT ID: 6858 3748 8454 2841Batch# : 9564 86808642 3515Sampled : 04/13/21Ordered : 04/13/21
Sample Size Received : 6 unitsTotal Weight/Volume : 1426 unitsCompleted : 04/20/21Expires: 04/20/22Sample Method : SOP.T.20.010
Page 3 of 5
Pesticides PASSEDPesticides LOD Units Action Level ResultABAMECTIN B1A 0.01 ppm 0.3 NDACEPHATE 0.01 ppm 3 NDACEQUINOCYL 0.01 ppm 2 NDACETAMIPRID 0.01 ppm 3 NDALDICARB 0.01 ppm 0.1 NDAZOXYSTROBIN 0.01 ppm 3 NDBIFENAZATE 0.01 ppm 3 NDBIFENTHRIN 0.01 ppm 0.5 NDBOSCALID 0.01 PPM 3 NDCARBARYL 0.05 ppm 0.5 NDCARBOFURAN 0.01 ppm 0.1 NDCHLORANTRANILIPROLE 0.1 ppm 3 NDCHLORMEQUAT CHLORIDE 0.1 ppm 3 NDCHLORPYRIFOS 0.01 ppm 0.1 NDCLOFENTEZINE 0.02 ppm 0.5 NDCOUMAPHOS 0.01 ppm 0.1 NDDAMINOZIDE 0.01 ppm 0.1 NDDIAZINON 0.01 ppm NDDICHLORVOS 0.01 ppm 0.1 NDDIMETHOATE 0.01 ppm 0.1 NDETHOPROPHOS 0.01 ppm 0.1 NDETOFENPROX 0.01 ppm 0.1 NDETOXAZOLE 0.01 ppm 1.5 NDFENHEXAMID 0.01 ppm 3 NDFENOXYCARB 0.01 ppm 0.1 NDFENPYROXIMATE 0.01 ppm 2 NDFIPRONIL 0.01 ppm 0.1 NDFLONICAMID 0.01 ppm 2 NDFLUDIOXONIL 0.01 ppm 3 NDHEXYTHIAZOX 0.01 ppm 2 NDIMAZALIL 0.01 ppm 0.1 NDIMIDACLOPRID 0.04 ppm 3 NDKRESOXIM-METHYL 0.01 ppm 1 NDMALATHION 0.02 ppm 2 NDMETALAXYL 0.01 ppm 3 NDMETHIOCARB 0.01 ppm 0.1 NDMETHOMYL 0.01 ppm 0.1 NDMEVINPHOS 0.01 ppm 0.1 NDMYCLOBUTANIL 0.01 ppm 3 NDNALED 0.025 ppm 0.5 NDOXAMYL 0.05 ppm 0.5 NDPACLOBUTRAZOL 0.01 ppm 0.1 NDPHOSMET 0.01 ppm 0.2 NDPIPERONYL BUTOXIDE 0.3 ppm 3 NDPRALLETHRIN 0.01 ppm 0.4 NDPROPICONAZOLE 0.01 ppm 1 ND
Pesticides LOD Units Action Level ResultPROPOXUR 0.01 ppm 0.1 NDPYRETHRINS 0.05 ppm 1 NDPYRIDABEN 0.02 ppm 3 NDSPIROMESIFEN 0.01 ppm 3 NDSPIROTETRAMAT 0.01 ppm 3 NDSPIROXAMINE 0.01 ppm 0.1 NDTEBUCONAZOLE 0.01 ppm 1 NDTHIACLOPRID 0.01 ppm 0.1 NDTHIAMETHOXAM 0.05 ppm 1 NDTOTAL CONTAMINANT LOAD(PESTICIDES)
0.05 PPM 20 ND
TOTAL DIMETHOMORPH 0.02 PPM 3 NDTOTAL PERMETHRIN 0.01 ppm 1 NDTOTAL SPINETORAM 0.02 PPM 3 NDTOTAL SPINOSAD 0.01 ppm 3 NDTRIFLOXYSTROBIN 0.01 ppm 3 NDPENTACHLORONITROBENZENE (PCNB)*
0.01 PPM 0.2 ND
PARATHION-METHYL * 0.01 PPM 0.1 NDCAPTAN * 0.025 PPM 3 NDCHLORDANE * 0.01 PPM 0.1 NDCHLORFENAPYR * 0.01 PPM 0.1 NDCYFLUTHRIN * 0.01 PPM 1 NDCYPERMETHRIN * 0.01 PPM 1 ND
