hwbdocuments.env.nm.gov alamos national labs/ta 54/32… · 644-11.18.09(hwb r-37 voc's) par :...
TRANSCRIPT
f)lC--I
Gr~( l V1cJ iN l fe Jshy
J2 --37
Environmental Division (ALS LvC-t-4 r CCJAY0 vCt~e 1-5t~~d
December 3 2009
Ms Kim Granzow New Mexico Environment Department DB 1183 Diamond Drive SUite B Los Alamos NM 87544
Re ALS Workorder 09-11-214 Project Name 644-111809(HWB R-37 VOCs) PAR Project Number 002731703
Dear Ms Granzow
Two water samples were received from New Mexico Environment Department DB on November 20 2009 The samples were scheduled for the following analysis
GCMS Volatiles pages 1-23
The results for this analysIs are contained in the enclosed report
Thank you for your confidence in ALS Laboratory Group Should you have any questions please calL
Sincerely
shy
ALS Laboratory Group Lance Steere Senior Project Manager
LRSmh Enclosure (s) Report and CD
ALS USA Corp 32300PM of the ALS Laborator4 Group
225 Commerce Drive Ft Collins Colorado 80524 Phone (970) 490middot1511 Fa (970) 490-1522 VJW alsenviro corn 11111111111111111111111111111111111
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ALS Laboratory Group -- Fe
Sample Number(s) Cross-Reference Table
R-37 S~r 1-111809
New Mexico Environment Department OB 644-111809(HWB R-37 VOCs) PAR
r 002731703 06-667 -55-01754
CDC Number Matrix Date Time Collected Collected
ALS Laboratory Group -- FePage 1 of 1 Date Printed Monday November 232009
Chain of Custody Record I d- I 4 SKIP TO MAIL REPORT TO fliff9ff BILL TO
Kim Glanzow kG Oilvlgt CobrUD Dflve NMEOmiddotOOE OlefSI9hl 8lJlI~iU (51SI pound614008 New Melllco Enlfrol Dev j-Iuartlous Waste gUleltJll
fort Collins CO 8Q524 183 Diamond Orje- Surfe A 2~S Rodeo P2IriI Driv~ East Bldg 1
(9l0) 490middot1511 tos Alamos Nw Mexico S75u Santa Fe NM 8750$ 2561
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DateTime Received By Required MS MSO BlAnk I b~Y L_- Tim~18ndord ____
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Page 1 Of 1
ali containers received intact (not broken or
at samples requiring no beadspace (VOC GRO RSKfMEE Rx CNS radon) free Size of bubble lt
(a leas 113 of container required)
samples checked for and free from the presence of residual chlorine when PM has indicated sample are from a chlorinatec water source note if fIeld preservation
sodIum thiosulfate was not observed)
Were cooler temperatures measured at O1-60degC IR lun used 2
Cooler I---shy
Temperature (C) 3 ~ No of custodv seals 01 cooler 0
External ~lRJhr reading
Backgrouncl ~lRhr reading 3 i Were exemai111Uhr readllljs S rwo lim backlTCltmri nnd within DOT acceptance criterin
NO
NO
NO
NO
---1
A-S Laboratory Group - Fort Collins
CONDITION OF SAMPLE UPO) RECEIPT FOMl
Client _Nyen-M---f=D~_______ Workordet No D4 I ~ I L --~--~-----~------
Prolecl Manager __LS_____________ Initials C DI Date 1 -gt= 0- () CJ
Additionallnformatiml PHOVlDE DETAILS BElOW FOR A NO RESIONS[ TCJ ANY (JUESTION ABOV EXCEPT III Al[ 16
---------~-----
If hbilt W ru YES 0 I NA (If Ijrojcct Manager Signature I Date -----l-f---1-tl__--~~_l_4I(--2_)-lt-(_middota_I_----------
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ALS Labofaton1 Group
Environmental Division Fort Cofiins Colorado
GCMS Volatiles Case Narrative
New Mexico Environmental Department OB 644-111809(HWB R-37 VOCs) PAR -- 002731703
Work Order Number 0911214
1 This report consists of 2 water samples The samples were received cool and intact by ALS on 1120109 The vial for sample 0911214-1 contained headspace prior to analysis because it was not received headspace free into the voatiles laboratory
The samples provided for volatiles had a pH gt 2 at the time of analysis
2 These samples were prepared according to SW-846 3rd Edition procedures Specifically the water samples were prepared by purging 10 mL using purge and trap procedures based on Method 5030C
3 The samples were analyzed using GCMS with an RTX-624 RTX-VMS or equivalent capillary column according to SOP 525 Revision 14 based on SW-846 Method 8260B All positive results were quantitated against the initial calibration standards using the intemal standard technique The identification of positive results was achieved by a comparison of the retention time and mass spectrum of trle sample versus the daily calibration standard
4 All initial calibration criteria for SPCCs and CCCs were met If average response factors were used in the initial calibration RSO was 15 If linear or higher order regression calibrations were used in the initial calibration the coefficient of determination (r2) ~099
5 All initial calibrations are verified by comparing a second source standard calibration verrrication (ICV) against the calibration curve All target compounds in the second source verification had a 0 of less than 25
6 All criteria for SPCCs and CCCs were met in daily (continuing) calibration verifications (CCV)
7 Methylene chloride acetone and 2-butanone are common laboratory contaminants In order to minimize the levels of these compounds detected in the gclms analysis ALS has designated its volatile laboratory as a restricted access area In addition the laboratory has been equipped with a dedicated air intake and exhaust system that operates under positive pressure in order to
1
minimize cross contamination of these compounds Due to fluctuations in ambient laboratory conditions reported sample values for common laboratory contaminants may be due to lab contamination even if the compound in question is not detected in the associated method blankmiddot
All method blank criteria were met
8 All laboratory control sample and laboratory control sample duplicate recoveries and RPDs were within the acceptance criteria
9 Since a sample from this order number was not the selected qualITy control (QC) sample matrix specific QC results are not included in this report
10 The samples were analyzed within the established holding time
11 All surrogate recoveries were within acceptance criteria
12 All internal standard recoveries were within acceptance criteria
14 Manual integrations are performed when needed to provide consistent and defensible data following the guidelines in SOP 939 ReVision 3
The data contained in the following report have been reviewed and approved by the personnel listed below In addition ALS certifies that the analyses reported herein are true complete and correct within the limits of the methods employed
n-o3-o5Sha~JobeS Date Organics Primary Data Reviewer
l~-O 1-01TAamp1~Orga~cs Final Data Reviewer Date
2
ALS Data Qualifier Flags Chromatography and Mass Spectrometry
U or NO This flag indicates that the compound was analyzed for but not detected
J This flag indicates an estimated value This flag is used as follows (1) when estimating a concentration for tentatively identified compounds (TICs) where a 11 response is assumed (2) when the mass spectral and retention time data indicate the presence of a compound that meets the volatile and semivolatile GCMS identification criteria and the result is less than the reporting limit (RL) but greater than the method detection limit (MOL) (3) when the retention time data indicate the presence of a compound that meets the GC identification criteria and the result is less than the RL but greater than the MOL and (4) the reported value is estimated
B This flag is used when the analyte is detected in the associated method blank as well as in the sample It indicates probable blank contamination and warns the data user This flag shall be used for a tentatively identified compound (TIC) as well as for a positively identified target compound
E This flag identifies compounds whose concentration exceeds the upper level of the calibration range
A This flag indicates that a tentatively identified compound is a suspected aldol-condensation product
X This flag indicates that the analyte was diluted below an accurate quantitation level
This flag indicates that a spike recovery is equal to or outside the control criteria used
+ This flag indicates that the relative percent difference (RPO) equals or exceeds the control criteria
3
ALS Laboratory Group -- Fe Sample Number(s) Cross-Reference Table
Paragon OrderNum 0911214 Client Name New Mexico Environment Department OB
Client Project Name 644-111809(HWB R-37 VOCs) PAR Client Project Number 002731703
Client PO Number 06-667-55-01754
Client Sample Number
Lab Sample Number
COC Number Matrix Date Collected
Time Collected
R-37 Scr 2-1 11809 0911214-1 WATER 18-Nov-09 1555 R-37 Scr 1-111809 0911214-2 WATER 18-Nov-09 1744
Page 1 of 1 ALS Laboratory Group -- Fe Date Printed Wednesday December 02 2009 LlMS Version 6317 A
4
Chain of Custody Record 1)11 d- I 4 SHIP To MAil REPORT TO HtitilJft BILL TO
Kim GrJOZOW KC [)il-e Cobra
NMFOmiddotDOE Overslghl Bwe3u 50S firt1middottoOB Hew Meico FnlliTtl1 Dep1 HaVIdthJS VvaMe Bureau ~orl Collins CO 80524shy
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CONDITIO] OF SAMPLE UPO) RECEIPT FORM
Client _-=-N--M---f-=-D________ IVorkorde No D4 J I 4 --~~~~~~------
PrO1 cc Manager L 5 lnitiais C D Date 1 -) ()- () C --~~~---------------------
1 there a cae Are the coe and bottle labels
Is the coe in agreement with samples received) of containers matrix requested anaiyses etc)
documents presen1 andor removable)
Are all aqueous samples requiring preservation preserved correctly ~- ----~-~~--- -~ -~-- ----~~~---------
volatiles)
14 Are all samples requiring no headspace (VOC GRG RSKlVIEE lb eNS radon)
free Size of bubble lt
$ Do perchlorate LCMS-MS samples have headspace (a~ least ]3 of container required)
NO
]6 Were samples checked for and free from the presence of residual chlorine (Appiicaole when PM has Indicated samples are from a chlonnated wat~ source note if field preservallor
witb sodIUm tlllosulfate wa not observed)
17 Were the lljIV~IOU on ice
IS Were cooler temperatures measured at 01-60degC IR ~Illl used 2
Coole I---
Temperature (C) 3 ~
NO
NO
NO
NO
NO
NO
NO
No of custodv seals Ol~ cooler 0 OOT ---- --- --- --l Surveyl EXlemlli flRhr n~ading I i AcceplanCfiltnforma tlon Background ulJhr reading 3 Were eX lema uRhf readl1lf5 tW(l tm bnckl1Ound and withllllxyr acceptance criterill
Additional Iuformation OVIDE DETAILS BELOW FOR A ND RESPONSE TO ANY (UESTION A80VE EXCEPT 1 ANI) 16
If applicable was the clienl contacted) YES i NO I
Project Manager Signature I Date
(1 Gun 112 Oaktoll SN 2992250020 jmiddot0066 lR Gun lie Oakton S~ 23n220101middot0(J02
Form 201r22gt15 (61109) Page 1 of _1
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7
GCMS Volatiles Method SW8260 _25B
Method Blank
Lab Name ALS Laboratory Group bullbull FC
Work Order Number 0911214
Client Name New Mexico Environment Department DB
ClientProject 10 644-111809(HWB Rmiddot37 VOCs) PAR 002731703
Lab 10 VL091125-4MB Sample Matrix WATER
Moisture NA Prep Batch VL091125-4
QCBatchlO VL091125-4-5
Sample Aliquot
Final Volume
10 ml
10 ml Date Collected NA Run 10 VL091125-4A Result Units UGL Date Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Date Analyzed 25middotNov-09 Basis NA
File Name 028043
CASNO Target Analyte DF
75-71-8 DICHLORODIFLUOROMETHANE
74-87-3 CHLOROMETHANE
75-01-4 VINYL CHLORIDE
74-83-9 BROMOMETHANE
75-00-3 CHLOROETHANE
75-69-4 TRICHLOROFLUOROMETHANE
107-02-8 ACROLEIN
75-35-4 11middotDICHLOROETHENE
67-64-1 ACETONE
74-88-4 IODOMETHANE
75-15-0 CARBON DISULFIDE
METHYLEN E CHLORIDE 75-09-2
156-60-5 TRANS-12middotDICHLOROETHENE
1634-04-4 METHYL TERTIARY BUTYL ETHER
107-13-1 ACRYLONITRILE
75-34-3 11-DICHLOROETHANE
108-05-4 VINYL ACETATE
156-59middot2 CIS-12middotDICHLOROETHENE
78-93-3 2middotBUTANONE
~ BROMOCHLOROMETHANE
67-66-3 CHLOROFORM
71-55-6 111middot TRICHLOROETHANE
594-20-7 22middotDICHLOROPROPANE
56-23-5 CARBON TETRACHLORIDE
563-58-6 11middotDICHLOROPROPENE
107-06middot2 l2middotDICHLOROETHAN E
71-43-2 BENZENE
79-01-6 TRICHLOROETHENE
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Result Reporting Limit
05 05
05 05
05 05
1 1
05 05
05 05
100 100
05 05
10 10
5 5
10 10
1 1
05 05
1 1
10 10
05 05
10 10
05 05
5 5
1 1
05 05
1 1
05 05
05 05
05 05
05 05
05 05
05 05
MDL Result EPA Qualifier Qualifier
017 U
017 U
017 U
017 U
017 U
017 U
17 U
017 U
33 U
017 U
017 U
017 U
017 U
017 U
17 U
017 U
067 U
017 U
17 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
Data Package 10 VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- Fe Page 1 of 4
llMS Version 6317 A
8
GCMS Volatiles Method SW8260 _25B
Method Blank
Lab Name ALS Laboratory Group -- FC
Work Order Number 0911214
Client Name New Mexico Environment Department 08
ClientProject 10 644-111809(HWEI R-37 voes) PAR 002731703
Lab 10 VL091125-4MB Sample Matrix WATER
Moisture NIA Prep Batch VL091125-4
QCBatchIO VL091125-4-5
Sample Aliquot
Final Volume
10 ml
10 ml Oate Collected NIA Run 10 VL091125-4A Result Units UGL Oate Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Date Analyzed 25-Nov-09 Basis NIA
File Name 028043
CASNO Target Analyte OF Result Reporting Limit
MOL Result Qualifier
EPA Qualifier
78-87-5 12middotDICHLOROPROPANE 1 05 05 017 U
74-95-3 DIBROMOMETHANE 1 05 05 017 U
75-27-4 BROMODICHLOROMETHANE 1 05 05 017 U
10061-01-5 CISmiddot13middotDICHLOROPROPENE 1 05 05 017 U
108-10-1 4-METHYL-2-PENT ANONE 1 5 5 17 U
108-88-3 TOLUENE 1 05 05 017 U
10061-02-6 TRANS-13-DICHLOROPROPENE 1 05 05 017 U
79-00-5 112-TRICHLOROETHANE 1 05 05 017 U
591-78-6 2-HEXANONE 1 10 10 17 U
127-18-4 TETRACHLOROETHENE 1 05 05 017 U
142-28-9 13-DICHLOROPROPANI 1 05 05 017 U
124-48-1 DIBROMOCHLOROMETHANE 1 1 1 017 U
106-93-4 12-DIBROMOETHANE 1 1 1 017 U
108-90-7 CHLOROBENZENE 1 05 05 017 U
630-20-6 1112-TETRACHLOROETHANE 1 05 05 017 U
100-41-4 ETHYLBENZENE 1 05 05 017 U
136777-61-2 M+P-XYLENE 1 1 1 017 U
95-47-6 O-XYLENE 1 05 05 017 U
100-42-5 STYRENE 1 05 05 017 U
75-25-2 BROMOFORM 1 05 05 017 U
98-82-8 ~YLBENZENE 1 05 05 017 U
96-18-4 123-TRICHLOROPROPANE 1 2 2 017 U
79-34-5 1122middot TETRACHLOROETHANE 1 05 05 017 U
108-86-1 BROMOBENZENE 1 05 05 017 U
103-65-1 N-PROPYLBENZENE 1 05 05 017 U
95-49-8 2-CHLOROTOLUENE 1 05 05 017 U
108-67-8 135-TRIMETHYLBENZENE 1 05 05 017 U
106-43-4 4-CHLOROTOLUENE 1 05 05 017 U
Data Package 10 VL0911214-1
Date Printed Wednesday December n 2009 AlS Laboratory Group -- FC Page 2 of 4
lMS VeCSiOIY 6317A
9
GCMS Volatiles Method SW8260 _258
Method Blank
Lab Name ALS Laboratory Group - FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-111B09(HWB R-37 VOCs) PAR 002731703
Lab 10 VL091125-4MB Sample Matrix WATER
Moisture NIA
Prep Batch VL091125-4
QCBatchlD VL091125-4-5
Sample Aliquot
Final Volume
10 ml
10 ml
Date Collected NIA Run ID VL091125-4A Result Units UGL
Date Extracted 25-Nov-09 Cleanup NONE Clean DF 1
Date Analyzed 25-Nov-09 Basis NA
File Name 028043
CASNO Target Analyte OF Result Reporting Limit
MOL Result Qualifier
EPA Qualifier
98-06-6 TERT-BUTYLBENZENE 1 05 05 017 U
95-63-6 124-TRIMETHYLBENZENE 1 05 05 017 U
135-98-8 SEC-BUTYLBENZENE 1 05 05 017 U
541-73-1 13-DlCHLOROBENZENE 1 05 05 017 U
99-87-6 P-ISOPROPYLTOLUENE 1 05 05 017 U
106-46-7 1 A-DICHLOROBENZENE 1 05 05 017 U
104-51-8 N-BUTYLBENZENE 1 05 05 017 U
95-50-1 12-DICHLOROBENZENE 1 05 05 017 U
96-12-B 12-DIBROMO-3-CHLOROPROPANE 1 2 2 067 U
120-82-1 124-TRiCHLOROBENZENE 1 05 05 017 U
87-68-3 HEXACHLOROBUTADIENE 1 05 05 017 U
91-20-3 NAPHTHALENE 1 05 05 017 U
87-61-6 123-TRICHLOROBENZENE 1 05 05 017 U
75-05-B ACETONITRILE 1 50 50 83 U
107-05-1 ALLYL CHLORIDE 1 50 50 017 U
110-57-6 TRANS-14-DICHLORO-2-BUTENE 1 5 5 17 U
64-17-5 ETHANOL 1 200 200 78 U
97-63-2 ETHYL METHACRYLATE 1 5 5 017 U
78-83-1 ISOBUTYL ALCOHOL 1 100 100 17 U
126-98-7 METHACRYLONITRILE 1 35 35 17 U
80-62-6 METHYL METHACRYLATE 1 5 5 17 U
107-12-0 PROPIONITRILE 1 25 25 33 U
126-99-8 CHLOROPRENE 1 5 5 017 U
75-65-0 TERT-BUTANOL 1 100 100 33 U
108-20-3 ISOPROPYL ETHER 1 2 2 033 U
637-92-3 ETHYL TERT-BUTYL ETHER 1 2 2 033 U
994-05-8 TERT-AMYL METHYL ETHER 1 2 2 033 U
67-72-1 HEXACHLOROETHANE 1 2 2 033 U
Data Package 10 VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -~ Fe Page 3 of 4
LlMS Version 6317 A
10
GCMS Volatiles Method SW8260 _258
Method Blank
Lab Name ALS Laboratory Group -- FC
Work Order Number 0911214
Client Name New Mexico Envirmment Department OB
ClientProject 10 644-111809(HWB R-37 VOCs) PAR 002731703
Lab 10 VL091125-4MB Sample Matrix WATER
Moisture NIA Prep Batch VL091125-4
QCBatchlO VL091125-4-5
Sample Aliquot
Final Volume
10 m
10m Date Collected NIA Run 10 VL091125-4A Result Units UGIL Date Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Date Analyzed 25-Nov-09 BasisNIA
File Name 028043
CASNO Target Analyte Result Reporting MOL Result EPAOF Limit Qualifier Qualifier
Surrogate Recovery
CASNO Surrogate Analyte Result Flag Spike Amount
Percent Recovery
Control Limits
460-00-4 4-BROMOFLUOROBENZENE 25 25 100 82 - 121
1868-53-7 DIBROMOFLUOROMETHANE 248 25 99 80 - 123
2037-26-5 TOLUENE-D8 26 25 104 85 - 116
Data Package 10 VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- FC Page 4 of4
LlMS Version 6317A
11
GCMS Volati les Method SW8260 _258
Sample Results
Lab Name ALS Laboratory Group -- FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-111809(HWB R-37 VOCs) PAR 002731703
Field 10 Rmiddot37 Ser 2middot111809
Lab 10 0911214middot1
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml
Moisture NA QCBatchlO VL091125-4-5 Final Volume 10mi Date Collected 18-Nov-09 Run 10 VL091125-4A Result Units UGL
Date Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Analysis ReqCode 104 Date Analyzed 25-Nov-09
Prep Method SW5030 Rev C Basis As Received
File Name 028044
CASNO Target Analyte Dilution Factor
75-71-8 DICHLORODIFLUOROMETHANE 1
74middot87-3 CHLOROMETHANE 1
75-01-4 VINYL CHLORIDE 1
74-83-9 BROMOMETHANE 1
75-00-3 CHLOROETHANE 1
75-69-4 TRICHLOROFLUOROMETHANE 1
107-02-8 ACROLEIN 1
75-35-4 11middotDICHLOROETHENE 1
67-64-1 ACETONE 1
74-88-4 IODOMETHANE 1
75-15-0 CARBON DISULFIDE 1
75-09-2 METHYLENE CHLORIDE 1
156-60-5 TRANSmiddot12middotDICHLOROETHENE 1
1634-04-4 METHYL TERTIARY BUTYL ETHER 1
107-13-1 ACRYLONITRILE 1
75-34-3 1-DICHLOROETHANE 1
i 108-05-4 VINYL ACETATE 1
156-59-2 CIS-12middotDICHLOROETHENE 1
78-93-3 2-BUTANONE 1
74-97-5 BROMOCHLOROMETHANE 67-66-3 CHLOROFORM 1
71-55-6 11-TRICHLOROETHANE 594-20-7 22-DICHLOROPROPANE 56-23-5 CARBON TETRACHLORIDE 563-58-6 -DICHLOROPROPENE 107-06-2 2-DICHLOROETHANE
Result Reporting Limit
05 05
05 05
05 05
1 1
05 05
05 05
100 100
05 05
10 10
5 5
10 10
1 1
05 05
1 1
10 10
05 05
10 10
05 05
5 5
1 1
05 05
1 1
05 05
05 05
05 05
05 05
MOL Result EPA Qualifier Qualifier
017 U
017 U
017 U
017 U
017 U
017 U
17 U
017 U
33 U
017 U
017 U
017 U
017 U
017 U
17 U
017 U
067 U
017 U
17 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
Data Package ID VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- Fe Page 1 of 8
UMS Version 6317A
12
GCMS Volatiles Method SW8260_25B
Sample Results
Lab Name ALS Laboratory Group - FC
Work Order Number 0911214
Client Name New Mexico nvironment Department OB
ClientProject 10 644-111809(HWB R-37 VOCs) PAR 002731703
Field 10 R-37 Scr 2-111809
Lab 10 0911214-1
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10ml
Moisture NA QCBatchlD VL091125-4-5 Final Volume 10ml
Date Collected l8-Nov-09 Run 10 VL091125-4A Result Units UGL
Date Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Analysis ReqCode 104 Date Analyzed 25-Nov-09 Basis As Received
Prep Method SW5030 Rev C File NameD28044
CASNO Target Analyte Dilution Factor
Result Reporting Limit
MDL Result Qualifier
EPA Qualifier
I
71-43-2 BENZENE 1 05 05 017 U
79-01-6 TRICHLOROETHENE 1 05 05 017 U
78-87-5
74middot95-3
75-27-4
10061-01-5
108middot10middot1
108middot88-3
10061-02middot6
79-00-5
591-78-6
12-DICHLOROPROPANE
DIBROMOMETHANE
BROMODCHLOROMETHANE
CIS-13-DICHLOROPROPEI~E
4-METHYL-2-PENTANONE
TOLUENE
TRANS-13-DICHLOROPROPENE
112-TRICHLOROETHANE
2-HEXANONE
1
1
1
1
1
1
1
1
1
05
05
05
05
5
031
05
05
10
05
05
05
05
5
05
05
05
10
017
017
017
017
17
017
017
017
17
U
U
U
U
U
J
U
U
U
127-18-4
142-28-9
124-48-1
106-93-4
108-90-7
630-20-6
100-41-4
136777-61-2
95-47-6
100-42middot5
75-25-2
98-82middot8
96-18-4
79-34-5
108-86-1
TETRACHLOROETHENE
13-DICHLOROPROPANE
DIBROMOCHLOROMETHANE
12-DIBROMOETHANE
CHLOROBENZENE
11 12-TETRACHLOROETHANE
ETHYLBENZENE
M+PmiddotXYLENE
OmiddotXYLENE
STYRENE
BROMOFORM
ISOPRO PYLBENZENE
123middotTRICHLOROPROPANE
1122-TETRACHLOROETHANE
BROMOBENZENE
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
05
05
1
1
05
05
05
1
05
05
05
05
2
05
05
05
05
1
1
05
05
05
1
05
05
05
05
2
05
05
017
017
017
017
017
017
017
017
017
017
017
017
017
017
017
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
i
Data Package 10 VL0911214-1
Date Printed Wednesday December 022009 AlS laboratory Group bullbull Fe Page 2 of 8
UMS Version 6317A
13
GCMS Volatiles Method SW8260_258
Sample Results
Lab Name ALS Laboratory Group bullbull FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject ID 644-111809(HWB R-37 VOCs) PAR 002731703
Field 10 R-37 Sor 2-111809
Lab ID 0911214middot1
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml
Moisture NA QCBatchlD VL091125-4-5 Final Volume 10 ml
Date Collected 18-Nov-09 Run ID VL091125-4A Result Units UGL
Date Extracted 25-Nov-09 Cleanup NONE Clean DF 1
Analysis ReqCode 104 Date Analyzed 25-Nov-09 Basis As Received
Prep Method SW5030 Rev C File Name 028044
CASNO Target Analyte Dilution Factor
103-65-1 NmiddotPROPYLBENZENE 1
95-49-8 2-CHLOROTOLUENE 1
108-67-8 135-TRIMETHYLBENZENE 1
106-43-4 4-CHLOROTOLUENE 1
98-06-6 TER I-BUTYLBENZENE 1
95-63-6 124-TRIMETHYLBENZENE 1
135-98-8 SEC-BUTYLBENZENE 1
541-73-1 13-OICHLOROBENZENE 1
99-87-6 P-ISOPROPYLTOLUENE 1
106-46-7 lA-DICHLOROBENZENE 1
104-51-8 N-BUTYLBENZENE 1
95-50-1 12-DICHLOROBENZENE 1
96-12-8 l2-DIBROMOmiddot3-CHLOROPROPANE 1
120-82-1 12A-TRICHLOROBENZENE 1
187-68-3 HEXACHLOROBUTADIENE 1
91-20-3 NAPHTHALENE 1
87-61middot6 123-TRICHLOROBENZENE 1
75-05-8 ACETONITRILE 1
107middot05middot1 ALLYL CHLORIDE 1
110-57-6 TRANS-14-DICHLORO-2-BUTENE 1
164-17-5 ETHANOL 1
97-63-2 ETHYL METHACRYLATE 1
78-83-1 ISOBUTYL ALCOHOL 1
126-98-7 METHACRYLONITRILE 1
80-62-6 METHYL METHACRYLATE 1
107-12-0 PROPIONITRILE 1
Result Reporting Limit
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
2 2
05 05
05 05
05 05
05 05
50 50
50 50
5 5
200 200
5 5
100 100
35 35
5 5
25 25
MDL Result EPA Qualifier Qualifier
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
067 U
017 U
017 U
017 U
017 U
83 U
017 U
U u 78 U
017 U
17 U
17 U
17 U
33 U
Data Package 10 VL0911214-1
Date Printed Wednesday December 022009 ALS Laboratory Group MM Fe Page 3 of 8
LlMS VerSion 6317A
14
GCMS Volati las Method SW8260_258
Sample Results
Lab Name ALS Laboratory Group - FC
Work Order Number 0911214
Client Name New Mexico Environment Department 08
ClientProject 10 644-111B09(HWB R-37 VOGs) PAR 002731703
Field 10 R-37 Ser 2-111809 Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10ml
Lab 10 0911214-1 Moisture NA
Date Collected 1B-Nov-09 QCBatchlO VL091125-4-5
Run 10 VL091125-4A
Final Volume 10ml
Result Units UGIL Date Extracted 25-Nov-09 Cleanup NONE Clean OF
Analysis ReqCode 104 Date Analyzed 25-Nov-09
Prep Method SW5030 Rev G Basis As Received
File Name 028044
CASNO Target Analyte Dilution Factor
Result Reporting Limit
MDL Result Qualifier
EPA Qualifier
126-99-8 CHLOROPRENE 1 5 5 017 U
75-65-0 TERT-BUTANOL 1 100 100 33 U
108-20-3 ISOPROPYL ETHER 1 2 2 033 U
637-92-3 ETHYL TERT-BUTYL ETHER 1 2 2 033 U
994-05-8 TERT-AMYL METHYL ETHER 1 2 2 033 U
67-72-1 HEXACHLOROETHANE 1 2 2 033 U
Surrogate Recovery
CASNO Surrogate Analyte Result Flag Spike Amount
Percent Recovery
Control Limits
460-00-4 4-BROMOFLUOHOBENZENE 246 25 98 82 - 121
1868-53-7 DIBROMOFLUOHOMETHANE 248 25 99 BO - 123
2037-26-5 TOLUENE-DB 258 25 103 85middot116
Data Package 10 VL0911214-1
Date Printed Wednesday December 022009 ALS Laboratory Group bullbull FC Page 4 of 8
LIMS Version 0317 A
15
GCMS Volati les Method SW8260_25B
Sample Results
Lab Name ALS Laboratory Group -- FC
Worlt Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-111809(HWB Rmiddot37 VOCs) PAR 002731703
Field 10 Rmiddot37 Scr jmiddot111809
Lab 10 0911214-2
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml Moisture NfA QCBatchID VL091125-4middot5 Final Volume 10 ml
Date Collected 18middotNov-09 Run 10 VL091125-4A Result Units UGfL Date Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Analysis ReqCode 104 Date Analyzed 25middotNov-09 Basis As Received Prep Method SW5030 Rev C File Name 028045
CASNO Target Analyte Dilution Factor
Result Reporting Limit
MOL Result Qualifier
EPA Qualifier
75-71-8 DICHLORODIFLUOROMETHANE 1 05 05 017 U
74-87-3 CHLOROMETHANE 1 05 05 017 U
75-01middot4 VINYL CHLORIDE 1 05 05 017 U
74-83-9 BROMOMETHANE 1 1 1 017 U
75middot00middot3 CHLOROETHANE j 05 05 017 U
75-69-4 TRICHLOROFLUOROMETHANE 1 05 05 017 U
107-02-8 ACROLEIN 1 100 100 17 U
i 75-35-4 11-DICHLOROETHENE 1 05 05 017 U
67-64middot1 ACETONE 1 10 10 33 U
74-8S-4 IODOMETHANE 1 5 5 017 U
75-15-0 CARBON DISULFIDE 1 10 10 017 U
75-09-2 METHYLENE CHLORIDE 1 1 1 017 U
156-60-5 TRANS-12-DICHLOROETHENE 1 05 05 017 U
1634-04-4 METHYL TERTIARY BUTYL ETHER 1 1 1 017 U
107-13-1 ACRYLONITRILE 1 10 10 17 U
75-34middot3 11-DICHLOROETHANE 05 05 017 U
i 108-05-4 VINYL ACETATE 1 10 10 067 U
115659-2 CISmiddot 2middotDICHLOROETHENE 1 05 05 017 U
178-933 2middotBUTANONE 1 5 5 17 U
74-97middot5 BROMOCHLOROMET HANE 1 1 1 017 U
67-66-3 CHLOROFORM 1 05 05 017 U
71-55middot6 111middotTRICHLOROETHANE 1 1 1 017 U
594-20-7 22middotDICHLOROPROPANE 1 05 05 017 U
56-23-5 CARBON TETRACHLORIDE 1 05 05 017 U
563-58-6 11middotDICHLOROPROPENE 1 05 05 017 U
107-06-2 12middotDICHL OROETHANE 1 05 05 017 U
Data Package ID VL0911214-1
Date Printed Wednesday December 022009 ALS Laboratory Group -- Fe Page 5 of 8
16
GCMS Volatiles Method SW8260_25B
Sample Results
Lab Name ALS Laboratory Group -- FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-111809(HW3 R-37 VOCs) PAR 002731703
Field 10 R-37 Scr 1-11 1809
Lab 10 0911214-2
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml
Moisture NIA QCBatchlO VL091125-4-5 Final Volume 10 ml
Date Collected 18-Nov-09 Run 10 VL091125-4A Result Units UGL
[late Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Analysis ReqCode 104 Date Analyzed 25-Nov-09
Prep Method SW5030 Rev C Basis As Received
File Name 028045
CASNO Target Analyte Dilution Factor
71-43-2 BENZENE 1
79-01-6 TRICHLOROETHENE 1
78-87-5 12-DICHLOROPROPANE 1
74-95-3 DIBROMOMETHANE 1
75-27-4 BROMODICHLOROMETHANE 1
10061-01-5 CIS-13-DICHLOROPROPENE 1
108-10-1 4-METHYL-2-PtNTANON 1
108-88-3 TOLUENE 1
10061-02-6 TRANS-13-DICHLOROPROPENE 1
79-00-5 112-TRICHLOROETHANE 1
591-78-6 2-HEXANONE 1
127-18-4 TETRACHLOROETHENE 1
142-28-9 13-DICHLOROPROPANt 1
124-48-1 DI3ROMOCHLOROMETHANE 1
106-93-4 12-DIBROMOETHANE 1
108-90-7 CHLOROBENZENE 1
OETHANE 1
- 1
LENE 1
ENE 1
ENE 1
OFORM 1
OPYlBENZENE 1
96-18-4 123-TRICHLOROPROPANE 1
79-34-5 1122-TETRACHLOROETHANE 1
108-86-1 BROMOBENZENE 1
Result Reporting Limit
05 05
05 05
05 05
05 05
05 05
05 05
5 5
025 05
05 05
05 05
10 10
05 05
05 05
1 1
1 1
05 05
05 05
05 05
1 1
05 05
05 05
05 05
05 05
2 2
05 05
05 05
MDL Result EPA Qualifier Qualifier
017 U
017 U
017 U
017 U
017 U
017 U
17 U
017 J
017 U
017 U
17 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
Data Package 10 VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- Fe Page 6 of 8
317A
17
GCMS Volatiles Method SW8260 _258
Sample Results
Lab Name ALS Laboratory Group -- FC
Work Order Number 0911214
Client Name New Mexico Environment Department 08
ClientProject 10 644-11S09(HWB R-37 VOCs) PAR 002731703
Field 10 Rmiddot37 Scr 1-111809
Lab 10 0911214-2
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml Moisture NA QCBatchlD VL091125-4-5 Final Volume 10 ml
Date Collected 18-Nov-09 Run 10 VL091125-4A Result Units UGL Date Extracted 25-Nol-09 Cleanup NONE Clean OF
Analysis ReqCode 104 Date Analyzed 25-Nov-09 Basis As Received Prep Method SW5030 Rev C File Name D28045
CASNO Target Analyte Dilution Factor
103-65-1 N-PROPYLBENZENE 1
95-49-8 2-CHLOROTOLUENE 1
108-67-8 135-TRIMETHYLBENZENE 1
106-43-4 4-CHLOROTOLUENE 1
98-06-6 TERT-BUTYLBENZENE 1
95-63-6 124-TRIMETHYLBENZENE 1
135-98-8 SEC-BUTYLBENZENE 1
i 541-73-1 13middotDICHLOROBENZENE 1
99-87-6 PmiddotISOPROPYL TOLUENE 1
106-46-7 I 14-DICHLOROBENZENE 1
104-51-8 I N-BUTYLBENZENE 1
95-50-1 l2-DICHLOROBENZENE 1
96-12-8 I 12-DIBROMO-3-CHLOROPROPANE 1
120-82-1 124-TRICHLOROBENZENE 1
87-68-3 HEXACHLOROBUT ADIENE 1
91-20-3 NAPHTHALENE 1
87-61-6 123-TRICHLOROBENZENE 1
75-05-S ACETONITRILE 1
107-05-1 ALLYL CH LORIDE 1
110-57-6 TRAN S-14-DICHLORO-2-BUTENE 1
64-17-5 ETHANOL 1
97-63-2 ETHYL METHACRYLATE 1
78-83-1 ISOBUTYL ALCOHOL 1
126-98-7 METHACRYLONITRILE 1
80-62-6 METHYL METHACRYLATE 1
107-12-0 I PROPIONITRILE 1
Result Reporting Limit
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
2 2
05 05
05 05
05 05
05 05
50 50
50 50 I 5 5
200 200
5 5
100 100
35 35
5 5
25 25
MDL
017
017
017
017
017
017
017
017
017
017
017
017
067
017
017
017
017
83
017
17
78
017
17
17
17
33
Result EPA Qualifier Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
Data Package 10 VL0911214-1
Date Printed Wednesday December 022009 ALS Laboratory Group -- Fe Page 7 of 8
LlMS Version 6317A
18
GCMS Volatiles Method SW8260_258
Sample Results
Lab Name ALS Laboratory Group bullbull FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644middot111B09(HWB R-37 VOCs) PAR 002731703
Sample Matrix WATER Prep Batch VL091125--4 Sample Aliquot 10 mlRmiddot37 Ser 1-111809 Moisture NA QCBatchlO VL091125--4-5 Final Volume 10 m
0911214-2 Date Collected 18-Nov-09 Run 10 VL091125--4A Result Units UGL Date Extracted 25-Nov-09 Cleanup NONE Clean OF 1 Date Analyzed 25-Nov-09 Basis As Received
10
Analysis ReqCode 104 Prep Method SW5030 Rev C File Name 028045
I
CASNO Target Analyte Dilution Factor
Result Reporting Limit
MDL Result Qualifier
EPA Qualifier
126-99-8 CHLOROPRENE 1 5 5 017 U
75-65-0 TERT-BUTANOL 1 100 100 33 U
108-20-3 ISOPROPYL ETHER 1 2 2 033 U
637-92-3 ETHYL TERT-BUTYL ETHER 1 2 2 033 U
994-05--8 TERT-AMYL MTHYL ETHER 1 2 2 033 U
67-72-1 HEXACHLOROETHANE 1 2 2 033 U
Surrogate Recovery
CASNO Surrogate Analyte Result Flag Spike Amount
Percent Control Recovery Limits
460-00-4 4middotBROMOFLUOROBENZENE 247 25 99 1
1868-53-7 DIBROMOFLUOROMETHANE 248 25 99 80 123
2037-26-5 TOLUENEmiddotDB 255 25 102 85 - 116
Data Package 10 VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- FC Page B of 8
LlMS Version 6317A
19
GCMS Volatiles Method SW8260_258
Laboratory Control Sample and Laboratory Control Sample Duplicate
Lab Name ALS Laboratory Group - FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-111809(HWB R-37 VOCs) PAR 002731703
Lab 10 VL091125-4LCS Sample Matrix WATER
Moisture NA Prep Batch VL091125-4
QCBatchlD VL091125-4-5
Sample Aliquot
Final Volume
10ml
10ml Date Collected NA Run 10 VL091125-4A Result Units UGIL Date Extracted 111252009 Cleanup NONE Clean OF 1 Date Analyzed 11252009 Basis NA
Prep Method SW5030C File Name 028040
CASNO
74-87-3
75-01-4
74-83-9
75-69-4
75-35-4
75-15-0
156-60-5
75-34-3
108-05-4
156-59-2
78-93-3
67 -66-3
71-55-6
i 56-23-5
107-06-2
71-43-2
79-01-6
78-87-5
75-27-4
108-88-3
79-00-5
591-78-6
127-18-4
106-93-4
108-90-7
63Q20-6
Target Analyte Spike Added
CHLOROMETHANE 10
VINYL CHLORIDE 10
BROMOMETHANE 10
TRICHLOROFLUOROMETHANE 10
11-DICHLOROETHENE 10
CARBON DISULFIDE 10
TRANS-12-DICHLOROETHENE 10
11-DICHLOROETHANE 10
VINYL ACETATE 10
CIS-12-DICHLOROETHENE 10
2middotBUTANONE 40
CHLOROFORM 10
111-TRICHL ORO ETHANE 10
CARBON TETRACHLORIDE 10
12-DICHLOROETHANE 10
BENZENE 10
TRICHLOROETHENE 10
12-DICHLOROPROPANE 10
BROMODICHLOROMETHANE 10
TOLUENE 10
112-TRICHLOROETHANE 10
2-HEXANONE 40
TETRACHLOROETHENE 10
12-DIBROMOETHANE 10
CHLOROBENZENE 10
1112-TETRACHLOROETHANE 10
LCS Reporting Result Result Limit Qualifier
932 05
863 05
943 1
908 05
96 05
95 10 J
996 05
992 05
10 10
102 05
412 5
993 05
974 1
943 05
106 05
983 05
962 05
10 05
988 05
974 05
989 05
409 10
956 05
991 1
984 05
101 05
LCS Control Rec Limits
93 49 -129
86 46 134
94 32-121
91 67 -152
96 61 -135
95 61 -140
100 70 -122
99 76 -119
100 62 182
102 75 126
103 61 -137
99 79 120
97 76 - 114
94 58middot135
106 75middot132
98 70 shy 125
96 74 121
100 81 -119
99 79 - 123
97 76 - 120
99 81 -126
102 45 168
96 56 -128
99 79 -123
98 75 -120
101 82 - 123
Data Package 10 VL0911214middot1
-Date Printed Wednesday December 02 2009 ALS Laboratory Group -- Fe Page 1 of 4
LiMS Version 6317A
20
GCMS Volatiles Method SW8260_25B
Laboratory Control Sample and Laboratory Control Sample Duplicate
Lab Name ALS Laboratory Group - FC
Work Order Number 0911214
Client Name New Mexico Envircnment Department OB
ClientProject 10 644-111809(HWB R-37 VOes) PAR 002731703
