11x17 main solids 06 23 11 - fun with...
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Thermal Analysisperform all 5 Parts
unless directed to stop in Thermal Explosives
Ignition ofO�-Gas Test
+
pH Test
Water SolubilityTest
Flour Test
pH Test
Organophosphate Quick Test
OrganophosphateTest
Copper WireTest
Oxidizer in Air Test
Metal AnalysisTest II
3 - 12
Aqua
Bothtests arenegative
+
dissolves
partlydissolves
formsgel
-color of
unknown
+
PesticideScreening
Test
sodium hypochlorite,calcium hypochlorite
copper salt
sinks orsuspends
noreaction
Chars
Tars
detergent
pumice
wax
Plastic
pollen�our
-
Purple manganese salt
Asbestos Test
asbestos
+ -
appearsinert
UnknownSolid
whiteor clear
Other
+
-
+
-
H A Z C A T
C H A R TS O L I D S
¨
foams,suds form in
Water SolubilityTest -
Alkaline Earth Metals Test
Sulfate/Sul�te Test
chlorides, sulfates,
cyanides (anion) Go to Metal Analysisto identify cation
lime
calcium sulfate,barium sulfate
+
9 -10 11-14
-+
0 - 2
yellowunknown
+
barium, strontiumor calcium salt,calcium silicate
chlorinatedpesticide
organophosphate
chromium salt
chlorocyanuratetrichloro-s-triazinone
sodiumperoxide
Oxidizer
Heavy Metals Test
chromium trioxide
potassium permanganateor manganese dioxide
Peroxide Test 1 +
-
Picric AcidTest-
+ picric acid
peroxide
whitephosphorus
Metal Analysis Test I(to identify cation)
red yellowlavender
borate (anion)
organophosphate,thiophosphate,carbamate
Blue cobalt salt
iron salt (ferric)
06/23/11
OxidizerTest
+
red/orangevapors
+
carbonate,bicarbonate (anion) Go to
Metal Analysisto identify cation
Cyanide Test 1
Ammonium Salts Test
-
PerchlorateTest
Ammoniumperchlorate
Ammoniumnitrate -
+
Urea Test
ammonium salt (cation)
arsenic
+
urea
containsnitrogen
�berglass
sand, or glass,silica, silicates metal oxide: zinc oxide,
titanium dioxide, aluminum oxideor magnesium silicate, talc, kaolin,bentonite. Green �ame color indicates boric acid
powder
+
+ThermalOxidizer
-ThermalOxidizer
+-
FormsRain Cloud
FlourTest
�our, baby powder, corn starch, powdered sugar
- +
AlcoholTest
Themal BehaviorTest
plastic
SugarTest
-
Go toOrganic Analysis
metal alloy,other metal
iron,cobalt
Magnetics Test
+ - Arsenic Test
+ -
-
+
ThermalBehavior
meltsin
TA3
alkali metal salt: eg.,lead, tin, zinc
boric acidlead oxidesodium borate
is unknown metallic?
+
Noreaction
white crust
+-
+-
RedRain
formsrain
cloud
+ThermalIgnition
new colorafter
cooling
nickel, ortungsten salt
chromium orcopper salt
molybdenumor cobalt salt
copper, iron ormanganese salt
iron salt
copper salt
green
tungsticoxide
DarkOrange
yellow
changescolor
Phenol Test
aromatichydrocarbon
phenol, cresol
+
4 - 8
-Crystals
Fibers
calcium hydroxideneat cementstrontium hydroxide red
blue
brown, black,orange
potassium, sodium or lithium iodide
redlava
lavendercalcium,strontium
barium, molybdenum
boron,copper
copperhalides
lead,bismuth
arsenic,zinc,
selenium
lithium
sodium
potassium
orangered
veryred
blue
whitesparks
magnesium,aluminum
orangered
sparks
iron, carbon
bluegreen
yellowgreen
whiteblue
yelloworange
color when hot - originalcolor returns
aftercooling
Go toAnionsChart
- recrystallizes formsa glass
-
-
purplevapors iodine, or iodide
go back & check other thermal analysis
results
BlackSpiderwebs
ThermalpH 9 -12
2 - 8organic amine, hexamine
red phosphorus
sugar, sucralose, fructose, dextose
sulfur
ignites on test tool
moreThermal
Explosivesresults check all Thermal Analysis results
-ThermalIgnition
+ThermalOxidizer
0 - 2
9 -12 3 - 8
ThermalpH
Thermal Analysisperform all 5 Parts
unless directed to stop in Thermal Explosivescheck all Thermal Analysis results
