900-lc p. van poppel – field support specialist october 2009

900-LC

P. van Poppel – Field Support Specialist October 2009

The 900 series LC

Analytical 920 LC Semi-Prep 940 LC

What will be covered

•Modules/ Options

•Parts Replacement Strategy

•Installation

•IMS diagnostics/ Troubleshooting

Modules

•Autosampler

•Fluorescence Detector

•Quaternary Pump

•Column Heater/ Manual Injector

•Fraction Collector (external)

•Scale Up module

•MIB

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•UV-vis Detector

•PDA Detector

•RI Detector (internal and external)

•ELSD (external)

•Isocratic Pump

•Sample Loading Pump

Modules

•Autosampler

•Fluorescence Detector

•Quaternary Pump

•Column Heater/ Manual Injector

•Scale Up module

•MIB

•And the IMS

Parts Replacement Strategy

•Ease of serviceability and a minimal number of parts will help field service representatives repair the instrument in an efficient and cost effective manner.

•We expect to service all modules to an assembly level, not to a sub assembly level. Component level repair of the circuit boards is not recommended.

•Warranty replacement of DOA modules within the system must be handled in accordance with the Instrument Escalation Procedure.Melbourne Field Support will not authorize the replacement of defective instruments unless there is an escalation.

Installation

•Hardware

•Network

•Software

Hardware Installation

•Plug & Play

•Pre-Plumbed

•Pre-Wired

Hardware Installation

Autosampler Detector

Sample vial tray screw

Syringe movement lock down bracket

Hardware Installation

Shipping Screw

Shipping Screw

Shipping Screw

Fluorescence Detector(bottom view)

Hardware Installation

Hardware Installation

Network Setup

Network Setup

Network Setup

Network Setup

Software Installation

Software Installation

Software Installation

Software Installation

Software Installation

Software Installation

Software Installation

Software Installation

Software Installation

Software Installation

Software Installation

IMS

IMS Actions

IMS Counters

IMS Service Tests

IMS Additional Tests

IMS Log Book

IMS Log Book

IMS Help

IMS Help

Modules

•Autosampler

•Fluorescence Detector

•Quaternary Pump

•Column Heater/ Manual Injector

•Scale Up module

•MIB

Auto Sampler

•Poor Reliability

• Injection Valve System• Injection Port System• LC System

•Contamination

• Injection Valve System• Injection Port System• Sample• LC System

•Electronics

Autosampler Electronics

•Electronics

• Not Initialising

• Error X, Y, Z

• S-Valve

• I-Valve

• System Busy/ Communications Error

IMS Autosampler Tests

•Autosampler Complete Test

•Autosampler Temperature Accuracy Test

IMS Autosampler Actions

•Injection port seal replaced

•Injection valve rotor replaced

•Syringe replaced

•Purge syringe

•Syringe valve rotor replaced

•Injection valve stator replaced

•Syringe valve stator replaced

•Needle replaced

•Wash needle

•Move to injection port

•Syringe needle adjustment

Fluorescence Detector

General Issues

• Noise

• Drift

• Poor Signal to Noise

• Leak Errors

• Power Problems

Electronics

• Lamp Errors

• Board Errors

• Data Errors

IMS Fluorescence Detector Actions

•150W xenon lamp replaced

•Long life xenon lamp replaced

•Mercury lamp replaced

•Flowcell cleaned/replaced

•Wavelength Accuracy

IMS Fluorescence Detector Tests

•Signal to Noise by Raman Light Scattering

•Detector Noise Test

Quaternary Pump Problems

General Issues

• Reproducibility

• Carryover

• No Peak Observed

• Mixing Ratio Accuracy

• Pressure Fluctuations

• Split Peaks

• Liquid does not Flow

• No Power

• Pump Motor does not Rotate

Quaternary Pump Problems

Degasser Issues

• Bubbles Generated at Outlet

• Bubbles Generated when Pump sucks

• Liquid does not flow

• Vacuum Pump does not work

• Vacuum Pump does not stop

Quaternary Pump Electronics

Electronics

• Motor Error

• Leaks

• Data & Board Errors

• Limit Errors

Quaternary Pump Electronics

Error generating condition

Initialization

Pump operation

Error generating condition

YES

YES

NO

NO

Power On

ROM ERROR RAM ERROR EPROM ERROR MOTOR INITIALIZATION ERROR ELINE ERROR

PRESSURE MAX LIMIT ERROR PRESSURE MIN LIMIT ERROR EXTERNAL STOP

IMS Quaternary Pump Actions

•Inlet check valve replaced

•Outlet check valve replaced

•Piston seal replaced

•Drain valve seal replaced

•Drain valve filter replaced

•Solenoid valve replaced

•Mixer filter replaced

•Solvent filter replaced

•Gradient four way joint replaced

•(Cam Position Adjustment)

IMS Quaternary Pump Tests

•Flow rate accuracy - Test meter method

•Flow rate accuracy test - Time volume method

•Flow Compositional accuracy test

•Flow Leak test

•Flow precision test

•Flow pulsation test

•Flow compositional Ripple Test

•Flow gradient linearity test

•Flow compositional precision test

Column Heater/ Manual Injector Problems

General Issues

• Heating Problems

• Leaks

• Pressure

Scale Up Module Problems

General Issues

• Leaks

• Pressure

MIB Problems

General Issues

• Communications

• Power

IMS Column Heater/ Manual Injector Actions & Tests

•Injector valve stator replaced

•Injector valve rotor replaced

•Column valve stator replaced

•Column valve rotor replaced

•Column heater temperature accuracy and stability

IMS Scale Up Module Actions & Tests

•Injector valve stator replaced (Manual)

•Injector valve rotor replaced (Manual)

•Injector valve stator replaced (SUM)

•Injector valve rotor replaced (SUM)

•Column valve stator replaced (SUM)

•Column valve rotor replaced (SUM)

IMS MIB Actions & Tests

•Backup the system configuration to a local folder

•Restore the system configuration from a previous backup

•Full System Test

Autosampler Practical

Person 1:

• X, Y, Z movement adjustment

Person 2:

• Vial Detection & Injection Valve Sensor adjustment

Person 3:

• X & Y movement adjustment Mechanism Rails

…Injection Port Position, Syringe Valve and Syringe Sensor adjustments…

Fluorescence Detector Practical

Person 1:

• Replacement of the Xenon Lamp and

• Positional Adjustment of the Xenon Lamp

Person 2:

• Replacement of the Mercury Lamp

• Perform a linearity test

Person 3:

• Clean the Flow Cell

• Perform a wavelength accuracy test

Pump Practical

Person 1:

• Replacement of the Pump Seal & Drain Valve Seal and Solvent Filter Wash

Person 2:

• Replacement & Cleaning the Inlet and Outlet check valves and Pressure Test Mode in IMS

Person 3:

• Remove the pump and Pump Board