Lab 10 VL091125-4LCS Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml
Moisture NIA QCBatchlO VL091125-4-5 Final Volume 10 mi
Date Collected NA Run 10 VL091125-4A Result Units UGL Date Extracted 11252009 Cleanup NONE Clean OF 1 Date Analyzed 111252009 Basis NA
Prep Method SW5030e File Name 028040
CASNO Target Analyte Spike Added
LCS Result
Reporting Limit
Result Qualifier
LCS Rec
Control Limits
100-41-4 ETHYLBENZENE 10 981 05 98 79 -114
136777-61-2 M+P-XYLENE 20 197 1 98 81-115
95-47-6 O-XYLENE 10 101 05 101 81 -115
95-49-8 2-CHLOROTOLUENE 10 97 05 97 80 -128
541-73-1 13-DICHLOROBENZiNt 10 977 05 98 81-116
106-46-7 14-DICHLOROBENZENE 10 979 05 98 81 -119
95-50-1 12-DICHLOROBENZENE 10 987 05 99 79 - 116
91-20-3 NAPHTHALENE 10 993 05 99 69 -126
87-61-6 123-TRICHLOROBENZENE 10 999 05 100 60 -137
Data Package ID VL0911214-1
Date Printed Wecnesday December 02 2009 ALS Laboratory Group -- Fe Page 2 of 4
21
GCMS Volatiles Method SW8260_25B
Laboratory Control Sample and Laboratory Control Sample Duplicate
Lab Name ALS Laboratory Group bullbull FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-11 1809(HWB R-37 VOCs) PAR 002731703
Lab 10 VL091125middot4LCSD Sample Matrix WATER
Moisture NIA Prep Batch VL091125-4
QCBatchlD VL091125-4-5
Sample Aliquot
Final Volume
10 ml
10ml Date Collected NIA Run ID VL091125-4A Result Units UGIL Date Extracted 112512009 Cleanup NONE Clean DF 1 Date Analyzed 1112512009 Basis NIA
Prep Method SW5030C File Name 028041
CASNO Target Analyte Spike Added
LCSD Result
Reporting Limit
Result Qualifier
LCSD Rec
RPD Limit
RPD
74-87-3 CHLOROMETHANE 10 897 05 90 30 4
75-01-4 VINYL CHLORIDE 10 831 05 83 25 4
74-83-9 BROMO METHANE 10 945 1 94 25 0
75-69-4 TRICHLOROFLUOROMETHANE 10 873 05 87 22 4
75-35-4 11-DICHLOROETHENE 10 909 05 91 18 5
75-15-0 CARBON DISULFIDE 10 941 10 J 94 20 1
156-60middot5 TRANS-l2middotDICHLOROETHENE 10 961 05 96 25 4
75middot34middot3 11-DICHLOROETHANE 10 977 05 98 25 2
108-05-4 VINYL ACETATE 10 993 10 J 99 20 1
156middot59-2 CIS-12-DlCHLOROETHENE 10 995 05 99 25 3
i 78-93-3 2-BUTANONE 40 419 5 105 30 2
67-66-3 CHLOROFORM 10 985 05 99 25 1
71-55-6 lll-TRICHLOROETHANE 10 942 1 94 25 3
56-23-5 CARBON TETRACHLORIDE 10 922 05 92 25 2
107middot06-2 12middotDICHLOROETHANE 10 106 05 106 25 0
71-43middot2 BENZENE 10 971 05 97 10 1
79middot01middot6 TRICHLOROETHENE 10 939 05 94 10 2
78middot87middot5 l2middotDICHLOROPROPANE 10 101 05 101 25 1
i 75middot27-4 BROMODICHLOROMETHANE 10 992 05 99 25 0
1108-88-3 TOLUENE 10 962 05 96 9 1
I 79005 112middotTRICHLOROETHANE 10 986 05 99 25 0
591middot78middot6 2-HEXANONE 40 418 10 104 20 2
127middot18-4 TETRACHLOROETHENE 10 918 05 92 25 4
106-93-4 12middotDIBROMOETHANE 10 999 1 100 15 1
108middot90-7 CHLOROBENZENE 10 997 05 100 11 1
630-20middot6 1112-TETRACHLOROETHANE 10 101 05 101 15 0
100-41-4 ETHYLBENZENE 10 968 05 97 25 1
Data Package ID VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- FC Page 3 of 4
lIMS Version 6317 A
22
GCMS Volatiles Method SW8260_25B
Laboratory Control Sample and Laboratory Control Sample Duplicate
Lab Name ALS Laboratory 13roup -- FC
Work Order Number 0911214
Client Name New Mexico Environment Department OS
ClientProject 10 644-11 1809(HWB R-37 VOCs) PAR 002731703
Lab 10 VL091125-4LCSD Sample Matrix WATER
Moisture NA Prep Batch VL091125-4
QCBatchlO VL091125-4-5
Sample Aliquot
Final Volume
10 ml
10ml Date Collected NA Run 10 VL091125-4A Result Units UGL Date Extracted 11252009 Cleanup NONE Clean OF Date Analyzed 11252009 Basis NIA
Prep Method SW5030C File Name 028041
CASNO Target Analyte Spike Added
LCSD Result
Reporting Limit
Result Qualifier
LCSD Rec
RPD Limit
RPD
136777-61-2 M+P-XYLENE 20 193 1 97 25 2
95-47-6 O-XYLENE 10 983 05 98 25 2
95-49-8 2middotCHLOROTOLUENE 10 9A9 05 95 15 2
541-73-1 13middotDICHLOROBENZENE 10 997 05 100 25 2
106-46-7 14-DICHLOROBeNZENE 10 974 05 97 25 1
95-50middot1 12middotDICHLOROBENZeNE 10 101 05 101 25 2
91middot20-3 NAPHTHALENe 10 105 05 105 24 6
87-61-6 123-TRICHLOROBENZENE 10 102 05 102 33 3
Surrogate Recovery LCSLCSD
CASNO Target Analyte Spike Added
LCS Rec
LCS Flag
LCSD Rec
LCSD Flag
Control Limits
460middot00-4 4-BROMOFLUOROBeNZENE 25 100 100 82 - 121
1868-53middot7 DIBROMOFLUOROMeTHANE 25 101 100 80middot 123
2037middot26-5 TOLUENEmiddotD8 25 102 100 85middot 116
Data Package 10 VL0911214-
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- Fe Page 4 of 4
UMS Verslmt 6317A
23
ALS Laboratory Group -- Fe
Sample Number(s) Cross-Reference Table
R-37 S~r 1-111809
New Mexico Environment Department OB 644-111809(HWB R-37 VOCs) PAR
r 002731703 06-667 -55-01754
CDC Number Matrix Date Time Collected Collected
ALS Laboratory Group -- FePage 1 of 1 Date Printed Monday November 232009
Chain of Custody Record I d- I 4 SKIP TO MAIL REPORT TO fliff9ff BILL TO
Kim Glanzow kG Oilvlgt CobrUD Dflve NMEOmiddotOOE OlefSI9hl 8lJlI~iU (51SI pound614008 New Melllco Enlfrol Dev j-Iuartlous Waste gUleltJll
fort Collins CO 8Q524 183 Diamond Orje- Surfe A 2~S Rodeo P2IriI Driv~ East Bldg 1
(9l0) 490middot1511 tos Alamos Nw Mexico S75u Santa Fe NM 8750$ 2561
kglanlowiafliQoi
~7t----1
IComments L bull ce PIase note tht VOC bullbullmplbullbullbullr not preserved with HCL~ Mmiddot elt~U 1~~
~ It I ~D ~ [11 _ ~~ ~I ~l sect
tltgtfttOt~ Project Number (Lab noice Us Dnly)
644--111809(HWB Rmiddot37 VOCsl PAR i ~ ~ ~ ~
j J~ i~ ~~1- ~1~ ~ltj ~8 g ___ ~j $ Btl_
iIt~ q s- D flt
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t~~Numbr ----NMED Sam~iro Dbull -------ITi~ --Rmiddot37 Scr 2middot11middot18middot09 11812009 _ ____ 1555+--_-+__
Imiddot~ Rmiddot37 Scr 1middot11middot18middot09 1111812009 1744=+_J-_+_+--=----__+-__f __+----_l _
HWB rnf God~ QQ27111J1
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3 46ml glU~ VOA val$ iQn~Preserved
--+--t---
-+-----~-~--~~ ----
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6 ) TIllaWo 01 $JfliM t 1----- _J__LJ__
Print NMEO DOE Oversiyh Bureau ~---lco 16g-J~pound[ ~~ Level Standard I i+-~ UV f_
DateTime Received By Required MS MSO BlAnk I b~Y L_- Tim~18ndord ____
1bik~0
j ~i~~Ff~6~~~~ Jq c=JPlace X in box fherbullbullrIbullbulls than 5 tolalsople for shipping costs_
Page 1 Of 1
ali containers received intact (not broken or
at samples requiring no beadspace (VOC GRO RSKfMEE Rx CNS radon) free Size of bubble lt
(a leas 113 of container required)
samples checked for and free from the presence of residual chlorine when PM has indicated sample are from a chlorinatec water source note if fIeld preservation
sodIum thiosulfate was not observed)
Were cooler temperatures measured at O1-60degC IR lun used 2
Cooler I---shy
Temperature (C) 3 ~ No of custodv seals 01 cooler 0
External ~lRJhr reading
Backgrouncl ~lRhr reading 3 i Were exemai111Uhr readllljs S rwo lim backlTCltmri nnd within DOT acceptance criterin
NO
NO
NO
NO
---1
A-S Laboratory Group - Fort Collins
CONDITION OF SAMPLE UPO) RECEIPT FOMl
Client _Nyen-M---f=D~_______ Workordet No D4 I ~ I L --~--~-----~------
Prolecl Manager __LS_____________ Initials C DI Date 1 -gt= 0- () CJ
Additionallnformatiml PHOVlDE DETAILS BElOW FOR A NO RESIONS[ TCJ ANY (JUESTION ABOV EXCEPT III Al[ 16
---------~-----
If hbilt W ru YES 0 I NA (If Ijrojcct Manager Signature I Date -----l-f---1-tl__--~~_l_4I(--2_)-lt-(_middota_I_----------
DnteTimc
in Gun 112 Oakton SN 299225[l020)middot()()66 m Cllll1li1 Oakton S~~ 2372220lOl(J002
Form 201r22xls (61109) Page 1 of i
FecEx~ US Airbill 9439 4324 BmipiennpoundUpyExpress 4a ExpressPeckageService
~ ~=~~l~h1 ~~DeJeIt1tlflrlMonallmiddot J~eSS SAilJR1JAYUI~~I_wt
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__ Packages up to 1511 Js Fed StaMard Overnight [J r~~xr~~~~tnIiWJenamplUtrnoonmiddot SrumBvtIMyNtn illblt C~l3ryftM4eU(ICatlOOt~
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_______~~~l--~bullbull~~--~----~~re~~~~--~------~
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8700 9439 4324
6 Special Handlillgand Delivery Signature Olllions
=J ~~~tr~~ ow MmINomht sx lD fnri1r
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Dry Ice Dlflt~9UN11M~ ___ bull ___
L Caflo Aircraft Only
TOIBIPacbges lotlllWeight
I--r-- 1If shy ______
Tawhbiiity~JamJnldtnl100lJnlmyO(jowm~t~SurmttFodfxSMlftGIKIktl1Wit
ALS Labofaton1 Group
Environmental Division Fort Cofiins Colorado
GCMS Volatiles Case Narrative
New Mexico Environmental Department OB 644-111809(HWB R-37 VOCs) PAR -- 002731703
Work Order Number 0911214
1 This report consists of 2 water samples The samples were received cool and intact by ALS on 1120109 The vial for sample 0911214-1 contained headspace prior to analysis because it was not received headspace free into the voatiles laboratory
The samples provided for volatiles had a pH gt 2 at the time of analysis
2 These samples were prepared according to SW-846 3rd Edition procedures Specifically the water samples were prepared by purging 10 mL using purge and trap procedures based on Method 5030C
3 The samples were analyzed using GCMS with an RTX-624 RTX-VMS or equivalent capillary column according to SOP 525 Revision 14 based on SW-846 Method 8260B All positive results were quantitated against the initial calibration standards using the intemal standard technique The identification of positive results was achieved by a comparison of the retention time and mass spectrum of trle sample versus the daily calibration standard
4 All initial calibration criteria for SPCCs and CCCs were met If average response factors were used in the initial calibration RSO was 15 If linear or higher order regression calibrations were used in the initial calibration the coefficient of determination (r2) ~099
5 All initial calibrations are verified by comparing a second source standard calibration verrrication (ICV) against the calibration curve All target compounds in the second source verification had a 0 of less than 25
6 All criteria for SPCCs and CCCs were met in daily (continuing) calibration verifications (CCV)
7 Methylene chloride acetone and 2-butanone are common laboratory contaminants In order to minimize the levels of these compounds detected in the gclms analysis ALS has designated its volatile laboratory as a restricted access area In addition the laboratory has been equipped with a dedicated air intake and exhaust system that operates under positive pressure in order to
1
minimize cross contamination of these compounds Due to fluctuations in ambient laboratory conditions reported sample values for common laboratory contaminants may be due to lab contamination even if the compound in question is not detected in the associated method blankmiddot
All method blank criteria were met
8 All laboratory control sample and laboratory control sample duplicate recoveries and RPDs were within the acceptance criteria
9 Since a sample from this order number was not the selected qualITy control (QC) sample matrix specific QC results are not included in this report
10 The samples were analyzed within the established holding time
11 All surrogate recoveries were within acceptance criteria
12 All internal standard recoveries were within acceptance criteria
14 Manual integrations are performed when needed to provide consistent and defensible data following the guidelines in SOP 939 ReVision 3
The data contained in the following report have been reviewed and approved by the personnel listed below In addition ALS certifies that the analyses reported herein are true complete and correct within the limits of the methods employed
n-o3-o5Sha~JobeS Date Organics Primary Data Reviewer
l~-O 1-01TAamp1~Orga~cs Final Data Reviewer Date
2
ALS Data Qualifier Flags Chromatography and Mass Spectrometry
U or NO This flag indicates that the compound was analyzed for but not detected
J This flag indicates an estimated value This flag is used as follows (1) when estimating a concentration for tentatively identified compounds (TICs) where a 11 response is assumed (2) when the mass spectral and retention time data indicate the presence of a compound that meets the volatile and semivolatile GCMS identification criteria and the result is less than the reporting limit (RL) but greater than the method detection limit (MOL) (3) when the retention time data indicate the presence of a compound that meets the GC identification criteria and the result is less than the RL but greater than the MOL and (4) the reported value is estimated
B This flag is used when the analyte is detected in the associated method blank as well as in the sample It indicates probable blank contamination and warns the data user This flag shall be used for a tentatively identified compound (TIC) as well as for a positively identified target compound
E This flag identifies compounds whose concentration exceeds the upper level of the calibration range
A This flag indicates that a tentatively identified compound is a suspected aldol-condensation product
X This flag indicates that the analyte was diluted below an accurate quantitation level
This flag indicates that a spike recovery is equal to or outside the control criteria used
+ This flag indicates that the relative percent difference (RPO) equals or exceeds the control criteria
3
ALS Laboratory Group -- Fe Sample Number(s) Cross-Reference Table
Paragon OrderNum 0911214 Client Name New Mexico Environment Department OB
Client Project Name 644-111809(HWB R-37 VOCs) PAR Client Project Number 002731703
Client PO Number 06-667-55-01754
Client Sample Number
Lab Sample Number
COC Number Matrix Date Collected
Time Collected
R-37 Scr 2-1 11809 0911214-1 WATER 18-Nov-09 1555 R-37 Scr 1-111809 0911214-2 WATER 18-Nov-09 1744
Page 1 of 1 ALS Laboratory Group -- Fe Date Printed Wednesday December 02 2009 LlMS Version 6317 A
4
Chain of Custody Record 1)11 d- I 4 SHIP To MAil REPORT TO HtitilJft BILL TO
Kim GrJOZOW KC [)il-e Cobra
NMFOmiddotDOE Overslghl Bwe3u 50S firt1middottoOB Hew Meico FnlliTtl1 Dep1 HaVIdthJS VvaMe Bureau ~orl Collins CO 80524shy
1UH Diamold Drive Stille 8 90S Rodeo P3M( D~lIe Ea~ Bldg(970) 90middot511
lo Alarr1(1l N~Muto 87544 83113 Fe liM 87505middot25-67
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Project Number (Llib invoice USI
Only)
o~_IIi~~__
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644middot111809(HWB Rmiddot37 VOCs) PAR
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S SSG 00
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567
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cI yl iComments Lanc~v fiias not~ that foe samples life not preg~-d with HCL bull
~ 4_~~~~S5 V~~~Vi~I_$ ~~~~5s~rvd __
3 4()ml glau VOA vials Non-PrlttIrv~d -----~--
OC Level Standard f 0~Y ~-t-~ (fv f_ QC Required MS MSD Bla~k
irU11 Around TieJTAT) ~_dbullr_d__~______
cJPlace X In bOK If there are less than 5 lotal sample for shipping cosls
IJl
PQf 1
---- ---- ---
ALS Laboratory GrouP - Fort Collins
CONDITIO] OF SAMPLE UPO) RECEIPT FORM
Client _-=-N--M---f-=-D________ IVorkorde No D4 J I 4 --~~~~~~------
PrO1 cc Manager L 5 lnitiais C D Date 1 -) ()- () C --~~~---------------------
1 there a cae Are the coe and bottle labels
Is the coe in agreement with samples received) of containers matrix requested anaiyses etc)
documents presen1 andor removable)
Are all aqueous samples requiring preservation preserved correctly ~- ----~-~~--- -~ -~-- ----~~~---------
volatiles)
14 Are all samples requiring no headspace (VOC GRG RSKlVIEE lb eNS radon)
free Size of bubble lt
$ Do perchlorate LCMS-MS samples have headspace (a~ least ]3 of container required)
NO
]6 Were samples checked for and free from the presence of residual chlorine (Appiicaole when PM has Indicated samples are from a chlonnated wat~ source note if field preservallor
witb sodIUm tlllosulfate wa not observed)
17 Were the lljIV~IOU on ice
IS Were cooler temperatures measured at 01-60degC IR ~Illl used 2
Coole I---
Temperature (C) 3 ~
NO
NO
NO
NO
NO
NO
NO
No of custodv seals Ol~ cooler 0 OOT ---- --- --- --l Surveyl EXlemlli flRhr n~ading I i AcceplanCfiltnforma tlon Background ulJhr reading 3 Were eX lema uRhf readl1lf5 tW(l tm bnckl1Ound and withllllxyr acceptance criterill
Additional Iuformation OVIDE DETAILS BELOW FOR A ND RESPONSE TO ANY (UESTION A80VE EXCEPT 1 ANI) 16
If applicable was the clienl contacted) YES i NO I
Project Manager Signature I Date
(1 Gun 112 Oaktoll SN 2992250020 jmiddot0066 lR Gun lie Oakton S~ 23n220101middot0(J02
Form 201r22gt15 (61109) Page 1 of _1
6
4a Express Package Service _ FadEx Pnority OvernightLJ ==lr-~MClncU1
lSlIIQSATUIIDAYlltIrwIlyis$Mf(1J
middot10_ FadEx SlaMard Ovemioht fMtRallw6ftIlfTampCI v
Stun1I1V OlIwtrlN01IMlIIbU1 PtnIttlgas IIfI ro 150lbs FedEx First OV1lmigtr ~Mmnm~rnollnll onwy9Itetlncalklfl bull SIItlmiIlYDNOTaBItOifi
FecEx~ US Airbill Express
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9439 4324
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4b ExpressfreightService - __ C0T1llanv
~~oalleJl =1~~ImOt $AUROAY ftlEdOeyF1tlitNbiDrnJtin
5 Packaging -1itIcIrme-- FadEgt r- FedEgt fak FedEx Box
kt1UoorFdrStNil~~Your Internal Billing Reference Enveiope Pol _
TD
Address Wa clMOfdeiinrto POlwuscrPo ZIP CGlJla
Address
6 Special Handlmlllilld Delivery SignalUlll Options
~~~l~__Iint_dUSabulld)IjhL Indirect Sianarurc ttMtrttISMIllFtdlHrtS ~~tlltl~ eeelMllnllrl$ICIIltctdeiMv-kll lt_noaIllaIMInt$ ~
OrvlceL- OtyiclItUN186 ___ ___
[ CaflO Aircraft Oniy
8700 9439 4324 ~rtl1~l__bPnD USA SRI
_____-----------~bull---~----- -------~~-------------------
7
GCMS Volatiles Method SW8260 _25B
Method Blank
Lab Name ALS Laboratory Group bullbull FC
Work Order Number 0911214
Client Name New Mexico Environment Department DB
ClientProject 10 644-111809(HWB Rmiddot37 VOCs) PAR 002731703
Lab 10 VL091125-4MB Sample Matrix WATER
Moisture NA Prep Batch VL091125-4
QCBatchlO VL091125-4-5
Sample Aliquot
Final Volume
10 ml
10 ml Date Collected NA Run 10 VL091125-4A Result Units UGL Date Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Date Analyzed 25middotNov-09 Basis NA
File Name 028043
CASNO Target Analyte DF
75-71-8 DICHLORODIFLUOROMETHANE
74-87-3 CHLOROMETHANE
75-01-4 VINYL CHLORIDE
74-83-9 BROMOMETHANE
75-00-3 CHLOROETHANE
75-69-4 TRICHLOROFLUOROMETHANE
107-02-8 ACROLEIN
75-35-4 11middotDICHLOROETHENE
67-64-1 ACETONE
74-88-4 IODOMETHANE
75-15-0 CARBON DISULFIDE
METHYLEN E CHLORIDE 75-09-2
156-60-5 TRANS-12middotDICHLOROETHENE
1634-04-4 METHYL TERTIARY BUTYL ETHER
107-13-1 ACRYLONITRILE
75-34-3 11-DICHLOROETHANE
108-05-4 VINYL ACETATE
156-59middot2 CIS-12middotDICHLOROETHENE
78-93-3 2middotBUTANONE
~ BROMOCHLOROMETHANE
67-66-3 CHLOROFORM
71-55-6 111middot TRICHLOROETHANE
594-20-7 22middotDICHLOROPROPANE
56-23-5 CARBON TETRACHLORIDE
563-58-6 11middotDICHLOROPROPENE
107-06middot2 l2middotDICHLOROETHAN E
71-43-2 BENZENE
79-01-6 TRICHLOROETHENE
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Result Reporting Limit
05 05
05 05
05 05
1 1
05 05
05 05
100 100
05 05
10 10
5 5
10 10
1 1
05 05
1 1
10 10
05 05
10 10
05 05
5 5
1 1
05 05
1 1
05 05
05 05
05 05
05 05
05 05
05 05
MDL Result EPA Qualifier Qualifier
017 U
017 U
017 U
017 U
017 U
017 U
17 U
017 U
33 U
017 U
017 U
017 U
017 U
017 U
17 U
017 U
067 U
017 U
17 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
Data Package 10 VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- Fe Page 1 of 4
llMS Version 6317 A
8
GCMS Volatiles Method SW8260 _25B
Method Blank
Lab Name ALS Laboratory Group -- FC
Work Order Number 0911214
Client Name New Mexico Environment Department 08
ClientProject 10 644-111809(HWEI R-37 voes) PAR 002731703
Lab 10 VL091125-4MB Sample Matrix WATER
Moisture NIA Prep Batch VL091125-4
QCBatchIO VL091125-4-5
Sample Aliquot
Final Volume
10 ml
10 ml Oate Collected NIA Run 10 VL091125-4A Result Units UGL Oate Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Date Analyzed 25-Nov-09 Basis NIA
File Name 028043
CASNO Target Analyte OF Result Reporting Limit
MOL Result Qualifier
EPA Qualifier
78-87-5 12middotDICHLOROPROPANE 1 05 05 017 U
74-95-3 DIBROMOMETHANE 1 05 05 017 U
75-27-4 BROMODICHLOROMETHANE 1 05 05 017 U
10061-01-5 CISmiddot13middotDICHLOROPROPENE 1 05 05 017 U
108-10-1 4-METHYL-2-PENT ANONE 1 5 5 17 U
108-88-3 TOLUENE 1 05 05 017 U
10061-02-6 TRANS-13-DICHLOROPROPENE 1 05 05 017 U
79-00-5 112-TRICHLOROETHANE 1 05 05 017 U
591-78-6 2-HEXANONE 1 10 10 17 U
127-18-4 TETRACHLOROETHENE 1 05 05 017 U
142-28-9 13-DICHLOROPROPANI 1 05 05 017 U
124-48-1 DIBROMOCHLOROMETHANE 1 1 1 017 U
106-93-4 12-DIBROMOETHANE 1 1 1 017 U
108-90-7 CHLOROBENZENE 1 05 05 017 U
630-20-6 1112-TETRACHLOROETHANE 1 05 05 017 U
100-41-4 ETHYLBENZENE 1 05 05 017 U
136777-61-2 M+P-XYLENE 1 1 1 017 U
95-47-6 O-XYLENE 1 05 05 017 U
100-42-5 STYRENE 1 05 05 017 U
75-25-2 BROMOFORM 1 05 05 017 U
98-82-8 ~YLBENZENE 1 05 05 017 U
96-18-4 123-TRICHLOROPROPANE 1 2 2 017 U
79-34-5 1122middot TETRACHLOROETHANE 1 05 05 017 U
108-86-1 BROMOBENZENE 1 05 05 017 U
103-65-1 N-PROPYLBENZENE 1 05 05 017 U
95-49-8 2-CHLOROTOLUENE 1 05 05 017 U
108-67-8 135-TRIMETHYLBENZENE 1 05 05 017 U
106-43-4 4-CHLOROTOLUENE 1 05 05 017 U
Data Package 10 VL0911214-1
Date Printed Wednesday December n 2009 AlS Laboratory Group -- FC Page 2 of 4
lMS VeCSiOIY 6317A
9
GCMS Volatiles Method SW8260 _258
Method Blank
Lab Name ALS Laboratory Group - FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-111B09(HWB R-37 VOCs) PAR 002731703
Lab 10 VL091125-4MB Sample Matrix WATER
Moisture NIA
Prep Batch VL091125-4
QCBatchlD VL091125-4-5
Sample Aliquot
Final Volume
10 ml
10 ml
Date Collected NIA Run ID VL091125-4A Result Units UGL
Date Extracted 25-Nov-09 Cleanup NONE Clean DF 1
Date Analyzed 25-Nov-09 Basis NA
File Name 028043
CASNO Target Analyte OF Result Reporting Limit
MOL Result Qualifier
EPA Qualifier
98-06-6 TERT-BUTYLBENZENE 1 05 05 017 U
95-63-6 124-TRIMETHYLBENZENE 1 05 05 017 U
135-98-8 SEC-BUTYLBENZENE 1 05 05 017 U
541-73-1 13-DlCHLOROBENZENE 1 05 05 017 U
99-87-6 P-ISOPROPYLTOLUENE 1 05 05 017 U
106-46-7 1 A-DICHLOROBENZENE 1 05 05 017 U
104-51-8 N-BUTYLBENZENE 1 05 05 017 U
95-50-1 12-DICHLOROBENZENE 1 05 05 017 U
96-12-B 12-DIBROMO-3-CHLOROPROPANE 1 2 2 067 U
120-82-1 124-TRiCHLOROBENZENE 1 05 05 017 U
87-68-3 HEXACHLOROBUTADIENE 1 05 05 017 U
91-20-3 NAPHTHALENE 1 05 05 017 U
87-61-6 123-TRICHLOROBENZENE 1 05 05 017 U
75-05-B ACETONITRILE 1 50 50 83 U
107-05-1 ALLYL CHLORIDE 1 50 50 017 U
110-57-6 TRANS-14-DICHLORO-2-BUTENE 1 5 5 17 U
64-17-5 ETHANOL 1 200 200 78 U
97-63-2 ETHYL METHACRYLATE 1 5 5 017 U
78-83-1 ISOBUTYL ALCOHOL 1 100 100 17 U
126-98-7 METHACRYLONITRILE 1 35 35 17 U
80-62-6 METHYL METHACRYLATE 1 5 5 17 U
107-12-0 PROPIONITRILE 1 25 25 33 U
126-99-8 CHLOROPRENE 1 5 5 017 U
75-65-0 TERT-BUTANOL 1 100 100 33 U
108-20-3 ISOPROPYL ETHER 1 2 2 033 U
637-92-3 ETHYL TERT-BUTYL ETHER 1 2 2 033 U
994-05-8 TERT-AMYL METHYL ETHER 1 2 2 033 U
67-72-1 HEXACHLOROETHANE 1 2 2 033 U
Data Package 10 VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -~ Fe Page 3 of 4
LlMS Version 6317 A
10
GCMS Volatiles Method SW8260 _258
Method Blank
Lab Name ALS Laboratory Group -- FC
Work Order Number 0911214
Client Name New Mexico Envirmment Department OB
ClientProject 10 644-111809(HWB R-37 VOCs) PAR 002731703
Lab 10 VL091125-4MB Sample Matrix WATER
Moisture NIA Prep Batch VL091125-4
QCBatchlO VL091125-4-5
Sample Aliquot
Final Volume
10 m
10m Date Collected NIA Run 10 VL091125-4A Result Units UGIL Date Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Date Analyzed 25-Nov-09 BasisNIA
File Name 028043
CASNO Target Analyte Result Reporting MOL Result EPAOF Limit Qualifier Qualifier
Surrogate Recovery
CASNO Surrogate Analyte Result Flag Spike Amount
Percent Recovery
Control Limits
460-00-4 4-BROMOFLUOROBENZENE 25 25 100 82 - 121
1868-53-7 DIBROMOFLUOROMETHANE 248 25 99 80 - 123
2037-26-5 TOLUENE-D8 26 25 104 85 - 116
Data Package 10 VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- FC Page 4 of4
LlMS Version 6317A
11
GCMS Volati les Method SW8260 _258
Sample Results
Lab Name ALS Laboratory Group -- FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-111809(HWB R-37 VOCs) PAR 002731703
Field 10 Rmiddot37 Ser 2middot111809
Lab 10 0911214middot1
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml
Moisture NA QCBatchlO VL091125-4-5 Final Volume 10mi Date Collected 18-Nov-09 Run 10 VL091125-4A Result Units UGL
Date Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Analysis ReqCode 104 Date Analyzed 25-Nov-09
Prep Method SW5030 Rev C Basis As Received
File Name 028044
CASNO Target Analyte Dilution Factor
75-71-8 DICHLORODIFLUOROMETHANE 1
74middot87-3 CHLOROMETHANE 1
75-01-4 VINYL CHLORIDE 1
74-83-9 BROMOMETHANE 1
75-00-3 CHLOROETHANE 1
75-69-4 TRICHLOROFLUOROMETHANE 1
107-02-8 ACROLEIN 1
75-35-4 11middotDICHLOROETHENE 1
67-64-1 ACETONE 1
74-88-4 IODOMETHANE 1
75-15-0 CARBON DISULFIDE 1
75-09-2 METHYLENE CHLORIDE 1
156-60-5 TRANSmiddot12middotDICHLOROETHENE 1
1634-04-4 METHYL TERTIARY BUTYL ETHER 1
107-13-1 ACRYLONITRILE 1
75-34-3 1-DICHLOROETHANE 1
i 108-05-4 VINYL ACETATE 1
156-59-2 CIS-12middotDICHLOROETHENE 1
78-93-3 2-BUTANONE 1
74-97-5 BROMOCHLOROMETHANE 67-66-3 CHLOROFORM 1
71-55-6 11-TRICHLOROETHANE 594-20-7 22-DICHLOROPROPANE 56-23-5 CARBON TETRACHLORIDE 563-58-6 -DICHLOROPROPENE 107-06-2 2-DICHLOROETHANE
Result Reporting Limit
05 05
05 05
05 05
1 1
05 05
05 05
100 100
05 05
10 10
5 5
10 10
1 1
05 05
1 1
10 10
05 05
10 10
05 05
5 5
1 1
05 05
1 1
05 05
05 05
05 05
05 05
MOL Result EPA Qualifier Qualifier
017 U
017 U
017 U
017 U
017 U
017 U
17 U
017 U
33 U
017 U
017 U
017 U
017 U
017 U
17 U
017 U
067 U
017 U
17 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
Data Package ID VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- Fe Page 1 of 8
UMS Version 6317A
12
GCMS Volatiles Method SW8260_25B
Sample Results
Lab Name ALS Laboratory Group - FC
Work Order Number 0911214
Client Name New Mexico nvironment Department OB
ClientProject 10 644-111809(HWB R-37 VOCs) PAR 002731703
Field 10 R-37 Scr 2-111809
Lab 10 0911214-1
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10ml
Moisture NA QCBatchlD VL091125-4-5 Final Volume 10ml
Date Collected l8-Nov-09 Run 10 VL091125-4A Result Units UGL
Date Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Analysis ReqCode 104 Date Analyzed 25-Nov-09 Basis As Received
Prep Method SW5030 Rev C File NameD28044
CASNO Target Analyte Dilution Factor
Result Reporting Limit
MDL Result Qualifier
EPA Qualifier
I
71-43-2 BENZENE 1 05 05 017 U
79-01-6 TRICHLOROETHENE 1 05 05 017 U
78-87-5
74middot95-3
75-27-4
10061-01-5
108middot10middot1
108middot88-3
10061-02middot6
79-00-5
591-78-6
12-DICHLOROPROPANE
DIBROMOMETHANE
BROMODCHLOROMETHANE
CIS-13-DICHLOROPROPEI~E
4-METHYL-2-PENTANONE
TOLUENE
TRANS-13-DICHLOROPROPENE
112-TRICHLOROETHANE
2-HEXANONE
1
1
1
1
1
1
1
1
1
05
05
05
05
5
031
05
05
10
05
05
05
05
5
05
05
05
10
017
017
017
017
17
017
017
017
17
U
U
U
U
U
J
U
U
U
127-18-4
142-28-9
124-48-1
106-93-4
108-90-7
630-20-6
100-41-4
136777-61-2
95-47-6
100-42middot5
75-25-2
98-82middot8
96-18-4
79-34-5
108-86-1
TETRACHLOROETHENE
13-DICHLOROPROPANE
DIBROMOCHLOROMETHANE
12-DIBROMOETHANE
CHLOROBENZENE
11 12-TETRACHLOROETHANE
ETHYLBENZENE
M+PmiddotXYLENE
OmiddotXYLENE
STYRENE
BROMOFORM
ISOPRO PYLBENZENE
123middotTRICHLOROPROPANE
1122-TETRACHLOROETHANE
BROMOBENZENE
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
05
05
1
1
05
05
05
1
05
05
05
05
2
05
05
05
05
1
1
05
05
05
1
05
05
05
05
2
05
05
017
017
017
017
017
017
017
017
017
017
017
017
017
017
017
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
i
Data Package 10 VL0911214-1
Date Printed Wednesday December 022009 AlS laboratory Group bullbull Fe Page 2 of 8
UMS Version 6317A
13
GCMS Volatiles Method SW8260_258
Sample Results
Lab Name ALS Laboratory Group bullbull FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject ID 644-111809(HWB R-37 VOCs) PAR 002731703
Field 10 R-37 Sor 2-111809
Lab ID 0911214middot1
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml
Moisture NA QCBatchlD VL091125-4-5 Final Volume 10 ml
Date Collected 18-Nov-09 Run ID VL091125-4A Result Units UGL
Date Extracted 25-Nov-09 Cleanup NONE Clean DF 1
Analysis ReqCode 104 Date Analyzed 25-Nov-09 Basis As Received
Prep Method SW5030 Rev C File Name 028044
CASNO Target Analyte Dilution Factor
103-65-1 NmiddotPROPYLBENZENE 1
95-49-8 2-CHLOROTOLUENE 1
108-67-8 135-TRIMETHYLBENZENE 1
106-43-4 4-CHLOROTOLUENE 1
98-06-6 TER I-BUTYLBENZENE 1
95-63-6 124-TRIMETHYLBENZENE 1
135-98-8 SEC-BUTYLBENZENE 1
541-73-1 13-OICHLOROBENZENE 1
99-87-6 P-ISOPROPYLTOLUENE 1
106-46-7 lA-DICHLOROBENZENE 1
104-51-8 N-BUTYLBENZENE 1
95-50-1 12-DICHLOROBENZENE 1
96-12-8 l2-DIBROMOmiddot3-CHLOROPROPANE 1
120-82-1 12A-TRICHLOROBENZENE 1
187-68-3 HEXACHLOROBUTADIENE 1
91-20-3 NAPHTHALENE 1
87-61middot6 123-TRICHLOROBENZENE 1
75-05-8 ACETONITRILE 1
107middot05middot1 ALLYL CHLORIDE 1
110-57-6 TRANS-14-DICHLORO-2-BUTENE 1
164-17-5 ETHANOL 1
97-63-2 ETHYL METHACRYLATE 1
78-83-1 ISOBUTYL ALCOHOL 1
126-98-7 METHACRYLONITRILE 1
80-62-6 METHYL METHACRYLATE 1
107-12-0 PROPIONITRILE 1
Result Reporting Limit
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
2 2
05 05
05 05
05 05
05 05
50 50
50 50
5 5
200 200
5 5
100 100
35 35
5 5
25 25
MDL Result EPA Qualifier Qualifier
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
067 U
017 U
017 U
017 U
017 U
83 U
017 U
U u 78 U
017 U
17 U
17 U
17 U
33 U
Data Package 10 VL0911214-1
Date Printed Wednesday December 022009 ALS Laboratory Group MM Fe Page 3 of 8
LlMS VerSion 6317A
14
GCMS Volati las Method SW8260_258
Sample Results
Lab Name ALS Laboratory Group - FC
Work Order Number 0911214
Client Name New Mexico Environment Department 08
ClientProject 10 644-111B09(HWB R-37 VOGs) PAR 002731703
Field 10 R-37 Ser 2-111809 Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10ml
Lab 10 0911214-1 Moisture NA
Date Collected 1B-Nov-09 QCBatchlO VL091125-4-5
Run 10 VL091125-4A
Final Volume 10ml
Result Units UGIL Date Extracted 25-Nov-09 Cleanup NONE Clean OF
Analysis ReqCode 104 Date Analyzed 25-Nov-09
Prep Method SW5030 Rev G Basis As Received
File Name 028044
CASNO Target Analyte Dilution Factor
Result Reporting Limit
MDL Result Qualifier
EPA Qualifier
126-99-8 CHLOROPRENE 1 5 5 017 U
75-65-0 TERT-BUTANOL 1 100 100 33 U
108-20-3 ISOPROPYL ETHER 1 2 2 033 U
637-92-3 ETHYL TERT-BUTYL ETHER 1 2 2 033 U
994-05-8 TERT-AMYL METHYL ETHER 1 2 2 033 U
67-72-1 HEXACHLOROETHANE 1 2 2 033 U
Surrogate Recovery
CASNO Surrogate Analyte Result Flag Spike Amount
Percent Recovery
Control Limits
460-00-4 4-BROMOFLUOHOBENZENE 246 25 98 82 - 121
1868-53-7 DIBROMOFLUOHOMETHANE 248 25 99 BO - 123
2037-26-5 TOLUENE-DB 258 25 103 85middot116
Data Package 10 VL0911214-1
Date Printed Wednesday December 022009 ALS Laboratory Group bullbull FC Page 4 of 8
LIMS Version 0317 A
15
GCMS Volati les Method SW8260_25B
Sample Results
Lab Name ALS Laboratory Group -- FC
Worlt Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-111809(HWB Rmiddot37 VOCs) PAR 002731703
Field 10 Rmiddot37 Scr jmiddot111809
Lab 10 0911214-2
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml Moisture NfA QCBatchID VL091125-4middot5 Final Volume 10 ml
Date Collected 18middotNov-09 Run 10 VL091125-4A Result Units UGfL Date Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Analysis ReqCode 104 Date Analyzed 25middotNov-09 Basis As Received Prep Method SW5030 Rev C File Name 028045
CASNO Target Analyte Dilution Factor
Result Reporting Limit
MOL Result Qualifier
EPA Qualifier
75-71-8 DICHLORODIFLUOROMETHANE 1 05 05 017 U
74-87-3 CHLOROMETHANE 1 05 05 017 U
75-01middot4 VINYL CHLORIDE 1 05 05 017 U
74-83-9 BROMOMETHANE 1 1 1 017 U
75middot00middot3 CHLOROETHANE j 05 05 017 U
75-69-4 TRICHLOROFLUOROMETHANE 1 05 05 017 U
107-02-8 ACROLEIN 1 100 100 17 U
i 75-35-4 11-DICHLOROETHENE 1 05 05 017 U
67-64middot1 ACETONE 1 10 10 33 U
74-8S-4 IODOMETHANE 1 5 5 017 U
75-15-0 CARBON DISULFIDE 1 10 10 017 U
75-09-2 METHYLENE CHLORIDE 1 1 1 017 U
156-60-5 TRANS-12-DICHLOROETHENE 1 05 05 017 U
1634-04-4 METHYL TERTIARY BUTYL ETHER 1 1 1 017 U
107-13-1 ACRYLONITRILE 1 10 10 17 U
75-34middot3 11-DICHLOROETHANE 05 05 017 U
i 108-05-4 VINYL ACETATE 1 10 10 067 U
115659-2 CISmiddot 2middotDICHLOROETHENE 1 05 05 017 U
178-933 2middotBUTANONE 1 5 5 17 U
74-97middot5 BROMOCHLOROMET HANE 1 1 1 017 U
67-66-3 CHLOROFORM 1 05 05 017 U
71-55middot6 111middotTRICHLOROETHANE 1 1 1 017 U
594-20-7 22middotDICHLOROPROPANE 1 05 05 017 U
56-23-5 CARBON TETRACHLORIDE 1 05 05 017 U
563-58-6 11middotDICHLOROPROPENE 1 05 05 017 U
107-06-2 12middotDICHL OROETHANE 1 05 05 017 U
Data Package ID VL0911214-1
Date Printed Wednesday December 022009 ALS Laboratory Group -- Fe Page 5 of 8
16
GCMS Volatiles Method SW8260_25B
Sample Results