Pesticides PASSED
Analyzed by Weight Extraction date Extracted By585 , 1665 0.2639g 04/14/21 12:04:43 1665 , 1665Analysis Method - SOP.T.30.065, SOP.T.40.065, SOP.T.40.066, SOP.T.40.070 , SOP.T.30.065,SOP.T40.070Analytical Batch - DA025019PES , DA024999VOL Reviewed On- 04/14/21
14:33:25Instrument Used : DA-LCMS-003 (PES) , DA-GCMS-006Running On : 04/14/21 17:02:27 , 04/14/21 15:40:06 Batch Date : 04/14/21 11:01:42
Reagent Dilution Consums. ID010421.R86 25 6524407-03041221.R20031721.R08041421.R05092820.59
Pesticide screen is performed using LC-MS and/or GC-MS which can screen down to below single digit ppbconcentrations for regulated Pesticides. Currently we analyze for 67 Pesticides. (Method: SOP.T.30.060Sample Preparation for Pesticides Analysis via LCMSMS and GCMSMS.SOP.T40.065/SOP.T.40.066/SOP.T.40.070 Procedure for Pesticide Quantification Using LCMS and GCMS). *Volatile Pesticide screening is performed using GC-MS which can screen down to below single digit ppbconcentrations for regulated Pesticides. Analytes marked with an asterisk were tested using GC-MS.
This report shall not be reproduced, unless in its entirety, without written approval from Kaycha Labs. This report isan Kaycha Labs certification. The results relate only to the material or product analyzed. Test results areconfidential unless explicitly waived otherwise. Void after 1 year from test end date. Cannabinoid content of batchmaterial may vary depending on sampling error. IC=In-control QC parameter, NC=Non-controlled QC parameter,ND=Not Detected, NA=Not Analyzed, ppm=Parts Per Million, ppb=Parts Per Billion. Limit of Detection (LoD) andLimit Of Quantitation (LoQ) are terms used to describe the smallest concentration that can be reliably measured byan analytical procedure. RPD=Reproducibility of two measurements. Action Levels are State determined thresholdsfor human safety for consumption and/or inhalation. The result >99% are variable based on uncertainty ofmeasurement (UM) for the analyte. The UM error is available from the lab upon request.The "Decision Rule" for thepass/fail does not include the UM. The limits are based on F.S. Rule 64-4.310.