Yellow
Metal AnalysisTest I
sodium metal
potassium metal
lithium metal
Yellow
Red
Lavender
Whitesparkles
magnesiummetal
Bluestreaks
zinc metal
calciummetal
burnssooty
calcium carbide
Water reactivepossible hydride
-+
pH Test
10 -14 5 - 9 0 - 4
burnsoxidizer paper
+
-
red-orangeshort lasting
-
pH Test
0 - 310 - 14
red orangeshort lasting
Go to Solid Acids
Chart
AcidTest
boils
any other
reaction odor noted
rotten egg garlic bitter
almond
Cyanide Test 1
Arsenic Test
++ +
CyanideArsenide
4 - 9
Appears metallic
+
burnspaper
stains paperyellow
mercury salt
13-14
othercolor
pyrophoric
�bers
phosphorus pentoxideGo to
Metal Analysisto identify cation
Appears metallic
-
Yellow Green
Go toAnions Chart
Red Rainfrom yellow
solid.sulfur
r
Heavy Metals Test
-
pH~ 7
pH< 5
phosphorus pentoxide
Phosphate Test
aluminum trichloride
Aluminum Salts Test
pH ofemulsion or �aky solid
Reactionon Explosives
Tool
Reactionon
Swab
Asbestos Test
asbestos
+
-
rust
dyed inorganic salt
white
charredorganic compound
white solid white smoke
benzoyl peroxide
red solidwhite smoke.
green
yellow may be an organic �ame color check for “+” Thermal Ignition
wood
sugar with arsenic (ant bait)
Go to Metal Analysis
and Go to Anions Chart
Go to Metal Analysis
sulfur
Ammonium Salts Test
e�ervesces reactsviolently
mercury
any other result
any other result
chromium
closedcontainer
black solid
Magnetics Test
+- iron,cobalt
+sulfate
Sul�de Test
color ofunknown
whte,brown
nitrate, chlorate, or picrate anion
nitrate anion
transition metal compound, cobalt manganese, iron
partlydissolves
orange yellow
glows when hot: titanium dioxide or zinc oxidemelts and recrystallizes: alkali nitrate
grey
calcium salt
Go to Anions Chart
lithiumsodiumpotassium
chloride?
vapors in TA4
purple
orangeyellow
iodide anion
clear
pink,purple,yellow
ThermalExplosives
-
-
Go to Organic Analysis
-
-
possibleant/rodent
poison
+
+
ArsenicTest
+-
DehydrationTest
+
+
--
- polyalcohol
possible soap, surfactant
cellulose
Chars &Tars
anyotherresult
Chars
Go toOrganic Analysis
Plastics Chart
foams,suds form in
Water SolubilityTest
+
black
Sul�ide Test
sul�de (anion)
dissolves
BoronTest
BoronTest-
sodium borate
-
anyotherresult
BoronTest
-+sodium
borohydride
STOPENERGETICMATERIALEXPLOSIVE
metal perchlorates,military explosive,azide
TATP, TNT, PETN,picrate
whitedetonates
metal periodates,
de�agrates
gunpowder, black powder, nitrocellulose
�oats
white�akes
Go toMetal Analysis
to identify cation
Go toAnions Chart
+
nitrite (anion)
Sul�deTest -
iron or cobaltsul�de+
white solidyellow �ame
ammonium perchlorate
yellow solidblue �ame
whooshsound
downwardburst of
�ame
snap,crackle,
pop
anyother
reaction
bisul�te, metabisul�te (anion)
Carbonate Test +
negative: carbonate,
positive: bisul�te
anyotherresult
sodium persulfate (pH 6)ammonium persulfate (pH 3)
color ofunknown
othercolor
whiteor clear
purpleor black
Thermal Analysisperform all 5 Parts
unless directed to stop in Thermal Explosives
0 - 3
9 -12
ThermalpH
ThermalOxidizer
red/orangevapors
percarbonate (anion)(pops like popcorn)
-
BoronTest
-
+
sodium perborate
bleachespaper
+
-
PhosphateTest
-+
mono-ammoniumphosphate
Go toAnions Chart
Sulfate/Sul�te Test
+sulfate
anyotherresult
magnesium sulfate,epsom salts
showerof red/orange
sparksferrocene
anyotherresult Go to
Thermal Analysis Chart
+-
- +
+
+
-Phosphate
Test
+-
cyanide (anion)
carbonate (anion)
phosphate (anion)
hydroxide or silicate (anion)
potassium
lithium
sodium
calcium hydroxide or carbonate
ChlorideTest
+
-
calcium chloride
Carbonate Test
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