Lab Name ALS Laboratory Group -- FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-111809(HW3 R-37 VOCs) PAR 002731703
Field 10 R-37 Scr 1-11 1809
Lab 10 0911214-2
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml
Moisture NIA QCBatchlO VL091125-4-5 Final Volume 10 ml
Date Collected 18-Nov-09 Run 10 VL091125-4A Result Units UGL
[late Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Analysis ReqCode 104 Date Analyzed 25-Nov-09
Prep Method SW5030 Rev C Basis As Received
File Name 028045
CASNO Target Analyte Dilution Factor
71-43-2 BENZENE 1
79-01-6 TRICHLOROETHENE 1
78-87-5 12-DICHLOROPROPANE 1
74-95-3 DIBROMOMETHANE 1
75-27-4 BROMODICHLOROMETHANE 1
10061-01-5 CIS-13-DICHLOROPROPENE 1
108-10-1 4-METHYL-2-PtNTANON 1
108-88-3 TOLUENE 1
10061-02-6 TRANS-13-DICHLOROPROPENE 1
79-00-5 112-TRICHLOROETHANE 1
591-78-6 2-HEXANONE 1
127-18-4 TETRACHLOROETHENE 1
142-28-9 13-DICHLOROPROPANt 1
124-48-1 DI3ROMOCHLOROMETHANE 1
106-93-4 12-DIBROMOETHANE 1
108-90-7 CHLOROBENZENE 1
OETHANE 1
- 1
LENE 1
ENE 1
ENE 1
OFORM 1
OPYlBENZENE 1
96-18-4 123-TRICHLOROPROPANE 1
79-34-5 1122-TETRACHLOROETHANE 1
108-86-1 BROMOBENZENE 1
Result Reporting Limit
05 05
05 05
05 05
05 05
05 05
05 05
5 5
025 05
05 05
05 05
10 10
05 05
05 05
1 1
1 1
05 05
05 05
05 05
1 1
05 05
05 05
05 05
05 05
2 2
05 05
05 05
MDL Result EPA Qualifier Qualifier
017 U
017 U
017 U
017 U
017 U
017 U
17 U
017 J
017 U
017 U
17 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
Data Package 10 VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- Fe Page 6 of 8
317A
17
GCMS Volatiles Method SW8260 _258
Sample Results
Lab Name ALS Laboratory Group -- FC
Work Order Number 0911214
Client Name New Mexico Environment Department 08
ClientProject 10 644-11S09(HWB R-37 VOCs) PAR 002731703
Field 10 Rmiddot37 Scr 1-111809
Lab 10 0911214-2
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml Moisture NA QCBatchlD VL091125-4-5 Final Volume 10 ml
Date Collected 18-Nov-09 Run 10 VL091125-4A Result Units UGL Date Extracted 25-Nol-09 Cleanup NONE Clean OF
Analysis ReqCode 104 Date Analyzed 25-Nov-09 Basis As Received Prep Method SW5030 Rev C File Name D28045
CASNO Target Analyte Dilution Factor
103-65-1 N-PROPYLBENZENE 1
95-49-8 2-CHLOROTOLUENE 1
108-67-8 135-TRIMETHYLBENZENE 1
106-43-4 4-CHLOROTOLUENE 1
98-06-6 TERT-BUTYLBENZENE 1
95-63-6 124-TRIMETHYLBENZENE 1
135-98-8 SEC-BUTYLBENZENE 1
i 541-73-1 13middotDICHLOROBENZENE 1
99-87-6 PmiddotISOPROPYL TOLUENE 1
106-46-7 I 14-DICHLOROBENZENE 1
104-51-8 I N-BUTYLBENZENE 1
95-50-1 l2-DICHLOROBENZENE 1
96-12-8 I 12-DIBROMO-3-CHLOROPROPANE 1
120-82-1 124-TRICHLOROBENZENE 1
87-68-3 HEXACHLOROBUT ADIENE 1
91-20-3 NAPHTHALENE 1
87-61-6 123-TRICHLOROBENZENE 1
75-05-S ACETONITRILE 1
107-05-1 ALLYL CH LORIDE 1
110-57-6 TRAN S-14-DICHLORO-2-BUTENE 1
64-17-5 ETHANOL 1
97-63-2 ETHYL METHACRYLATE 1
78-83-1 ISOBUTYL ALCOHOL 1
126-98-7 METHACRYLONITRILE 1
80-62-6 METHYL METHACRYLATE 1
107-12-0 I PROPIONITRILE 1
Result Reporting Limit
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
2 2
05 05
05 05
05 05
05 05
50 50
50 50 I 5 5
200 200
5 5
100 100
35 35
5 5
25 25
MDL
017
017
017
017
017
017
017
017
017
017
017
017
067
017
017
017
017
83
017
17
78
017
17
17
17
33
Result EPA Qualifier Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
Data Package 10 VL0911214-1
Date Printed Wednesday December 022009 ALS Laboratory Group -- Fe Page 7 of 8
LlMS Version 6317A
18
GCMS Volatiles Method SW8260_258
Sample Results
Lab Name ALS Laboratory Group bullbull FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644middot111B09(HWB R-37 VOCs) PAR 002731703
Sample Matrix WATER Prep Batch VL091125--4 Sample Aliquot 10 mlRmiddot37 Ser 1-111809 Moisture NA QCBatchlO VL091125--4-5 Final Volume 10 m
0911214-2 Date Collected 18-Nov-09 Run 10 VL091125--4A Result Units UGL Date Extracted 25-Nov-09 Cleanup NONE Clean OF 1 Date Analyzed 25-Nov-09 Basis As Received
10
Analysis ReqCode 104 Prep Method SW5030 Rev C File Name 028045
I
CASNO Target Analyte Dilution Factor
Result Reporting Limit
MDL Result Qualifier
EPA Qualifier
126-99-8 CHLOROPRENE 1 5 5 017 U
75-65-0 TERT-BUTANOL 1 100 100 33 U
108-20-3 ISOPROPYL ETHER 1 2 2 033 U
637-92-3 ETHYL TERT-BUTYL ETHER 1 2 2 033 U
994-05--8 TERT-AMYL MTHYL ETHER 1 2 2 033 U
67-72-1 HEXACHLOROETHANE 1 2 2 033 U
Surrogate Recovery
CASNO Surrogate Analyte Result Flag Spike Amount
Percent Control Recovery Limits
460-00-4 4middotBROMOFLUOROBENZENE 247 25 99 1
1868-53-7 DIBROMOFLUOROMETHANE 248 25 99 80 123
2037-26-5 TOLUENEmiddotDB 255 25 102 85 - 116
Data Package 10 VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- FC Page B of 8
LlMS Version 6317A
19
GCMS Volatiles Method SW8260_258
Laboratory Control Sample and Laboratory Control Sample Duplicate
Lab Name ALS Laboratory Group - FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-111809(HWB R-37 VOCs) PAR 002731703
Lab 10 VL091125-4LCS Sample Matrix WATER
Moisture NA Prep Batch VL091125-4
QCBatchlD VL091125-4-5
Sample Aliquot
Final Volume
10ml
10ml Date Collected NA Run 10 VL091125-4A Result Units UGIL Date Extracted 111252009 Cleanup NONE Clean OF 1 Date Analyzed 11252009 Basis NA
Prep Method SW5030C File Name 028040
CASNO
74-87-3
75-01-4
74-83-9
75-69-4
75-35-4
75-15-0
156-60-5
75-34-3
108-05-4
156-59-2
78-93-3
67 -66-3
71-55-6
i 56-23-5
107-06-2
71-43-2
79-01-6
78-87-5
75-27-4
108-88-3
79-00-5
591-78-6
127-18-4
106-93-4
108-90-7
63Q20-6
Target Analyte Spike Added
CHLOROMETHANE 10
VINYL CHLORIDE 10
BROMOMETHANE 10
TRICHLOROFLUOROMETHANE 10
11-DICHLOROETHENE 10
CARBON DISULFIDE 10
TRANS-12-DICHLOROETHENE 10
11-DICHLOROETHANE 10
VINYL ACETATE 10
CIS-12-DICHLOROETHENE 10
2middotBUTANONE 40
CHLOROFORM 10
111-TRICHL ORO ETHANE 10
CARBON TETRACHLORIDE 10
12-DICHLOROETHANE 10
BENZENE 10
TRICHLOROETHENE 10
12-DICHLOROPROPANE 10
BROMODICHLOROMETHANE 10
TOLUENE 10
112-TRICHLOROETHANE 10
2-HEXANONE 40
TETRACHLOROETHENE 10
12-DIBROMOETHANE 10
CHLOROBENZENE 10
1112-TETRACHLOROETHANE 10
LCS Reporting Result Result Limit Qualifier
932 05
863 05
943 1
908 05
96 05
95 10 J
996 05
992 05
10 10
102 05
412 5
993 05
974 1
943 05
106 05
983 05
962 05
10 05
988 05
974 05
989 05
409 10
956 05
991 1
984 05
101 05
LCS Control Rec Limits
93 49 -129
86 46 134
94 32-121
91 67 -152
96 61 -135
95 61 -140
100 70 -122
99 76 -119
100 62 182
102 75 126
103 61 -137
99 79 120
97 76 - 114
94 58middot135
106 75middot132
98 70 shy 125
96 74 121
100 81 -119
99 79 - 123
97 76 - 120
99 81 -126
102 45 168
96 56 -128
99 79 -123
98 75 -120
101 82 - 123
Data Package 10 VL0911214middot1
-Date Printed Wednesday December 02 2009 ALS Laboratory Group -- Fe Page 1 of 4
LiMS Version 6317A
20
GCMS Volatiles Method SW8260_25B
Laboratory Control Sample and Laboratory Control Sample Duplicate
Lab Name ALS Laboratory Group - FC
Work Order Number 0911214
Client Name New Mexico Envircnment Department OB
ClientProject 10 644-111809(HWB R-37 VOes) PAR 002731703
Lab 10 VL091125-4LCS Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml
Moisture NIA QCBatchlO VL091125-4-5 Final Volume 10 mi
Date Collected NA Run 10 VL091125-4A Result Units UGL Date Extracted 11252009 Cleanup NONE Clean OF 1 Date Analyzed 111252009 Basis NA
Prep Method SW5030e File Name 028040
CASNO Target Analyte Spike Added
LCS Result
Reporting Limit
Result Qualifier
LCS Rec
Control Limits
100-41-4 ETHYLBENZENE 10 981 05 98 79 -114
136777-61-2 M+P-XYLENE 20 197 1 98 81-115
95-47-6 O-XYLENE 10 101 05 101 81 -115
95-49-8 2-CHLOROTOLUENE 10 97 05 97 80 -128
541-73-1 13-DICHLOROBENZiNt 10 977 05 98 81-116
106-46-7 14-DICHLOROBENZENE 10 979 05 98 81 -119
95-50-1 12-DICHLOROBENZENE 10 987 05 99 79 - 116
91-20-3 NAPHTHALENE 10 993 05 99 69 -126
87-61-6 123-TRICHLOROBENZENE 10 999 05 100 60 -137
Data Package ID VL0911214-1
Date Printed Wecnesday December 02 2009 ALS Laboratory Group -- Fe Page 2 of 4
21
GCMS Volatiles Method SW8260_25B
Laboratory Control Sample and Laboratory Control Sample Duplicate
Lab Name ALS Laboratory Group bullbull FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-11 1809(HWB R-37 VOCs) PAR 002731703
Lab 10 VL091125middot4LCSD Sample Matrix WATER
Moisture NIA Prep Batch VL091125-4
QCBatchlD VL091125-4-5
Sample Aliquot
Final Volume
10 ml
10ml Date Collected NIA Run ID VL091125-4A Result Units UGIL Date Extracted 112512009 Cleanup NONE Clean DF 1 Date Analyzed 1112512009 Basis NIA
Prep Method SW5030C File Name 028041
CASNO Target Analyte Spike Added
LCSD Result
Reporting Limit
Result Qualifier
LCSD Rec
RPD Limit
RPD
74-87-3 CHLOROMETHANE 10 897 05 90 30 4
75-01-4 VINYL CHLORIDE 10 831 05 83 25 4
74-83-9 BROMO METHANE 10 945 1 94 25 0
75-69-4 TRICHLOROFLUOROMETHANE 10 873 05 87 22 4
75-35-4 11-DICHLOROETHENE 10 909 05 91 18 5
75-15-0 CARBON DISULFIDE 10 941 10 J 94 20 1
156-60middot5 TRANS-l2middotDICHLOROETHENE 10 961 05 96 25 4
75middot34middot3 11-DICHLOROETHANE 10 977 05 98 25 2
108-05-4 VINYL ACETATE 10 993 10 J 99 20 1
156middot59-2 CIS-12-DlCHLOROETHENE 10 995 05 99 25 3
i 78-93-3 2-BUTANONE 40 419 5 105 30 2
67-66-3 CHLOROFORM 10 985 05 99 25 1
71-55-6 lll-TRICHLOROETHANE 10 942 1 94 25 3
56-23-5 CARBON TETRACHLORIDE 10 922 05 92 25 2
107middot06-2 12middotDICHLOROETHANE 10 106 05 106 25 0
71-43middot2 BENZENE 10 971 05 97 10 1
79middot01middot6 TRICHLOROETHENE 10 939 05 94 10 2
78middot87middot5 l2middotDICHLOROPROPANE 10 101 05 101 25 1
i 75middot27-4 BROMODICHLOROMETHANE 10 992 05 99 25 0
1108-88-3 TOLUENE 10 962 05 96 9 1
I 79005 112middotTRICHLOROETHANE 10 986 05 99 25 0
591middot78middot6 2-HEXANONE 40 418 10 104 20 2
127middot18-4 TETRACHLOROETHENE 10 918 05 92 25 4
106-93-4 12middotDIBROMOETHANE 10 999 1 100 15 1
108middot90-7 CHLOROBENZENE 10 997 05 100 11 1
630-20middot6 1112-TETRACHLOROETHANE 10 101 05 101 15 0
100-41-4 ETHYLBENZENE 10 968 05 97 25 1
Data Package ID VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- FC Page 3 of 4
lIMS Version 6317 A
22
GCMS Volatiles Method SW8260_25B
Laboratory Control Sample and Laboratory Control Sample Duplicate
Lab Name ALS Laboratory 13roup -- FC
Work Order Number 0911214
Client Name New Mexico Environment Department OS
ClientProject 10 644-11 1809(HWB R-37 VOCs) PAR 002731703
Lab 10 VL091125-4LCSD Sample Matrix WATER
Moisture NA Prep Batch VL091125-4
QCBatchlO VL091125-4-5
Sample Aliquot
Final Volume
10 ml
10ml Date Collected NA Run 10 VL091125-4A Result Units UGL Date Extracted 11252009 Cleanup NONE Clean OF Date Analyzed 11252009 Basis NIA
Prep Method SW5030C File Name 028041
CASNO Target Analyte Spike Added
LCSD Result
Reporting Limit
Result Qualifier
LCSD Rec
RPD Limit
RPD
136777-61-2 M+P-XYLENE 20 193 1 97 25 2
95-47-6 O-XYLENE 10 983 05 98 25 2
95-49-8 2middotCHLOROTOLUENE 10 9A9 05 95 15 2
541-73-1 13middotDICHLOROBENZENE 10 997 05 100 25 2
106-46-7 14-DICHLOROBeNZENE 10 974 05 97 25 1
95-50middot1 12middotDICHLOROBENZeNE 10 101 05 101 25 2
91middot20-3 NAPHTHALENe 10 105 05 105 24 6
87-61-6 123-TRICHLOROBENZENE 10 102 05 102 33 3
Surrogate Recovery LCSLCSD
CASNO Target Analyte Spike Added
LCS Rec
LCS Flag
LCSD Rec
LCSD Flag
Control Limits
460middot00-4 4-BROMOFLUOROBeNZENE 25 100 100 82 - 121
1868-53middot7 DIBROMOFLUOROMeTHANE 25 101 100 80middot 123
2037middot26-5 TOLUENEmiddotD8 25 102 100 85middot 116
Data Package 10 VL0911214-
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- Fe Page 4 of 4
UMS Verslmt 6317A
23
Chain of Custody Record I d- I 4 SKIP TO MAIL REPORT TO fliff9ff BILL TO
Kim Glanzow kG Oilvlgt CobrUD Dflve NMEOmiddotOOE OlefSI9hl 8lJlI~iU (51SI pound614008 New Melllco Enlfrol Dev j-Iuartlous Waste gUleltJll
fort Collins CO 8Q524 183 Diamond Orje- Surfe A 2~S Rodeo P2IriI Driv~ East Bldg 1
(9l0) 490middot1511 tos Alamos Nw Mexico S75u Santa Fe NM 8750$ 2561
kglanlowiafliQoi
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~ It I ~D ~ [11 _ ~~ ~I ~l sect
tltgtfttOt~ Project Number (Lab noice Us Dnly)
644--111809(HWB Rmiddot37 VOCsl PAR i ~ ~ ~ ~
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DateTime Received By Required MS MSO BlAnk I b~Y L_- Tim~18ndord ____
1bik~0
j ~i~~Ff~6~~~~ Jq c=JPlace X in box fherbullbullrIbullbulls than 5 tolalsople for shipping costs_
Page 1 Of 1
ali containers received intact (not broken or
at samples requiring no beadspace (VOC GRO RSKfMEE Rx CNS radon) free Size of bubble lt
(a leas 113 of container required)
samples checked for and free from the presence of residual chlorine when PM has indicated sample are from a chlorinatec water source note if fIeld preservation
sodIum thiosulfate was not observed)
Were cooler temperatures measured at O1-60degC IR lun used 2
Cooler I---shy
Temperature (C) 3 ~ No of custodv seals 01 cooler 0
External ~lRJhr reading
Backgrouncl ~lRhr reading 3 i Were exemai111Uhr readllljs S rwo lim backlTCltmri nnd within DOT acceptance criterin
NO
NO
NO
NO
---1
A-S Laboratory Group - Fort Collins
CONDITION OF SAMPLE UPO) RECEIPT FOMl
Client _Nyen-M---f=D~_______ Workordet No D4 I ~ I L --~--~-----~------
Prolecl Manager __LS_____________ Initials C DI Date 1 -gt= 0- () CJ
Additionallnformatiml PHOVlDE DETAILS BElOW FOR A NO RESIONS[ TCJ ANY (JUESTION ABOV EXCEPT III Al[ 16
---------~-----
If hbilt W ru YES 0 I NA (If Ijrojcct Manager Signature I Date -----l-f---1-tl__--~~_l_4I(--2_)-lt-(_middota_I_----------
DnteTimc
in Gun 112 Oakton SN 299225[l020)middot()()66 m Cllll1li1 Oakton S~~ 2372220lOl(J002
Form 201r22xls (61109) Page 1 of i
FecEx~ US Airbill 9439 4324 BmipiennpoundUpyExpress 4a ExpressPeckageService
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8700 9439 4324
6 Special Handlillgand Delivery Signature Olllions
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Dry Ice Dlflt~9UN11M~ ___ bull ___
L Caflo Aircraft Only
TOIBIPacbges lotlllWeight
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Tawhbiiity~JamJnldtnl100lJnlmyO(jowm~t~SurmttFodfxSMlftGIKIktl1Wit
ALS Labofaton1 Group
Environmental Division Fort Cofiins Colorado
GCMS Volatiles Case Narrative
New Mexico Environmental Department OB 644-111809(HWB R-37 VOCs) PAR -- 002731703
Work Order Number 0911214
1 This report consists of 2 water samples The samples were received cool and intact by ALS on 1120109 The vial for sample 0911214-1 contained headspace prior to analysis because it was not received headspace free into the voatiles laboratory
The samples provided for volatiles had a pH gt 2 at the time of analysis
2 These samples were prepared according to SW-846 3rd Edition procedures Specifically the water samples were prepared by purging 10 mL using purge and trap procedures based on Method 5030C
3 The samples were analyzed using GCMS with an RTX-624 RTX-VMS or equivalent capillary column according to SOP 525 Revision 14 based on SW-846 Method 8260B All positive results were quantitated against the initial calibration standards using the intemal standard technique The identification of positive results was achieved by a comparison of the retention time and mass spectrum of trle sample versus the daily calibration standard
4 All initial calibration criteria for SPCCs and CCCs were met If average response factors were used in the initial calibration RSO was 15 If linear or higher order regression calibrations were used in the initial calibration the coefficient of determination (r2) ~099
5 All initial calibrations are verified by comparing a second source standard calibration verrrication (ICV) against the calibration curve All target compounds in the second source verification had a 0 of less than 25
6 All criteria for SPCCs and CCCs were met in daily (continuing) calibration verifications (CCV)
7 Methylene chloride acetone and 2-butanone are common laboratory contaminants In order to minimize the levels of these compounds detected in the gclms analysis ALS has designated its volatile laboratory as a restricted access area In addition the laboratory has been equipped with a dedicated air intake and exhaust system that operates under positive pressure in order to
1
minimize cross contamination of these compounds Due to fluctuations in ambient laboratory conditions reported sample values for common laboratory contaminants may be due to lab contamination even if the compound in question is not detected in the associated method blankmiddot
All method blank criteria were met
8 All laboratory control sample and laboratory control sample duplicate recoveries and RPDs were within the acceptance criteria
9 Since a sample from this order number was not the selected qualITy control (QC) sample matrix specific QC results are not included in this report
10 The samples were analyzed within the established holding time
11 All surrogate recoveries were within acceptance criteria
12 All internal standard recoveries were within acceptance criteria
14 Manual integrations are performed when needed to provide consistent and defensible data following the guidelines in SOP 939 ReVision 3
The data contained in the following report have been reviewed and approved by the personnel listed below In addition ALS certifies that the analyses reported herein are true complete and correct within the limits of the methods employed
n-o3-o5Sha~JobeS Date Organics Primary Data Reviewer
l~-O 1-01TAamp1~Orga~cs Final Data Reviewer Date
2
ALS Data Qualifier Flags Chromatography and Mass Spectrometry
U or NO This flag indicates that the compound was analyzed for but not detected
J This flag indicates an estimated value This flag is used as follows (1) when estimating a concentration for tentatively identified compounds (TICs) where a 11 response is assumed (2) when the mass spectral and retention time data indicate the presence of a compound that meets the volatile and semivolatile GCMS identification criteria and the result is less than the reporting limit (RL) but greater than the method detection limit (MOL) (3) when the retention time data indicate the presence of a compound that meets the GC identification criteria and the result is less than the RL but greater than the MOL and (4) the reported value is estimated
B This flag is used when the analyte is detected in the associated method blank as well as in the sample It indicates probable blank contamination and warns the data user This flag shall be used for a tentatively identified compound (TIC) as well as for a positively identified target compound
E This flag identifies compounds whose concentration exceeds the upper level of the calibration range
A This flag indicates that a tentatively identified compound is a suspected aldol-condensation product
X This flag indicates that the analyte was diluted below an accurate quantitation level
This flag indicates that a spike recovery is equal to or outside the control criteria used
+ This flag indicates that the relative percent difference (RPO) equals or exceeds the control criteria
3
ALS Laboratory Group -- Fe Sample Number(s) Cross-Reference Table
Paragon OrderNum 0911214 Client Name New Mexico Environment Department OB
Client Project Name 644-111809(HWB R-37 VOCs) PAR Client Project Number 002731703
Client PO Number 06-667-55-01754
Client Sample Number
Lab Sample Number
COC Number Matrix Date Collected
Time Collected
R-37 Scr 2-1 11809 0911214-1 WATER 18-Nov-09 1555 R-37 Scr 1-111809 0911214-2 WATER 18-Nov-09 1744
Page 1 of 1 ALS Laboratory Group -- Fe Date Printed Wednesday December 02 2009 LlMS Version 6317 A
4
Chain of Custody Record 1)11 d- I 4 SHIP To MAil REPORT TO HtitilJft BILL TO
Kim GrJOZOW KC [)il-e Cobra
NMFOmiddotDOE Overslghl Bwe3u 50S firt1middottoOB Hew Meico FnlliTtl1 Dep1 HaVIdthJS VvaMe Bureau ~orl Collins CO 80524shy
1UH Diamold Drive Stille 8 90S Rodeo P3M( D~lIe Ea~ Bldg(970) 90middot511
lo Alarr1(1l N~Muto 87544 83113 Fe liM 87505middot25-67
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cI yl iComments Lanc~v fiias not~ that foe samples life not preg~-d with HCL bull
~ 4_~~~~S5 V~~~Vi~I_$ ~~~~5s~rvd __
3 4()ml glau VOA vials Non-PrlttIrv~d -----~--
OC Level Standard f 0~Y ~-t-~ (fv f_ QC Required MS MSD Bla~k
irU11 Around TieJTAT) ~_dbullr_d__~______
cJPlace X In bOK If there are less than 5 lotal sample for shipping cosls
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ALS Laboratory GrouP - Fort Collins
CONDITIO] OF SAMPLE UPO) RECEIPT FORM
Client _-=-N--M---f-=-D________ IVorkorde No D4 J I 4 --~~~~~~------
PrO1 cc Manager L 5 lnitiais C D Date 1 -) ()- () C --~~~---------------------
1 there a cae Are the coe and bottle labels
Is the coe in agreement with samples received) of containers matrix requested anaiyses etc)
documents presen1 andor removable)
Are all aqueous samples requiring preservation preserved correctly ~- ----~-~~--- -~ -~-- ----~~~---------
volatiles)
14 Are all samples requiring no headspace (VOC GRG RSKlVIEE lb eNS radon)
free Size of bubble lt
$ Do perchlorate LCMS-MS samples have headspace (a~ least ]3 of container required)
NO
]6 Were samples checked for and free from the presence of residual chlorine (Appiicaole when PM has Indicated samples are from a chlonnated wat~ source note if field preservallor
witb sodIUm tlllosulfate wa not observed)
17 Were the lljIV~IOU on ice
IS Were cooler temperatures measured at 01-60degC IR ~Illl used 2
Coole I---
Temperature (C) 3 ~
NO
NO
NO
NO
NO
NO
NO
No of custodv seals Ol~ cooler 0 OOT ---- --- --- --l Surveyl EXlemlli flRhr n~ading I i AcceplanCfiltnforma tlon Background ulJhr reading 3 Were eX lema uRhf readl1lf5 tW(l tm bnckl1Ound and withllllxyr acceptance criterill
Additional Iuformation OVIDE DETAILS BELOW FOR A ND RESPONSE TO ANY (UESTION A80VE EXCEPT 1 ANI) 16
If applicable was the clienl contacted) YES i NO I
Project Manager Signature I Date
(1 Gun 112 Oaktoll SN 2992250020 jmiddot0066 lR Gun lie Oakton S~ 23n220101middot0(J02
Form 201r22gt15 (61109) Page 1 of _1
6
4a Express Package Service _ FadEx Pnority OvernightLJ ==lr-~MClncU1
lSlIIQSATUIIDAYlltIrwIlyis$Mf(1J
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Address Wa clMOfdeiinrto POlwuscrPo ZIP CGlJla
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6 Special Handlmlllilld Delivery SignalUlll Options
~~~l~__Iint_dUSabulld)IjhL Indirect Sianarurc ttMtrttISMIllFtdlHrtS ~~tlltl~ eeelMllnllrl$ICIIltctdeiMv-kll lt_noaIllaIMInt$ ~
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8700 9439 4324 ~rtl1~l__bPnD USA SRI
_____-----------~bull---~----- -------~~-------------------
7
GCMS Volatiles Method SW8260 _25B
Method Blank
Lab Name ALS Laboratory Group bullbull FC
Work Order Number 0911214
Client Name New Mexico Environment Department DB
ClientProject 10 644-111809(HWB Rmiddot37 VOCs) PAR 002731703
Lab 10 VL091125-4MB Sample Matrix WATER
Moisture NA Prep Batch VL091125-4
QCBatchlO VL091125-4-5
Sample Aliquot
Final Volume
10 ml
10 ml Date Collected NA Run 10 VL091125-4A Result Units UGL Date Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Date Analyzed 25middotNov-09 Basis NA
File Name 028043
CASNO Target Analyte DF
75-71-8 DICHLORODIFLUOROMETHANE
74-87-3 CHLOROMETHANE
75-01-4 VINYL CHLORIDE
74-83-9 BROMOMETHANE
75-00-3 CHLOROETHANE
75-69-4 TRICHLOROFLUOROMETHANE
107-02-8 ACROLEIN
75-35-4 11middotDICHLOROETHENE
67-64-1 ACETONE
74-88-4 IODOMETHANE
75-15-0 CARBON DISULFIDE
METHYLEN E CHLORIDE 75-09-2
156-60-5 TRANS-12middotDICHLOROETHENE
1634-04-4 METHYL TERTIARY BUTYL ETHER
107-13-1 ACRYLONITRILE
75-34-3 11-DICHLOROETHANE
108-05-4 VINYL ACETATE
156-59middot2 CIS-12middotDICHLOROETHENE
78-93-3 2middotBUTANONE
~ BROMOCHLOROMETHANE
67-66-3 CHLOROFORM
71-55-6 111middot TRICHLOROETHANE
594-20-7 22middotDICHLOROPROPANE
56-23-5 CARBON TETRACHLORIDE
563-58-6 11middotDICHLOROPROPENE
107-06middot2 l2middotDICHLOROETHAN E
71-43-2 BENZENE
79-01-6 TRICHLOROETHENE
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Result Reporting Limit
05 05
05 05
05 05
1 1
05 05
05 05
100 100
05 05
10 10
5 5
10 10
1 1
05 05
1 1
10 10
05 05
10 10
05 05
5 5
1 1
05 05
1 1
05 05
05 05
05 05
05 05
05 05
05 05
MDL Result EPA Qualifier Qualifier
017 U
017 U
017 U
017 U
017 U
017 U
17 U
017 U
33 U
017 U
017 U
017 U
017 U
017 U
17 U
017 U
067 U
017 U
17 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
Data Package 10 VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- Fe Page 1 of 4
llMS Version 6317 A
8
GCMS Volatiles Method SW8260 _25B
Method Blank
Lab Name ALS Laboratory Group -- FC
Work Order Number 0911214
Client Name New Mexico Environment Department 08
ClientProject 10 644-111809(HWEI R-37 voes) PAR 002731703
Lab 10 VL091125-4MB Sample Matrix WATER
Moisture NIA Prep Batch VL091125-4
QCBatchIO VL091125-4-5
Sample Aliquot
Final Volume
10 ml
10 ml Oate Collected NIA Run 10 VL091125-4A Result Units UGL Oate Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Date Analyzed 25-Nov-09 Basis NIA
File Name 028043
CASNO Target Analyte OF Result Reporting Limit
MOL Result Qualifier
EPA Qualifier
78-87-5 12middotDICHLOROPROPANE 1 05 05 017 U
74-95-3 DIBROMOMETHANE 1 05 05 017 U
75-27-4 BROMODICHLOROMETHANE 1 05 05 017 U
10061-01-5 CISmiddot13middotDICHLOROPROPENE 1 05 05 017 U
108-10-1 4-METHYL-2-PENT ANONE 1 5 5 17 U
108-88-3 TOLUENE 1 05 05 017 U
10061-02-6 TRANS-13-DICHLOROPROPENE 1 05 05 017 U
79-00-5 112-TRICHLOROETHANE 1 05 05 017 U
591-78-6 2-HEXANONE 1 10 10 17 U
127-18-4 TETRACHLOROETHENE 1 05 05 017 U
142-28-9 13-DICHLOROPROPANI 1 05 05 017 U
124-48-1 DIBROMOCHLOROMETHANE 1 1 1 017 U
106-93-4 12-DIBROMOETHANE 1 1 1 017 U
108-90-7 CHLOROBENZENE 1 05 05 017 U
630-20-6 1112-TETRACHLOROETHANE 1 05 05 017 U
100-41-4 ETHYLBENZENE 1 05 05 017 U
136777-61-2 M+P-XYLENE 1 1 1 017 U
95-47-6 O-XYLENE 1 05 05 017 U
100-42-5 STYRENE 1 05 05 017 U
75-25-2 BROMOFORM 1 05 05 017 U
98-82-8 ~YLBENZENE 1 05 05 017 U
96-18-4 123-TRICHLOROPROPANE 1 2 2 017 U
79-34-5 1122middot TETRACHLOROETHANE 1 05 05 017 U
108-86-1 BROMOBENZENE 1 05 05 017 U
103-65-1 N-PROPYLBENZENE 1 05 05 017 U
95-49-8 2-CHLOROTOLUENE 1 05 05 017 U
108-67-8 135-TRIMETHYLBENZENE 1 05 05 017 U
106-43-4 4-CHLOROTOLUENE 1 05 05 017 U
Data Package 10 VL0911214-1
Date Printed Wednesday December n 2009 AlS Laboratory Group -- FC Page 2 of 4
lMS VeCSiOIY 6317A
9
GCMS Volatiles Method SW8260 _258
Method Blank
Lab Name ALS Laboratory Group - FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-111B09(HWB R-37 VOCs) PAR 002731703
Lab 10 VL091125-4MB Sample Matrix WATER
Moisture NIA
Prep Batch VL091125-4
QCBatchlD VL091125-4-5
Sample Aliquot
Final Volume
10 ml
10 ml
Date Collected NIA Run ID VL091125-4A Result Units UGL
Date Extracted 25-Nov-09 Cleanup NONE Clean DF 1
Date Analyzed 25-Nov-09 Basis NA
File Name 028043
CASNO Target Analyte OF Result Reporting Limit
MOL Result Qualifier
EPA Qualifier
98-06-6 TERT-BUTYLBENZENE 1 05 05 017 U
95-63-6 124-TRIMETHYLBENZENE 1 05 05 017 U
135-98-8 SEC-BUTYLBENZENE 1 05 05 017 U
541-73-1 13-DlCHLOROBENZENE 1 05 05 017 U
99-87-6 P-ISOPROPYLTOLUENE 1 05 05 017 U
106-46-7 1 A-DICHLOROBENZENE 1 05 05 017 U
104-51-8 N-BUTYLBENZENE 1 05 05 017 U
95-50-1 12-DICHLOROBENZENE 1 05 05 017 U
96-12-B 12-DIBROMO-3-CHLOROPROPANE 1 2 2 067 U
120-82-1 124-TRiCHLOROBENZENE 1 05 05 017 U
87-68-3 HEXACHLOROBUTADIENE 1 05 05 017 U
91-20-3 NAPHTHALENE 1 05 05 017 U
87-61-6 123-TRICHLOROBENZENE 1 05 05 017 U
75-05-B ACETONITRILE 1 50 50 83 U
107-05-1 ALLYL CHLORIDE 1 50 50 017 U
110-57-6 TRANS-14-DICHLORO-2-BUTENE 1 5 5 17 U
64-17-5 ETHANOL 1 200 200 78 U
97-63-2 ETHYL METHACRYLATE 1 5 5 017 U
78-83-1 ISOBUTYL ALCOHOL 1 100 100 17 U
126-98-7 METHACRYLONITRILE 1 35 35 17 U
80-62-6 METHYL METHACRYLATE 1 5 5 17 U
107-12-0 PROPIONITRILE 1 25 25 33 U
126-99-8 CHLOROPRENE 1 5 5 017 U
75-65-0 TERT-BUTANOL 1 100 100 33 U
108-20-3 ISOPROPYL ETHER 1 2 2 033 U
637-92-3 ETHYL TERT-BUTYL ETHER 1 2 2 033 U
994-05-8 TERT-AMYL METHYL ETHER 1 2 2 033 U
67-72-1 HEXACHLOROETHANE 1 2 2 033 U
Data Package 10 VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -~ Fe Page 3 of 4
LlMS Version 6317 A
10
GCMS Volatiles Method SW8260 _258
Method Blank
Lab Name ALS Laboratory Group -- FC
Work Order Number 0911214
Client Name New Mexico Envirmment Department OB
ClientProject 10 644-111809(HWB R-37 VOCs) PAR 002731703
Lab 10 VL091125-4MB Sample Matrix WATER
Moisture NIA Prep Batch VL091125-4
QCBatchlO VL091125-4-5
Sample Aliquot
Final Volume
10 m
10m Date Collected NIA Run 10 VL091125-4A Result Units UGIL Date Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Date Analyzed 25-Nov-09 BasisNIA
File Name 028043
CASNO Target Analyte Result Reporting MOL Result EPAOF Limit Qualifier Qualifier
Surrogate Recovery
CASNO Surrogate Analyte Result Flag Spike Amount
Percent Recovery
Control Limits
460-00-4 4-BROMOFLUOROBENZENE 25 25 100 82 - 121
1868-53-7 DIBROMOFLUOROMETHANE 248 25 99 80 - 123
2037-26-5 TOLUENE-D8 26 25 104 85 - 116
Data Package 10 VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- FC Page 4 of4
LlMS Version 6317A
11
GCMS Volati les Method SW8260 _258
Sample Results
Lab Name ALS Laboratory Group -- FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-111809(HWB R-37 VOCs) PAR 002731703
Field 10 Rmiddot37 Ser 2middot111809
Lab 10 0911214middot1
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml
Moisture NA QCBatchlO VL091125-4-5 Final Volume 10mi Date Collected 18-Nov-09 Run 10 VL091125-4A Result Units UGL
Date Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Analysis ReqCode 104 Date Analyzed 25-Nov-09
Prep Method SW5030 Rev C Basis As Received
File Name 028044
CASNO Target Analyte Dilution Factor
75-71-8 DICHLORODIFLUOROMETHANE 1
74middot87-3 CHLOROMETHANE 1
75-01-4 VINYL CHLORIDE 1
74-83-9 BROMOMETHANE 1
75-00-3 CHLOROETHANE 1
75-69-4 TRICHLOROFLUOROMETHANE 1
107-02-8 ACROLEIN 1
75-35-4 11middotDICHLOROETHENE 1
67-64-1 ACETONE 1
74-88-4 IODOMETHANE 1
75-15-0 CARBON DISULFIDE 1
75-09-2 METHYLENE CHLORIDE 1
156-60-5 TRANSmiddot12middotDICHLOROETHENE 1
1634-04-4 METHYL TERTIARY BUTYL ETHER 1
107-13-1 ACRYLONITRILE 1
75-34-3 1-DICHLOROETHANE 1
i 108-05-4 VINYL ACETATE 1
156-59-2 CIS-12middotDICHLOROETHENE 1
78-93-3 2-BUTANONE 1
74-97-5 BROMOCHLOROMETHANE 67-66-3 CHLOROFORM 1
71-55-6 11-TRICHLOROETHANE 594-20-7 22-DICHLOROPROPANE 56-23-5 CARBON TETRACHLORIDE 563-58-6 -DICHLOROPROPENE 107-06-2 2-DICHLOROETHANE
Result Reporting Limit
05 05
05 05
05 05
1 1
05 05
05 05
100 100
05 05
10 10
5 5
10 10
1 1
05 05
1 1
10 10
05 05
10 10
05 05
5 5
1 1
05 05
1 1
05 05
05 05
05 05
05 05
MOL Result EPA Qualifier Qualifier
017 U
017 U
017 U
017 U
017 U
017 U
17 U
017 U
33 U
017 U
017 U
017 U
017 U
017 U
17 U
017 U
067 U
017 U
17 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
Data Package ID VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- Fe Page 1 of 8
UMS Version 6317A
12
GCMS Volatiles Method SW8260_25B
Sample Results
Lab Name ALS Laboratory Group - FC
Work Order Number 0911214
Client Name New Mexico nvironment Department OB
ClientProject 10 644-111809(HWB R-37 VOCs) PAR 002731703
Field 10 R-37 Scr 2-111809
Lab 10 0911214-1
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10ml
Moisture NA QCBatchlD VL091125-4-5 Final Volume 10ml
Date Collected l8-Nov-09 Run 10 VL091125-4A Result Units UGL
Date Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Analysis ReqCode 104 Date Analyzed 25-Nov-09 Basis As Received
Prep Method SW5030 Rev C File NameD28044
CASNO Target Analyte Dilution Factor
Result Reporting Limit
MDL Result Qualifier
EPA Qualifier
I
71-43-2 BENZENE 1 05 05 017 U
79-01-6 TRICHLOROETHENE 1 05 05 017 U
78-87-5
74middot95-3
75-27-4
10061-01-5
108middot10middot1
108middot88-3
10061-02middot6
79-00-5
591-78-6
12-DICHLOROPROPANE
DIBROMOMETHANE
BROMODCHLOROMETHANE
CIS-13-DICHLOROPROPEI~E
4-METHYL-2-PENTANONE
TOLUENE
TRANS-13-DICHLOROPROPENE
112-TRICHLOROETHANE
2-HEXANONE
1
1
1
1
1
1
1
1
1
05
05
05
05
5
031
05
05
10
05
05
05
05
5
05
05
05
10
017
017
017
017
17
017
017
017
17
U
U
U
U
U
J
U
U
U
127-18-4
142-28-9
124-48-1
106-93-4
108-90-7
630-20-6
100-41-4
136777-61-2
95-47-6
100-42middot5
75-25-2
98-82middot8
96-18-4
79-34-5
108-86-1
TETRACHLOROETHENE
13-DICHLOROPROPANE
DIBROMOCHLOROMETHANE
12-DIBROMOETHANE
CHLOROBENZENE
11 12-TETRACHLOROETHANE
ETHYLBENZENE
M+PmiddotXYLENE
OmiddotXYLENE
STYRENE
BROMOFORM
ISOPRO PYLBENZENE
123middotTRICHLOROPROPANE
1122-TETRACHLOROETHANE
BROMOBENZENE
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
05
05
1
1
05
05
05
1
05
05
05
05
2
05
05
05
05
1
1
05
05
05
1
05
05
05
05
2
05
05
017
017
017
017
017
017
017
017
017
017
017
017
017
017
017
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
i
Data Package 10 VL0911214-1
Date Printed Wednesday December 022009 AlS laboratory Group bullbull Fe Page 2 of 8
UMS Version 6317A
13
GCMS Volatiles Method SW8260_258
Sample Results
Lab Name ALS Laboratory Group bullbull FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject ID 644-111809(HWB R-37 VOCs) PAR 002731703
Field 10 R-37 Sor 2-111809
Lab ID 0911214middot1