Jorge SegredoLab Director
State License # CMTL-0002ISO Accreditation # ISO/IEC17025:2017 Accreditation
PJLA-Testing 97164
___________________Signature
04/20/2021
___________________Signed On
4131 SW 47th AVENUE SUITE 1408DAVIE, FL, 33314, US
Kaycha LabsMíami Vibes Drops 11,25g
Miami VibesMatrix : Derivative
Certificate of Analysis PASSEDFLUENT
82 NE 26th streetMiami, FL, 33137, USTelephone: (305) 900-6266Email: Sam@getfluent.com
Sample : DA10414006-005Harvest/LOT ID: 6858 3748 8454 2841Batch# : 9564 86808642 3515Sampled : 04/13/21Ordered : 04/13/21
Sample Size Received : 6 unitsTotal Weight/Volume : 1426 unitsCompleted : 04/20/21Expires: 04/20/22Sample Method : SOP.T.20.010
Page 4 of 5
Residual Solvents PASSED
Solvent LOD Units ActionLevel(PPM)
Pass/Fail Result
METHANOL 25 ppm 250 PASS ND
ETHANOL 500 ppm 5000 PASS ND
PENTANES (N-PENTANE) 75 ppm 750 PASS ND
ETHYL ETHER 50 ppm 500 PASS ND
ACETONE 75 ppm 750 PASS ND
2-PROPANOL 50 ppm 500 PASS <250.000
ACETONITRILE 6 ppm 60 PASS ND
DICHLOROMETHANE 12.5 ppm 125 PASS ND
N-HEXANE 25 ppm 250 PASS ND
ETHYL ACETATE 40 ppm 400 PASS ND
BENZENE 0.1 ppm 1 PASS ND
HEPTANE 500 ppm 5000 PASS ND
TOLUENE 15 ppm 150 PASS ND
TOTAL XYLENES 15 ppm 150 PASS ND
PROPANE 500 ppm 5000 PASS ND
CHLOROFORM 0.2 ppm 2 PASS ND
1,2-DICHLOROETHANE 0.2 ppm 2 PASS ND
BUTANES (N-BUTANE) 500 ppm 5000 PASS ND
ETHYLENE OXIDE 0.5 ppm 5 PASS ND
1,1-DICHLOROETHENE 0.8 ppm 8 PASS ND
TRICHLOROETHYLENE 2.5 ppm 25 PASS ND
Residual Solvents PASSED
Analyzed by Weight Extraction date Extracted By850 0.0285g 04/15/21 04:04:55 850
Analysis Method -SOP.T.40.032Analytical Batch -DA025079SOL Reviewed On - 04/16/21 16:00:16Instrument Used : DA-GCMS-002Running On :Batch Date : 04/15/21 15:53:05
Reagent Dilution Consums. ID
1 G201.162R2017.217
Residual solvents screening is performed using GC-MS which can detect belowsingle digit ppm concentrations. Currently we analyze for 21 Residualsolvents.(Method: SOP.T.40.032 Residual Solvents Analysis via GC-MS).
This report shall not be reproduced, unless in its entirety, without written approval from Kaycha Labs. This report isan Kaycha Labs certification. The results relate only to the material or product analyzed. Test results areconfidential unless explicitly waived otherwise. Void after 1 year from test end date. Cannabinoid content of batchmaterial may vary depending on sampling error. IC=In-control QC parameter, NC=Non-controlled QC parameter,ND=Not Detected, NA=Not Analyzed, ppm=Parts Per Million, ppb=Parts Per Billion. Limit of Detection (LoD) andLimit Of Quantitation (LoQ) are terms used to describe the smallest concentration that can be reliably measured byan analytical procedure. RPD=Reproducibility of two measurements. Action Levels are State determined thresholdsfor human safety for consumption and/or inhalation. The result >99% are variable based on uncertainty ofmeasurement (UM) for the analyte. The UM error is available from the lab upon request.The "Decision Rule" for thepass/fail does not include the UM. The limits are based on F.S. Rule 64-4.310.