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml
Moisture NA QCBatchlD VL091125-4-5 Final Volume 10 ml
Date Collected 18-Nov-09 Run ID VL091125-4A Result Units UGL
Date Extracted 25-Nov-09 Cleanup NONE Clean DF 1
Analysis ReqCode 104 Date Analyzed 25-Nov-09 Basis As Received
Prep Method SW5030 Rev C File Name 028044
CASNO Target Analyte Dilution Factor
103-65-1 NmiddotPROPYLBENZENE 1
95-49-8 2-CHLOROTOLUENE 1
108-67-8 135-TRIMETHYLBENZENE 1
106-43-4 4-CHLOROTOLUENE 1
98-06-6 TER I-BUTYLBENZENE 1
95-63-6 124-TRIMETHYLBENZENE 1
135-98-8 SEC-BUTYLBENZENE 1
541-73-1 13-OICHLOROBENZENE 1
99-87-6 P-ISOPROPYLTOLUENE 1
106-46-7 lA-DICHLOROBENZENE 1
104-51-8 N-BUTYLBENZENE 1
95-50-1 12-DICHLOROBENZENE 1
96-12-8 l2-DIBROMOmiddot3-CHLOROPROPANE 1
120-82-1 12A-TRICHLOROBENZENE 1
187-68-3 HEXACHLOROBUTADIENE 1
91-20-3 NAPHTHALENE 1
87-61middot6 123-TRICHLOROBENZENE 1
75-05-8 ACETONITRILE 1
107middot05middot1 ALLYL CHLORIDE 1
110-57-6 TRANS-14-DICHLORO-2-BUTENE 1
164-17-5 ETHANOL 1
97-63-2 ETHYL METHACRYLATE 1
78-83-1 ISOBUTYL ALCOHOL 1
126-98-7 METHACRYLONITRILE 1
80-62-6 METHYL METHACRYLATE 1
107-12-0 PROPIONITRILE 1
Result Reporting Limit
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
2 2
05 05
05 05
05 05
05 05
50 50
50 50
5 5
200 200
5 5
100 100
35 35
5 5
25 25
MDL Result EPA Qualifier Qualifier
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
067 U
017 U
017 U
017 U
017 U
83 U
017 U
U u 78 U
017 U
17 U
17 U
17 U
33 U
Data Package 10 VL0911214-1
Date Printed Wednesday December 022009 ALS Laboratory Group MM Fe Page 3 of 8
LlMS VerSion 6317A
14
GCMS Volati las Method SW8260_258
Sample Results
Lab Name ALS Laboratory Group - FC
Work Order Number 0911214
Client Name New Mexico Environment Department 08
ClientProject 10 644-111B09(HWB R-37 VOGs) PAR 002731703
Field 10 R-37 Ser 2-111809 Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10ml
Lab 10 0911214-1 Moisture NA
Date Collected 1B-Nov-09 QCBatchlO VL091125-4-5
Run 10 VL091125-4A
Final Volume 10ml
Result Units UGIL Date Extracted 25-Nov-09 Cleanup NONE Clean OF
Analysis ReqCode 104 Date Analyzed 25-Nov-09
Prep Method SW5030 Rev G Basis As Received
File Name 028044
CASNO Target Analyte Dilution Factor
Result Reporting Limit
MDL Result Qualifier
EPA Qualifier
126-99-8 CHLOROPRENE 1 5 5 017 U
75-65-0 TERT-BUTANOL 1 100 100 33 U
108-20-3 ISOPROPYL ETHER 1 2 2 033 U
637-92-3 ETHYL TERT-BUTYL ETHER 1 2 2 033 U
994-05-8 TERT-AMYL METHYL ETHER 1 2 2 033 U
67-72-1 HEXACHLOROETHANE 1 2 2 033 U
Surrogate Recovery
CASNO Surrogate Analyte Result Flag Spike Amount
Percent Recovery
Control Limits
460-00-4 4-BROMOFLUOHOBENZENE 246 25 98 82 - 121
1868-53-7 DIBROMOFLUOHOMETHANE 248 25 99 BO - 123
2037-26-5 TOLUENE-DB 258 25 103 85middot116
Data Package 10 VL0911214-1
Date Printed Wednesday December 022009 ALS Laboratory Group bullbull FC Page 4 of 8
LIMS Version 0317 A
15
GCMS Volati les Method SW8260_25B
Sample Results
Lab Name ALS Laboratory Group -- FC
Worlt Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-111809(HWB Rmiddot37 VOCs) PAR 002731703
Field 10 Rmiddot37 Scr jmiddot111809
Lab 10 0911214-2
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml Moisture NfA QCBatchID VL091125-4middot5 Final Volume 10 ml
Date Collected 18middotNov-09 Run 10 VL091125-4A Result Units UGfL Date Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Analysis ReqCode 104 Date Analyzed 25middotNov-09 Basis As Received Prep Method SW5030 Rev C File Name 028045
CASNO Target Analyte Dilution Factor
Result Reporting Limit
MOL Result Qualifier
EPA Qualifier
75-71-8 DICHLORODIFLUOROMETHANE 1 05 05 017 U
74-87-3 CHLOROMETHANE 1 05 05 017 U
75-01middot4 VINYL CHLORIDE 1 05 05 017 U
74-83-9 BROMOMETHANE 1 1 1 017 U
75middot00middot3 CHLOROETHANE j 05 05 017 U
75-69-4 TRICHLOROFLUOROMETHANE 1 05 05 017 U
107-02-8 ACROLEIN 1 100 100 17 U
i 75-35-4 11-DICHLOROETHENE 1 05 05 017 U
67-64middot1 ACETONE 1 10 10 33 U
74-8S-4 IODOMETHANE 1 5 5 017 U
75-15-0 CARBON DISULFIDE 1 10 10 017 U
75-09-2 METHYLENE CHLORIDE 1 1 1 017 U
156-60-5 TRANS-12-DICHLOROETHENE 1 05 05 017 U
1634-04-4 METHYL TERTIARY BUTYL ETHER 1 1 1 017 U
107-13-1 ACRYLONITRILE 1 10 10 17 U
75-34middot3 11-DICHLOROETHANE 05 05 017 U
i 108-05-4 VINYL ACETATE 1 10 10 067 U
115659-2 CISmiddot 2middotDICHLOROETHENE 1 05 05 017 U
178-933 2middotBUTANONE 1 5 5 17 U
74-97middot5 BROMOCHLOROMET HANE 1 1 1 017 U
67-66-3 CHLOROFORM 1 05 05 017 U
71-55middot6 111middotTRICHLOROETHANE 1 1 1 017 U
594-20-7 22middotDICHLOROPROPANE 1 05 05 017 U
56-23-5 CARBON TETRACHLORIDE 1 05 05 017 U
563-58-6 11middotDICHLOROPROPENE 1 05 05 017 U
107-06-2 12middotDICHL OROETHANE 1 05 05 017 U
Data Package ID VL0911214-1
Date Printed Wednesday December 022009 ALS Laboratory Group -- Fe Page 5 of 8
16
GCMS Volatiles Method SW8260_25B
Sample Results
Lab Name ALS Laboratory Group -- FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-111809(HW3 R-37 VOCs) PAR 002731703
Field 10 R-37 Scr 1-11 1809
Lab 10 0911214-2
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml
Moisture NIA QCBatchlO VL091125-4-5 Final Volume 10 ml
Date Collected 18-Nov-09 Run 10 VL091125-4A Result Units UGL
[late Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Analysis ReqCode 104 Date Analyzed 25-Nov-09
Prep Method SW5030 Rev C Basis As Received
File Name 028045
CASNO Target Analyte Dilution Factor
71-43-2 BENZENE 1
79-01-6 TRICHLOROETHENE 1
78-87-5 12-DICHLOROPROPANE 1
74-95-3 DIBROMOMETHANE 1
75-27-4 BROMODICHLOROMETHANE 1
10061-01-5 CIS-13-DICHLOROPROPENE 1
108-10-1 4-METHYL-2-PtNTANON 1
108-88-3 TOLUENE 1
10061-02-6 TRANS-13-DICHLOROPROPENE 1
79-00-5 112-TRICHLOROETHANE 1
591-78-6 2-HEXANONE 1
127-18-4 TETRACHLOROETHENE 1
142-28-9 13-DICHLOROPROPANt 1
124-48-1 DI3ROMOCHLOROMETHANE 1
106-93-4 12-DIBROMOETHANE 1
108-90-7 CHLOROBENZENE 1
OETHANE 1
- 1
LENE 1
ENE 1
ENE 1
OFORM 1
OPYlBENZENE 1
96-18-4 123-TRICHLOROPROPANE 1
79-34-5 1122-TETRACHLOROETHANE 1
108-86-1 BROMOBENZENE 1
Result Reporting Limit
05 05
05 05
05 05
05 05
05 05
05 05
5 5
025 05
05 05
05 05
10 10
05 05
05 05
1 1
1 1
05 05
05 05
05 05
1 1
05 05
05 05
05 05
05 05
2 2
05 05
05 05
MDL Result EPA Qualifier Qualifier
017 U
017 U
017 U
017 U
017 U
017 U
17 U
017 J
017 U
017 U
17 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
Data Package 10 VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- Fe Page 6 of 8
317A
17
GCMS Volatiles Method SW8260 _258
Sample Results
Lab Name ALS Laboratory Group -- FC
Work Order Number 0911214
Client Name New Mexico Environment Department 08
ClientProject 10 644-11S09(HWB R-37 VOCs) PAR 002731703
Field 10 Rmiddot37 Scr 1-111809
Lab 10 0911214-2
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml Moisture NA QCBatchlD VL091125-4-5 Final Volume 10 ml
Date Collected 18-Nov-09 Run 10 VL091125-4A Result Units UGL Date Extracted 25-Nol-09 Cleanup NONE Clean OF
Analysis ReqCode 104 Date Analyzed 25-Nov-09 Basis As Received Prep Method SW5030 Rev C File Name D28045
CASNO Target Analyte Dilution Factor
103-65-1 N-PROPYLBENZENE 1
95-49-8 2-CHLOROTOLUENE 1
108-67-8 135-TRIMETHYLBENZENE 1
106-43-4 4-CHLOROTOLUENE 1
98-06-6 TERT-BUTYLBENZENE 1
95-63-6 124-TRIMETHYLBENZENE 1
135-98-8 SEC-BUTYLBENZENE 1
i 541-73-1 13middotDICHLOROBENZENE 1
99-87-6 PmiddotISOPROPYL TOLUENE 1
106-46-7 I 14-DICHLOROBENZENE 1
104-51-8 I N-BUTYLBENZENE 1
95-50-1 l2-DICHLOROBENZENE 1
96-12-8 I 12-DIBROMO-3-CHLOROPROPANE 1
120-82-1 124-TRICHLOROBENZENE 1
87-68-3 HEXACHLOROBUT ADIENE 1
91-20-3 NAPHTHALENE 1
87-61-6 123-TRICHLOROBENZENE 1
75-05-S ACETONITRILE 1
107-05-1 ALLYL CH LORIDE 1
110-57-6 TRAN S-14-DICHLORO-2-BUTENE 1
64-17-5 ETHANOL 1
97-63-2 ETHYL METHACRYLATE 1
78-83-1 ISOBUTYL ALCOHOL 1
126-98-7 METHACRYLONITRILE 1
80-62-6 METHYL METHACRYLATE 1
107-12-0 I PROPIONITRILE 1
Result Reporting Limit
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
2 2
05 05
05 05
05 05
05 05
50 50
50 50 I 5 5
200 200
5 5
100 100
35 35
5 5
25 25
MDL
017
017
017
017
017
017
017
017
017
017
017
017
067
017
017
017
017
83
017
17
78
017
17
17
17
33
Result EPA Qualifier Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
Data Package 10 VL0911214-1
Date Printed Wednesday December 022009 ALS Laboratory Group -- Fe Page 7 of 8
LlMS Version 6317A
18
GCMS Volatiles Method SW8260_258
Sample Results
Lab Name ALS Laboratory Group bullbull FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644middot111B09(HWB R-37 VOCs) PAR 002731703
Sample Matrix WATER Prep Batch VL091125--4 Sample Aliquot 10 mlRmiddot37 Ser 1-111809 Moisture NA QCBatchlO VL091125--4-5 Final Volume 10 m
0911214-2 Date Collected 18-Nov-09 Run 10 VL091125--4A Result Units UGL Date Extracted 25-Nov-09 Cleanup NONE Clean OF 1 Date Analyzed 25-Nov-09 Basis As Received
10
Analysis ReqCode 104 Prep Method SW5030 Rev C File Name 028045
I
CASNO Target Analyte Dilution Factor
Result Reporting Limit
MDL Result Qualifier
EPA Qualifier
126-99-8 CHLOROPRENE 1 5 5 017 U
75-65-0 TERT-BUTANOL 1 100 100 33 U
108-20-3 ISOPROPYL ETHER 1 2 2 033 U
637-92-3 ETHYL TERT-BUTYL ETHER 1 2 2 033 U
994-05--8 TERT-AMYL MTHYL ETHER 1 2 2 033 U
67-72-1 HEXACHLOROETHANE 1 2 2 033 U
Surrogate Recovery
CASNO Surrogate Analyte Result Flag Spike Amount
Percent Control Recovery Limits
460-00-4 4middotBROMOFLUOROBENZENE 247 25 99 1
1868-53-7 DIBROMOFLUOROMETHANE 248 25 99 80 123
2037-26-5 TOLUENEmiddotDB 255 25 102 85 - 116
Data Package 10 VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- FC Page B of 8
LlMS Version 6317A
19
GCMS Volatiles Method SW8260_258
Laboratory Control Sample and Laboratory Control Sample Duplicate
Lab Name ALS Laboratory Group - FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-111809(HWB R-37 VOCs) PAR 002731703
Lab 10 VL091125-4LCS Sample Matrix WATER
Moisture NA Prep Batch VL091125-4
QCBatchlD VL091125-4-5
Sample Aliquot
Final Volume
10ml
10ml Date Collected NA Run 10 VL091125-4A Result Units UGIL Date Extracted 111252009 Cleanup NONE Clean OF 1 Date Analyzed 11252009 Basis NA
Prep Method SW5030C File Name 028040
CASNO
74-87-3
75-01-4
74-83-9
75-69-4
75-35-4
75-15-0
156-60-5
75-34-3
108-05-4
156-59-2
78-93-3
67 -66-3
71-55-6
i 56-23-5
107-06-2
71-43-2
79-01-6
78-87-5
75-27-4
108-88-3
79-00-5
591-78-6
127-18-4
106-93-4
108-90-7
63Q20-6
Target Analyte Spike Added
CHLOROMETHANE 10
VINYL CHLORIDE 10
BROMOMETHANE 10
TRICHLOROFLUOROMETHANE 10
11-DICHLOROETHENE 10
CARBON DISULFIDE 10
TRANS-12-DICHLOROETHENE 10
11-DICHLOROETHANE 10
VINYL ACETATE 10
CIS-12-DICHLOROETHENE 10
2middotBUTANONE 40
CHLOROFORM 10
111-TRICHL ORO ETHANE 10
CARBON TETRACHLORIDE 10
12-DICHLOROETHANE 10
BENZENE 10
TRICHLOROETHENE 10
12-DICHLOROPROPANE 10
BROMODICHLOROMETHANE 10
TOLUENE 10
112-TRICHLOROETHANE 10
2-HEXANONE 40
TETRACHLOROETHENE 10
12-DIBROMOETHANE 10
CHLOROBENZENE 10
1112-TETRACHLOROETHANE 10
LCS Reporting Result Result Limit Qualifier
932 05
863 05
943 1
908 05
96 05
95 10 J
996 05
992 05
10 10
102 05
412 5
993 05
974 1
943 05
106 05
983 05
962 05
10 05
988 05
974 05
989 05
409 10
956 05
991 1
984 05
101 05
LCS Control Rec Limits
93 49 -129
86 46 134
94 32-121
91 67 -152
96 61 -135
95 61 -140
100 70 -122
99 76 -119
100 62 182
102 75 126
103 61 -137
99 79 120
97 76 - 114
94 58middot135
106 75middot132
98 70 shy 125
96 74 121
100 81 -119
99 79 - 123
97 76 - 120
99 81 -126
102 45 168
96 56 -128
99 79 -123
98 75 -120
101 82 - 123
Data Package 10 VL0911214middot1
-Date Printed Wednesday December 02 2009 ALS Laboratory Group -- Fe Page 1 of 4
LiMS Version 6317A
20
GCMS Volatiles Method SW8260_25B
Laboratory Control Sample and Laboratory Control Sample Duplicate
Lab Name ALS Laboratory Group - FC
Work Order Number 0911214
Client Name New Mexico Envircnment Department OB
ClientProject 10 644-111809(HWB R-37 VOes) PAR 002731703
Lab 10 VL091125-4LCS Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml
Moisture NIA QCBatchlO VL091125-4-5 Final Volume 10 mi
Date Collected NA Run 10 VL091125-4A Result Units UGL Date Extracted 11252009 Cleanup NONE Clean OF 1 Date Analyzed 111252009 Basis NA
Prep Method SW5030e File Name 028040
CASNO Target Analyte Spike Added
LCS Result
Reporting Limit
Result Qualifier
LCS Rec
Control Limits
100-41-4 ETHYLBENZENE 10 981 05 98 79 -114
136777-61-2 M+P-XYLENE 20 197 1 98 81-115
95-47-6 O-XYLENE 10 101 05 101 81 -115
95-49-8 2-CHLOROTOLUENE 10 97 05 97 80 -128
541-73-1 13-DICHLOROBENZiNt 10 977 05 98 81-116
106-46-7 14-DICHLOROBENZENE 10 979 05 98 81 -119
95-50-1 12-DICHLOROBENZENE 10 987 05 99 79 - 116
91-20-3 NAPHTHALENE 10 993 05 99 69 -126
87-61-6 123-TRICHLOROBENZENE 10 999 05 100 60 -137
Data Package ID VL0911214-1
Date Printed Wecnesday December 02 2009 ALS Laboratory Group -- Fe Page 2 of 4
21
GCMS Volatiles Method SW8260_25B
Laboratory Control Sample and Laboratory Control Sample Duplicate
Lab Name ALS Laboratory Group bullbull FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-11 1809(HWB R-37 VOCs) PAR 002731703
Lab 10 VL091125middot4LCSD Sample Matrix WATER
Moisture NIA Prep Batch VL091125-4
QCBatchlD VL091125-4-5
Sample Aliquot
Final Volume
10 ml
10ml Date Collected NIA Run ID VL091125-4A Result Units UGIL Date Extracted 112512009 Cleanup NONE Clean DF 1 Date Analyzed 1112512009 Basis NIA
Prep Method SW5030C File Name 028041
CASNO Target Analyte Spike Added
LCSD Result
Reporting Limit
Result Qualifier
LCSD Rec
RPD Limit
RPD
74-87-3 CHLOROMETHANE 10 897 05 90 30 4
75-01-4 VINYL CHLORIDE 10 831 05 83 25 4
74-83-9 BROMO METHANE 10 945 1 94 25 0
75-69-4 TRICHLOROFLUOROMETHANE 10 873 05 87 22 4
75-35-4 11-DICHLOROETHENE 10 909 05 91 18 5
75-15-0 CARBON DISULFIDE 10 941 10 J 94 20 1
156-60middot5 TRANS-l2middotDICHLOROETHENE 10 961 05 96 25 4
75middot34middot3 11-DICHLOROETHANE 10 977 05 98 25 2
108-05-4 VINYL ACETATE 10 993 10 J 99 20 1
156middot59-2 CIS-12-DlCHLOROETHENE 10 995 05 99 25 3
i 78-93-3 2-BUTANONE 40 419 5 105 30 2
67-66-3 CHLOROFORM 10 985 05 99 25 1
71-55-6 lll-TRICHLOROETHANE 10 942 1 94 25 3
56-23-5 CARBON TETRACHLORIDE 10 922 05 92 25 2
107middot06-2 12middotDICHLOROETHANE 10 106 05 106 25 0
71-43middot2 BENZENE 10 971 05 97 10 1
79middot01middot6 TRICHLOROETHENE 10 939 05 94 10 2
78middot87middot5 l2middotDICHLOROPROPANE 10 101 05 101 25 1
i 75middot27-4 BROMODICHLOROMETHANE 10 992 05 99 25 0
1108-88-3 TOLUENE 10 962 05 96 9 1
I 79005 112middotTRICHLOROETHANE 10 986 05 99 25 0
591middot78middot6 2-HEXANONE 40 418 10 104 20 2
127middot18-4 TETRACHLOROETHENE 10 918 05 92 25 4
106-93-4 12middotDIBROMOETHANE 10 999 1 100 15 1
108middot90-7 CHLOROBENZENE 10 997 05 100 11 1
630-20middot6 1112-TETRACHLOROETHANE 10 101 05 101 15 0
100-41-4 ETHYLBENZENE 10 968 05 97 25 1
Data Package ID VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- FC Page 3 of 4
lIMS Version 6317 A
22
GCMS Volatiles Method SW8260_25B
Laboratory Control Sample and Laboratory Control Sample Duplicate
Lab Name ALS Laboratory 13roup -- FC
Work Order Number 0911214
Client Name New Mexico Environment Department OS
ClientProject 10 644-11 1809(HWB R-37 VOCs) PAR 002731703
Lab 10 VL091125-4LCSD Sample Matrix WATER
Moisture NA Prep Batch VL091125-4
QCBatchlO VL091125-4-5
Sample Aliquot
Final Volume
10 ml
10ml Date Collected NA Run 10 VL091125-4A Result Units UGL Date Extracted 11252009 Cleanup NONE Clean OF Date Analyzed 11252009 Basis NIA
Prep Method SW5030C File Name 028041
CASNO Target Analyte Spike Added
LCSD Result
Reporting Limit
Result Qualifier
LCSD Rec
RPD Limit
RPD
136777-61-2 M+P-XYLENE 20 193 1 97 25 2
95-47-6 O-XYLENE 10 983 05 98 25 2
95-49-8 2middotCHLOROTOLUENE 10 9A9 05 95 15 2
541-73-1 13middotDICHLOROBENZENE 10 997 05 100 25 2
106-46-7 14-DICHLOROBeNZENE 10 974 05 97 25 1
95-50middot1 12middotDICHLOROBENZeNE 10 101 05 101 25 2
91middot20-3 NAPHTHALENe 10 105 05 105 24 6
87-61-6 123-TRICHLOROBENZENE 10 102 05 102 33 3
Surrogate Recovery LCSLCSD
CASNO Target Analyte Spike Added
LCS Rec
LCS Flag
LCSD Rec
LCSD Flag
Control Limits
460middot00-4 4-BROMOFLUOROBeNZENE 25 100 100 82 - 121
1868-53middot7 DIBROMOFLUOROMeTHANE 25 101 100 80middot 123
2037middot26-5 TOLUENEmiddotD8 25 102 100 85middot 116
Data Package 10 VL0911214-
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- Fe Page 4 of 4
UMS Verslmt 6317A
23
ali containers received intact (not broken or
at samples requiring no beadspace (VOC GRO RSKfMEE Rx CNS radon) free Size of bubble lt
(a leas 113 of container required)
samples checked for and free from the presence of residual chlorine when PM has indicated sample are from a chlorinatec water source note if fIeld preservation
sodIum thiosulfate was not observed)
Were cooler temperatures measured at O1-60degC IR lun used 2
Cooler I---shy
Temperature (C) 3 ~ No of custodv seals 01 cooler 0
External ~lRJhr reading
Backgrouncl ~lRhr reading 3 i Were exemai111Uhr readllljs S rwo lim backlTCltmri nnd within DOT acceptance criterin
NO
NO
NO
NO
---1
A-S Laboratory Group - Fort Collins
CONDITION OF SAMPLE UPO) RECEIPT FOMl
Client _Nyen-M---f=D~_______ Workordet No D4 I ~ I L --~--~-----~------
Prolecl Manager __LS_____________ Initials C DI Date 1 -gt= 0- () CJ
Additionallnformatiml PHOVlDE DETAILS BElOW FOR A NO RESIONS[ TCJ ANY (JUESTION ABOV EXCEPT III Al[ 16
---------~-----
If hbilt W ru YES 0 I NA (If Ijrojcct Manager Signature I Date -----l-f---1-tl__--~~_l_4I(--2_)-lt-(_middota_I_----------
DnteTimc
in Gun 112 Oakton SN 299225[l020)middot()()66 m Cllll1li1 Oakton S~~ 2372220lOl(J002
Form 201r22xls (61109) Page 1 of i
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8700 9439 4324
6 Special Handlillgand Delivery Signature Olllions
=J ~~~tr~~ ow MmINomht sx lD fnri1r
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Dry Ice Dlflt~9UN11M~ ___ bull ___
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TOIBIPacbges lotlllWeight
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Tawhbiiity~JamJnldtnl100lJnlmyO(jowm~t~SurmttFodfxSMlftGIKIktl1Wit
ALS Labofaton1 Group
Environmental Division Fort Cofiins Colorado
GCMS Volatiles Case Narrative
New Mexico Environmental Department OB 644-111809(HWB R-37 VOCs) PAR -- 002731703
Work Order Number 0911214
1 This report consists of 2 water samples The samples were received cool and intact by ALS on 1120109 The vial for sample 0911214-1 contained headspace prior to analysis because it was not received headspace free into the voatiles laboratory
The samples provided for volatiles had a pH gt 2 at the time of analysis
2 These samples were prepared according to SW-846 3rd Edition procedures Specifically the water samples were prepared by purging 10 mL using purge and trap procedures based on Method 5030C
3 The samples were analyzed using GCMS with an RTX-624 RTX-VMS or equivalent capillary column according to SOP 525 Revision 14 based on SW-846 Method 8260B All positive results were quantitated against the initial calibration standards using the intemal standard technique The identification of positive results was achieved by a comparison of the retention time and mass spectrum of trle sample versus the daily calibration standard
4 All initial calibration criteria for SPCCs and CCCs were met If average response factors were used in the initial calibration RSO was 15 If linear or higher order regression calibrations were used in the initial calibration the coefficient of determination (r2) ~099
5 All initial calibrations are verified by comparing a second source standard calibration verrrication (ICV) against the calibration curve All target compounds in the second source verification had a 0 of less than 25
6 All criteria for SPCCs and CCCs were met in daily (continuing) calibration verifications (CCV)
7 Methylene chloride acetone and 2-butanone are common laboratory contaminants In order to minimize the levels of these compounds detected in the gclms analysis ALS has designated its volatile laboratory as a restricted access area In addition the laboratory has been equipped with a dedicated air intake and exhaust system that operates under positive pressure in order to
1
minimize cross contamination of these compounds Due to fluctuations in ambient laboratory conditions reported sample values for common laboratory contaminants may be due to lab contamination even if the compound in question is not detected in the associated method blankmiddot
All method blank criteria were met
8 All laboratory control sample and laboratory control sample duplicate recoveries and RPDs were within the acceptance criteria
9 Since a sample from this order number was not the selected qualITy control (QC) sample matrix specific QC results are not included in this report
10 The samples were analyzed within the established holding time
11 All surrogate recoveries were within acceptance criteria
12 All internal standard recoveries were within acceptance criteria
14 Manual integrations are performed when needed to provide consistent and defensible data following the guidelines in SOP 939 ReVision 3
The data contained in the following report have been reviewed and approved by the personnel listed below In addition ALS certifies that the analyses reported herein are true complete and correct within the limits of the methods employed
n-o3-o5Sha~JobeS Date Organics Primary Data Reviewer
l~-O 1-01TAamp1~Orga~cs Final Data Reviewer Date
2
ALS Data Qualifier Flags Chromatography and Mass Spectrometry
U or NO This flag indicates that the compound was analyzed for but not detected
J This flag indicates an estimated value This flag is used as follows (1) when estimating a concentration for tentatively identified compounds (TICs) where a 11 response is assumed (2) when the mass spectral and retention time data indicate the presence of a compound that meets the volatile and semivolatile GCMS identification criteria and the result is less than the reporting limit (RL) but greater than the method detection limit (MOL) (3) when the retention time data indicate the presence of a compound that meets the GC identification criteria and the result is less than the RL but greater than the MOL and (4) the reported value is estimated
B This flag is used when the analyte is detected in the associated method blank as well as in the sample It indicates probable blank contamination and warns the data user This flag shall be used for a tentatively identified compound (TIC) as well as for a positively identified target compound
E This flag identifies compounds whose concentration exceeds the upper level of the calibration range
A This flag indicates that a tentatively identified compound is a suspected aldol-condensation product
X This flag indicates that the analyte was diluted below an accurate quantitation level
This flag indicates that a spike recovery is equal to or outside the control criteria used
+ This flag indicates that the relative percent difference (RPO) equals or exceeds the control criteria
3
ALS Laboratory Group -- Fe Sample Number(s) Cross-Reference Table
Paragon OrderNum 0911214 Client Name New Mexico Environment Department OB
Client Project Name 644-111809(HWB R-37 VOCs) PAR Client Project Number 002731703
Client PO Number 06-667-55-01754
Client Sample Number
Lab Sample Number
COC Number Matrix Date Collected
Time Collected
R-37 Scr 2-1 11809 0911214-1 WATER 18-Nov-09 1555 R-37 Scr 1-111809 0911214-2 WATER 18-Nov-09 1744
Page 1 of 1 ALS Laboratory Group -- Fe Date Printed Wednesday December 02 2009 LlMS Version 6317 A
4
Chain of Custody Record 1)11 d- I 4 SHIP To MAil REPORT TO HtitilJft BILL TO
Kim GrJOZOW KC [)il-e Cobra
NMFOmiddotDOE Overslghl Bwe3u 50S firt1middottoOB Hew Meico FnlliTtl1 Dep1 HaVIdthJS VvaMe Bureau ~orl Collins CO 80524shy
1UH Diamold Drive Stille 8 90S Rodeo P3M( D~lIe Ea~ Bldg(970) 90middot511
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cI yl iComments Lanc~v fiias not~ that foe samples life not preg~-d with HCL bull
~ 4_~~~~S5 V~~~Vi~I_$ ~~~~5s~rvd __
3 4()ml glau VOA vials Non-PrlttIrv~d -----~--
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irU11 Around TieJTAT) ~_dbullr_d__~______
cJPlace X In bOK If there are less than 5 lotal sample for shipping cosls
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ALS Laboratory GrouP - Fort Collins
CONDITIO] OF SAMPLE UPO) RECEIPT FORM
Client _-=-N--M---f-=-D________ IVorkorde No D4 J I 4 --~~~~~~------
PrO1 cc Manager L 5 lnitiais C D Date 1 -) ()- () C --~~~---------------------
1 there a cae Are the coe and bottle labels
Is the coe in agreement with samples received) of containers matrix requested anaiyses etc)
documents presen1 andor removable)
Are all aqueous samples requiring preservation preserved correctly ~- ----~-~~--- -~ -~-- ----~~~---------
volatiles)
14 Are all samples requiring no headspace (VOC GRG RSKlVIEE lb eNS radon)
free Size of bubble lt
$ Do perchlorate LCMS-MS samples have headspace (a~ least ]3 of container required)
NO
]6 Were samples checked for and free from the presence of residual chlorine (Appiicaole when PM has Indicated samples are from a chlonnated wat~ source note if field preservallor
witb sodIUm tlllosulfate wa not observed)
17 Were the lljIV~IOU on ice
IS Were cooler temperatures measured at 01-60degC IR ~Illl used 2
Coole I---
Temperature (C) 3 ~
NO
NO
NO
NO
NO
NO
NO
No of custodv seals Ol~ cooler 0 OOT ---- --- --- --l Surveyl EXlemlli flRhr n~ading I i AcceplanCfiltnforma tlon Background ulJhr reading 3 Were eX lema uRhf readl1lf5 tW(l tm bnckl1Ound and withllllxyr acceptance criterill
Additional Iuformation OVIDE DETAILS BELOW FOR A ND RESPONSE TO ANY (UESTION A80VE EXCEPT 1 ANI) 16
If applicable was the clienl contacted) YES i NO I
Project Manager Signature I Date
(1 Gun 112 Oaktoll SN 2992250020 jmiddot0066 lR Gun lie Oakton S~ 23n220101middot0(J02
Form 201r22gt15 (61109) Page 1 of _1
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7
GCMS Volatiles Method SW8260 _25B
Method Blank
Lab Name ALS Laboratory Group bullbull FC
Work Order Number 0911214
Client Name New Mexico Environment Department DB
ClientProject 10 644-111809(HWB Rmiddot37 VOCs) PAR 002731703
Lab 10 VL091125-4MB Sample Matrix WATER
Moisture NA Prep Batch VL091125-4
QCBatchlO VL091125-4-5
Sample Aliquot
Final Volume
10 ml
10 ml Date Collected NA Run 10 VL091125-4A Result Units UGL Date Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Date Analyzed 25middotNov-09 Basis NA
File Name 028043
CASNO Target Analyte DF
75-71-8 DICHLORODIFLUOROMETHANE
74-87-3 CHLOROMETHANE
75-01-4 VINYL CHLORIDE
74-83-9 BROMOMETHANE
75-00-3 CHLOROETHANE
75-69-4 TRICHLOROFLUOROMETHANE
107-02-8 ACROLEIN
75-35-4 11middotDICHLOROETHENE
67-64-1 ACETONE
74-88-4 IODOMETHANE
75-15-0 CARBON DISULFIDE
METHYLEN E CHLORIDE 75-09-2
156-60-5 TRANS-12middotDICHLOROETHENE
1634-04-4 METHYL TERTIARY BUTYL ETHER
107-13-1 ACRYLONITRILE
75-34-3 11-DICHLOROETHANE
108-05-4 VINYL ACETATE
156-59middot2 CIS-12middotDICHLOROETHENE
78-93-3 2middotBUTANONE
~ BROMOCHLOROMETHANE
67-66-3 CHLOROFORM
71-55-6 111middot TRICHLOROETHANE
594-20-7 22middotDICHLOROPROPANE
56-23-5 CARBON TETRACHLORIDE
563-58-6 11middotDICHLOROPROPENE
107-06middot2 l2middotDICHLOROETHAN E
71-43-2 BENZENE
79-01-6 TRICHLOROETHENE
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Result Reporting Limit
05 05
05 05
05 05
1 1
05 05
05 05
100 100
05 05
10 10
5 5
10 10
1 1
05 05
1 1
10 10
05 05
10 10
05 05
5 5
1 1
05 05
1 1
05 05
05 05
05 05
05 05
05 05
05 05
MDL Result EPA Qualifier Qualifier
017 U
017 U
017 U
017 U
017 U
017 U
17 U
017 U
33 U
017 U
017 U
017 U
017 U
017 U
17 U
017 U
067 U
017 U
17 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
Data Package 10 VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- Fe Page 1 of 4
llMS Version 6317 A
8
GCMS Volatiles Method SW8260 _25B
Method Blank
Lab Name ALS Laboratory Group -- FC
Work Order Number 0911214
Client Name New Mexico Environment Department 08
ClientProject 10 644-111809(HWEI R-37 voes) PAR 002731703
Lab 10 VL091125-4MB Sample Matrix WATER
Moisture NIA Prep Batch VL091125-4
QCBatchIO VL091125-4-5
Sample Aliquot
Final Volume
10 ml
10 ml Oate Collected NIA Run 10 VL091125-4A Result Units UGL Oate Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Date Analyzed 25-Nov-09 Basis NIA
File Name 028043
CASNO Target Analyte OF Result Reporting Limit
MOL Result Qualifier
EPA Qualifier
78-87-5 12middotDICHLOROPROPANE 1 05 05 017 U
74-95-3 DIBROMOMETHANE 1 05 05 017 U
75-27-4 BROMODICHLOROMETHANE 1 05 05 017 U
10061-01-5 CISmiddot13middotDICHLOROPROPENE 1 05 05 017 U
108-10-1 4-METHYL-2-PENT ANONE 1 5 5 17 U
108-88-3 TOLUENE 1 05 05 017 U
10061-02-6 TRANS-13-DICHLOROPROPENE 1 05 05 017 U
79-00-5 112-TRICHLOROETHANE 1 05 05 017 U
591-78-6 2-HEXANONE 1 10 10 17 U
127-18-4 TETRACHLOROETHENE 1 05 05 017 U
142-28-9 13-DICHLOROPROPANI 1 05 05 017 U
124-48-1 DIBROMOCHLOROMETHANE 1 1 1 017 U
106-93-4 12-DIBROMOETHANE 1 1 1 017 U
108-90-7 CHLOROBENZENE 1 05 05 017 U
630-20-6 1112-TETRACHLOROETHANE 1 05 05 017 U
100-41-4 ETHYLBENZENE 1 05 05 017 U
136777-61-2 M+P-XYLENE 1 1 1 017 U
95-47-6 O-XYLENE 1 05 05 017 U
100-42-5 STYRENE 1 05 05 017 U
75-25-2 BROMOFORM 1 05 05 017 U
98-82-8 ~YLBENZENE 1 05 05 017 U
96-18-4 123-TRICHLOROPROPANE 1 2 2 017 U
79-34-5 1122middot TETRACHLOROETHANE 1 05 05 017 U
108-86-1 BROMOBENZENE 1 05 05 017 U
103-65-1 N-PROPYLBENZENE 1 05 05 017 U
95-49-8 2-CHLOROTOLUENE 1 05 05 017 U
108-67-8 135-TRIMETHYLBENZENE 1 05 05 017 U
106-43-4 4-CHLOROTOLUENE 1 05 05 017 U
Data Package 10 VL0911214-1
Date Printed Wednesday December n 2009 AlS Laboratory Group -- FC Page 2 of 4
lMS VeCSiOIY 6317A
9
GCMS Volatiles Method SW8260 _258
Method Blank
Lab Name ALS Laboratory Group - FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-111B09(HWB R-37 VOCs) PAR 002731703
Lab 10 VL091125-4MB Sample Matrix WATER
Moisture NIA
Prep Batch VL091125-4
QCBatchlD VL091125-4-5
Sample Aliquot
Final Volume
10 ml
10 ml
Date Collected NIA Run ID VL091125-4A Result Units UGL
Date Extracted 25-Nov-09 Cleanup NONE Clean DF 1
Date Analyzed 25-Nov-09 Basis NA
File Name 028043
CASNO Target Analyte OF Result Reporting Limit
MOL Result Qualifier
EPA Qualifier
98-06-6 TERT-BUTYLBENZENE 1 05 05 017 U
95-63-6 124-TRIMETHYLBENZENE 1 05 05 017 U
135-98-8 SEC-BUTYLBENZENE 1 05 05 017 U
541-73-1 13-DlCHLOROBENZENE 1 05 05 017 U
99-87-6 P-ISOPROPYLTOLUENE 1 05 05 017 U
106-46-7 1 A-DICHLOROBENZENE 1 05 05 017 U
104-51-8 N-BUTYLBENZENE 1 05 05 017 U
95-50-1 12-DICHLOROBENZENE 1 05 05 017 U
96-12-B 12-DIBROMO-3-CHLOROPROPANE 1 2 2 067 U
120-82-1 124-TRiCHLOROBENZENE 1 05 05 017 U
87-68-3 HEXACHLOROBUTADIENE 1 05 05 017 U
91-20-3 NAPHTHALENE 1 05 05 017 U
87-61-6 123-TRICHLOROBENZENE 1 05 05 017 U
75-05-B ACETONITRILE 1 50 50 83 U
107-05-1 ALLYL CHLORIDE 1 50 50 017 U
110-57-6 TRANS-14-DICHLORO-2-BUTENE 1 5 5 17 U
64-17-5 ETHANOL 1 200 200 78 U
97-63-2 ETHYL METHACRYLATE 1 5 5 017 U
78-83-1 ISOBUTYL ALCOHOL 1 100 100 17 U
126-98-7 METHACRYLONITRILE 1 35 35 17 U
80-62-6 METHYL METHACRYLATE 1 5 5 17 U
107-12-0 PROPIONITRILE 1 25 25 33 U
126-99-8 CHLOROPRENE 1 5 5 017 U
75-65-0 TERT-BUTANOL 1 100 100 33 U
108-20-3 ISOPROPYL ETHER 1 2 2 033 U
637-92-3 ETHYL TERT-BUTYL ETHER 1 2 2 033 U
994-05-8 TERT-AMYL METHYL ETHER 1 2 2 033 U
67-72-1 HEXACHLOROETHANE 1 2 2 033 U
Data Package 10 VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -~ Fe Page 3 of 4
LlMS Version 6317 A
10
GCMS Volatiles Method SW8260 _258
Method Blank
Lab Name ALS Laboratory Group -- FC
Work Order Number 0911214
Client Name New Mexico Envirmment Department OB
ClientProject 10 644-111809(HWB R-37 VOCs) PAR 002731703
Lab 10 VL091125-4MB Sample Matrix WATER
Moisture NIA Prep Batch VL091125-4
QCBatchlO VL091125-4-5
Sample Aliquot
Final Volume
10 m
10m Date Collected NIA Run 10 VL091125-4A Result Units UGIL Date Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Date Analyzed 25-Nov-09 BasisNIA
File Name 028043
CASNO Target Analyte Result Reporting MOL Result EPAOF Limit Qualifier Qualifier
Surrogate Recovery
CASNO Surrogate Analyte Result Flag Spike Amount
Percent Recovery
Control Limits
460-00-4 4-BROMOFLUOROBENZENE 25 25 100 82 - 121
1868-53-7 DIBROMOFLUOROMETHANE 248 25 99 80 - 123
2037-26-5 TOLUENE-D8 26 25 104 85 - 116
Data Package 10 VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- FC Page 4 of4
LlMS Version 6317A
11
GCMS Volati les Method SW8260 _258
Sample Results
Lab Name ALS Laboratory Group -- FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-111809(HWB R-37 VOCs) PAR 002731703
Field 10 Rmiddot37 Ser 2middot111809
Lab 10 0911214middot1
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml
Moisture NA QCBatchlO VL091125-4-5 Final Volume 10mi Date Collected 18-Nov-09 Run 10 VL091125-4A Result Units UGL
Date Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Analysis ReqCode 104 Date Analyzed 25-Nov-09
Prep Method SW5030 Rev C Basis As Received
File Name 028044
CASNO Target Analyte Dilution Factor
75-71-8 DICHLORODIFLUOROMETHANE 1
74middot87-3 CHLOROMETHANE 1
75-01-4 VINYL CHLORIDE 1
74-83-9 BROMOMETHANE 1
75-00-3 CHLOROETHANE 1
75-69-4 TRICHLOROFLUOROMETHANE 1
107-02-8 ACROLEIN 1
75-35-4 11middotDICHLOROETHENE 1
67-64-1 ACETONE 1
74-88-4 IODOMETHANE 1
75-15-0 CARBON DISULFIDE 1
75-09-2 METHYLENE CHLORIDE 1
156-60-5 TRANSmiddot12middotDICHLOROETHENE 1
1634-04-4 METHYL TERTIARY BUTYL ETHER 1
107-13-1 ACRYLONITRILE 1
75-34-3 1-DICHLOROETHANE 1
i 108-05-4 VINYL ACETATE 1
156-59-2 CIS-12middotDICHLOROETHENE 1
78-93-3 2-BUTANONE 1
74-97-5 BROMOCHLOROMETHANE 67-66-3 CHLOROFORM 1
71-55-6 11-TRICHLOROETHANE 594-20-7 22-DICHLOROPROPANE 56-23-5 CARBON TETRACHLORIDE 563-58-6 -DICHLOROPROPENE 107-06-2 2-DICHLOROETHANE
Result Reporting Limit
05 05
05 05
05 05
1 1
05 05
05 05
100 100
05 05
10 10
5 5
10 10
1 1
05 05
1 1
10 10
05 05
10 10
05 05
5 5
1 1
05 05
1 1
05 05
05 05
05 05
05 05
MOL Result EPA Qualifier Qualifier
017 U
017 U
017 U
017 U
017 U
017 U
17 U
017 U
33 U
017 U
017 U
017 U
017 U
017 U
17 U
017 U
067 U
017 U
17 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
Data Package ID VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- Fe Page 1 of 8
UMS Version 6317A
12
GCMS Volatiles Method SW8260_25B
Sample Results
Lab Name ALS Laboratory Group - FC
Work Order Number 0911214
Client Name New Mexico nvironment Department OB
ClientProject 10 644-111809(HWB R-37 VOCs) PAR 002731703
Field 10 R-37 Scr 2-111809
Lab 10 0911214-1
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10ml
Moisture NA QCBatchlD VL091125-4-5 Final Volume 10ml
Date Collected l8-Nov-09 Run 10 VL091125-4A Result Units UGL
Date Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Analysis ReqCode 104 Date Analyzed 25-Nov-09 Basis As Received
Prep Method SW5030 Rev C File NameD28044
CASNO Target Analyte Dilution Factor
Result Reporting Limit
MDL Result Qualifier
EPA Qualifier
I
71-43-2 BENZENE 1 05 05 017 U
79-01-6 TRICHLOROETHENE 1 05 05 017 U
78-87-5
74middot95-3
75-27-4
10061-01-5
108middot10middot1
108middot88-3
10061-02middot6
79-00-5
591-78-6
12-DICHLOROPROPANE
DIBROMOMETHANE
BROMODCHLOROMETHANE
CIS-13-DICHLOROPROPEI~E
4-METHYL-2-PENTANONE
TOLUENE
TRANS-13-DICHLOROPROPENE
112-TRICHLOROETHANE
2-HEXANONE
1
1
1
1
1
1
1
1
1
05
05
05
05
5
031
05
05
10
05
05
05
05
5
05
05
05
10
017
017
017
017
17
017
017
017
17
U
U
U
U
U
J
U
U
U
127-18-4
142-28-9
124-48-1
106-93-4
108-90-7
630-20-6
100-41-4
136777-61-2
95-47-6
100-42middot5
75-25-2
98-82middot8
96-18-4
79-34-5
108-86-1
TETRACHLOROETHENE
13-DICHLOROPROPANE
DIBROMOCHLOROMETHANE
12-DIBROMOETHANE
CHLOROBENZENE
11 12-TETRACHLOROETHANE
ETHYLBENZENE
M+PmiddotXYLENE
OmiddotXYLENE
STYRENE
BROMOFORM
ISOPRO PYLBENZENE
123middotTRICHLOROPROPANE
1122-TETRACHLOROETHANE
BROMOBENZENE
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
05
05
1
1
05
05
05
1
05
05
05
05
2
05
05
05
05
1
1
05
05
05
1
05
05
05
05
2
05
05
017
017
017
017
017
017
017
017
017
017
017
017
017
017
017
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
i
Data Package 10 VL0911214-1
Date Printed Wednesday December 022009 AlS laboratory Group bullbull Fe Page 2 of 8
UMS Version 6317A
13
GCMS Volatiles Method SW8260_258
Sample Results
Lab Name ALS Laboratory Group bullbull FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject ID 644-111809(HWB R-37 VOCs) PAR 002731703
Field 10 R-37 Sor 2-111809
Lab ID 0911214middot1
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml
Moisture NA QCBatchlD VL091125-4-5 Final Volume 10 ml
Date Collected 18-Nov-09 Run ID VL091125-4A Result Units UGL
Date Extracted 25-Nov-09 Cleanup NONE Clean DF 1
Analysis ReqCode 104 Date Analyzed 25-Nov-09 Basis As Received
Prep Method SW5030 Rev C File Name 028044
CASNO Target Analyte Dilution Factor
103-65-1 NmiddotPROPYLBENZENE 1
95-49-8 2-CHLOROTOLUENE 1
108-67-8 135-TRIMETHYLBENZENE 1
106-43-4 4-CHLOROTOLUENE 1
98-06-6 TER I-BUTYLBENZENE 1
95-63-6 124-TRIMETHYLBENZENE 1
135-98-8 SEC-BUTYLBENZENE 1
541-73-1 13-OICHLOROBENZENE 1
99-87-6 P-ISOPROPYLTOLUENE 1
106-46-7 lA-DICHLOROBENZENE 1
104-51-8 N-BUTYLBENZENE 1
95-50-1 12-DICHLOROBENZENE 1
96-12-8 l2-DIBROMOmiddot3-CHLOROPROPANE 1
120-82-1 12A-TRICHLOROBENZENE 1
187-68-3 HEXACHLOROBUTADIENE 1
91-20-3 NAPHTHALENE 1
87-61middot6 123-TRICHLOROBENZENE 1
75-05-8 ACETONITRILE 1
107middot05middot1 ALLYL CHLORIDE 1
110-57-6 TRANS-14-DICHLORO-2-BUTENE 1
164-17-5 ETHANOL 1
97-63-2 ETHYL METHACRYLATE 1
78-83-1 ISOBUTYL ALCOHOL 1
126-98-7 METHACRYLONITRILE 1
80-62-6 METHYL METHACRYLATE 1
107-12-0 PROPIONITRILE 1
Result Reporting Limit
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
2 2
05 05
05 05
05 05
05 05
50 50
50 50
5 5
200 200
5 5
100 100
35 35
5 5
25 25
MDL Result EPA Qualifier Qualifier
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
067 U
017 U
017 U
017 U
017 U
83 U
017 U
U u 78 U
017 U
17 U
17 U
17 U
33 U
Data Package 10 VL0911214-1
Date Printed Wednesday December 022009 ALS Laboratory Group MM Fe Page 3 of 8
LlMS VerSion 6317A
14
GCMS Volati las Method SW8260_258
Sample Results
Lab Name ALS Laboratory Group - FC
Work Order Number 0911214
Client Name New Mexico Environment Department 08
ClientProject 10 644-111B09(HWB R-37 VOGs) PAR 002731703
Field 10 R-37 Ser 2-111809 Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10ml
Lab 10 0911214-1 Moisture NA
Date Collected 1B-Nov-09 QCBatchlO VL091125-4-5
Run 10 VL091125-4A
Final Volume 10ml
Result Units UGIL Date Extracted 25-Nov-09 Cleanup NONE Clean OF
Analysis ReqCode 104 Date Analyzed 25-Nov-09
Prep Method SW5030 Rev G Basis As Received
File Name 028044
CASNO Target Analyte Dilution Factor
Result Reporting Limit
MDL Result Qualifier
EPA Qualifier
126-99-8 CHLOROPRENE 1 5 5 017 U
75-65-0 TERT-BUTANOL 1 100 100 33 U
108-20-3 ISOPROPYL ETHER 1 2 2 033 U
637-92-3 ETHYL TERT-BUTYL ETHER 1 2 2 033 U
994-05-8 TERT-AMYL METHYL ETHER 1 2 2 033 U
67-72-1 HEXACHLOROETHANE 1 2 2 033 U
Surrogate Recovery
CASNO Surrogate Analyte Result Flag Spike Amount
Percent Recovery
Control Limits
460-00-4 4-BROMOFLUOHOBENZENE 246 25 98 82 - 121
1868-53-7 DIBROMOFLUOHOMETHANE 248 25 99 BO - 123
2037-26-5 TOLUENE-DB 258 25 103 85middot116
Data Package 10 VL0911214-1
Date Printed Wednesday December 022009 ALS Laboratory Group bullbull FC Page 4 of 8
LIMS Version 0317 A
15
GCMS Volati les Method SW8260_25B
Sample Results
Lab Name ALS Laboratory Group -- FC
Worlt Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-111809(HWB Rmiddot37 VOCs) PAR 002731703
Field 10 Rmiddot37 Scr jmiddot111809
Lab 10 0911214-2
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml Moisture NfA QCBatchID VL091125-4middot5 Final Volume 10 ml
Date Collected 18middotNov-09 Run 10 VL091125-4A Result Units UGfL Date Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Analysis ReqCode 104 Date Analyzed 25middotNov-09 Basis As Received Prep Method SW5030 Rev C File Name 028045
CASNO Target Analyte Dilution Factor
Result Reporting Limit
MOL Result Qualifier
EPA Qualifier
75-71-8 DICHLORODIFLUOROMETHANE 1 05 05 017 U
74-87-3 CHLOROMETHANE 1 05 05 017 U
75-01middot4 VINYL CHLORIDE 1 05 05 017 U
74-83-9 BROMOMETHANE 1 1 1 017 U
75middot00middot3 CHLOROETHANE j 05 05 017 U
75-69-4 TRICHLOROFLUOROMETHANE 1 05 05 017 U
107-02-8 ACROLEIN 1 100 100 17 U
i 75-35-4 11-DICHLOROETHENE 1 05 05 017 U
67-64middot1 ACETONE 1 10 10 33 U
74-8S-4 IODOMETHANE 1 5 5 017 U
75-15-0 CARBON DISULFIDE 1 10 10 017 U
75-09-2 METHYLENE CHLORIDE 1 1 1 017 U
156-60-5 TRANS-12-DICHLOROETHENE 1 05 05 017 U
1634-04-4 METHYL TERTIARY BUTYL ETHER 1 1 1 017 U
107-13-1 ACRYLONITRILE 1 10 10 17 U
75-34middot3 11-DICHLOROETHANE 05 05 017 U
i 108-05-4 VINYL ACETATE 1 10 10 067 U
115659-2 CISmiddot 2middotDICHLOROETHENE 1 05 05 017 U
178-933 2middotBUTANONE 1 5 5 17 U
74-97middot5 BROMOCHLOROMET HANE 1 1 1 017 U
67-66-3 CHLOROFORM 1 05 05 017 U
71-55middot6 111middotTRICHLOROETHANE 1 1 1 017 U
594-20-7 22middotDICHLOROPROPANE 1 05 05 017 U
56-23-5 CARBON TETRACHLORIDE 1 05 05 017 U
563-58-6 11middotDICHLOROPROPENE 1 05 05 017 U
107-06-2 12middotDICHL OROETHANE 1 05 05 017 U
Data Package ID VL0911214-1
Date Printed Wednesday December 022009 ALS Laboratory Group -- Fe Page 5 of 8
16
GCMS Volatiles Method SW8260_25B
Sample Results
Lab Name ALS Laboratory Group -- FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-111809(HW3 R-37 VOCs) PAR 002731703
Field 10 R-37 Scr 1-11 1809
Lab 10 0911214-2
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml
Moisture NIA QCBatchlO VL091125-4-5 Final Volume 10 ml
Date Collected 18-Nov-09 Run 10 VL091125-4A Result Units UGL
[late Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Analysis ReqCode 104 Date Analyzed 25-Nov-09
Prep Method SW5030 Rev C Basis As Received
File Name 028045
CASNO Target Analyte Dilution Factor
71-43-2 BENZENE 1
79-01-6 TRICHLOROETHENE 1
78-87-5 12-DICHLOROPROPANE 1
74-95-3 DIBROMOMETHANE 1
75-27-4 BROMODICHLOROMETHANE 1
10061-01-5 CIS-13-DICHLOROPROPENE 1
108-10-1 4-METHYL-2-PtNTANON 1
108-88-3 TOLUENE 1
10061-02-6 TRANS-13-DICHLOROPROPENE 1
79-00-5 112-TRICHLOROETHANE 1
591-78-6 2-HEXANONE 1
127-18-4 TETRACHLOROETHENE 1
142-28-9 13-DICHLOROPROPANt 1
124-48-1 DI3ROMOCHLOROMETHANE 1
106-93-4 12-DIBROMOETHANE 1
108-90-7 CHLOROBENZENE 1
OETHANE 1
- 1
LENE 1
ENE 1
ENE 1
OFORM 1
OPYlBENZENE 1
96-18-4 123-TRICHLOROPROPANE 1
79-34-5 1122-TETRACHLOROETHANE 1
108-86-1 BROMOBENZENE 1
Result Reporting Limit
05 05
05 05
05 05
05 05
05 05
05 05
5 5
025 05
05 05
05 05
10 10
05 05
05 05
1 1
1 1
05 05
05 05
05 05
1 1
05 05
05 05
05 05
05 05
2 2
05 05
05 05
MDL Result EPA Qualifier Qualifier
017 U
017 U
017 U
017 U
017 U
017 U
17 U
017 J
017 U
017 U
17 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
Data Package 10 VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- Fe Page 6 of 8
317A
17
GCMS Volatiles Method SW8260 _258
Sample Results
Lab Name ALS Laboratory Group -- FC
Work Order Number 0911214
Client Name New Mexico Environment Department 08
ClientProject 10 644-11S09(HWB R-37 VOCs) PAR 002731703
Field 10 Rmiddot37 Scr 1-111809
Lab 10 0911214-2
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml Moisture NA QCBatchlD VL091125-4-5 Final Volume 10 ml
Date Collected 18-Nov-09 Run 10 VL091125-4A Result Units UGL Date Extracted 25-Nol-09 Cleanup NONE Clean OF
Analysis ReqCode 104 Date Analyzed 25-Nov-09 Basis As Received Prep Method SW5030 Rev C File Name D28045
CASNO Target Analyte Dilution Factor
103-65-1 N-PROPYLBENZENE 1
95-49-8 2-CHLOROTOLUENE 1
108-67-8 135-TRIMETHYLBENZENE 1
106-43-4 4-CHLOROTOLUENE 1
98-06-6 TERT-BUTYLBENZENE 1
95-63-6 124-TRIMETHYLBENZENE 1
135-98-8 SEC-BUTYLBENZENE 1
i 541-73-1 13middotDICHLOROBENZENE 1
99-87-6 PmiddotISOPROPYL TOLUENE 1
106-46-7 I 14-DICHLOROBENZENE 1
104-51-8 I N-BUTYLBENZENE 1
95-50-1 l2-DICHLOROBENZENE 1
96-12-8 I 12-DIBROMO-3-CHLOROPROPANE 1
120-82-1 124-TRICHLOROBENZENE 1
87-68-3 HEXACHLOROBUT ADIENE 1
91-20-3 NAPHTHALENE 1
87-61-6 123-TRICHLOROBENZENE 1
75-05-S ACETONITRILE 1
107-05-1 ALLYL CH LORIDE 1
110-57-6 TRAN S-14-DICHLORO-2-BUTENE 1
64-17-5 ETHANOL 1
97-63-2 ETHYL METHACRYLATE 1
78-83-1 ISOBUTYL ALCOHOL 1
126-98-7 METHACRYLONITRILE 1
80-62-6 METHYL METHACRYLATE 1
107-12-0 I PROPIONITRILE 1
Result Reporting Limit
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
2 2
05 05
05 05
05 05
05 05
50 50
50 50 I 5 5
200 200
5 5
100 100
35 35
5 5
25 25
MDL
017
017
017
017
017
017
017
017
017
017
017
017
067
017
017
017
017
83
017
17
78
017
17
17
17
33
Result EPA Qualifier Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
Data Package 10 VL0911214-1
Date Printed Wednesday December 022009 ALS Laboratory Group -- Fe Page 7 of 8
LlMS Version 6317A
18
GCMS Volatiles Method SW8260_258
Sample Results
Lab Name ALS Laboratory Group bullbull FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644middot111B09(HWB R-37 VOCs) PAR 002731703
Sample Matrix WATER Prep Batch VL091125--4 Sample Aliquot 10 mlRmiddot37 Ser 1-111809 Moisture NA QCBatchlO VL091125--4-5 Final Volume 10 m
0911214-2 Date Collected 18-Nov-09 Run 10 VL091125--4A Result Units UGL Date Extracted 25-Nov-09 Cleanup NONE Clean OF 1 Date Analyzed 25-Nov-09 Basis As Received
10
Analysis ReqCode 104 Prep Method SW5030 Rev C File Name 028045
I
CASNO Target Analyte Dilution Factor
Result Reporting Limit
MDL Result Qualifier
EPA Qualifier
126-99-8 CHLOROPRENE 1 5 5 017 U
75-65-0 TERT-BUTANOL 1 100 100 33 U
108-20-3 ISOPROPYL ETHER 1 2 2 033 U
637-92-3 ETHYL TERT-BUTYL ETHER 1 2 2 033 U
994-05--8 TERT-AMYL MTHYL ETHER 1 2 2 033 U
67-72-1 HEXACHLOROETHANE 1 2 2 033 U
Surrogate Recovery
CASNO Surrogate Analyte Result Flag Spike Amount
Percent Control Recovery Limits
460-00-4 4middotBROMOFLUOROBENZENE 247 25 99 1
1868-53-7 DIBROMOFLUOROMETHANE 248 25 99 80 123
2037-26-5 TOLUENEmiddotDB 255 25 102 85 - 116
Data Package 10 VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- FC Page B of 8
LlMS Version 6317A
19
GCMS Volatiles Method SW8260_258
Laboratory Control Sample and Laboratory Control Sample Duplicate
Lab Name ALS Laboratory Group - FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-111809(HWB R-37 VOCs) PAR 002731703
Lab 10 VL091125-4LCS Sample Matrix WATER
Moisture NA Prep Batch VL091125-4
QCBatchlD VL091125-4-5
Sample Aliquot
Final Volume
10ml
10ml Date Collected NA Run 10 VL091125-4A Result Units UGIL Date Extracted 111252009 Cleanup NONE Clean OF 1 Date Analyzed 11252009 Basis NA
Prep Method SW5030C File Name 028040
CASNO
74-87-3
75-01-4
74-83-9
75-69-4
75-35-4
75-15-0
156-60-5
75-34-3
108-05-4
156-59-2
78-93-3
67 -66-3
71-55-6
i 56-23-5
107-06-2
71-43-2
79-01-6
78-87-5
75-27-4
108-88-3
79-00-5
591-78-6
127-18-4
106-93-4
108-90-7
63Q20-6
Target Analyte Spike Added
CHLOROMETHANE 10
VINYL CHLORIDE 10
BROMOMETHANE 10
TRICHLOROFLUOROMETHANE 10
11-DICHLOROETHENE 10
CARBON DISULFIDE 10
TRANS-12-DICHLOROETHENE 10
11-DICHLOROETHANE 10
VINYL ACETATE 10
CIS-12-DICHLOROETHENE 10
2middotBUTANONE 40
CHLOROFORM 10
111-TRICHL ORO ETHANE 10
CARBON TETRACHLORIDE 10
12-DICHLOROETHANE 10
BENZENE 10
TRICHLOROETHENE 10
12-DICHLOROPROPANE 10
BROMODICHLOROMETHANE 10
TOLUENE 10
112-TRICHLOROETHANE 10
2-HEXANONE 40
TETRACHLOROETHENE 10
12-DIBROMOETHANE 10
CHLOROBENZENE 10
1112-TETRACHLOROETHANE 10
LCS Reporting Result Result Limit Qualifier
932 05
863 05
943 1
908 05
96 05
95 10 J
996 05
992 05
10 10
102 05
412 5
993 05
974 1
943 05
106 05
983 05
962 05
10 05
988 05
974 05
989 05
409 10
956 05
991 1
984 05
101 05
LCS Control Rec Limits
93 49 -129
86 46 134
94 32-121
91 67 -152
96 61 -135
95 61 -140
100 70 -122
99 76 -119
100 62 182
102 75 126
103 61 -137
99 79 120
97 76 - 114
94 58middot135
106 75middot132
98 70 shy 125
96 74 121
100 81 -119
99 79 - 123
97 76 - 120
99 81 -126
102 45 168
96 56 -128
99 79 -123
98 75 -120
101 82 - 123
Data Package 10 VL0911214middot1
-Date Printed Wednesday December 02 2009 ALS Laboratory Group -- Fe Page 1 of 4
LiMS Version 6317A
20
GCMS Volatiles Method SW8260_25B
Laboratory Control Sample and Laboratory Control Sample Duplicate
Lab Name ALS Laboratory Group - FC
Work Order Number 0911214
Client Name New Mexico Envircnment Department OB
ClientProject 10 644-111809(HWB R-37 VOes) PAR 002731703
Lab 10 VL091125-4LCS Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml
Moisture NIA QCBatchlO VL091125-4-5 Final Volume 10 mi
Date Collected NA Run 10 VL091125-4A Result Units UGL Date Extracted 11252009 Cleanup NONE Clean OF 1 Date Analyzed 111252009 Basis NA
Prep Method SW5030e File Name 028040
CASNO Target Analyte Spike Added
LCS Result
Reporting Limit
Result Qualifier
LCS Rec
Control Limits
100-41-4 ETHYLBENZENE 10 981 05 98 79 -114
136777-61-2 M+P-XYLENE 20 197 1 98 81-115
95-47-6 O-XYLENE 10 101 05 101 81 -115
95-49-8 2-CHLOROTOLUENE 10 97 05 97 80 -128
541-73-1 13-DICHLOROBENZiNt 10 977 05 98 81-116
106-46-7 14-DICHLOROBENZENE 10 979 05 98 81 -119
95-50-1 12-DICHLOROBENZENE 10 987 05 99 79 - 116
91-20-3 NAPHTHALENE 10 993 05 99 69 -126
87-61-6 123-TRICHLOROBENZENE 10 999 05 100 60 -137
Data Package ID VL0911214-1
Date Printed Wecnesday December 02 2009 ALS Laboratory Group -- Fe Page 2 of 4
21
GCMS Volatiles Method SW8260_25B
Laboratory Control Sample and Laboratory Control Sample Duplicate
Lab Name ALS Laboratory Group bullbull FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-11 1809(HWB R-37 VOCs) PAR 002731703
Lab 10 VL091125middot4LCSD Sample Matrix WATER
Moisture NIA Prep Batch VL091125-4
QCBatchlD VL091125-4-5
Sample Aliquot
Final Volume
10 ml
10ml Date Collected NIA Run ID VL091125-4A Result Units UGIL Date Extracted 112512009 Cleanup NONE Clean DF 1 Date Analyzed 1112512009 Basis NIA
Prep Method SW5030C File Name 028041
CASNO Target Analyte Spike Added
LCSD Result
Reporting Limit
Result Qualifier
LCSD Rec
RPD Limit
RPD
74-87-3 CHLOROMETHANE 10 897 05 90 30 4
75-01-4 VINYL CHLORIDE 10 831 05 83 25 4
74-83-9 BROMO METHANE 10 945 1 94 25 0
75-69-4 TRICHLOROFLUOROMETHANE 10 873 05 87 22 4
75-35-4 11-DICHLOROETHENE 10 909 05 91 18 5
75-15-0 CARBON DISULFIDE 10 941 10 J 94 20 1
156-60middot5 TRANS-l2middotDICHLOROETHENE 10 961 05 96 25 4
75middot34middot3 11-DICHLOROETHANE 10 977 05 98 25 2
108-05-4 VINYL ACETATE 10 993 10 J 99 20 1
156middot59-2 CIS-12-DlCHLOROETHENE 10 995 05 99 25 3
i 78-93-3 2-BUTANONE 40 419 5 105 30 2
67-66-3 CHLOROFORM 10 985 05 99 25 1
71-55-6 lll-TRICHLOROETHANE 10 942 1 94 25 3
56-23-5 CARBON TETRACHLORIDE 10 922 05 92 25 2
107middot06-2 12middotDICHLOROETHANE 10 106 05 106 25 0
71-43middot2 BENZENE 10 971 05 97 10 1
79middot01middot6 TRICHLOROETHENE 10 939 05 94 10 2
78middot87middot5 l2middotDICHLOROPROPANE 10 101 05 101 25 1
i 75middot27-4 BROMODICHLOROMETHANE 10 992 05 99 25 0
1108-88-3 TOLUENE 10 962 05 96 9 1
I 79005 112middotTRICHLOROETHANE 10 986 05 99 25 0
591middot78middot6 2-HEXANONE 40 418 10 104 20 2
127middot18-4 TETRACHLOROETHENE 10 918 05 92 25 4
106-93-4 12middotDIBROMOETHANE 10 999 1 100 15 1
108middot90-7 CHLOROBENZENE 10 997 05 100 11 1
630-20middot6 1112-TETRACHLOROETHANE 10 101 05 101 15 0
100-41-4 ETHYLBENZENE 10 968 05 97 25 1
Data Package ID VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- FC Page 3 of 4
lIMS Version 6317 A
22
GCMS Volatiles Method SW8260_25B
Laboratory Control Sample and Laboratory Control Sample Duplicate
Lab Name ALS Laboratory 13roup -- FC
Work Order Number 0911214
Client Name New Mexico Environment Department OS
ClientProject 10 644-11 1809(HWB R-37 VOCs) PAR 002731703
Lab 10 VL091125-4LCSD Sample Matrix WATER
Moisture NA Prep Batch VL091125-4
QCBatchlO VL091125-4-5
Sample Aliquot
Final Volume
10 ml
10ml Date Collected NA Run 10 VL091125-4A Result Units UGL Date Extracted 11252009 Cleanup NONE Clean OF Date Analyzed 11252009 Basis NIA
Prep Method SW5030C File Name 028041
CASNO Target Analyte Spike Added
LCSD Result
Reporting Limit
Result Qualifier
LCSD Rec
RPD Limit
RPD
136777-61-2 M+P-XYLENE 20 193 1 97 25 2
95-47-6 O-XYLENE 10 983 05 98 25 2
95-49-8 2middotCHLOROTOLUENE 10 9A9 05 95 15 2
541-73-1 13middotDICHLOROBENZENE 10 997 05 100 25 2
106-46-7 14-DICHLOROBeNZENE 10 974 05 97 25 1
95-50middot1 12middotDICHLOROBENZeNE 10 101 05 101 25 2
91middot20-3 NAPHTHALENe 10 105 05 105 24 6
87-61-6 123-TRICHLOROBENZENE 10 102 05 102 33 3
Surrogate Recovery LCSLCSD
CASNO Target Analyte Spike Added
LCS Rec
LCS Flag
LCSD Rec
LCSD Flag
Control Limits
460middot00-4 4-BROMOFLUOROBeNZENE 25 100 100 82 - 121
1868-53middot7 DIBROMOFLUOROMeTHANE 25 101 100 80middot 123
2037middot26-5 TOLUENEmiddotD8 25 102 100 85middot 116
Data Package 10 VL0911214-
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- Fe Page 4 of 4
UMS Verslmt 6317A
23
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ALS Labofaton1 Group
Environmental Division Fort Cofiins Colorado
GCMS Volatiles Case Narrative
New Mexico Environmental Department OB 644-111809(HWB R-37 VOCs) PAR -- 002731703
Work Order Number 0911214
1 This report consists of 2 water samples The samples were received cool and intact by ALS on 1120109 The vial for sample 0911214-1 contained headspace prior to analysis because it was not received headspace free into the voatiles laboratory
The samples provided for volatiles had a pH gt 2 at the time of analysis
2 These samples were prepared according to SW-846 3rd Edition procedures Specifically the water samples were prepared by purging 10 mL using purge and trap procedures based on Method 5030C
3 The samples were analyzed using GCMS with an RTX-624 RTX-VMS or equivalent capillary column according to SOP 525 Revision 14 based on SW-846 Method 8260B All positive results were quantitated against the initial calibration standards using the intemal standard technique The identification of positive results was achieved by a comparison of the retention time and mass spectrum of trle sample versus the daily calibration standard
4 All initial calibration criteria for SPCCs and CCCs were met If average response factors were used in the initial calibration RSO was 15 If linear or higher order regression calibrations were used in the initial calibration the coefficient of determination (r2) ~099
5 All initial calibrations are verified by comparing a second source standard calibration verrrication (ICV) against the calibration curve All target compounds in the second source verification had a 0 of less than 25
6 All criteria for SPCCs and CCCs were met in daily (continuing) calibration verifications (CCV)
7 Methylene chloride acetone and 2-butanone are common laboratory contaminants In order to minimize the levels of these compounds detected in the gclms analysis ALS has designated its volatile laboratory as a restricted access area In addition the laboratory has been equipped with a dedicated air intake and exhaust system that operates under positive pressure in order to
1
minimize cross contamination of these compounds Due to fluctuations in ambient laboratory conditions reported sample values for common laboratory contaminants may be due to lab contamination even if the compound in question is not detected in the associated method blankmiddot
All method blank criteria were met
8 All laboratory control sample and laboratory control sample duplicate recoveries and RPDs were within the acceptance criteria
9 Since a sample from this order number was not the selected qualITy control (QC) sample matrix specific QC results are not included in this report
10 The samples were analyzed within the established holding time
11 All surrogate recoveries were within acceptance criteria
12 All internal standard recoveries were within acceptance criteria
14 Manual integrations are performed when needed to provide consistent and defensible data following the guidelines in SOP 939 ReVision 3
The data contained in the following report have been reviewed and approved by the personnel listed below In addition ALS certifies that the analyses reported herein are true complete and correct within the limits of the methods employed
n-o3-o5Sha~JobeS Date Organics Primary Data Reviewer
l~-O 1-01TAamp1~Orga~cs Final Data Reviewer Date
2
ALS Data Qualifier Flags Chromatography and Mass Spectrometry
U or NO This flag indicates that the compound was analyzed for but not detected
J This flag indicates an estimated value This flag is used as follows (1) when estimating a concentration for tentatively identified compounds (TICs) where a 11 response is assumed (2) when the mass spectral and retention time data indicate the presence of a compound that meets the volatile and semivolatile GCMS identification criteria and the result is less than the reporting limit (RL) but greater than the method detection limit (MOL) (3) when the retention time data indicate the presence of a compound that meets the GC identification criteria and the result is less than the RL but greater than the MOL and (4) the reported value is estimated
B This flag is used when the analyte is detected in the associated method blank as well as in the sample It indicates probable blank contamination and warns the data user This flag shall be used for a tentatively identified compound (TIC) as well as for a positively identified target compound
E This flag identifies compounds whose concentration exceeds the upper level of the calibration range
A This flag indicates that a tentatively identified compound is a suspected aldol-condensation product
X This flag indicates that the analyte was diluted below an accurate quantitation level
This flag indicates that a spike recovery is equal to or outside the control criteria used
+ This flag indicates that the relative percent difference (RPO) equals or exceeds the control criteria
3
ALS Laboratory Group -- Fe Sample Number(s) Cross-Reference Table
Paragon OrderNum 0911214 Client Name New Mexico Environment Department OB
Client Project Name 644-111809(HWB R-37 VOCs) PAR Client Project Number 002731703
Client PO Number 06-667-55-01754
Client Sample Number
Lab Sample Number
COC Number Matrix Date Collected
Time Collected
R-37 Scr 2-1 11809 0911214-1 WATER 18-Nov-09 1555 R-37 Scr 1-111809 0911214-2 WATER 18-Nov-09 1744
Page 1 of 1 ALS Laboratory Group -- Fe Date Printed Wednesday December 02 2009 LlMS Version 6317 A
4
Chain of Custody Record 1)11 d- I 4 SHIP To MAil REPORT TO HtitilJft BILL TO
Kim GrJOZOW KC [)il-e Cobra
NMFOmiddotDOE Overslghl Bwe3u 50S firt1middottoOB Hew Meico FnlliTtl1 Dep1 HaVIdthJS VvaMe Bureau ~orl Collins CO 80524shy
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CONDITIO] OF SAMPLE UPO) RECEIPT FORM
Client _-=-N--M---f-=-D________ IVorkorde No D4 J I 4 --~~~~~~------
PrO1 cc Manager L 5 lnitiais C D Date 1 -) ()- () C --~~~---------------------
1 there a cae Are the coe and bottle labels
Is the coe in agreement with samples received) of containers matrix requested anaiyses etc)
documents presen1 andor removable)
Are all aqueous samples requiring preservation preserved correctly ~- ----~-~~--- -~ -~-- ----~~~---------
volatiles)
14 Are all samples requiring no headspace (VOC GRG RSKlVIEE lb eNS radon)
free Size of bubble lt
$ Do perchlorate LCMS-MS samples have headspace (a~ least ]3 of container required)
NO
]6 Were samples checked for and free from the presence of residual chlorine (Appiicaole when PM has Indicated samples are from a chlonnated wat~ source note if field preservallor
witb sodIUm tlllosulfate wa not observed)
17 Were the lljIV~IOU on ice
IS Were cooler temperatures measured at 01-60degC IR ~Illl used 2
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Temperature (C) 3 ~
NO
NO
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NO
NO
NO
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Additional Iuformation OVIDE DETAILS BELOW FOR A ND RESPONSE TO ANY (UESTION A80VE EXCEPT 1 ANI) 16
If applicable was the clienl contacted) YES i NO I
Project Manager Signature I Date
(1 Gun 112 Oaktoll SN 2992250020 jmiddot0066 lR Gun lie Oakton S~ 23n220101middot0(J02
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7
GCMS Volatiles Method SW8260 _25B
Method Blank
Lab Name ALS Laboratory Group bullbull FC
Work Order Number 0911214
Client Name New Mexico Environment Department DB
ClientProject 10 644-111809(HWB Rmiddot37 VOCs) PAR 002731703
Lab 10 VL091125-4MB Sample Matrix WATER
Moisture NA Prep Batch VL091125-4
QCBatchlO VL091125-4-5
Sample Aliquot
Final Volume
10 ml
10 ml Date Collected NA Run 10 VL091125-4A Result Units UGL Date Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Date Analyzed 25middotNov-09 Basis NA
File Name 028043
CASNO Target Analyte DF
75-71-8 DICHLORODIFLUOROMETHANE
74-87-3 CHLOROMETHANE
75-01-4 VINYL CHLORIDE
74-83-9 BROMOMETHANE
75-00-3 CHLOROETHANE
75-69-4 TRICHLOROFLUOROMETHANE
107-02-8 ACROLEIN
75-35-4 11middotDICHLOROETHENE
67-64-1 ACETONE
74-88-4 IODOMETHANE
75-15-0 CARBON DISULFIDE
METHYLEN E CHLORIDE 75-09-2
156-60-5 TRANS-12middotDICHLOROETHENE
1634-04-4 METHYL TERTIARY BUTYL ETHER
107-13-1 ACRYLONITRILE
75-34-3 11-DICHLOROETHANE
108-05-4 VINYL ACETATE
156-59middot2 CIS-12middotDICHLOROETHENE
78-93-3 2middotBUTANONE
~ BROMOCHLOROMETHANE
67-66-3 CHLOROFORM
71-55-6 111middot TRICHLOROETHANE
594-20-7 22middotDICHLOROPROPANE
56-23-5 CARBON TETRACHLORIDE
563-58-6 11middotDICHLOROPROPENE
107-06middot2 l2middotDICHLOROETHAN E
71-43-2 BENZENE
79-01-6 TRICHLOROETHENE
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Result Reporting Limit
05 05
05 05
05 05
1 1
05 05
05 05
100 100
05 05
10 10
5 5
10 10
1 1
05 05
1 1
10 10
05 05
10 10
05 05
5 5
1 1
05 05
1 1
05 05
05 05
05 05
05 05
05 05
05 05
MDL Result EPA Qualifier Qualifier
017 U
017 U
017 U
017 U
017 U
017 U
17 U
017 U
33 U
017 U
017 U
017 U
017 U
017 U
17 U
017 U
067 U
017 U
17 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
Data Package 10 VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- Fe Page 1 of 4
llMS Version 6317 A
8
GCMS Volatiles Method SW8260 _25B
Method Blank
Lab Name ALS Laboratory Group -- FC
Work Order Number 0911214
Client Name New Mexico Environment Department 08
ClientProject 10 644-111809(HWEI R-37 voes) PAR 002731703
Lab 10 VL091125-4MB Sample Matrix WATER
Moisture NIA Prep Batch VL091125-4
QCBatchIO VL091125-4-5
Sample Aliquot
Final Volume
10 ml
10 ml Oate Collected NIA Run 10 VL091125-4A Result Units UGL Oate Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Date Analyzed 25-Nov-09 Basis NIA
File Name 028043
CASNO Target Analyte OF Result Reporting Limit
MOL Result Qualifier
EPA Qualifier
78-87-5 12middotDICHLOROPROPANE 1 05 05 017 U
74-95-3 DIBROMOMETHANE 1 05 05 017 U
75-27-4 BROMODICHLOROMETHANE 1 05 05 017 U
10061-01-5 CISmiddot13middotDICHLOROPROPENE 1 05 05 017 U
108-10-1 4-METHYL-2-PENT ANONE 1 5 5 17 U
108-88-3 TOLUENE 1 05 05 017 U
10061-02-6 TRANS-13-DICHLOROPROPENE 1 05 05 017 U
79-00-5 112-TRICHLOROETHANE 1 05 05 017 U
591-78-6 2-HEXANONE 1 10 10 17 U
127-18-4 TETRACHLOROETHENE 1 05 05 017 U
142-28-9 13-DICHLOROPROPANI 1 05 05 017 U
124-48-1 DIBROMOCHLOROMETHANE 1 1 1 017 U
106-93-4 12-DIBROMOETHANE 1 1 1 017 U
108-90-7 CHLOROBENZENE 1 05 05 017 U
630-20-6 1112-TETRACHLOROETHANE 1 05 05 017 U
100-41-4 ETHYLBENZENE 1 05 05 017 U
136777-61-2 M+P-XYLENE 1 1 1 017 U
95-47-6 O-XYLENE 1 05 05 017 U
100-42-5 STYRENE 1 05 05 017 U
75-25-2 BROMOFORM 1 05 05 017 U
98-82-8 ~YLBENZENE 1 05 05 017 U
96-18-4 123-TRICHLOROPROPANE 1 2 2 017 U
79-34-5 1122middot TETRACHLOROETHANE 1 05 05 017 U
108-86-1 BROMOBENZENE 1 05 05 017 U
103-65-1 N-PROPYLBENZENE 1 05 05 017 U
95-49-8 2-CHLOROTOLUENE 1 05 05 017 U
108-67-8 135-TRIMETHYLBENZENE 1 05 05 017 U
106-43-4 4-CHLOROTOLUENE 1 05 05 017 U
Data Package 10 VL0911214-1
Date Printed Wednesday December n 2009 AlS Laboratory Group -- FC Page 2 of 4
lMS VeCSiOIY 6317A
9
GCMS Volatiles Method SW8260 _258
Method Blank
Lab Name ALS Laboratory Group - FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-111B09(HWB R-37 VOCs) PAR 002731703
Lab 10 VL091125-4MB Sample Matrix WATER
Moisture NIA
Prep Batch VL091125-4
QCBatchlD VL091125-4-5
Sample Aliquot
Final Volume
10 ml
10 ml
Date Collected NIA Run ID VL091125-4A Result Units UGL
Date Extracted 25-Nov-09 Cleanup NONE Clean DF 1
Date Analyzed 25-Nov-09 Basis NA
File Name 028043
CASNO Target Analyte OF Result Reporting Limit
MOL Result Qualifier
EPA Qualifier
98-06-6 TERT-BUTYLBENZENE 1 05 05 017 U
95-63-6 124-TRIMETHYLBENZENE 1 05 05 017 U
135-98-8 SEC-BUTYLBENZENE 1 05 05 017 U
541-73-1 13-DlCHLOROBENZENE 1 05 05 017 U
99-87-6 P-ISOPROPYLTOLUENE 1 05 05 017 U
106-46-7 1 A-DICHLOROBENZENE 1 05 05 017 U
104-51-8 N-BUTYLBENZENE 1 05 05 017 U
95-50-1 12-DICHLOROBENZENE 1 05 05 017 U
96-12-B 12-DIBROMO-3-CHLOROPROPANE 1 2 2 067 U
120-82-1 124-TRiCHLOROBENZENE 1 05 05 017 U
87-68-3 HEXACHLOROBUTADIENE 1 05 05 017 U
91-20-3 NAPHTHALENE 1 05 05 017 U
87-61-6 123-TRICHLOROBENZENE 1 05 05 017 U
75-05-B ACETONITRILE 1 50 50 83 U
107-05-1 ALLYL CHLORIDE 1 50 50 017 U
110-57-6 TRANS-14-DICHLORO-2-BUTENE 1 5 5 17 U
64-17-5 ETHANOL 1 200 200 78 U
97-63-2 ETHYL METHACRYLATE 1 5 5 017 U
78-83-1 ISOBUTYL ALCOHOL 1 100 100 17 U
126-98-7 METHACRYLONITRILE 1 35 35 17 U
80-62-6 METHYL METHACRYLATE 1 5 5 17 U
107-12-0 PROPIONITRILE 1 25 25 33 U
126-99-8 CHLOROPRENE 1 5 5 017 U
75-65-0 TERT-BUTANOL 1 100 100 33 U
108-20-3 ISOPROPYL ETHER 1 2 2 033 U
637-92-3 ETHYL TERT-BUTYL ETHER 1 2 2 033 U
994-05-8 TERT-AMYL METHYL ETHER 1 2 2 033 U
67-72-1 HEXACHLOROETHANE 1 2 2 033 U
Data Package 10 VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -~ Fe Page 3 of 4
LlMS Version 6317 A
10
GCMS Volatiles Method SW8260 _258
Method Blank
Lab Name ALS Laboratory Group -- FC
Work Order Number 0911214
Client Name New Mexico Envirmment Department OB
ClientProject 10 644-111809(HWB R-37 VOCs) PAR 002731703
Lab 10 VL091125-4MB Sample Matrix WATER
Moisture NIA Prep Batch VL091125-4
QCBatchlO VL091125-4-5