Jorge SegredoLab Director
State License # CMTL-0002ISO Accreditation # ISO/IEC17025:2017 Accreditation
PJLA-Testing 97164
___________________Signature
04/20/2021
___________________Signed On
4131 SW 47th AVENUE SUITE 1408DAVIE, FL, 33314, US
Kaycha LabsMíami Vibes Drops 11,25g
Miami VibesMatrix : Derivative
Certificate of Analysis PASSEDFLUENT
82 NE 26th streetMiami, FL, 33137, USTelephone: (305) 900-6266Email: Sam@getfluent.com
Sample : DA10414006-005Harvest/LOT ID: 6858 3748 8454 2841Batch# : 9564 86808642 3515Sampled : 04/13/21Ordered : 04/13/21
Sample Size Received : 6 unitsTotal Weight/Volume : 1426 unitsCompleted : 04/20/21Expires: 04/20/22Sample Method : SOP.T.20.010
Page 5 of 5
Microbials PASSED
Analyte LOD Result Action Level (cfu/g)ESCHERICHIA_COLI_SHIGELLA_SPP not present in 1 gram.SALMONELLA_SPECIFIC_GENE not present in 1 gram.ASPERGILLUS_FLAVUS not present in 1 gram.ASPERGILLUS_FUMIGATUS not present in 1 gram.ASPERGILLUS_TERREUS not present in 1 gram.ASPERGILLUS_NIGER not present in 1 gram.TOTAL YEAST AND MOLD 10 <10 CFU 100000
Analysis Method -SOP.T.40.043 / SOP.T.40.044 / SOP.T.40.041Analytical Batch -DA024994MIC , DA024995TYM Batch Date : 04/14/21, 04/14/21Instrument Used : PathogenDx Scanner DA-111,Running On : 04/14/21, 04/14/21
Analyzed by Weight Extraction date Extracted By1794, 1794 1.4859g 04/15/21 513,
Reagent Consums. ID Consums. ID Consums. ID Consums. ID Consums. ID032421.09021921.28
200103-274311021891700200511.12.2020.MIC11989-024CC-024
28040292803033D012D011A15A12
28070142810026A280900604028040322808009
281102120324012020009C6-009200507119C914C4-914AK
929C6-929H
Microbiological testing for Fungal and Bacterial Identification via Polymerase Chain Reaction (PCR) methodconsisting of sample DNA amplified via tandem Polymerase Chain Reaction (PCR) as a crude lysate which avoidspurification. (Method SOP.T.40.043) If a pathogenic Escherichia Coli, Salmonella, Aspergillus fumigatus,Aspergillus flavus, Aspergillus niger, or Aspergillus terreus is detected in 1g of a sample, the sample fails themicrobiological-impurity testing. Pour-plating is used for quantitation and confirmation, Total Yeast and Mold hasan action limit of 100,000 CFU.
Mycotoxins PASSED
Analyte LOD Units Result Action Level (PPM)AFLATOXIN G2 0.002 ppm ND 0.02AFLATOXIN G1 0.002 ppm ND 0.02AFLATOXIN B2 0.002 ppm ND 0.02AFLATOXIN B1 0.002 ppm ND 0.02TOTAL OCHRATOXIN A 0.002 PPM ND 0.02
Analysis Method -SOP.T.30.065, SOP.T.40.065Analytical Batch -DA025021MYC | Reviewed On - 04/15/21 12:53:09Instrument Used :Running On : 04/14/21 17:02:35Batch Date : 04/14/21 11:03:45
Analyzed by Weight Extraction date Extracted By585 NA 04/14/21 03:04:44 585
Aflatoxins B1, B2, G1, G2, and Ochratoxins A testing using LC-MS. (Method: SOP.T.30.065 forSample Preparation and SOP.T40.065 Procedure for Mycotoxins Quantification Using LCMS. LOQ 1.0ppb). Aflatoxin B1, B2, G1, and G2 must individually be <20ug/Kg. Ochratoxins must be <20µg/Kg.
Heavy Metals PASSED
Reagent Reagent Dilution Consums. ID041221.R18041221.R16040621.R15040621.R02040521.R07040521.R06
040721.R14041221.R03031121.23022521.06030420.08040121.01
100 89401-566
Metal LOD Unit Result Action Level (PPM)
ARSENIC 0.02 PPM ND 1.5CADMIUM 0.02 PPM ND 0.5MERCURY 0.02 PPM ND 3LEAD 0.05 PPM ND 0.5
Analyzed by Weight Extraction date Extracted By1022 0.2323g 04/14/21 01:04:41 1879
Analysis Method -SOP.T.40.050, SOP.T.30.052Analytical Batch -DA025018HEA | Reviewed On - 04/15/21 11:28:34Instrument Used : DA-ICPMS-002Running On : 04/14/21 15:56:49Batch Date : 04/14/21 10:48:27
Heavy Metals screening is performed using ICP-MS (Inductively Coupled Plasma – MassSpectrometer) which can screen down to below single digit ppb concentrations for regulated heavymetals using Method SOP.T.30.052 Sample Preparation for Heavy Metals Analysis via ICP-MS andSOP.T.40.050 Heavy Metals Analysis via ICP-MS.
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