Sample Aliquot
Final Volume
10 m
10m Date Collected NIA Run 10 VL091125-4A Result Units UGIL Date Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Date Analyzed 25-Nov-09 BasisNIA
File Name 028043
CASNO Target Analyte Result Reporting MOL Result EPAOF Limit Qualifier Qualifier
Surrogate Recovery
CASNO Surrogate Analyte Result Flag Spike Amount
Percent Recovery
Control Limits
460-00-4 4-BROMOFLUOROBENZENE 25 25 100 82 - 121
1868-53-7 DIBROMOFLUOROMETHANE 248 25 99 80 - 123
2037-26-5 TOLUENE-D8 26 25 104 85 - 116
Data Package 10 VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- FC Page 4 of4
LlMS Version 6317A
11
GCMS Volati les Method SW8260 _258
Sample Results
Lab Name ALS Laboratory Group -- FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-111809(HWB R-37 VOCs) PAR 002731703
Field 10 Rmiddot37 Ser 2middot111809
Lab 10 0911214middot1
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml
Moisture NA QCBatchlO VL091125-4-5 Final Volume 10mi Date Collected 18-Nov-09 Run 10 VL091125-4A Result Units UGL
Date Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Analysis ReqCode 104 Date Analyzed 25-Nov-09
Prep Method SW5030 Rev C Basis As Received
File Name 028044
CASNO Target Analyte Dilution Factor
75-71-8 DICHLORODIFLUOROMETHANE 1
74middot87-3 CHLOROMETHANE 1
75-01-4 VINYL CHLORIDE 1
74-83-9 BROMOMETHANE 1
75-00-3 CHLOROETHANE 1
75-69-4 TRICHLOROFLUOROMETHANE 1
107-02-8 ACROLEIN 1
75-35-4 11middotDICHLOROETHENE 1
67-64-1 ACETONE 1
74-88-4 IODOMETHANE 1
75-15-0 CARBON DISULFIDE 1
75-09-2 METHYLENE CHLORIDE 1
156-60-5 TRANSmiddot12middotDICHLOROETHENE 1
1634-04-4 METHYL TERTIARY BUTYL ETHER 1
107-13-1 ACRYLONITRILE 1
75-34-3 1-DICHLOROETHANE 1
i 108-05-4 VINYL ACETATE 1
156-59-2 CIS-12middotDICHLOROETHENE 1
78-93-3 2-BUTANONE 1
74-97-5 BROMOCHLOROMETHANE 67-66-3 CHLOROFORM 1
71-55-6 11-TRICHLOROETHANE 594-20-7 22-DICHLOROPROPANE 56-23-5 CARBON TETRACHLORIDE 563-58-6 -DICHLOROPROPENE 107-06-2 2-DICHLOROETHANE
Result Reporting Limit
05 05
05 05
05 05
1 1
05 05
05 05
100 100
05 05
10 10
5 5
10 10
1 1
05 05
1 1
10 10
05 05
10 10
05 05
5 5
1 1
05 05
1 1
05 05
05 05
05 05
05 05
MOL Result EPA Qualifier Qualifier
017 U
017 U
017 U
017 U
017 U
017 U
17 U
017 U
33 U
017 U
017 U
017 U
017 U
017 U
17 U
017 U
067 U
017 U
17 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
Data Package ID VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- Fe Page 1 of 8
UMS Version 6317A
12
GCMS Volatiles Method SW8260_25B
Sample Results
Lab Name ALS Laboratory Group - FC
Work Order Number 0911214
Client Name New Mexico nvironment Department OB
ClientProject 10 644-111809(HWB R-37 VOCs) PAR 002731703
Field 10 R-37 Scr 2-111809
Lab 10 0911214-1
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10ml
Moisture NA QCBatchlD VL091125-4-5 Final Volume 10ml
Date Collected l8-Nov-09 Run 10 VL091125-4A Result Units UGL
Date Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Analysis ReqCode 104 Date Analyzed 25-Nov-09 Basis As Received
Prep Method SW5030 Rev C File NameD28044
CASNO Target Analyte Dilution Factor
Result Reporting Limit
MDL Result Qualifier
EPA Qualifier
I
71-43-2 BENZENE 1 05 05 017 U
79-01-6 TRICHLOROETHENE 1 05 05 017 U
78-87-5
74middot95-3
75-27-4
10061-01-5
108middot10middot1
108middot88-3
10061-02middot6
79-00-5
591-78-6
12-DICHLOROPROPANE
DIBROMOMETHANE
BROMODCHLOROMETHANE
CIS-13-DICHLOROPROPEI~E
4-METHYL-2-PENTANONE
TOLUENE
TRANS-13-DICHLOROPROPENE
112-TRICHLOROETHANE
2-HEXANONE
1
1
1
1
1
1
1
1
1
05
05
05
05
5
031
05
05
10
05
05
05
05
5
05
05
05
10
017
017
017
017
17
017
017
017
17
U
U
U
U
U
J
U
U
U
127-18-4
142-28-9
124-48-1
106-93-4
108-90-7
630-20-6
100-41-4
136777-61-2
95-47-6
100-42middot5
75-25-2
98-82middot8
96-18-4
79-34-5
108-86-1
TETRACHLOROETHENE
13-DICHLOROPROPANE
DIBROMOCHLOROMETHANE
12-DIBROMOETHANE
CHLOROBENZENE
11 12-TETRACHLOROETHANE
ETHYLBENZENE
M+PmiddotXYLENE
OmiddotXYLENE
STYRENE
BROMOFORM
ISOPRO PYLBENZENE
123middotTRICHLOROPROPANE
1122-TETRACHLOROETHANE
BROMOBENZENE
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
05
05
1
1
05
05
05
1
05
05
05
05
2
05
05
05
05
1
1
05
05
05
1
05
05
05
05
2
05
05
017
017
017
017
017
017
017
017
017
017
017
017
017
017
017
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
i
Data Package 10 VL0911214-1
Date Printed Wednesday December 022009 AlS laboratory Group bullbull Fe Page 2 of 8
UMS Version 6317A
13
GCMS Volatiles Method SW8260_258
Sample Results
Lab Name ALS Laboratory Group bullbull FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject ID 644-111809(HWB R-37 VOCs) PAR 002731703
Field 10 R-37 Sor 2-111809
Lab ID 0911214middot1
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml
Moisture NA QCBatchlD VL091125-4-5 Final Volume 10 ml
Date Collected 18-Nov-09 Run ID VL091125-4A Result Units UGL
Date Extracted 25-Nov-09 Cleanup NONE Clean DF 1
Analysis ReqCode 104 Date Analyzed 25-Nov-09 Basis As Received
Prep Method SW5030 Rev C File Name 028044
CASNO Target Analyte Dilution Factor
103-65-1 NmiddotPROPYLBENZENE 1
95-49-8 2-CHLOROTOLUENE 1
108-67-8 135-TRIMETHYLBENZENE 1
106-43-4 4-CHLOROTOLUENE 1
98-06-6 TER I-BUTYLBENZENE 1
95-63-6 124-TRIMETHYLBENZENE 1
135-98-8 SEC-BUTYLBENZENE 1
541-73-1 13-OICHLOROBENZENE 1
99-87-6 P-ISOPROPYLTOLUENE 1
106-46-7 lA-DICHLOROBENZENE 1
104-51-8 N-BUTYLBENZENE 1
95-50-1 12-DICHLOROBENZENE 1
96-12-8 l2-DIBROMOmiddot3-CHLOROPROPANE 1
120-82-1 12A-TRICHLOROBENZENE 1
187-68-3 HEXACHLOROBUTADIENE 1
91-20-3 NAPHTHALENE 1
87-61middot6 123-TRICHLOROBENZENE 1
75-05-8 ACETONITRILE 1
107middot05middot1 ALLYL CHLORIDE 1
110-57-6 TRANS-14-DICHLORO-2-BUTENE 1
164-17-5 ETHANOL 1
97-63-2 ETHYL METHACRYLATE 1
78-83-1 ISOBUTYL ALCOHOL 1
126-98-7 METHACRYLONITRILE 1
80-62-6 METHYL METHACRYLATE 1
107-12-0 PROPIONITRILE 1
Result Reporting Limit
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
2 2
05 05
05 05
05 05
05 05
50 50
50 50
5 5
200 200
5 5
100 100
35 35
5 5
25 25
MDL Result EPA Qualifier Qualifier
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
067 U
017 U
017 U
017 U
017 U
83 U
017 U
U u 78 U
017 U
17 U
17 U
17 U
33 U
Data Package 10 VL0911214-1
Date Printed Wednesday December 022009 ALS Laboratory Group MM Fe Page 3 of 8
LlMS VerSion 6317A
14
GCMS Volati las Method SW8260_258
Sample Results
Lab Name ALS Laboratory Group - FC
Work Order Number 0911214
Client Name New Mexico Environment Department 08
ClientProject 10 644-111B09(HWB R-37 VOGs) PAR 002731703
Field 10 R-37 Ser 2-111809 Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10ml
Lab 10 0911214-1 Moisture NA
Date Collected 1B-Nov-09 QCBatchlO VL091125-4-5
Run 10 VL091125-4A
Final Volume 10ml
Result Units UGIL Date Extracted 25-Nov-09 Cleanup NONE Clean OF
Analysis ReqCode 104 Date Analyzed 25-Nov-09
Prep Method SW5030 Rev G Basis As Received
File Name 028044
CASNO Target Analyte Dilution Factor
Result Reporting Limit
MDL Result Qualifier
EPA Qualifier
126-99-8 CHLOROPRENE 1 5 5 017 U
75-65-0 TERT-BUTANOL 1 100 100 33 U
108-20-3 ISOPROPYL ETHER 1 2 2 033 U
637-92-3 ETHYL TERT-BUTYL ETHER 1 2 2 033 U
994-05-8 TERT-AMYL METHYL ETHER 1 2 2 033 U
67-72-1 HEXACHLOROETHANE 1 2 2 033 U
Surrogate Recovery
CASNO Surrogate Analyte Result Flag Spike Amount
Percent Recovery
Control Limits
460-00-4 4-BROMOFLUOHOBENZENE 246 25 98 82 - 121
1868-53-7 DIBROMOFLUOHOMETHANE 248 25 99 BO - 123
2037-26-5 TOLUENE-DB 258 25 103 85middot116
Data Package 10 VL0911214-1
Date Printed Wednesday December 022009 ALS Laboratory Group bullbull FC Page 4 of 8
LIMS Version 0317 A
15
GCMS Volati les Method SW8260_25B
Sample Results
Lab Name ALS Laboratory Group -- FC
Worlt Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-111809(HWB Rmiddot37 VOCs) PAR 002731703
Field 10 Rmiddot37 Scr jmiddot111809
Lab 10 0911214-2
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml Moisture NfA QCBatchID VL091125-4middot5 Final Volume 10 ml
Date Collected 18middotNov-09 Run 10 VL091125-4A Result Units UGfL Date Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Analysis ReqCode 104 Date Analyzed 25middotNov-09 Basis As Received Prep Method SW5030 Rev C File Name 028045
CASNO Target Analyte Dilution Factor
Result Reporting Limit
MOL Result Qualifier
EPA Qualifier
75-71-8 DICHLORODIFLUOROMETHANE 1 05 05 017 U
74-87-3 CHLOROMETHANE 1 05 05 017 U
75-01middot4 VINYL CHLORIDE 1 05 05 017 U
74-83-9 BROMOMETHANE 1 1 1 017 U
75middot00middot3 CHLOROETHANE j 05 05 017 U
75-69-4 TRICHLOROFLUOROMETHANE 1 05 05 017 U
107-02-8 ACROLEIN 1 100 100 17 U
i 75-35-4 11-DICHLOROETHENE 1 05 05 017 U
67-64middot1 ACETONE 1 10 10 33 U
74-8S-4 IODOMETHANE 1 5 5 017 U
75-15-0 CARBON DISULFIDE 1 10 10 017 U
75-09-2 METHYLENE CHLORIDE 1 1 1 017 U
156-60-5 TRANS-12-DICHLOROETHENE 1 05 05 017 U
1634-04-4 METHYL TERTIARY BUTYL ETHER 1 1 1 017 U
107-13-1 ACRYLONITRILE 1 10 10 17 U
75-34middot3 11-DICHLOROETHANE 05 05 017 U
i 108-05-4 VINYL ACETATE 1 10 10 067 U
115659-2 CISmiddot 2middotDICHLOROETHENE 1 05 05 017 U
178-933 2middotBUTANONE 1 5 5 17 U
74-97middot5 BROMOCHLOROMET HANE 1 1 1 017 U
67-66-3 CHLOROFORM 1 05 05 017 U
71-55middot6 111middotTRICHLOROETHANE 1 1 1 017 U
594-20-7 22middotDICHLOROPROPANE 1 05 05 017 U
56-23-5 CARBON TETRACHLORIDE 1 05 05 017 U
563-58-6 11middotDICHLOROPROPENE 1 05 05 017 U
107-06-2 12middotDICHL OROETHANE 1 05 05 017 U
Data Package ID VL0911214-1
Date Printed Wednesday December 022009 ALS Laboratory Group -- Fe Page 5 of 8
16
GCMS Volatiles Method SW8260_25B
Sample Results
Lab Name ALS Laboratory Group -- FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-111809(HW3 R-37 VOCs) PAR 002731703
Field 10 R-37 Scr 1-11 1809
Lab 10 0911214-2
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml
Moisture NIA QCBatchlO VL091125-4-5 Final Volume 10 ml
Date Collected 18-Nov-09 Run 10 VL091125-4A Result Units UGL
[late Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Analysis ReqCode 104 Date Analyzed 25-Nov-09
Prep Method SW5030 Rev C Basis As Received
File Name 028045
CASNO Target Analyte Dilution Factor
71-43-2 BENZENE 1
79-01-6 TRICHLOROETHENE 1
78-87-5 12-DICHLOROPROPANE 1
74-95-3 DIBROMOMETHANE 1
75-27-4 BROMODICHLOROMETHANE 1
10061-01-5 CIS-13-DICHLOROPROPENE 1
108-10-1 4-METHYL-2-PtNTANON 1
108-88-3 TOLUENE 1
10061-02-6 TRANS-13-DICHLOROPROPENE 1
79-00-5 112-TRICHLOROETHANE 1
591-78-6 2-HEXANONE 1
127-18-4 TETRACHLOROETHENE 1
142-28-9 13-DICHLOROPROPANt 1
124-48-1 DI3ROMOCHLOROMETHANE 1
106-93-4 12-DIBROMOETHANE 1
108-90-7 CHLOROBENZENE 1
OETHANE 1
- 1
LENE 1
ENE 1
ENE 1
OFORM 1
OPYlBENZENE 1
96-18-4 123-TRICHLOROPROPANE 1
79-34-5 1122-TETRACHLOROETHANE 1
108-86-1 BROMOBENZENE 1
Result Reporting Limit
05 05
05 05
05 05
05 05
05 05
05 05
5 5
025 05
05 05
05 05
10 10
05 05
05 05
1 1
1 1
05 05
05 05
05 05
1 1
05 05
05 05
05 05
05 05
2 2
05 05
05 05
MDL Result EPA Qualifier Qualifier
017 U
017 U
017 U
017 U
017 U
017 U
17 U
017 J
017 U
017 U
17 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
Data Package 10 VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- Fe Page 6 of 8
317A
17
GCMS Volatiles Method SW8260 _258
Sample Results
Lab Name ALS Laboratory Group -- FC
Work Order Number 0911214
Client Name New Mexico Environment Department 08
ClientProject 10 644-11S09(HWB R-37 VOCs) PAR 002731703
Field 10 Rmiddot37 Scr 1-111809
Lab 10 0911214-2
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml Moisture NA QCBatchlD VL091125-4-5 Final Volume 10 ml
Date Collected 18-Nov-09 Run 10 VL091125-4A Result Units UGL Date Extracted 25-Nol-09 Cleanup NONE Clean OF
Analysis ReqCode 104 Date Analyzed 25-Nov-09 Basis As Received Prep Method SW5030 Rev C File Name D28045
CASNO Target Analyte Dilution Factor
103-65-1 N-PROPYLBENZENE 1
95-49-8 2-CHLOROTOLUENE 1
108-67-8 135-TRIMETHYLBENZENE 1
106-43-4 4-CHLOROTOLUENE 1
98-06-6 TERT-BUTYLBENZENE 1
95-63-6 124-TRIMETHYLBENZENE 1
135-98-8 SEC-BUTYLBENZENE 1
i 541-73-1 13middotDICHLOROBENZENE 1
99-87-6 PmiddotISOPROPYL TOLUENE 1
106-46-7 I 14-DICHLOROBENZENE 1
104-51-8 I N-BUTYLBENZENE 1
95-50-1 l2-DICHLOROBENZENE 1
96-12-8 I 12-DIBROMO-3-CHLOROPROPANE 1
120-82-1 124-TRICHLOROBENZENE 1
87-68-3 HEXACHLOROBUT ADIENE 1
91-20-3 NAPHTHALENE 1
87-61-6 123-TRICHLOROBENZENE 1
75-05-S ACETONITRILE 1
107-05-1 ALLYL CH LORIDE 1
110-57-6 TRAN S-14-DICHLORO-2-BUTENE 1
64-17-5 ETHANOL 1
97-63-2 ETHYL METHACRYLATE 1
78-83-1 ISOBUTYL ALCOHOL 1
126-98-7 METHACRYLONITRILE 1
80-62-6 METHYL METHACRYLATE 1
107-12-0 I PROPIONITRILE 1
Result Reporting Limit
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
2 2
05 05
05 05
05 05
05 05
50 50
50 50 I 5 5
200 200
5 5
100 100
35 35
5 5
25 25
MDL
017
017
017
017
017
017
017
017
017
017
017
017
067
017
017
017
017
83
017
17
78
017
17
17
17
33
Result EPA Qualifier Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
Data Package 10 VL0911214-1
Date Printed Wednesday December 022009 ALS Laboratory Group -- Fe Page 7 of 8
LlMS Version 6317A
18
GCMS Volatiles Method SW8260_258
Sample Results
Lab Name ALS Laboratory Group bullbull FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644middot111B09(HWB R-37 VOCs) PAR 002731703
Sample Matrix WATER Prep Batch VL091125--4 Sample Aliquot 10 mlRmiddot37 Ser 1-111809 Moisture NA QCBatchlO VL091125--4-5 Final Volume 10 m
0911214-2 Date Collected 18-Nov-09 Run 10 VL091125--4A Result Units UGL Date Extracted 25-Nov-09 Cleanup NONE Clean OF 1 Date Analyzed 25-Nov-09 Basis As Received
10
Analysis ReqCode 104 Prep Method SW5030 Rev C File Name 028045
I
CASNO Target Analyte Dilution Factor
Result Reporting Limit
MDL Result Qualifier
EPA Qualifier
126-99-8 CHLOROPRENE 1 5 5 017 U
75-65-0 TERT-BUTANOL 1 100 100 33 U
108-20-3 ISOPROPYL ETHER 1 2 2 033 U
637-92-3 ETHYL TERT-BUTYL ETHER 1 2 2 033 U
994-05--8 TERT-AMYL MTHYL ETHER 1 2 2 033 U
67-72-1 HEXACHLOROETHANE 1 2 2 033 U
Surrogate Recovery
CASNO Surrogate Analyte Result Flag Spike Amount
Percent Control Recovery Limits
460-00-4 4middotBROMOFLUOROBENZENE 247 25 99 1
1868-53-7 DIBROMOFLUOROMETHANE 248 25 99 80 123
2037-26-5 TOLUENEmiddotDB 255 25 102 85 - 116
Data Package 10 VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- FC Page B of 8
LlMS Version 6317A
19
GCMS Volatiles Method SW8260_258
Laboratory Control Sample and Laboratory Control Sample Duplicate
Lab Name ALS Laboratory Group - FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-111809(HWB R-37 VOCs) PAR 002731703
Lab 10 VL091125-4LCS Sample Matrix WATER
Moisture NA Prep Batch VL091125-4
QCBatchlD VL091125-4-5
Sample Aliquot
Final Volume
10ml
10ml Date Collected NA Run 10 VL091125-4A Result Units UGIL Date Extracted 111252009 Cleanup NONE Clean OF 1 Date Analyzed 11252009 Basis NA
Prep Method SW5030C File Name 028040
CASNO
74-87-3
75-01-4
74-83-9
75-69-4
75-35-4
75-15-0
156-60-5
75-34-3
108-05-4
156-59-2
78-93-3
67 -66-3
71-55-6
i 56-23-5
107-06-2
71-43-2
79-01-6
78-87-5
75-27-4
108-88-3
79-00-5
591-78-6
127-18-4
106-93-4
108-90-7
63Q20-6
Target Analyte Spike Added
CHLOROMETHANE 10
VINYL CHLORIDE 10
BROMOMETHANE 10
TRICHLOROFLUOROMETHANE 10
11-DICHLOROETHENE 10
CARBON DISULFIDE 10
TRANS-12-DICHLOROETHENE 10
11-DICHLOROETHANE 10
VINYL ACETATE 10
CIS-12-DICHLOROETHENE 10
2middotBUTANONE 40
CHLOROFORM 10
111-TRICHL ORO ETHANE 10
CARBON TETRACHLORIDE 10
12-DICHLOROETHANE 10
BENZENE 10
TRICHLOROETHENE 10
12-DICHLOROPROPANE 10
BROMODICHLOROMETHANE 10
TOLUENE 10
112-TRICHLOROETHANE 10
2-HEXANONE 40
TETRACHLOROETHENE 10
12-DIBROMOETHANE 10
CHLOROBENZENE 10
1112-TETRACHLOROETHANE 10
LCS Reporting Result Result Limit Qualifier
932 05
863 05
943 1
908 05
96 05
95 10 J
996 05
992 05
10 10
102 05
412 5
993 05
974 1
943 05
106 05
983 05
962 05
10 05
988 05
974 05
989 05
409 10
956 05
991 1
984 05
101 05
LCS Control Rec Limits
93 49 -129
86 46 134
94 32-121
91 67 -152
96 61 -135
95 61 -140
100 70 -122
99 76 -119
100 62 182
102 75 126
103 61 -137
99 79 120
97 76 - 114
94 58middot135
106 75middot132
98 70 shy 125
96 74 121
100 81 -119
99 79 - 123
97 76 - 120
99 81 -126
102 45 168
96 56 -128
99 79 -123
98 75 -120
101 82 - 123
Data Package 10 VL0911214middot1
-Date Printed Wednesday December 02 2009 ALS Laboratory Group -- Fe Page 1 of 4
LiMS Version 6317A
20
GCMS Volatiles Method SW8260_25B
Laboratory Control Sample and Laboratory Control Sample Duplicate
Lab Name ALS Laboratory Group - FC
Work Order Number 0911214
Client Name New Mexico Envircnment Department OB
ClientProject 10 644-111809(HWB R-37 VOes) PAR 002731703
Lab 10 VL091125-4LCS Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml
Moisture NIA QCBatchlO VL091125-4-5 Final Volume 10 mi
Date Collected NA Run 10 VL091125-4A Result Units UGL Date Extracted 11252009 Cleanup NONE Clean OF 1 Date Analyzed 111252009 Basis NA
Prep Method SW5030e File Name 028040
CASNO Target Analyte Spike Added
LCS Result
Reporting Limit
Result Qualifier
LCS Rec
Control Limits
100-41-4 ETHYLBENZENE 10 981 05 98 79 -114
136777-61-2 M+P-XYLENE 20 197 1 98 81-115
95-47-6 O-XYLENE 10 101 05 101 81 -115
95-49-8 2-CHLOROTOLUENE 10 97 05 97 80 -128
541-73-1 13-DICHLOROBENZiNt 10 977 05 98 81-116
106-46-7 14-DICHLOROBENZENE 10 979 05 98 81 -119
95-50-1 12-DICHLOROBENZENE 10 987 05 99 79 - 116
91-20-3 NAPHTHALENE 10 993 05 99 69 -126
87-61-6 123-TRICHLOROBENZENE 10 999 05 100 60 -137
Data Package ID VL0911214-1
Date Printed Wecnesday December 02 2009 ALS Laboratory Group -- Fe Page 2 of 4
21
GCMS Volatiles Method SW8260_25B
Laboratory Control Sample and Laboratory Control Sample Duplicate
Lab Name ALS Laboratory Group bullbull FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-11 1809(HWB R-37 VOCs) PAR 002731703
Lab 10 VL091125middot4LCSD Sample Matrix WATER
Moisture NIA Prep Batch VL091125-4
QCBatchlD VL091125-4-5
Sample Aliquot
Final Volume
10 ml
10ml Date Collected NIA Run ID VL091125-4A Result Units UGIL Date Extracted 112512009 Cleanup NONE Clean DF 1 Date Analyzed 1112512009 Basis NIA
Prep Method SW5030C File Name 028041
CASNO Target Analyte Spike Added
LCSD Result
Reporting Limit
Result Qualifier
LCSD Rec
RPD Limit
RPD
74-87-3 CHLOROMETHANE 10 897 05 90 30 4
75-01-4 VINYL CHLORIDE 10 831 05 83 25 4
74-83-9 BROMO METHANE 10 945 1 94 25 0
75-69-4 TRICHLOROFLUOROMETHANE 10 873 05 87 22 4
75-35-4 11-DICHLOROETHENE 10 909 05 91 18 5
75-15-0 CARBON DISULFIDE 10 941 10 J 94 20 1
156-60middot5 TRANS-l2middotDICHLOROETHENE 10 961 05 96 25 4
75middot34middot3 11-DICHLOROETHANE 10 977 05 98 25 2
108-05-4 VINYL ACETATE 10 993 10 J 99 20 1
156middot59-2 CIS-12-DlCHLOROETHENE 10 995 05 99 25 3
i 78-93-3 2-BUTANONE 40 419 5 105 30 2
67-66-3 CHLOROFORM 10 985 05 99 25 1
71-55-6 lll-TRICHLOROETHANE 10 942 1 94 25 3
56-23-5 CARBON TETRACHLORIDE 10 922 05 92 25 2
107middot06-2 12middotDICHLOROETHANE 10 106 05 106 25 0
71-43middot2 BENZENE 10 971 05 97 10 1
79middot01middot6 TRICHLOROETHENE 10 939 05 94 10 2
78middot87middot5 l2middotDICHLOROPROPANE 10 101 05 101 25 1
i 75middot27-4 BROMODICHLOROMETHANE 10 992 05 99 25 0
1108-88-3 TOLUENE 10 962 05 96 9 1
I 79005 112middotTRICHLOROETHANE 10 986 05 99 25 0
591middot78middot6 2-HEXANONE 40 418 10 104 20 2
127middot18-4 TETRACHLOROETHENE 10 918 05 92 25 4
106-93-4 12middotDIBROMOETHANE 10 999 1 100 15 1
108middot90-7 CHLOROBENZENE 10 997 05 100 11 1
630-20middot6 1112-TETRACHLOROETHANE 10 101 05 101 15 0
100-41-4 ETHYLBENZENE 10 968 05 97 25 1
Data Package ID VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- FC Page 3 of 4
lIMS Version 6317 A
22
GCMS Volatiles Method SW8260_25B
Laboratory Control Sample and Laboratory Control Sample Duplicate
Lab Name ALS Laboratory 13roup -- FC
Work Order Number 0911214
Client Name New Mexico Environment Department OS
ClientProject 10 644-11 1809(HWB R-37 VOCs) PAR 002731703
Lab 10 VL091125-4LCSD Sample Matrix WATER
Moisture NA Prep Batch VL091125-4
QCBatchlO VL091125-4-5
Sample Aliquot
Final Volume
10 ml
10ml Date Collected NA Run 10 VL091125-4A Result Units UGL Date Extracted 11252009 Cleanup NONE Clean OF Date Analyzed 11252009 Basis NIA
Prep Method SW5030C File Name 028041
CASNO Target Analyte Spike Added
LCSD Result
Reporting Limit
Result Qualifier
LCSD Rec
RPD Limit
RPD
136777-61-2 M+P-XYLENE 20 193 1 97 25 2
95-47-6 O-XYLENE 10 983 05 98 25 2
95-49-8 2middotCHLOROTOLUENE 10 9A9 05 95 15 2
541-73-1 13middotDICHLOROBENZENE 10 997 05 100 25 2
106-46-7 14-DICHLOROBeNZENE 10 974 05 97 25 1
95-50middot1 12middotDICHLOROBENZeNE 10 101 05 101 25 2
91middot20-3 NAPHTHALENe 10 105 05 105 24 6
87-61-6 123-TRICHLOROBENZENE 10 102 05 102 33 3
Surrogate Recovery LCSLCSD
CASNO Target Analyte Spike Added
LCS Rec
LCS Flag
LCSD Rec
LCSD Flag
Control Limits
460middot00-4 4-BROMOFLUOROBeNZENE 25 100 100 82 - 121
1868-53middot7 DIBROMOFLUOROMeTHANE 25 101 100 80middot 123
2037middot26-5 TOLUENEmiddotD8 25 102 100 85middot 116
Data Package 10 VL0911214-
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- Fe Page 4 of 4
UMS Verslmt 6317A
23
ALS Labofaton1 Group
Environmental Division Fort Cofiins Colorado
GCMS Volatiles Case Narrative
New Mexico Environmental Department OB 644-111809(HWB R-37 VOCs) PAR -- 002731703
Work Order Number 0911214
1 This report consists of 2 water samples The samples were received cool and intact by ALS on 1120109 The vial for sample 0911214-1 contained headspace prior to analysis because it was not received headspace free into the voatiles laboratory
The samples provided for volatiles had a pH gt 2 at the time of analysis
2 These samples were prepared according to SW-846 3rd Edition procedures Specifically the water samples were prepared by purging 10 mL using purge and trap procedures based on Method 5030C
3 The samples were analyzed using GCMS with an RTX-624 RTX-VMS or equivalent capillary column according to SOP 525 Revision 14 based on SW-846 Method 8260B All positive results were quantitated against the initial calibration standards using the intemal standard technique The identification of positive results was achieved by a comparison of the retention time and mass spectrum of trle sample versus the daily calibration standard
4 All initial calibration criteria for SPCCs and CCCs were met If average response factors were used in the initial calibration RSO was 15 If linear or higher order regression calibrations were used in the initial calibration the coefficient of determination (r2) ~099
5 All initial calibrations are verified by comparing a second source standard calibration verrrication (ICV) against the calibration curve All target compounds in the second source verification had a 0 of less than 25
6 All criteria for SPCCs and CCCs were met in daily (continuing) calibration verifications (CCV)
7 Methylene chloride acetone and 2-butanone are common laboratory contaminants In order to minimize the levels of these compounds detected in the gclms analysis ALS has designated its volatile laboratory as a restricted access area In addition the laboratory has been equipped with a dedicated air intake and exhaust system that operates under positive pressure in order to
1
minimize cross contamination of these compounds Due to fluctuations in ambient laboratory conditions reported sample values for common laboratory contaminants may be due to lab contamination even if the compound in question is not detected in the associated method blankmiddot
All method blank criteria were met
8 All laboratory control sample and laboratory control sample duplicate recoveries and RPDs were within the acceptance criteria
9 Since a sample from this order number was not the selected qualITy control (QC) sample matrix specific QC results are not included in this report
10 The samples were analyzed within the established holding time
11 All surrogate recoveries were within acceptance criteria
12 All internal standard recoveries were within acceptance criteria
14 Manual integrations are performed when needed to provide consistent and defensible data following the guidelines in SOP 939 ReVision 3
The data contained in the following report have been reviewed and approved by the personnel listed below In addition ALS certifies that the analyses reported herein are true complete and correct within the limits of the methods employed
n-o3-o5Sha~JobeS Date Organics Primary Data Reviewer
l~-O 1-01TAamp1~Orga~cs Final Data Reviewer Date
2
ALS Data Qualifier Flags Chromatography and Mass Spectrometry
U or NO This flag indicates that the compound was analyzed for but not detected
J This flag indicates an estimated value This flag is used as follows (1) when estimating a concentration for tentatively identified compounds (TICs) where a 11 response is assumed (2) when the mass spectral and retention time data indicate the presence of a compound that meets the volatile and semivolatile GCMS identification criteria and the result is less than the reporting limit (RL) but greater than the method detection limit (MOL) (3) when the retention time data indicate the presence of a compound that meets the GC identification criteria and the result is less than the RL but greater than the MOL and (4) the reported value is estimated
B This flag is used when the analyte is detected in the associated method blank as well as in the sample It indicates probable blank contamination and warns the data user This flag shall be used for a tentatively identified compound (TIC) as well as for a positively identified target compound
E This flag identifies compounds whose concentration exceeds the upper level of the calibration range
A This flag indicates that a tentatively identified compound is a suspected aldol-condensation product
X This flag indicates that the analyte was diluted below an accurate quantitation level
This flag indicates that a spike recovery is equal to or outside the control criteria used
+ This flag indicates that the relative percent difference (RPO) equals or exceeds the control criteria
3
ALS Laboratory Group -- Fe Sample Number(s) Cross-Reference Table
Paragon OrderNum 0911214 Client Name New Mexico Environment Department OB
Client Project Name 644-111809(HWB R-37 VOCs) PAR Client Project Number 002731703
Client PO Number 06-667-55-01754
Client Sample Number
Lab Sample Number
COC Number Matrix Date Collected
Time Collected
R-37 Scr 2-1 11809 0911214-1 WATER 18-Nov-09 1555 R-37 Scr 1-111809 0911214-2 WATER 18-Nov-09 1744
Page 1 of 1 ALS Laboratory Group -- Fe Date Printed Wednesday December 02 2009 LlMS Version 6317 A
4
Chain of Custody Record 1)11 d- I 4 SHIP To MAil REPORT TO HtitilJft BILL TO
Kim GrJOZOW KC [)il-e Cobra
NMFOmiddotDOE Overslghl Bwe3u 50S firt1middottoOB Hew Meico FnlliTtl1 Dep1 HaVIdthJS VvaMe Bureau ~orl Collins CO 80524shy
1UH Diamold Drive Stille 8 90S Rodeo P3M( D~lIe Ea~ Bldg(970) 90middot511
lo Alarr1(1l N~Muto 87544 83113 Fe liM 87505middot25-67
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Project Number (Llib invoice USI
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644middot111809(HWB Rmiddot37 VOCs) PAR
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cI yl iComments Lanc~v fiias not~ that foe samples life not preg~-d with HCL bull
~ 4_~~~~S5 V~~~Vi~I_$ ~~~~5s~rvd __
3 4()ml glau VOA vials Non-PrlttIrv~d -----~--
OC Level Standard f 0~Y ~-t-~ (fv f_ QC Required MS MSD Bla~k
irU11 Around TieJTAT) ~_dbullr_d__~______
cJPlace X In bOK If there are less than 5 lotal sample for shipping cosls
IJl
PQf 1
---- ---- ---
ALS Laboratory GrouP - Fort Collins
CONDITIO] OF SAMPLE UPO) RECEIPT FORM
Client _-=-N--M---f-=-D________ IVorkorde No D4 J I 4 --~~~~~~------
PrO1 cc Manager L 5 lnitiais C D Date 1 -) ()- () C --~~~---------------------
1 there a cae Are the coe and bottle labels
Is the coe in agreement with samples received) of containers matrix requested anaiyses etc)
documents presen1 andor removable)
Are all aqueous samples requiring preservation preserved correctly ~- ----~-~~--- -~ -~-- ----~~~---------
volatiles)
14 Are all samples requiring no headspace (VOC GRG RSKlVIEE lb eNS radon)
free Size of bubble lt
$ Do perchlorate LCMS-MS samples have headspace (a~ least ]3 of container required)
NO
]6 Were samples checked for and free from the presence of residual chlorine (Appiicaole when PM has Indicated samples are from a chlonnated wat~ source note if field preservallor
witb sodIUm tlllosulfate wa not observed)
17 Were the lljIV~IOU on ice
IS Were cooler temperatures measured at 01-60degC IR ~Illl used 2
Coole I---
Temperature (C) 3 ~
NO
NO
NO
NO
NO
NO
NO
No of custodv seals Ol~ cooler 0 OOT ---- --- --- --l Surveyl EXlemlli flRhr n~ading I i AcceplanCfiltnforma tlon Background ulJhr reading 3 Were eX lema uRhf readl1lf5 tW(l tm bnckl1Ound and withllllxyr acceptance criterill
Additional Iuformation OVIDE DETAILS BELOW FOR A ND RESPONSE TO ANY (UESTION A80VE EXCEPT 1 ANI) 16
If applicable was the clienl contacted) YES i NO I
Project Manager Signature I Date
(1 Gun 112 Oaktoll SN 2992250020 jmiddot0066 lR Gun lie Oakton S~ 23n220101middot0(J02
Form 201r22gt15 (61109) Page 1 of _1
6
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kt1UoorFdrStNil~~Your Internal Billing Reference Enveiope Pol _
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Address Wa clMOfdeiinrto POlwuscrPo ZIP CGlJla
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6 Special Handlmlllilld Delivery SignalUlll Options
~~~l~__Iint_dUSabulld)IjhL Indirect Sianarurc ttMtrttISMIllFtdlHrtS ~~tlltl~ eeelMllnllrl$ICIIltctdeiMv-kll lt_noaIllaIMInt$ ~
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7
GCMS Volatiles Method SW8260 _25B
Method Blank
Lab Name ALS Laboratory Group bullbull FC
Work Order Number 0911214
Client Name New Mexico Environment Department DB
ClientProject 10 644-111809(HWB Rmiddot37 VOCs) PAR 002731703
Lab 10 VL091125-4MB Sample Matrix WATER
Moisture NA Prep Batch VL091125-4
QCBatchlO VL091125-4-5
Sample Aliquot
Final Volume
10 ml
10 ml Date Collected NA Run 10 VL091125-4A Result Units UGL Date Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Date Analyzed 25middotNov-09 Basis NA
File Name 028043
CASNO Target Analyte DF
75-71-8 DICHLORODIFLUOROMETHANE
74-87-3 CHLOROMETHANE
75-01-4 VINYL CHLORIDE
74-83-9 BROMOMETHANE
75-00-3 CHLOROETHANE
75-69-4 TRICHLOROFLUOROMETHANE
107-02-8 ACROLEIN
75-35-4 11middotDICHLOROETHENE
67-64-1 ACETONE
74-88-4 IODOMETHANE
75-15-0 CARBON DISULFIDE
METHYLEN E CHLORIDE 75-09-2
156-60-5 TRANS-12middotDICHLOROETHENE
1634-04-4 METHYL TERTIARY BUTYL ETHER
107-13-1 ACRYLONITRILE
75-34-3 11-DICHLOROETHANE
108-05-4 VINYL ACETATE
156-59middot2 CIS-12middotDICHLOROETHENE
78-93-3 2middotBUTANONE
~ BROMOCHLOROMETHANE
67-66-3 CHLOROFORM
71-55-6 111middot TRICHLOROETHANE
594-20-7 22middotDICHLOROPROPANE
56-23-5 CARBON TETRACHLORIDE
563-58-6 11middotDICHLOROPROPENE
107-06middot2 l2middotDICHLOROETHAN E
71-43-2 BENZENE
79-01-6 TRICHLOROETHENE
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Result Reporting Limit
05 05
05 05
05 05
1 1
05 05
05 05
100 100
05 05
10 10
5 5
10 10
1 1
05 05
1 1
10 10
05 05
10 10
05 05
5 5
1 1
05 05
1 1
05 05
05 05
05 05
05 05
05 05
05 05
MDL Result EPA Qualifier Qualifier
017 U
017 U
017 U
017 U
017 U
017 U
17 U
017 U
33 U
017 U
017 U
017 U
017 U
017 U
17 U
017 U
067 U
017 U
17 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
Data Package 10 VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- Fe Page 1 of 4
llMS Version 6317 A
8
GCMS Volatiles Method SW8260 _25B
Method Blank
Lab Name ALS Laboratory Group -- FC
Work Order Number 0911214
Client Name New Mexico Environment Department 08
ClientProject 10 644-111809(HWEI R-37 voes) PAR 002731703
Lab 10 VL091125-4MB Sample Matrix WATER
Moisture NIA Prep Batch VL091125-4
QCBatchIO VL091125-4-5
Sample Aliquot
Final Volume
10 ml
10 ml Oate Collected NIA Run 10 VL091125-4A Result Units UGL Oate Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Date Analyzed 25-Nov-09 Basis NIA
File Name 028043
CASNO Target Analyte OF Result Reporting Limit
MOL Result Qualifier
EPA Qualifier
78-87-5 12middotDICHLOROPROPANE 1 05 05 017 U
74-95-3 DIBROMOMETHANE 1 05 05 017 U
75-27-4 BROMODICHLOROMETHANE 1 05 05 017 U
10061-01-5 CISmiddot13middotDICHLOROPROPENE 1 05 05 017 U
108-10-1 4-METHYL-2-PENT ANONE 1 5 5 17 U
108-88-3 TOLUENE 1 05 05 017 U
10061-02-6 TRANS-13-DICHLOROPROPENE 1 05 05 017 U
79-00-5 112-TRICHLOROETHANE 1 05 05 017 U
591-78-6 2-HEXANONE 1 10 10 17 U
127-18-4 TETRACHLOROETHENE 1 05 05 017 U
142-28-9 13-DICHLOROPROPANI 1 05 05 017 U
124-48-1 DIBROMOCHLOROMETHANE 1 1 1 017 U
106-93-4 12-DIBROMOETHANE 1 1 1 017 U
108-90-7 CHLOROBENZENE 1 05 05 017 U
630-20-6 1112-TETRACHLOROETHANE 1 05 05 017 U
100-41-4 ETHYLBENZENE 1 05 05 017 U
136777-61-2 M+P-XYLENE 1 1 1 017 U
95-47-6 O-XYLENE 1 05 05 017 U
100-42-5 STYRENE 1 05 05 017 U
75-25-2 BROMOFORM 1 05 05 017 U
98-82-8 ~YLBENZENE 1 05 05 017 U
96-18-4 123-TRICHLOROPROPANE 1 2 2 017 U
79-34-5 1122middot TETRACHLOROETHANE 1 05 05 017 U
108-86-1 BROMOBENZENE 1 05 05 017 U
103-65-1 N-PROPYLBENZENE 1 05 05 017 U
95-49-8 2-CHLOROTOLUENE 1 05 05 017 U
108-67-8 135-TRIMETHYLBENZENE 1 05 05 017 U
106-43-4 4-CHLOROTOLUENE 1 05 05 017 U
Data Package 10 VL0911214-1
Date Printed Wednesday December n 2009 AlS Laboratory Group -- FC Page 2 of 4
lMS VeCSiOIY 6317A
9
GCMS Volatiles Method SW8260 _258
Method Blank
Lab Name ALS Laboratory Group - FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-111B09(HWB R-37 VOCs) PAR 002731703
Lab 10 VL091125-4MB Sample Matrix WATER
Moisture NIA
Prep Batch VL091125-4
QCBatchlD VL091125-4-5
Sample Aliquot
Final Volume
10 ml
10 ml
Date Collected NIA Run ID VL091125-4A Result Units UGL
Date Extracted 25-Nov-09 Cleanup NONE Clean DF 1
Date Analyzed 25-Nov-09 Basis NA
File Name 028043
CASNO Target Analyte OF Result Reporting Limit
MOL Result Qualifier
EPA Qualifier
98-06-6 TERT-BUTYLBENZENE 1 05 05 017 U
95-63-6 124-TRIMETHYLBENZENE 1 05 05 017 U
135-98-8 SEC-BUTYLBENZENE 1 05 05 017 U
541-73-1 13-DlCHLOROBENZENE 1 05 05 017 U
99-87-6 P-ISOPROPYLTOLUENE 1 05 05 017 U
106-46-7 1 A-DICHLOROBENZENE 1 05 05 017 U
104-51-8 N-BUTYLBENZENE 1 05 05 017 U
95-50-1 12-DICHLOROBENZENE 1 05 05 017 U
96-12-B 12-DIBROMO-3-CHLOROPROPANE 1 2 2 067 U
120-82-1 124-TRiCHLOROBENZENE 1 05 05 017 U
87-68-3 HEXACHLOROBUTADIENE 1 05 05 017 U
91-20-3 NAPHTHALENE 1 05 05 017 U
87-61-6 123-TRICHLOROBENZENE 1 05 05 017 U
75-05-B ACETONITRILE 1 50 50 83 U
107-05-1 ALLYL CHLORIDE 1 50 50 017 U
110-57-6 TRANS-14-DICHLORO-2-BUTENE 1 5 5 17 U
64-17-5 ETHANOL 1 200 200 78 U
97-63-2 ETHYL METHACRYLATE 1 5 5 017 U
78-83-1 ISOBUTYL ALCOHOL 1 100 100 17 U
126-98-7 METHACRYLONITRILE 1 35 35 17 U
80-62-6 METHYL METHACRYLATE 1 5 5 17 U
107-12-0 PROPIONITRILE 1 25 25 33 U
126-99-8 CHLOROPRENE 1 5 5 017 U
75-65-0 TERT-BUTANOL 1 100 100 33 U
108-20-3 ISOPROPYL ETHER 1 2 2 033 U
637-92-3 ETHYL TERT-BUTYL ETHER 1 2 2 033 U
994-05-8 TERT-AMYL METHYL ETHER 1 2 2 033 U
67-72-1 HEXACHLOROETHANE 1 2 2 033 U
Data Package 10 VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -~ Fe Page 3 of 4
LlMS Version 6317 A
10
GCMS Volatiles Method SW8260 _258
Method Blank
Lab Name ALS Laboratory Group -- FC
Work Order Number 0911214
Client Name New Mexico Envirmment Department OB
ClientProject 10 644-111809(HWB R-37 VOCs) PAR 002731703
Lab 10 VL091125-4MB Sample Matrix WATER
Moisture NIA Prep Batch VL091125-4
QCBatchlO VL091125-4-5
Sample Aliquot
Final Volume
10 m
10m Date Collected NIA Run 10 VL091125-4A Result Units UGIL Date Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Date Analyzed 25-Nov-09 BasisNIA
File Name 028043
CASNO Target Analyte Result Reporting MOL Result EPAOF Limit Qualifier Qualifier
Surrogate Recovery
CASNO Surrogate Analyte Result Flag Spike Amount
Percent Recovery
Control Limits
460-00-4 4-BROMOFLUOROBENZENE 25 25 100 82 - 121
1868-53-7 DIBROMOFLUOROMETHANE 248 25 99 80 - 123
2037-26-5 TOLUENE-D8 26 25 104 85 - 116
Data Package 10 VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- FC Page 4 of4
LlMS Version 6317A
11
GCMS Volati les Method SW8260 _258
Sample Results
Lab Name ALS Laboratory Group -- FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-111809(HWB R-37 VOCs) PAR 002731703
Field 10 Rmiddot37 Ser 2middot111809
Lab 10 0911214middot1
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml
Moisture NA QCBatchlO VL091125-4-5 Final Volume 10mi Date Collected 18-Nov-09 Run 10 VL091125-4A Result Units UGL
Date Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Analysis ReqCode 104 Date Analyzed 25-Nov-09
Prep Method SW5030 Rev C Basis As Received
File Name 028044
CASNO Target Analyte Dilution Factor
75-71-8 DICHLORODIFLUOROMETHANE 1
74middot87-3 CHLOROMETHANE 1
75-01-4 VINYL CHLORIDE 1
74-83-9 BROMOMETHANE 1
75-00-3 CHLOROETHANE 1
75-69-4 TRICHLOROFLUOROMETHANE 1
107-02-8 ACROLEIN 1
75-35-4 11middotDICHLOROETHENE 1
67-64-1 ACETONE 1
74-88-4 IODOMETHANE 1
75-15-0 CARBON DISULFIDE 1
75-09-2 METHYLENE CHLORIDE 1
156-60-5 TRANSmiddot12middotDICHLOROETHENE 1
1634-04-4 METHYL TERTIARY BUTYL ETHER 1
107-13-1 ACRYLONITRILE 1
75-34-3 1-DICHLOROETHANE 1
i 108-05-4 VINYL ACETATE 1
156-59-2 CIS-12middotDICHLOROETHENE 1
78-93-3 2-BUTANONE 1
74-97-5 BROMOCHLOROMETHANE 67-66-3 CHLOROFORM 1
71-55-6 11-TRICHLOROETHANE 594-20-7 22-DICHLOROPROPANE 56-23-5 CARBON TETRACHLORIDE 563-58-6 -DICHLOROPROPENE 107-06-2 2-DICHLOROETHANE
Result Reporting Limit
05 05
05 05
05 05
1 1
05 05
05 05
100 100
05 05
10 10
5 5
10 10
1 1
05 05
1 1
10 10
05 05
10 10
05 05
5 5
1 1
05 05
1 1
05 05
05 05
05 05
05 05
MOL Result EPA Qualifier Qualifier
017 U
017 U
017 U
017 U
017 U
017 U
17 U
017 U
33 U
017 U
017 U
017 U
017 U
017 U
17 U
017 U
067 U
017 U
17 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
Data Package ID VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- Fe Page 1 of 8
UMS Version 6317A
12
GCMS Volatiles Method SW8260_25B
Sample Results
Lab Name ALS Laboratory Group - FC
Work Order Number 0911214
Client Name New Mexico nvironment Department OB
ClientProject 10 644-111809(HWB R-37 VOCs) PAR 002731703
Field 10 R-37 Scr 2-111809
Lab 10 0911214-1
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10ml
Moisture NA QCBatchlD VL091125-4-5 Final Volume 10ml
Date Collected l8-Nov-09 Run 10 VL091125-4A Result Units UGL
Date Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Analysis ReqCode 104 Date Analyzed 25-Nov-09 Basis As Received
Prep Method SW5030 Rev C File NameD28044
CASNO Target Analyte Dilution Factor
Result Reporting Limit
MDL Result Qualifier
EPA Qualifier
I
71-43-2 BENZENE 1 05 05 017 U
79-01-6 TRICHLOROETHENE 1 05 05 017 U
78-87-5
74middot95-3
75-27-4
10061-01-5
108middot10middot1
108middot88-3
10061-02middot6
79-00-5
591-78-6
12-DICHLOROPROPANE
DIBROMOMETHANE
BROMODCHLOROMETHANE
CIS-13-DICHLOROPROPEI~E
4-METHYL-2-PENTANONE
TOLUENE
TRANS-13-DICHLOROPROPENE
112-TRICHLOROETHANE
2-HEXANONE
1
1
1
1
1
1
1
1
1
05
05
05
05
5
031
05
05
10
05
05
05
05
5
05
05
05
10
017
017
017
017
17
017
017
017
17
U
U
U
U
U
J
U
U
U
127-18-4
142-28-9
124-48-1
106-93-4
108-90-7
630-20-6
100-41-4
136777-61-2
95-47-6
100-42middot5
75-25-2
98-82middot8
96-18-4
79-34-5
108-86-1
TETRACHLOROETHENE
13-DICHLOROPROPANE
DIBROMOCHLOROMETHANE
12-DIBROMOETHANE
CHLOROBENZENE
11 12-TETRACHLOROETHANE
ETHYLBENZENE
M+PmiddotXYLENE
OmiddotXYLENE
STYRENE
BROMOFORM
ISOPRO PYLBENZENE
123middotTRICHLOROPROPANE
1122-TETRACHLOROETHANE
BROMOBENZENE
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
05
05
1
1
05
05
05
1
05
05
05
05
2
05
05
05
05
1
1
05
05
05
1
05
05
05
05
2
05
05
017
017
017
017
017
017
017
017
017
017
017
017
017
017
017
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
i
Data Package 10 VL0911214-1
Date Printed Wednesday December 022009 AlS laboratory Group bullbull Fe Page 2 of 8
UMS Version 6317A
13
GCMS Volatiles Method SW8260_258
Sample Results
Lab Name ALS Laboratory Group bullbull FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject ID 644-111809(HWB R-37 VOCs) PAR 002731703
Field 10 R-37 Sor 2-111809
Lab ID 0911214middot1
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml
Moisture NA QCBatchlD VL091125-4-5 Final Volume 10 ml
Date Collected 18-Nov-09 Run ID VL091125-4A Result Units UGL
Date Extracted 25-Nov-09 Cleanup NONE Clean DF 1
Analysis ReqCode 104 Date Analyzed 25-Nov-09 Basis As Received
Prep Method SW5030 Rev C File Name 028044
CASNO Target Analyte Dilution Factor
103-65-1 NmiddotPROPYLBENZENE 1
95-49-8 2-CHLOROTOLUENE 1
108-67-8 135-TRIMETHYLBENZENE 1
106-43-4 4-CHLOROTOLUENE 1
98-06-6 TER I-BUTYLBENZENE 1
95-63-6 124-TRIMETHYLBENZENE 1
135-98-8 SEC-BUTYLBENZENE 1
541-73-1 13-OICHLOROBENZENE 1
99-87-6 P-ISOPROPYLTOLUENE 1
106-46-7 lA-DICHLOROBENZENE 1
104-51-8 N-BUTYLBENZENE 1
95-50-1 12-DICHLOROBENZENE 1
96-12-8 l2-DIBROMOmiddot3-CHLOROPROPANE 1
120-82-1 12A-TRICHLOROBENZENE 1
187-68-3 HEXACHLOROBUTADIENE 1
91-20-3 NAPHTHALENE 1
87-61middot6 123-TRICHLOROBENZENE 1
75-05-8 ACETONITRILE 1
107middot05middot1 ALLYL CHLORIDE 1
110-57-6 TRANS-14-DICHLORO-2-BUTENE 1
164-17-5 ETHANOL 1
97-63-2 ETHYL METHACRYLATE 1
78-83-1 ISOBUTYL ALCOHOL 1
126-98-7 METHACRYLONITRILE 1
80-62-6 METHYL METHACRYLATE 1
107-12-0 PROPIONITRILE 1
Result Reporting Limit
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
2 2
05 05
05 05
05 05
05 05
50 50
50 50
5 5
200 200
5 5
100 100
35 35
5 5
25 25
MDL Result EPA Qualifier Qualifier
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
067 U
017 U
017 U
017 U
017 U
83 U
017 U
U u 78 U
017 U
17 U
17 U
17 U
33 U
Data Package 10 VL0911214-1
Date Printed Wednesday December 022009 ALS Laboratory Group MM Fe Page 3 of 8
LlMS VerSion 6317A
14
GCMS Volati las Method SW8260_258
Sample Results
Lab Name ALS Laboratory Group - FC
Work Order Number 0911214
Client Name New Mexico Environment Department 08
ClientProject 10 644-111B09(HWB R-37 VOGs) PAR 002731703
Field 10 R-37 Ser 2-111809 Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10ml
Lab 10 0911214-1 Moisture NA
Date Collected 1B-Nov-09 QCBatchlO VL091125-4-5
Run 10 VL091125-4A
Final Volume 10ml
Result Units UGIL Date Extracted 25-Nov-09 Cleanup NONE Clean OF
Analysis ReqCode 104 Date Analyzed 25-Nov-09
Prep Method SW5030 Rev G Basis As Received
File Name 028044
CASNO Target Analyte Dilution Factor
Result Reporting Limit
MDL Result Qualifier
EPA Qualifier
126-99-8 CHLOROPRENE 1 5 5 017 U
75-65-0 TERT-BUTANOL 1 100 100 33 U
108-20-3 ISOPROPYL ETHER 1 2 2 033 U
637-92-3 ETHYL TERT-BUTYL ETHER 1 2 2 033 U
994-05-8 TERT-AMYL METHYL ETHER 1 2 2 033 U
67-72-1 HEXACHLOROETHANE 1 2 2 033 U
Surrogate Recovery
CASNO Surrogate Analyte Result Flag Spike Amount
Percent Recovery
Control Limits
460-00-4 4-BROMOFLUOHOBENZENE 246 25 98 82 - 121
1868-53-7 DIBROMOFLUOHOMETHANE 248 25 99 BO - 123
2037-26-5 TOLUENE-DB 258 25 103 85middot116
Data Package 10 VL0911214-1
Date Printed Wednesday December 022009 ALS Laboratory Group bullbull FC Page 4 of 8
LIMS Version 0317 A
15
GCMS Volati les Method SW8260_25B
Sample Results
Lab Name ALS Laboratory Group -- FC
Worlt Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-111809(HWB Rmiddot37 VOCs) PAR 002731703
Field 10 Rmiddot37 Scr jmiddot111809
Lab 10 0911214-2
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml Moisture NfA QCBatchID VL091125-4middot5 Final Volume 10 ml
Date Collected 18middotNov-09 Run 10 VL091125-4A Result Units UGfL Date Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Analysis ReqCode 104 Date Analyzed 25middotNov-09 Basis As Received Prep Method SW5030 Rev C File Name 028045
CASNO Target Analyte Dilution Factor
Result Reporting Limit
MOL Result Qualifier
EPA Qualifier
75-71-8 DICHLORODIFLUOROMETHANE 1 05 05 017 U
74-87-3 CHLOROMETHANE 1 05 05 017 U
75-01middot4 VINYL CHLORIDE 1 05 05 017 U
74-83-9 BROMOMETHANE 1 1 1 017 U
75middot00middot3 CHLOROETHANE j 05 05 017 U
75-69-4 TRICHLOROFLUOROMETHANE 1 05 05 017 U
107-02-8 ACROLEIN 1 100 100 17 U
i 75-35-4 11-DICHLOROETHENE 1 05 05 017 U
67-64middot1 ACETONE 1 10 10 33 U
74-8S-4 IODOMETHANE 1 5 5 017 U
75-15-0 CARBON DISULFIDE 1 10 10 017 U
75-09-2 METHYLENE CHLORIDE 1 1 1 017 U
156-60-5 TRANS-12-DICHLOROETHENE 1 05 05 017 U
1634-04-4 METHYL TERTIARY BUTYL ETHER 1 1 1 017 U
107-13-1 ACRYLONITRILE 1 10 10 17 U
75-34middot3 11-DICHLOROETHANE 05 05 017 U
i 108-05-4 VINYL ACETATE 1 10 10 067 U
115659-2 CISmiddot 2middotDICHLOROETHENE 1 05 05 017 U
178-933 2middotBUTANONE 1 5 5 17 U
74-97middot5 BROMOCHLOROMET HANE 1 1 1 017 U
67-66-3 CHLOROFORM 1 05 05 017 U
71-55middot6 111middotTRICHLOROETHANE 1 1 1 017 U
594-20-7 22middotDICHLOROPROPANE 1 05 05 017 U
56-23-5 CARBON TETRACHLORIDE 1 05 05 017 U
563-58-6 11middotDICHLOROPROPENE 1 05 05 017 U
107-06-2 12middotDICHL OROETHANE 1 05 05 017 U
Data Package ID VL0911214-1
Date Printed Wednesday December 022009 ALS Laboratory Group -- Fe Page 5 of 8
16
GCMS Volatiles Method SW8260_25B
Sample Results
Lab Name ALS Laboratory Group -- FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-111809(HW3 R-37 VOCs) PAR 002731703
Field 10 R-37 Scr 1-11 1809
Lab 10 0911214-2
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml
Moisture NIA QCBatchlO VL091125-4-5 Final Volume 10 ml
Date Collected 18-Nov-09 Run 10 VL091125-4A Result Units UGL
[late Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Analysis ReqCode 104 Date Analyzed 25-Nov-09
Prep Method SW5030 Rev C Basis As Received
File Name 028045
CASNO Target Analyte Dilution Factor
71-43-2 BENZENE 1
79-01-6 TRICHLOROETHENE 1
78-87-5 12-DICHLOROPROPANE 1
74-95-3 DIBROMOMETHANE 1
75-27-4 BROMODICHLOROMETHANE 1
10061-01-5 CIS-13-DICHLOROPROPENE 1
108-10-1 4-METHYL-2-PtNTANON 1
108-88-3 TOLUENE 1
10061-02-6 TRANS-13-DICHLOROPROPENE 1
79-00-5 112-TRICHLOROETHANE 1
591-78-6 2-HEXANONE 1
127-18-4 TETRACHLOROETHENE 1
142-28-9 13-DICHLOROPROPANt 1
124-48-1 DI3ROMOCHLOROMETHANE 1
106-93-4 12-DIBROMOETHANE 1
108-90-7 CHLOROBENZENE 1
OETHANE 1
- 1
LENE 1
ENE 1
ENE 1
OFORM 1
OPYlBENZENE 1
96-18-4 123-TRICHLOROPROPANE 1
79-34-5 1122-TETRACHLOROETHANE 1
108-86-1 BROMOBENZENE 1
Result Reporting Limit
05 05
05 05
05 05
05 05
05 05
05 05
5 5
025 05
05 05
05 05
10 10
05 05
05 05
1 1
1 1
05 05
05 05
05 05
1 1
05 05
05 05
05 05
05 05
2 2
05 05
05 05
MDL Result EPA Qualifier Qualifier
017 U
017 U
017 U
017 U
017 U
017 U
17 U
017 J
017 U
017 U
17 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
Data Package 10 VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- Fe Page 6 of 8
317A
17
GCMS Volatiles Method SW8260 _258
Sample Results
Lab Name ALS Laboratory Group -- FC
Work Order Number 0911214
Client Name New Mexico Environment Department 08
ClientProject 10 644-11S09(HWB R-37 VOCs) PAR 002731703
Field 10 Rmiddot37 Scr 1-111809
Lab 10 0911214-2
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml Moisture NA QCBatchlD VL091125-4-5 Final Volume 10 ml
Date Collected 18-Nov-09 Run 10 VL091125-4A Result Units UGL Date Extracted 25-Nol-09 Cleanup NONE Clean OF
Analysis ReqCode 104 Date Analyzed 25-Nov-09 Basis As Received Prep Method SW5030 Rev C File Name D28045
CASNO Target Analyte Dilution Factor
103-65-1 N-PROPYLBENZENE 1
95-49-8 2-CHLOROTOLUENE 1
108-67-8 135-TRIMETHYLBENZENE 1
106-43-4 4-CHLOROTOLUENE 1
98-06-6 TERT-BUTYLBENZENE 1
95-63-6 124-TRIMETHYLBENZENE 1
135-98-8 SEC-BUTYLBENZENE 1
i 541-73-1 13middotDICHLOROBENZENE 1
99-87-6 PmiddotISOPROPYL TOLUENE 1
106-46-7 I 14-DICHLOROBENZENE 1
104-51-8 I N-BUTYLBENZENE 1
95-50-1 l2-DICHLOROBENZENE 1
96-12-8 I 12-DIBROMO-3-CHLOROPROPANE 1
120-82-1 124-TRICHLOROBENZENE 1
87-68-3 HEXACHLOROBUT ADIENE 1
91-20-3 NAPHTHALENE 1
87-61-6 123-TRICHLOROBENZENE 1
75-05-S ACETONITRILE 1
107-05-1 ALLYL CH LORIDE 1
110-57-6 TRAN S-14-DICHLORO-2-BUTENE 1
64-17-5 ETHANOL 1
97-63-2 ETHYL METHACRYLATE 1
78-83-1 ISOBUTYL ALCOHOL 1
126-98-7 METHACRYLONITRILE 1
80-62-6 METHYL METHACRYLATE 1
107-12-0 I PROPIONITRILE 1
Result Reporting Limit
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
2 2
05 05
05 05
05 05
05 05
50 50
50 50 I 5 5
200 200
5 5
100 100
35 35
5 5
25 25
MDL
017
017
017
017
017
017
017
017
017
017
017
017
067
017
017
017
017
83
017
17
78
017
17
17
17
33
Result EPA Qualifier Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
Data Package 10 VL0911214-1
Date Printed Wednesday December 022009 ALS Laboratory Group -- Fe Page 7 of 8
LlMS Version 6317A
18
GCMS Volatiles Method SW8260_258
Sample Results
Lab Name ALS Laboratory Group bullbull FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644middot111B09(HWB R-37 VOCs) PAR 002731703
Sample Matrix WATER Prep Batch VL091125--4 Sample Aliquot 10 mlRmiddot37 Ser 1-111809 Moisture NA QCBatchlO VL091125--4-5 Final Volume 10 m
0911214-2 Date Collected 18-Nov-09 Run 10 VL091125--4A Result Units UGL Date Extracted 25-Nov-09 Cleanup NONE Clean OF 1 Date Analyzed 25-Nov-09 Basis As Received
10
Analysis ReqCode 104 Prep Method SW5030 Rev C File Name 028045
I
CASNO Target Analyte Dilution Factor
Result Reporting Limit
MDL Result Qualifier
EPA Qualifier
126-99-8 CHLOROPRENE 1 5 5 017 U
75-65-0 TERT-BUTANOL 1 100 100 33 U
108-20-3 ISOPROPYL ETHER 1 2 2 033 U
637-92-3 ETHYL TERT-BUTYL ETHER 1 2 2 033 U
994-05--8 TERT-AMYL MTHYL ETHER 1 2 2 033 U
67-72-1 HEXACHLOROETHANE 1 2 2 033 U
Surrogate Recovery
CASNO Surrogate Analyte Result Flag Spike Amount
Percent Control Recovery Limits
460-00-4 4middotBROMOFLUOROBENZENE 247 25 99 1
1868-53-7 DIBROMOFLUOROMETHANE 248 25 99 80 123
2037-26-5 TOLUENEmiddotDB 255 25 102 85 - 116
Data Package 10 VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- FC Page B of 8
LlMS Version 6317A
19
GCMS Volatiles Method SW8260_258
Laboratory Control Sample and Laboratory Control Sample Duplicate
Lab Name ALS Laboratory Group - FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-111809(HWB R-37 VOCs) PAR 002731703
Lab 10 VL091125-4LCS Sample Matrix WATER
Moisture NA Prep Batch VL091125-4
QCBatchlD VL091125-4-5
Sample Aliquot
Final Volume
10ml
10ml Date Collected NA Run 10 VL091125-4A Result Units UGIL Date Extracted 111252009 Cleanup NONE Clean OF 1 Date Analyzed 11252009 Basis NA
Prep Method SW5030C File Name 028040
CASNO
74-87-3
75-01-4
74-83-9
75-69-4
75-35-4
75-15-0
156-60-5
75-34-3
108-05-4
156-59-2
78-93-3
67 -66-3
71-55-6
i 56-23-5
107-06-2
71-43-2
79-01-6
78-87-5
75-27-4
108-88-3
79-00-5
591-78-6
127-18-4
106-93-4
108-90-7
63Q20-6
Target Analyte Spike Added
CHLOROMETHANE 10
VINYL CHLORIDE 10
BROMOMETHANE 10
TRICHLOROFLUOROMETHANE 10
11-DICHLOROETHENE 10
CARBON DISULFIDE 10
TRANS-12-DICHLOROETHENE 10
11-DICHLOROETHANE 10
VINYL ACETATE 10
CIS-12-DICHLOROETHENE 10
2middotBUTANONE 40
CHLOROFORM 10
111-TRICHL ORO ETHANE 10
CARBON TETRACHLORIDE 10
12-DICHLOROETHANE 10
BENZENE 10
TRICHLOROETHENE 10
12-DICHLOROPROPANE 10
BROMODICHLOROMETHANE 10
TOLUENE 10
112-TRICHLOROETHANE 10
2-HEXANONE 40
TETRACHLOROETHENE 10
12-DIBROMOETHANE 10
CHLOROBENZENE 10
1112-TETRACHLOROETHANE 10
LCS Reporting Result Result Limit Qualifier
932 05
863 05
943 1
908 05
96 05
95 10 J
996 05
992 05
10 10
102 05
412 5
993 05
974 1
943 05
106 05
983 05
962 05
10 05
988 05
974 05
989 05
409 10
956 05
991 1
984 05
101 05
LCS Control Rec Limits
93 49 -129
86 46 134
94 32-121
91 67 -152
96 61 -135
95 61 -140
100 70 -122
99 76 -119
100 62 182
102 75 126
103 61 -137
99 79 120
97 76 - 114
94 58middot135
106 75middot132
98 70 shy 125
96 74 121
100 81 -119
99 79 - 123
97 76 - 120
99 81 -126
102 45 168
96 56 -128
99 79 -123
98 75 -120
101 82 - 123
Data Package 10 VL0911214middot1
-Date Printed Wednesday December 02 2009 ALS Laboratory Group -- Fe Page 1 of 4
LiMS Version 6317A
20
GCMS Volatiles Method SW8260_25B
Laboratory Control Sample and Laboratory Control Sample Duplicate
Lab Name ALS Laboratory Group - FC
Work Order Number 0911214
Client Name New Mexico Envircnment Department OB
ClientProject 10 644-111809(HWB R-37 VOes) PAR 002731703
Lab 10 VL091125-4LCS Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml
Moisture NIA QCBatchlO VL091125-4-5 Final Volume 10 mi
Date Collected NA Run 10 VL091125-4A Result Units UGL Date Extracted 11252009 Cleanup NONE Clean OF 1 Date Analyzed 111252009 Basis NA
Prep Method SW5030e File Name 028040
CASNO Target Analyte Spike Added
LCS Result
Reporting Limit
Result Qualifier
LCS Rec
Control Limits
100-41-4 ETHYLBENZENE 10 981 05 98 79 -114
136777-61-2 M+P-XYLENE 20 197 1 98 81-115
95-47-6 O-XYLENE 10 101 05 101 81 -115
95-49-8 2-CHLOROTOLUENE 10 97 05 97 80 -128
541-73-1 13-DICHLOROBENZiNt 10 977 05 98 81-116
106-46-7 14-DICHLOROBENZENE 10 979 05 98 81 -119
95-50-1 12-DICHLOROBENZENE 10 987 05 99 79 - 116
91-20-3 NAPHTHALENE 10 993 05 99 69 -126
87-61-6 123-TRICHLOROBENZENE 10 999 05 100 60 -137
Data Package ID VL0911214-1
Date Printed Wecnesday December 02 2009 ALS Laboratory Group -- Fe Page 2 of 4
21
GCMS Volatiles Method SW8260_25B
Laboratory Control Sample and Laboratory Control Sample Duplicate
Lab Name ALS Laboratory Group bullbull FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-11 1809(HWB R-37 VOCs) PAR 002731703
Lab 10 VL091125middot4LCSD Sample Matrix WATER
Moisture NIA Prep Batch VL091125-4
QCBatchlD VL091125-4-5
Sample Aliquot
Final Volume
10 ml
10ml Date Collected NIA Run ID VL091125-4A Result Units UGIL Date Extracted 112512009 Cleanup NONE Clean DF 1 Date Analyzed 1112512009 Basis NIA
Prep Method SW5030C File Name 028041
CASNO Target Analyte Spike Added
LCSD Result
Reporting Limit
Result Qualifier
LCSD Rec
RPD Limit
RPD
74-87-3 CHLOROMETHANE 10 897 05 90 30 4
75-01-4 VINYL CHLORIDE 10 831 05 83 25 4
74-83-9 BROMO METHANE 10 945 1 94 25 0
75-69-4 TRICHLOROFLUOROMETHANE 10 873 05 87 22 4
75-35-4 11-DICHLOROETHENE 10 909 05 91 18 5
75-15-0 CARBON DISULFIDE 10 941 10 J 94 20 1
156-60middot5 TRANS-l2middotDICHLOROETHENE 10 961 05 96 25 4
75middot34middot3 11-DICHLOROETHANE 10 977 05 98 25 2
108-05-4 VINYL ACETATE 10 993 10 J 99 20 1
156middot59-2 CIS-12-DlCHLOROETHENE 10 995 05 99 25 3
i 78-93-3 2-BUTANONE 40 419 5 105 30 2
67-66-3 CHLOROFORM 10 985 05 99 25 1
71-55-6 lll-TRICHLOROETHANE 10 942 1 94 25 3
56-23-5 CARBON TETRACHLORIDE 10 922 05 92 25 2
107middot06-2 12middotDICHLOROETHANE 10 106 05 106 25 0
71-43middot2 BENZENE 10 971 05 97 10 1
79middot01middot6 TRICHLOROETHENE 10 939 05 94 10 2
78middot87middot5 l2middotDICHLOROPROPANE 10 101 05 101 25 1
i 75middot27-4 BROMODICHLOROMETHANE 10 992 05 99 25 0
1108-88-3 TOLUENE 10 962 05 96 9 1
I 79005 112middotTRICHLOROETHANE 10 986 05 99 25 0
591middot78middot6 2-HEXANONE 40 418 10 104 20 2
127middot18-4 TETRACHLOROETHENE 10 918 05 92 25 4
106-93-4 12middotDIBROMOETHANE 10 999 1 100 15 1
108middot90-7 CHLOROBENZENE 10 997 05 100 11 1
630-20middot6 1112-TETRACHLOROETHANE 10 101 05 101 15 0
100-41-4 ETHYLBENZENE 10 968 05 97 25 1
Data Package ID VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- FC Page 3 of 4
lIMS Version 6317 A
22
GCMS Volatiles Method SW8260_25B
Laboratory Control Sample and Laboratory Control Sample Duplicate
Lab Name ALS Laboratory 13roup -- FC
Work Order Number 0911214
Client Name New Mexico Environment Department OS
ClientProject 10 644-11 1809(HWB R-37 VOCs) PAR 002731703
Lab 10 VL091125-4LCSD Sample Matrix WATER
Moisture NA Prep Batch VL091125-4
QCBatchlO VL091125-4-5
Sample Aliquot
Final Volume
10 ml
10ml Date Collected NA Run 10 VL091125-4A Result Units UGL Date Extracted 11252009 Cleanup NONE Clean OF Date Analyzed 11252009 Basis NIA
Prep Method SW5030C File Name 028041
CASNO Target Analyte Spike Added
LCSD Result
Reporting Limit
Result Qualifier
LCSD Rec
RPD Limit
RPD
136777-61-2 M+P-XYLENE 20 193 1 97 25 2
95-47-6 O-XYLENE 10 983 05 98 25 2
95-49-8 2middotCHLOROTOLUENE 10 9A9 05 95 15 2
541-73-1 13middotDICHLOROBENZENE 10 997 05 100 25 2
106-46-7 14-DICHLOROBeNZENE 10 974 05 97 25 1
95-50middot1 12middotDICHLOROBENZeNE 10 101 05 101 25 2
91middot20-3 NAPHTHALENe 10 105 05 105 24 6
87-61-6 123-TRICHLOROBENZENE 10 102 05 102 33 3
Surrogate Recovery LCSLCSD
CASNO Target Analyte Spike Added
LCS Rec
LCS Flag
LCSD Rec
LCSD Flag
Control Limits
460middot00-4 4-BROMOFLUOROBeNZENE 25 100 100 82 - 121
1868-53middot7 DIBROMOFLUOROMeTHANE 25 101 100 80middot 123
2037middot26-5 TOLUENEmiddotD8 25 102 100 85middot 116
Data Package 10 VL0911214-
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- Fe Page 4 of 4
UMS Verslmt 6317A
23
minimize cross contamination of these compounds Due to fluctuations in ambient laboratory conditions reported sample values for common laboratory contaminants may be due to lab contamination even if the compound in question is not detected in the associated method blankmiddot
All method blank criteria were met
8 All laboratory control sample and laboratory control sample duplicate recoveries and RPDs were within the acceptance criteria
9 Since a sample from this order number was not the selected qualITy control (QC) sample matrix specific QC results are not included in this report
10 The samples were analyzed within the established holding time
11 All surrogate recoveries were within acceptance criteria
12 All internal standard recoveries were within acceptance criteria
14 Manual integrations are performed when needed to provide consistent and defensible data following the guidelines in SOP 939 ReVision 3
The data contained in the following report have been reviewed and approved by the personnel listed below In addition ALS certifies that the analyses reported herein are true complete and correct within the limits of the methods employed
n-o3-o5Sha~JobeS Date Organics Primary Data Reviewer
l~-O 1-01TAamp1~Orga~cs Final Data Reviewer Date
2
ALS Data Qualifier Flags Chromatography and Mass Spectrometry
U or NO This flag indicates that the compound was analyzed for but not detected
J This flag indicates an estimated value This flag is used as follows (1) when estimating a concentration for tentatively identified compounds (TICs) where a 11 response is assumed (2) when the mass spectral and retention time data indicate the presence of a compound that meets the volatile and semivolatile GCMS identification criteria and the result is less than the reporting limit (RL) but greater than the method detection limit (MOL) (3) when the retention time data indicate the presence of a compound that meets the GC identification criteria and the result is less than the RL but greater than the MOL and (4) the reported value is estimated
B This flag is used when the analyte is detected in the associated method blank as well as in the sample It indicates probable blank contamination and warns the data user This flag shall be used for a tentatively identified compound (TIC) as well as for a positively identified target compound
E This flag identifies compounds whose concentration exceeds the upper level of the calibration range
A This flag indicates that a tentatively identified compound is a suspected aldol-condensation product
X This flag indicates that the analyte was diluted below an accurate quantitation level
This flag indicates that a spike recovery is equal to or outside the control criteria used
+ This flag indicates that the relative percent difference (RPO) equals or exceeds the control criteria
3
ALS Laboratory Group -- Fe Sample Number(s) Cross-Reference Table
Paragon OrderNum 0911214 Client Name New Mexico Environment Department OB
Client Project Name 644-111809(HWB R-37 VOCs) PAR Client Project Number 002731703
Client PO Number 06-667-55-01754
Client Sample Number
Lab Sample Number
COC Number Matrix Date Collected
Time Collected
R-37 Scr 2-1 11809 0911214-1 WATER 18-Nov-09 1555 R-37 Scr 1-111809 0911214-2 WATER 18-Nov-09 1744
Page 1 of 1 ALS Laboratory Group -- Fe Date Printed Wednesday December 02 2009 LlMS Version 6317 A
4
Chain of Custody Record 1)11 d- I 4 SHIP To MAil REPORT TO HtitilJft BILL TO
Kim GrJOZOW KC [)il-e Cobra
NMFOmiddotDOE Overslghl Bwe3u 50S firt1middottoOB Hew Meico FnlliTtl1 Dep1 HaVIdthJS VvaMe Bureau ~orl Collins CO 80524shy
1UH Diamold Drive Stille 8 90S Rodeo P3M( D~lIe Ea~ Bldg(970) 90middot511
lo Alarr1(1l N~Muto 87544 83113 Fe liM 87505middot25-67
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Only)
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644middot111809(HWB Rmiddot37 VOCs) PAR
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cI yl iComments Lanc~v fiias not~ that foe samples life not preg~-d with HCL bull
~ 4_~~~~S5 V~~~Vi~I_$ ~~~~5s~rvd __
3 4()ml glau VOA vials Non-PrlttIrv~d -----~--
OC Level Standard f 0~Y ~-t-~ (fv f_ QC Required MS MSD Bla~k
irU11 Around TieJTAT) ~_dbullr_d__~______
cJPlace X In bOK If there are less than 5 lotal sample for shipping cosls
IJl
PQf 1
---- ---- ---
ALS Laboratory GrouP - Fort Collins
CONDITIO] OF SAMPLE UPO) RECEIPT FORM
Client _-=-N--M---f-=-D________ IVorkorde No D4 J I 4 --~~~~~~------
PrO1 cc Manager L 5 lnitiais C D Date 1 -) ()- () C --~~~---------------------
1 there a cae Are the coe and bottle labels
Is the coe in agreement with samples received) of containers matrix requested anaiyses etc)
documents presen1 andor removable)
Are all aqueous samples requiring preservation preserved correctly ~- ----~-~~--- -~ -~-- ----~~~---------
volatiles)
14 Are all samples requiring no headspace (VOC GRG RSKlVIEE lb eNS radon)
free Size of bubble lt
$ Do perchlorate LCMS-MS samples have headspace (a~ least ]3 of container required)
NO
]6 Were samples checked for and free from the presence of residual chlorine (Appiicaole when PM has Indicated samples are from a chlonnated wat~ source note if field preservallor
witb sodIUm tlllosulfate wa not observed)
17 Were the lljIV~IOU on ice
IS Were cooler temperatures measured at 01-60degC IR ~Illl used 2
Coole I---
Temperature (C) 3 ~
NO
NO
NO
NO
NO
NO
NO
No of custodv seals Ol~ cooler 0 OOT ---- --- --- --l Surveyl EXlemlli flRhr n~ading I i AcceplanCfiltnforma tlon Background ulJhr reading 3 Were eX lema uRhf readl1lf5 tW(l tm bnckl1Ound and withllllxyr acceptance criterill
Additional Iuformation OVIDE DETAILS BELOW FOR A ND RESPONSE TO ANY (UESTION A80VE EXCEPT 1 ANI) 16
If applicable was the clienl contacted) YES i NO I
Project Manager Signature I Date
(1 Gun 112 Oaktoll SN 2992250020 jmiddot0066 lR Gun lie Oakton S~ 23n220101middot0(J02
Form 201r22gt15 (61109) Page 1 of _1
6
4a Express Package Service _ FadEx Pnority OvernightLJ ==lr-~MClncU1
lSlIIQSATUIIDAYlltIrwIlyis$Mf(1J
middot10_ FadEx SlaMard Ovemioht fMtRallw6ftIlfTampCI v
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9439 4324
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~~oalleJl =1~~ImOt $AUROAY ftlEdOeyF1tlitNbiDrnJtin
5 Packaging -1itIcIrme-- FadEgt r- FedEgt fak FedEx Box
kt1UoorFdrStNil~~Your Internal Billing Reference Enveiope Pol _
TD
Address Wa clMOfdeiinrto POlwuscrPo ZIP CGlJla
Address
6 Special Handlmlllilld Delivery SignalUlll Options
~~~l~__Iint_dUSabulld)IjhL Indirect Sianarurc ttMtrttISMIllFtdlHrtS ~~tlltl~ eeelMllnllrl$ICIIltctdeiMv-kll lt_noaIllaIMInt$ ~
OrvlceL- OtyiclItUN186 ___ ___
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8700 9439 4324 ~rtl1~l__bPnD USA SRI
_____-----------~bull---~----- -------~~-------------------
7
GCMS Volatiles Method SW8260 _25B
Method Blank
Lab Name ALS Laboratory Group bullbull FC
Work Order Number 0911214
Client Name New Mexico Environment Department DB
ClientProject 10 644-111809(HWB Rmiddot37 VOCs) PAR 002731703
Lab 10 VL091125-4MB Sample Matrix WATER
Moisture NA Prep Batch VL091125-4
QCBatchlO VL091125-4-5
Sample Aliquot
Final Volume
10 ml
10 ml Date Collected NA Run 10 VL091125-4A Result Units UGL Date Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Date Analyzed 25middotNov-09 Basis NA
File Name 028043
CASNO Target Analyte DF
75-71-8 DICHLORODIFLUOROMETHANE
74-87-3 CHLOROMETHANE
75-01-4 VINYL CHLORIDE
74-83-9 BROMOMETHANE
75-00-3 CHLOROETHANE
75-69-4 TRICHLOROFLUOROMETHANE
107-02-8 ACROLEIN
75-35-4 11middotDICHLOROETHENE
67-64-1 ACETONE
74-88-4 IODOMETHANE
75-15-0 CARBON DISULFIDE
METHYLEN E CHLORIDE 75-09-2
156-60-5 TRANS-12middotDICHLOROETHENE
1634-04-4 METHYL TERTIARY BUTYL ETHER
107-13-1 ACRYLONITRILE
75-34-3 11-DICHLOROETHANE
108-05-4 VINYL ACETATE
156-59middot2 CIS-12middotDICHLOROETHENE
78-93-3 2middotBUTANONE
~ BROMOCHLOROMETHANE
67-66-3 CHLOROFORM
71-55-6 111middot TRICHLOROETHANE
594-20-7 22middotDICHLOROPROPANE
56-23-5 CARBON TETRACHLORIDE
563-58-6 11middotDICHLOROPROPENE
107-06middot2 l2middotDICHLOROETHAN E
71-43-2 BENZENE
79-01-6 TRICHLOROETHENE
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Result Reporting Limit
05 05
05 05
05 05
1 1
05 05
05 05
100 100
05 05
10 10
5 5
10 10
1 1
05 05
1 1
10 10
05 05
10 10
05 05
5 5
1 1
05 05
1 1
05 05
05 05
05 05
05 05
05 05
05 05
MDL Result EPA Qualifier Qualifier
017 U
017 U
017 U
017 U
017 U
017 U
17 U
017 U
33 U
017 U
017 U
017 U
017 U
017 U
17 U
017 U
067 U
017 U
17 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
Data Package 10 VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- Fe Page 1 of 4
llMS Version 6317 A
8
GCMS Volatiles Method SW8260 _25B
Method Blank
Lab Name ALS Laboratory Group -- FC
Work Order Number 0911214
Client Name New Mexico Environment Department 08
ClientProject 10 644-111809(HWEI R-37 voes) PAR 002731703
Lab 10 VL091125-4MB Sample Matrix WATER
Moisture NIA Prep Batch VL091125-4
QCBatchIO VL091125-4-5
Sample Aliquot
Final Volume
10 ml
10 ml Oate Collected NIA Run 10 VL091125-4A Result Units UGL Oate Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Date Analyzed 25-Nov-09 Basis NIA
File Name 028043
CASNO Target Analyte OF Result Reporting Limit
MOL Result Qualifier
EPA Qualifier
78-87-5 12middotDICHLOROPROPANE 1 05 05 017 U
74-95-3 DIBROMOMETHANE 1 05 05 017 U
75-27-4 BROMODICHLOROMETHANE 1 05 05 017 U
10061-01-5 CISmiddot13middotDICHLOROPROPENE 1 05 05 017 U
108-10-1 4-METHYL-2-PENT ANONE 1 5 5 17 U
108-88-3 TOLUENE 1 05 05 017 U
10061-02-6 TRANS-13-DICHLOROPROPENE 1 05 05 017 U
79-00-5 112-TRICHLOROETHANE 1 05 05 017 U
591-78-6 2-HEXANONE 1 10 10 17 U
127-18-4 TETRACHLOROETHENE 1 05 05 017 U
142-28-9 13-DICHLOROPROPANI 1 05 05 017 U
124-48-1 DIBROMOCHLOROMETHANE 1 1 1 017 U
106-93-4 12-DIBROMOETHANE 1 1 1 017 U
108-90-7 CHLOROBENZENE 1 05 05 017 U
630-20-6 1112-TETRACHLOROETHANE 1 05 05 017 U
100-41-4 ETHYLBENZENE 1 05 05 017 U
136777-61-2 M+P-XYLENE 1 1 1 017 U
95-47-6 O-XYLENE 1 05 05 017 U
100-42-5 STYRENE 1 05 05 017 U
75-25-2 BROMOFORM 1 05 05 017 U
98-82-8 ~YLBENZENE 1 05 05 017 U
96-18-4 123-TRICHLOROPROPANE 1 2 2 017 U
79-34-5 1122middot TETRACHLOROETHANE 1 05 05 017 U
108-86-1 BROMOBENZENE 1 05 05 017 U
103-65-1 N-PROPYLBENZENE 1 05 05 017 U
95-49-8 2-CHLOROTOLUENE 1 05 05 017 U
108-67-8 135-TRIMETHYLBENZENE 1 05 05 017 U
106-43-4 4-CHLOROTOLUENE 1 05 05 017 U
Data Package 10 VL0911214-1
Date Printed Wednesday December n 2009 AlS Laboratory Group -- FC Page 2 of 4
lMS VeCSiOIY 6317A
9
GCMS Volatiles Method SW8260 _258
Method Blank
Lab Name ALS Laboratory Group - FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-111B09(HWB R-37 VOCs) PAR 002731703
Lab 10 VL091125-4MB Sample Matrix WATER
Moisture NIA
Prep Batch VL091125-4
QCBatchlD VL091125-4-5
Sample Aliquot
Final Volume
10 ml
10 ml
Date Collected NIA Run ID VL091125-4A Result Units UGL
Date Extracted 25-Nov-09 Cleanup NONE Clean DF 1
Date Analyzed 25-Nov-09 Basis NA
File Name 028043
CASNO Target Analyte OF Result Reporting Limit
MOL Result Qualifier
EPA Qualifier
98-06-6 TERT-BUTYLBENZENE 1 05 05 017 U
95-63-6 124-TRIMETHYLBENZENE 1 05 05 017 U
135-98-8 SEC-BUTYLBENZENE 1 05 05 017 U
541-73-1 13-DlCHLOROBENZENE 1 05 05 017 U
99-87-6 P-ISOPROPYLTOLUENE 1 05 05 017 U
106-46-7 1 A-DICHLOROBENZENE 1 05 05 017 U
104-51-8 N-BUTYLBENZENE 1 05 05 017 U
95-50-1 12-DICHLOROBENZENE 1 05 05 017 U
96-12-B 12-DIBROMO-3-CHLOROPROPANE 1 2 2 067 U
120-82-1 124-TRiCHLOROBENZENE 1 05 05 017 U
87-68-3 HEXACHLOROBUTADIENE 1 05 05 017 U
91-20-3 NAPHTHALENE 1 05 05 017 U
87-61-6 123-TRICHLOROBENZENE 1 05 05 017 U
75-05-B ACETONITRILE 1 50 50 83 U
107-05-1 ALLYL CHLORIDE 1 50 50 017 U
110-57-6 TRANS-14-DICHLORO-2-BUTENE 1 5 5 17 U
64-17-5 ETHANOL 1 200 200 78 U
97-63-2 ETHYL METHACRYLATE 1 5 5 017 U
78-83-1 ISOBUTYL ALCOHOL 1 100 100 17 U
126-98-7 METHACRYLONITRILE 1 35 35 17 U
80-62-6 METHYL METHACRYLATE 1 5 5 17 U
107-12-0 PROPIONITRILE 1 25 25 33 U
126-99-8 CHLOROPRENE 1 5 5 017 U
75-65-0 TERT-BUTANOL 1 100 100 33 U
108-20-3 ISOPROPYL ETHER 1 2 2 033 U
637-92-3 ETHYL TERT-BUTYL ETHER 1 2 2 033 U
994-05-8 TERT-AMYL METHYL ETHER 1 2 2 033 U
67-72-1 HEXACHLOROETHANE 1 2 2 033 U
Data Package 10 VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -~ Fe Page 3 of 4
LlMS Version 6317 A
10
GCMS Volatiles Method SW8260 _258
Method Blank
Lab Name ALS Laboratory Group -- FC
Work Order Number 0911214
Client Name New Mexico Envirmment Department OB
ClientProject 10 644-111809(HWB R-37 VOCs) PAR 002731703
Lab 10 VL091125-4MB Sample Matrix WATER
Moisture NIA Prep Batch VL091125-4
QCBatchlO VL091125-4-5
Sample Aliquot
Final Volume
10 m
10m Date Collected NIA Run 10 VL091125-4A Result Units UGIL Date Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Date Analyzed 25-Nov-09 BasisNIA
File Name 028043
CASNO Target Analyte Result Reporting MOL Result EPAOF Limit Qualifier Qualifier
Surrogate Recovery
CASNO Surrogate Analyte Result Flag Spike Amount
Percent Recovery
Control Limits
460-00-4 4-BROMOFLUOROBENZENE 25 25 100 82 - 121
1868-53-7 DIBROMOFLUOROMETHANE 248 25 99 80 - 123
2037-26-5 TOLUENE-D8 26 25 104 85 - 116
Data Package 10 VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- FC Page 4 of4
LlMS Version 6317A
11
GCMS Volati les Method SW8260 _258
Sample Results
Lab Name ALS Laboratory Group -- FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-111809(HWB R-37 VOCs) PAR 002731703
Field 10 Rmiddot37 Ser 2middot111809
Lab 10 0911214middot1
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml
Moisture NA QCBatchlO VL091125-4-5 Final Volume 10mi Date Collected 18-Nov-09 Run 10 VL091125-4A Result Units UGL
Date Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Analysis ReqCode 104 Date Analyzed 25-Nov-09
Prep Method SW5030 Rev C Basis As Received
File Name 028044
CASNO Target Analyte Dilution Factor
75-71-8 DICHLORODIFLUOROMETHANE 1
74middot87-3 CHLOROMETHANE 1
75-01-4 VINYL CHLORIDE 1
74-83-9 BROMOMETHANE 1
75-00-3 CHLOROETHANE 1
75-69-4 TRICHLOROFLUOROMETHANE 1
107-02-8 ACROLEIN 1
75-35-4 11middotDICHLOROETHENE 1
67-64-1 ACETONE 1
74-88-4 IODOMETHANE 1
75-15-0 CARBON DISULFIDE 1
75-09-2 METHYLENE CHLORIDE 1
156-60-5 TRANSmiddot12middotDICHLOROETHENE 1
1634-04-4 METHYL TERTIARY BUTYL ETHER 1
107-13-1 ACRYLONITRILE 1
75-34-3 1-DICHLOROETHANE 1
i 108-05-4 VINYL ACETATE 1
156-59-2 CIS-12middotDICHLOROETHENE 1
78-93-3 2-BUTANONE 1
74-97-5 BROMOCHLOROMETHANE 67-66-3 CHLOROFORM 1
71-55-6 11-TRICHLOROETHANE 594-20-7 22-DICHLOROPROPANE 56-23-5 CARBON TETRACHLORIDE 563-58-6 -DICHLOROPROPENE 107-06-2 2-DICHLOROETHANE
Result Reporting Limit
05 05
05 05
05 05
1 1
05 05
05 05
100 100
05 05
10 10
5 5
10 10
1 1
05 05
1 1
10 10
05 05
10 10
05 05
5 5
1 1
05 05
1 1
05 05
05 05
05 05
05 05
MOL Result EPA Qualifier Qualifier
017 U
017 U
017 U
017 U
017 U
017 U
17 U
017 U
33 U
017 U
017 U
017 U
017 U
017 U
17 U
017 U
067 U
017 U
17 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
Data Package ID VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- Fe Page 1 of 8
UMS Version 6317A
12
GCMS Volatiles Method SW8260_25B
Sample Results
Lab Name ALS Laboratory Group - FC
Work Order Number 0911214
Client Name New Mexico nvironment Department OB
ClientProject 10 644-111809(HWB R-37 VOCs) PAR 002731703
Field 10 R-37 Scr 2-111809
Lab 10 0911214-1
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10ml
Moisture NA QCBatchlD VL091125-4-5 Final Volume 10ml
Date Collected l8-Nov-09 Run 10 VL091125-4A Result Units UGL
Date Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Analysis ReqCode 104 Date Analyzed 25-Nov-09 Basis As Received
Prep Method SW5030 Rev C File NameD28044
CASNO Target Analyte Dilution Factor
Result Reporting Limit
MDL Result Qualifier
EPA Qualifier
I
71-43-2 BENZENE 1 05 05 017 U
79-01-6 TRICHLOROETHENE 1 05 05 017 U
78-87-5
74middot95-3
75-27-4
10061-01-5
108middot10middot1
108middot88-3
10061-02middot6
79-00-5
591-78-6
12-DICHLOROPROPANE
DIBROMOMETHANE
BROMODCHLOROMETHANE
CIS-13-DICHLOROPROPEI~E
4-METHYL-2-PENTANONE
TOLUENE
TRANS-13-DICHLOROPROPENE
112-TRICHLOROETHANE
2-HEXANONE
1
1
1
1
1
1
1
1
1
05
05
05
05
5
031
05
05
10
05
05
05
05
5
05
05
05
10
017
017
017
017
17
017
017
017
17
U
U
U
U
U
J
U
U
U
127-18-4
142-28-9
124-48-1
106-93-4
108-90-7
630-20-6
100-41-4
136777-61-2
95-47-6
100-42middot5
75-25-2
98-82middot8
96-18-4
79-34-5
108-86-1
TETRACHLOROETHENE
13-DICHLOROPROPANE
DIBROMOCHLOROMETHANE
12-DIBROMOETHANE
CHLOROBENZENE
11 12-TETRACHLOROETHANE
ETHYLBENZENE
M+PmiddotXYLENE
OmiddotXYLENE
STYRENE
BROMOFORM
ISOPRO PYLBENZENE
123middotTRICHLOROPROPANE
1122-TETRACHLOROETHANE
BROMOBENZENE
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
05
05
1
1
05
05
05
1
05
05
05
05
2
05
05
05
05
1
1
05
05
05
1
05
05
05
05
2
05
05
017
017
017
017
017
017
017
017
017
017
017
017
017
017
017
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
i
Data Package 10 VL0911214-1
Date Printed Wednesday December 022009 AlS laboratory Group bullbull Fe Page 2 of 8
UMS Version 6317A
13
GCMS Volatiles Method SW8260_258
Sample Results
Lab Name ALS Laboratory Group bullbull FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject ID 644-111809(HWB R-37 VOCs) PAR 002731703
Field 10 R-37 Sor 2-111809
Lab ID 0911214middot1
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml
Moisture NA QCBatchlD VL091125-4-5 Final Volume 10 ml
Date Collected 18-Nov-09 Run ID VL091125-4A Result Units UGL
Date Extracted 25-Nov-09 Cleanup NONE Clean DF 1
Analysis ReqCode 104 Date Analyzed 25-Nov-09 Basis As Received
Prep Method SW5030 Rev C File Name 028044
CASNO Target Analyte Dilution Factor
103-65-1 NmiddotPROPYLBENZENE 1
95-49-8 2-CHLOROTOLUENE 1
108-67-8 135-TRIMETHYLBENZENE 1
106-43-4 4-CHLOROTOLUENE 1
98-06-6 TER I-BUTYLBENZENE 1
95-63-6 124-TRIMETHYLBENZENE 1
135-98-8 SEC-BUTYLBENZENE 1
541-73-1 13-OICHLOROBENZENE 1
99-87-6 P-ISOPROPYLTOLUENE 1
106-46-7 lA-DICHLOROBENZENE 1
104-51-8 N-BUTYLBENZENE 1
95-50-1 12-DICHLOROBENZENE 1
96-12-8 l2-DIBROMOmiddot3-CHLOROPROPANE 1
120-82-1 12A-TRICHLOROBENZENE 1
187-68-3 HEXACHLOROBUTADIENE 1
91-20-3 NAPHTHALENE 1
87-61middot6 123-TRICHLOROBENZENE 1
75-05-8 ACETONITRILE 1
107middot05middot1 ALLYL CHLORIDE 1
110-57-6 TRANS-14-DICHLORO-2-BUTENE 1
164-17-5 ETHANOL 1
97-63-2 ETHYL METHACRYLATE 1
78-83-1 ISOBUTYL ALCOHOL 1
126-98-7 METHACRYLONITRILE 1
80-62-6 METHYL METHACRYLATE 1
107-12-0 PROPIONITRILE 1
Result Reporting Limit
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
2 2
05 05
05 05
05 05
05 05
50 50
50 50
5 5
200 200
5 5
100 100
35 35
5 5
25 25
MDL Result EPA Qualifier Qualifier
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
067 U
017 U
017 U
017 U
017 U
83 U
017 U
U u 78 U
017 U
17 U
17 U
17 U
33 U
Data Package 10 VL0911214-1
Date Printed Wednesday December 022009 ALS Laboratory Group MM Fe Page 3 of 8
LlMS VerSion 6317A
14
GCMS Volati las Method SW8260_258
Sample Results
Lab Name ALS Laboratory Group - FC
Work Order Number 0911214
Client Name New Mexico Environment Department 08
ClientProject 10 644-111B09(HWB R-37 VOGs) PAR 002731703
Field 10 R-37 Ser 2-111809 Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10ml
Lab 10 0911214-1 Moisture NA
Date Collected 1B-Nov-09 QCBatchlO VL091125-4-5
Run 10 VL091125-4A
Final Volume 10ml
Result Units UGIL Date Extracted 25-Nov-09 Cleanup NONE Clean OF
Analysis ReqCode 104 Date Analyzed 25-Nov-09
Prep Method SW5030 Rev G Basis As Received
File Name 028044
CASNO Target Analyte Dilution Factor
Result Reporting Limit
MDL Result Qualifier
EPA Qualifier
126-99-8 CHLOROPRENE 1 5 5 017 U
75-65-0 TERT-BUTANOL 1 100 100 33 U
108-20-3 ISOPROPYL ETHER 1 2 2 033 U
637-92-3 ETHYL TERT-BUTYL ETHER 1 2 2 033 U
994-05-8 TERT-AMYL METHYL ETHER 1 2 2 033 U
67-72-1 HEXACHLOROETHANE 1 2 2 033 U
Surrogate Recovery
CASNO Surrogate Analyte Result Flag Spike Amount
Percent Recovery
Control Limits
460-00-4 4-BROMOFLUOHOBENZENE 246 25 98 82 - 121
1868-53-7 DIBROMOFLUOHOMETHANE 248 25 99 BO - 123
2037-26-5 TOLUENE-DB 258 25 103 85middot116
Data Package 10 VL0911214-1
Date Printed Wednesday December 022009 ALS Laboratory Group bullbull FC Page 4 of 8
LIMS Version 0317 A
15
GCMS Volati les Method SW8260_25B
Sample Results
Lab Name ALS Laboratory Group -- FC
Worlt Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-111809(HWB Rmiddot37 VOCs) PAR 002731703
Field 10 Rmiddot37 Scr jmiddot111809
Lab 10 0911214-2
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml Moisture NfA QCBatchID VL091125-4middot5 Final Volume 10 ml
Date Collected 18middotNov-09 Run 10 VL091125-4A Result Units UGfL Date Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Analysis ReqCode 104 Date Analyzed 25middotNov-09 Basis As Received Prep Method SW5030 Rev C File Name 028045
CASNO Target Analyte Dilution Factor
Result Reporting Limit
MOL Result Qualifier
EPA Qualifier
75-71-8 DICHLORODIFLUOROMETHANE 1 05 05 017 U
74-87-3 CHLOROMETHANE 1 05 05 017 U
75-01middot4 VINYL CHLORIDE 1 05 05 017 U
74-83-9 BROMOMETHANE 1 1 1 017 U
75middot00middot3 CHLOROETHANE j 05 05 017 U
75-69-4 TRICHLOROFLUOROMETHANE 1 05 05 017 U
107-02-8 ACROLEIN 1 100 100 17 U
i 75-35-4 11-DICHLOROETHENE 1 05 05 017 U
67-64middot1 ACETONE 1 10 10 33 U
74-8S-4 IODOMETHANE 1 5 5 017 U
75-15-0 CARBON DISULFIDE 1 10 10 017 U
75-09-2 METHYLENE CHLORIDE 1 1 1 017 U
156-60-5 TRANS-12-DICHLOROETHENE 1 05 05 017 U
1634-04-4 METHYL TERTIARY BUTYL ETHER 1 1 1 017 U
107-13-1 ACRYLONITRILE 1 10 10 17 U
75-34middot3 11-DICHLOROETHANE 05 05 017 U
i 108-05-4 VINYL ACETATE 1 10 10 067 U
115659-2 CISmiddot 2middotDICHLOROETHENE 1 05 05 017 U
178-933 2middotBUTANONE 1 5 5 17 U
74-97middot5 BROMOCHLOROMET HANE 1 1 1 017 U
67-66-3 CHLOROFORM 1 05 05 017 U
71-55middot6 111middotTRICHLOROETHANE 1 1 1 017 U
594-20-7 22middotDICHLOROPROPANE 1 05 05 017 U
56-23-5 CARBON TETRACHLORIDE 1 05 05 017 U
563-58-6 11middotDICHLOROPROPENE 1 05 05 017 U
107-06-2 12middotDICHL OROETHANE 1 05 05 017 U
Data Package ID VL0911214-1
Date Printed Wednesday December 022009 ALS Laboratory Group -- Fe Page 5 of 8
16
GCMS Volatiles Method SW8260_25B
Sample Results
Lab Name ALS Laboratory Group -- FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-111809(HW3 R-37 VOCs) PAR 002731703
Field 10 R-37 Scr 1-11 1809
Lab 10 0911214-2
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml
Moisture NIA QCBatchlO VL091125-4-5 Final Volume 10 ml
Date Collected 18-Nov-09 Run 10 VL091125-4A Result Units UGL
[late Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Analysis ReqCode 104 Date Analyzed 25-Nov-09
Prep Method SW5030 Rev C Basis As Received
File Name 028045
CASNO Target Analyte Dilution Factor
71-43-2 BENZENE 1
79-01-6 TRICHLOROETHENE 1
78-87-5 12-DICHLOROPROPANE 1
74-95-3 DIBROMOMETHANE 1
75-27-4 BROMODICHLOROMETHANE 1
10061-01-5 CIS-13-DICHLOROPROPENE 1
108-10-1 4-METHYL-2-PtNTANON 1
108-88-3 TOLUENE 1
10061-02-6 TRANS-13-DICHLOROPROPENE 1
79-00-5 112-TRICHLOROETHANE 1
591-78-6 2-HEXANONE 1
127-18-4 TETRACHLOROETHENE 1
142-28-9 13-DICHLOROPROPANt 1
124-48-1 DI3ROMOCHLOROMETHANE 1
106-93-4 12-DIBROMOETHANE 1
108-90-7 CHLOROBENZENE 1
OETHANE 1
- 1
LENE 1
ENE 1
ENE 1
OFORM 1
OPYlBENZENE 1
96-18-4 123-TRICHLOROPROPANE 1
79-34-5 1122-TETRACHLOROETHANE 1
108-86-1 BROMOBENZENE 1
Result Reporting Limit
05 05
05 05
05 05
05 05
05 05
05 05
5 5
025 05
05 05
05 05
10 10
05 05
05 05
1 1
1 1
05 05
05 05
05 05
1 1
05 05
05 05
05 05
05 05
2 2
05 05
05 05
MDL Result EPA Qualifier Qualifier
017 U
017 U
017 U
017 U
017 U
017 U
17 U
017 J
017 U
017 U
17 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
Data Package 10 VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- Fe Page 6 of 8
317A
17
GCMS Volatiles Method SW8260 _258
Sample Results
Lab Name ALS Laboratory Group -- FC
Work Order Number 0911214
Client Name New Mexico Environment Department 08
ClientProject 10 644-11S09(HWB R-37 VOCs) PAR 002731703
Field 10 Rmiddot37 Scr 1-111809
Lab 10 0911214-2
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml Moisture NA QCBatchlD VL091125-4-5 Final Volume 10 ml
Date Collected 18-Nov-09 Run 10 VL091125-4A Result Units UGL Date Extracted 25-Nol-09 Cleanup NONE Clean OF
Analysis ReqCode 104 Date Analyzed 25-Nov-09 Basis As Received Prep Method SW5030 Rev C File Name D28045
CASNO Target Analyte Dilution Factor
103-65-1 N-PROPYLBENZENE 1
95-49-8 2-CHLOROTOLUENE 1
108-67-8 135-TRIMETHYLBENZENE 1
106-43-4 4-CHLOROTOLUENE 1
98-06-6 TERT-BUTYLBENZENE 1
95-63-6 124-TRIMETHYLBENZENE 1
135-98-8 SEC-BUTYLBENZENE 1
i 541-73-1 13middotDICHLOROBENZENE 1
99-87-6 PmiddotISOPROPYL TOLUENE 1
106-46-7 I 14-DICHLOROBENZENE 1
104-51-8 I N-BUTYLBENZENE 1
95-50-1 l2-DICHLOROBENZENE 1
96-12-8 I 12-DIBROMO-3-CHLOROPROPANE 1
120-82-1 124-TRICHLOROBENZENE 1
87-68-3 HEXACHLOROBUT ADIENE 1
91-20-3 NAPHTHALENE 1
87-61-6 123-TRICHLOROBENZENE 1
75-05-S ACETONITRILE 1
107-05-1 ALLYL CH LORIDE 1
110-57-6 TRAN S-14-DICHLORO-2-BUTENE 1
64-17-5 ETHANOL 1
97-63-2 ETHYL METHACRYLATE 1
78-83-1 ISOBUTYL ALCOHOL 1
126-98-7 METHACRYLONITRILE 1
80-62-6 METHYL METHACRYLATE 1
107-12-0 I PROPIONITRILE 1
Result Reporting Limit
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
2 2
05 05
05 05
05 05
05 05
50 50
50 50 I 5 5
200 200
5 5
100 100
35 35
5 5
25 25
MDL
017
017
017
017
017
017
017
017
017
017
017
017
067
017
017
017
017
83
017
17
78
017
17
17
17
33
Result EPA Qualifier Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
Data Package 10 VL0911214-1
Date Printed Wednesday December 022009 ALS Laboratory Group -- Fe Page 7 of 8
LlMS Version 6317A
18
GCMS Volatiles Method SW8260_258
Sample Results
Lab Name ALS Laboratory Group bullbull FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644middot111B09(HWB R-37 VOCs) PAR 002731703
Sample Matrix WATER Prep Batch VL091125--4 Sample Aliquot 10 mlRmiddot37 Ser 1-111809 Moisture NA QCBatchlO VL091125--4-5 Final Volume 10 m
0911214-2 Date Collected 18-Nov-09 Run 10 VL091125--4A Result Units UGL Date Extracted 25-Nov-09 Cleanup NONE Clean OF 1 Date Analyzed 25-Nov-09 Basis As Received
10
Analysis ReqCode 104 Prep Method SW5030 Rev C File Name 028045
I
CASNO Target Analyte Dilution Factor
Result Reporting Limit
MDL Result Qualifier
EPA Qualifier
126-99-8 CHLOROPRENE 1 5 5 017 U
75-65-0 TERT-BUTANOL 1 100 100 33 U
108-20-3 ISOPROPYL ETHER 1 2 2 033 U
637-92-3 ETHYL TERT-BUTYL ETHER 1 2 2 033 U
994-05--8 TERT-AMYL MTHYL ETHER 1 2 2 033 U
67-72-1 HEXACHLOROETHANE 1 2 2 033 U
Surrogate Recovery
CASNO Surrogate Analyte Result Flag Spike Amount
Percent Control Recovery Limits
460-00-4 4middotBROMOFLUOROBENZENE 247 25 99 1
1868-53-7 DIBROMOFLUOROMETHANE 248 25 99 80 123
2037-26-5 TOLUENEmiddotDB 255 25 102 85 - 116
Data Package 10 VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- FC Page B of 8
LlMS Version 6317A
19
GCMS Volatiles Method SW8260_258
Laboratory Control Sample and Laboratory Control Sample Duplicate
Lab Name ALS Laboratory Group - FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-111809(HWB R-37 VOCs) PAR 002731703
Lab 10 VL091125-4LCS Sample Matrix WATER
Moisture NA Prep Batch VL091125-4
QCBatchlD VL091125-4-5
Sample Aliquot
Final Volume
10ml
10ml Date Collected NA Run 10 VL091125-4A Result Units UGIL Date Extracted 111252009 Cleanup NONE Clean OF 1 Date Analyzed 11252009 Basis NA
Prep Method SW5030C File Name 028040
CASNO
74-87-3
75-01-4
74-83-9
75-69-4
75-35-4
75-15-0
156-60-5
75-34-3
108-05-4
156-59-2
78-93-3
67 -66-3
71-55-6
i 56-23-5
107-06-2
71-43-2
79-01-6
78-87-5
75-27-4
108-88-3
79-00-5
591-78-6
127-18-4
106-93-4
108-90-7
63Q20-6
Target Analyte Spike Added
CHLOROMETHANE 10
VINYL CHLORIDE 10
BROMOMETHANE 10
TRICHLOROFLUOROMETHANE 10
11-DICHLOROETHENE 10
CARBON DISULFIDE 10
TRANS-12-DICHLOROETHENE 10
11-DICHLOROETHANE 10
VINYL ACETATE 10
CIS-12-DICHLOROETHENE 10
2middotBUTANONE 40
CHLOROFORM 10
111-TRICHL ORO ETHANE 10
CARBON TETRACHLORIDE 10
12-DICHLOROETHANE 10
BENZENE 10
TRICHLOROETHENE 10
12-DICHLOROPROPANE 10
BROMODICHLOROMETHANE 10
TOLUENE 10
112-TRICHLOROETHANE 10
2-HEXANONE 40
TETRACHLOROETHENE 10
12-DIBROMOETHANE 10
CHLOROBENZENE 10
1112-TETRACHLOROETHANE 10
LCS Reporting Result Result Limit Qualifier
932 05
863 05
943 1
908 05
96 05
95 10 J
996 05
992 05
10 10
102 05
412 5
993 05
974 1
943 05
106 05
983 05
962 05
10 05
988 05
974 05
989 05
409 10
956 05
991 1
984 05
101 05
LCS Control Rec Limits
93 49 -129
86 46 134
94 32-121
91 67 -152
96 61 -135
95 61 -140
100 70 -122
99 76 -119
100 62 182
102 75 126
103 61 -137
99 79 120
97 76 - 114
94 58middot135
106 75middot132
98 70 shy 125
96 74 121
100 81 -119
99 79 - 123
97 76 - 120
99 81 -126
102 45 168
96 56 -128
99 79 -123
98 75 -120
101 82 - 123
Data Package 10 VL0911214middot1
-Date Printed Wednesday December 02 2009 ALS Laboratory Group -- Fe Page 1 of 4
LiMS Version 6317A
20
GCMS Volatiles Method SW8260_25B
Laboratory Control Sample and Laboratory Control Sample Duplicate
Lab Name ALS Laboratory Group - FC
Work Order Number 0911214
Client Name New Mexico Envircnment Department OB
ClientProject 10 644-111809(HWB R-37 VOes) PAR 002731703
Lab 10 VL091125-4LCS Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml
Moisture NIA QCBatchlO VL091125-4-5 Final Volume 10 mi
Date Collected NA Run 10 VL091125-4A Result Units UGL Date Extracted 11252009 Cleanup NONE Clean OF 1 Date Analyzed 111252009 Basis NA
Prep Method SW5030e File Name 028040
CASNO Target Analyte Spike Added
LCS Result
Reporting Limit
Result Qualifier
LCS Rec
Control Limits
100-41-4 ETHYLBENZENE 10 981 05 98 79 -114
136777-61-2 M+P-XYLENE 20 197 1 98 81-115
95-47-6 O-XYLENE 10 101 05 101 81 -115
95-49-8 2-CHLOROTOLUENE 10 97 05 97 80 -128
541-73-1 13-DICHLOROBENZiNt 10 977 05 98 81-116
106-46-7 14-DICHLOROBENZENE 10 979 05 98 81 -119
95-50-1 12-DICHLOROBENZENE 10 987 05 99 79 - 116
91-20-3 NAPHTHALENE 10 993 05 99 69 -126
87-61-6 123-TRICHLOROBENZENE 10 999 05 100 60 -137
Data Package ID VL0911214-1
Date Printed Wecnesday December 02 2009 ALS Laboratory Group -- Fe Page 2 of 4
21
GCMS Volatiles Method SW8260_25B
Laboratory Control Sample and Laboratory Control Sample Duplicate
Lab Name ALS Laboratory Group bullbull FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-11 1809(HWB R-37 VOCs) PAR 002731703
Lab 10 VL091125middot4LCSD Sample Matrix WATER
Moisture NIA Prep Batch VL091125-4
QCBatchlD VL091125-4-5
Sample Aliquot
Final Volume
10 ml
10ml Date Collected NIA Run ID VL091125-4A Result Units UGIL Date Extracted 112512009 Cleanup NONE Clean DF 1 Date Analyzed 1112512009 Basis NIA
Prep Method SW5030C File Name 028041
CASNO Target Analyte Spike Added
LCSD Result
Reporting Limit
Result Qualifier
LCSD Rec
RPD Limit
RPD
74-87-3 CHLOROMETHANE 10 897 05 90 30 4
75-01-4 VINYL CHLORIDE 10 831 05 83 25 4
74-83-9 BROMO METHANE 10 945 1 94 25 0
75-69-4 TRICHLOROFLUOROMETHANE 10 873 05 87 22 4
75-35-4 11-DICHLOROETHENE 10 909 05 91 18 5
75-15-0 CARBON DISULFIDE 10 941 10 J 94 20 1
156-60middot5 TRANS-l2middotDICHLOROETHENE 10 961 05 96 25 4
75middot34middot3 11-DICHLOROETHANE 10 977 05 98 25 2
108-05-4 VINYL ACETATE 10 993 10 J 99 20 1
156middot59-2 CIS-12-DlCHLOROETHENE 10 995 05 99 25 3
i 78-93-3 2-BUTANONE 40 419 5 105 30 2
67-66-3 CHLOROFORM 10 985 05 99 25 1
71-55-6 lll-TRICHLOROETHANE 10 942 1 94 25 3
56-23-5 CARBON TETRACHLORIDE 10 922 05 92 25 2
107middot06-2 12middotDICHLOROETHANE 10 106 05 106 25 0
71-43middot2 BENZENE 10 971 05 97 10 1
79middot01middot6 TRICHLOROETHENE 10 939 05 94 10 2
78middot87middot5 l2middotDICHLOROPROPANE 10 101 05 101 25 1
i 75middot27-4 BROMODICHLOROMETHANE 10 992 05 99 25 0
1108-88-3 TOLUENE 10 962 05 96 9 1
I 79005 112middotTRICHLOROETHANE 10 986 05 99 25 0
591middot78middot6 2-HEXANONE 40 418 10 104 20 2
127middot18-4 TETRACHLOROETHENE 10 918 05 92 25 4
106-93-4 12middotDIBROMOETHANE 10 999 1 100 15 1
108middot90-7 CHLOROBENZENE 10 997 05 100 11 1
630-20middot6 1112-TETRACHLOROETHANE 10 101 05 101 15 0
100-41-4 ETHYLBENZENE 10 968 05 97 25 1
Data Package ID VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- FC Page 3 of 4
lIMS Version 6317 A
22
GCMS Volatiles Method SW8260_25B
Laboratory Control Sample and Laboratory Control Sample Duplicate
Lab Name ALS Laboratory 13roup -- FC
Work Order Number 0911214
Client Name New Mexico Environment Department OS
ClientProject 10 644-11 1809(HWB R-37 VOCs) PAR 002731703
Lab 10 VL091125-4LCSD Sample Matrix WATER
Moisture NA Prep Batch VL091125-4
QCBatchlO VL091125-4-5
Sample Aliquot
Final Volume
10 ml
10ml Date Collected NA Run 10 VL091125-4A Result Units UGL Date Extracted 11252009 Cleanup NONE Clean OF Date Analyzed 11252009 Basis NIA
Prep Method SW5030C File Name 028041
CASNO Target Analyte Spike Added
LCSD Result
Reporting Limit
Result Qualifier
LCSD Rec
RPD Limit
RPD
136777-61-2 M+P-XYLENE 20 193 1 97 25 2
95-47-6 O-XYLENE 10 983 05 98 25 2
95-49-8 2middotCHLOROTOLUENE 10 9A9 05 95 15 2
541-73-1 13middotDICHLOROBENZENE 10 997 05 100 25 2
106-46-7 14-DICHLOROBeNZENE 10 974 05 97 25 1
95-50middot1 12middotDICHLOROBENZeNE 10 101 05 101 25 2
91middot20-3 NAPHTHALENe 10 105 05 105 24 6
87-61-6 123-TRICHLOROBENZENE 10 102 05 102 33 3
Surrogate Recovery LCSLCSD
CASNO Target Analyte Spike Added
LCS Rec
LCS Flag
LCSD Rec
LCSD Flag
Control Limits
460middot00-4 4-BROMOFLUOROBeNZENE 25 100 100 82 - 121
1868-53middot7 DIBROMOFLUOROMeTHANE 25 101 100 80middot 123
2037middot26-5 TOLUENEmiddotD8 25 102 100 85middot 116
Data Package 10 VL0911214-
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- Fe Page 4 of 4
UMS Verslmt 6317A
23
ALS Data Qualifier Flags Chromatography and Mass Spectrometry
U or NO This flag indicates that the compound was analyzed for but not detected
J This flag indicates an estimated value This flag is used as follows (1) when estimating a concentration for tentatively identified compounds (TICs) where a 11 response is assumed (2) when the mass spectral and retention time data indicate the presence of a compound that meets the volatile and semivolatile GCMS identification criteria and the result is less than the reporting limit (RL) but greater than the method detection limit (MOL) (3) when the retention time data indicate the presence of a compound that meets the GC identification criteria and the result is less than the RL but greater than the MOL and (4) the reported value is estimated
B This flag is used when the analyte is detected in the associated method blank as well as in the sample It indicates probable blank contamination and warns the data user This flag shall be used for a tentatively identified compound (TIC) as well as for a positively identified target compound
E This flag identifies compounds whose concentration exceeds the upper level of the calibration range
A This flag indicates that a tentatively identified compound is a suspected aldol-condensation product
X This flag indicates that the analyte was diluted below an accurate quantitation level
This flag indicates that a spike recovery is equal to or outside the control criteria used
+ This flag indicates that the relative percent difference (RPO) equals or exceeds the control criteria
3
ALS Laboratory Group -- Fe Sample Number(s) Cross-Reference Table
Paragon OrderNum 0911214 Client Name New Mexico Environment Department OB
Client Project Name 644-111809(HWB R-37 VOCs) PAR Client Project Number 002731703
Client PO Number 06-667-55-01754
Client Sample Number
Lab Sample Number
COC Number Matrix Date Collected
Time Collected
R-37 Scr 2-1 11809 0911214-1 WATER 18-Nov-09 1555 R-37 Scr 1-111809 0911214-2 WATER 18-Nov-09 1744
Page 1 of 1 ALS Laboratory Group -- Fe Date Printed Wednesday December 02 2009 LlMS Version 6317 A
4
Chain of Custody Record 1)11 d- I 4 SHIP To MAil REPORT TO HtitilJft BILL TO
Kim GrJOZOW KC [)il-e Cobra
NMFOmiddotDOE Overslghl Bwe3u 50S firt1middottoOB Hew Meico FnlliTtl1 Dep1 HaVIdthJS VvaMe Bureau ~orl Collins CO 80524shy
1UH Diamold Drive Stille 8 90S Rodeo P3M( D~lIe Ea~ Bldg(970) 90middot511
lo Alarr1(1l N~Muto 87544 83113 Fe liM 87505middot25-67
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Project Number (Llib invoice USI
Only)
o~_IIi~~__
~ i ~
~ ~ j
~ f rn E Il J ~laquo
644middot111809(HWB Rmiddot37 VOCs) PAR
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HW8 Cost Code OoU110J
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309
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cI yl iComments Lanc~v fiias not~ that foe samples life not preg~-d with HCL bull
~ 4_~~~~S5 V~~~Vi~I_$ ~~~~5s~rvd __
3 4()ml glau VOA vials Non-PrlttIrv~d -----~--
OC Level Standard f 0~Y ~-t-~ (fv f_ QC Required MS MSD Bla~k
irU11 Around TieJTAT) ~_dbullr_d__~______
cJPlace X In bOK If there are less than 5 lotal sample for shipping cosls
IJl
PQf 1
---- ---- ---
ALS Laboratory GrouP - Fort Collins
CONDITIO] OF SAMPLE UPO) RECEIPT FORM
Client _-=-N--M---f-=-D________ IVorkorde No D4 J I 4 --~~~~~~------
PrO1 cc Manager L 5 lnitiais C D Date 1 -) ()- () C --~~~---------------------
1 there a cae Are the coe and bottle labels
Is the coe in agreement with samples received) of containers matrix requested anaiyses etc)
documents presen1 andor removable)
Are all aqueous samples requiring preservation preserved correctly ~- ----~-~~--- -~ -~-- ----~~~---------
volatiles)
14 Are all samples requiring no headspace (VOC GRG RSKlVIEE lb eNS radon)
free Size of bubble lt
$ Do perchlorate LCMS-MS samples have headspace (a~ least ]3 of container required)
NO
]6 Were samples checked for and free from the presence of residual chlorine (Appiicaole when PM has Indicated samples are from a chlonnated wat~ source note if field preservallor
witb sodIUm tlllosulfate wa not observed)
17 Were the lljIV~IOU on ice
IS Were cooler temperatures measured at 01-60degC IR ~Illl used 2
Coole I---
Temperature (C) 3 ~
NO
NO
NO
NO
NO
NO
NO
No of custodv seals Ol~ cooler 0 OOT ---- --- --- --l Surveyl EXlemlli flRhr n~ading I i AcceplanCfiltnforma tlon Background ulJhr reading 3 Were eX lema uRhf readl1lf5 tW(l tm bnckl1Ound and withllllxyr acceptance criterill
Additional Iuformation OVIDE DETAILS BELOW FOR A ND RESPONSE TO ANY (UESTION A80VE EXCEPT 1 ANI) 16
If applicable was the clienl contacted) YES i NO I
Project Manager Signature I Date
(1 Gun 112 Oaktoll SN 2992250020 jmiddot0066 lR Gun lie Oakton S~ 23n220101middot0(J02
Form 201r22gt15 (61109) Page 1 of _1
6
4a Express Package Service _ FadEx Pnority OvernightLJ ==lr-~MClncU1
lSlIIQSATUIIDAYlltIrwIlyis$Mf(1J
middot10_ FadEx SlaMard Ovemioht fMtRallw6ftIlfTampCI v
Stun1I1V OlIwtrlN01IMlIIbU1 PtnIttlgas IIfI ro 150lbs FedEx First OV1lmigtr ~Mmnm~rnollnll onwy9Itetlncalklfl bull SIItlmiIlYDNOTaBItOifi
FecEx~ US Airbill Express
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9439 4324
~ FadEx2Dav FadEx ExDress Saver ~ 5leoMlMmmdayenlh~ TlifaoIUillltrtalllmiddot L ~wqb9di1l~flKlonMool8V SatuIOIyDdillllYldIT~
unRISSSAl1JRDAYOeilwrvI$Mde~
4b ExpressfreightService - __ C0T1llanv
~~oalleJl =1~~ImOt $AUROAY ftlEdOeyF1tlitNbiDrnJtin
5 Packaging -1itIcIrme-- FadEgt r- FedEgt fak FedEx Box
kt1UoorFdrStNil~~Your Internal Billing Reference Enveiope Pol _
TD
Address Wa clMOfdeiinrto POlwuscrPo ZIP CGlJla
Address
6 Special Handlmlllilld Delivery SignalUlll Options
~~~l~__Iint_dUSabulld)IjhL Indirect Sianarurc ttMtrttISMIllFtdlHrtS ~~tlltl~ eeelMllnllrl$ICIIltctdeiMv-kll lt_noaIllaIMInt$ ~
OrvlceL- OtyiclItUN186 ___ ___
[ CaflO Aircraft Oniy
8700 9439 4324 ~rtl1~l__bPnD USA SRI
_____-----------~bull---~----- -------~~-------------------
7
GCMS Volatiles Method SW8260 _25B
Method Blank
Lab Name ALS Laboratory Group bullbull FC
Work Order Number 0911214
Client Name New Mexico Environment Department DB
ClientProject 10 644-111809(HWB Rmiddot37 VOCs) PAR 002731703
Lab 10 VL091125-4MB Sample Matrix WATER
Moisture NA Prep Batch VL091125-4
QCBatchlO VL091125-4-5
Sample Aliquot
Final Volume
10 ml
10 ml Date Collected NA Run 10 VL091125-4A Result Units UGL Date Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Date Analyzed 25middotNov-09 Basis NA
File Name 028043
CASNO Target Analyte DF
75-71-8 DICHLORODIFLUOROMETHANE
74-87-3 CHLOROMETHANE
75-01-4 VINYL CHLORIDE
74-83-9 BROMOMETHANE
75-00-3 CHLOROETHANE
75-69-4 TRICHLOROFLUOROMETHANE
107-02-8 ACROLEIN
75-35-4 11middotDICHLOROETHENE
67-64-1 ACETONE
74-88-4 IODOMETHANE
75-15-0 CARBON DISULFIDE
METHYLEN E CHLORIDE 75-09-2
156-60-5 TRANS-12middotDICHLOROETHENE
1634-04-4 METHYL TERTIARY BUTYL ETHER
107-13-1 ACRYLONITRILE
75-34-3 11-DICHLOROETHANE
108-05-4 VINYL ACETATE
156-59middot2 CIS-12middotDICHLOROETHENE
78-93-3 2middotBUTANONE
~ BROMOCHLOROMETHANE
67-66-3 CHLOROFORM
71-55-6 111middot TRICHLOROETHANE
594-20-7 22middotDICHLOROPROPANE
56-23-5 CARBON TETRACHLORIDE
563-58-6 11middotDICHLOROPROPENE
107-06middot2 l2middotDICHLOROETHAN E
71-43-2 BENZENE
79-01-6 TRICHLOROETHENE
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Result Reporting Limit
05 05
05 05
05 05
1 1
05 05
05 05
100 100
05 05
10 10
5 5
10 10
1 1
05 05
1 1
10 10
05 05
10 10
05 05
5 5
1 1
05 05
1 1
05 05
05 05
05 05
05 05
05 05
05 05
MDL Result EPA Qualifier Qualifier
017 U
017 U
017 U
017 U
017 U
017 U
17 U
017 U
33 U
017 U
017 U
017 U
017 U
017 U
17 U
017 U
067 U
017 U
17 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
Data Package 10 VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- Fe Page 1 of 4
llMS Version 6317 A
8
GCMS Volatiles Method SW8260 _25B
Method Blank
Lab Name ALS Laboratory Group -- FC
Work Order Number 0911214
Client Name New Mexico Environment Department 08
ClientProject 10 644-111809(HWEI R-37 voes) PAR 002731703
Lab 10 VL091125-4MB Sample Matrix WATER
Moisture NIA Prep Batch VL091125-4
QCBatchIO VL091125-4-5
Sample Aliquot
Final Volume
10 ml
10 ml Oate Collected NIA Run 10 VL091125-4A Result Units UGL Oate Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Date Analyzed 25-Nov-09 Basis NIA
File Name 028043
CASNO Target Analyte OF Result Reporting Limit
MOL Result Qualifier
EPA Qualifier
78-87-5 12middotDICHLOROPROPANE 1 05 05 017 U
74-95-3 DIBROMOMETHANE 1 05 05 017 U
75-27-4 BROMODICHLOROMETHANE 1 05 05 017 U
10061-01-5 CISmiddot13middotDICHLOROPROPENE 1 05 05 017 U
108-10-1 4-METHYL-2-PENT ANONE 1 5 5 17 U
108-88-3 TOLUENE 1 05 05 017 U
10061-02-6 TRANS-13-DICHLOROPROPENE 1 05 05 017 U
79-00-5 112-TRICHLOROETHANE 1 05 05 017 U
591-78-6 2-HEXANONE 1 10 10 17 U
127-18-4 TETRACHLOROETHENE 1 05 05 017 U
142-28-9 13-DICHLOROPROPANI 1 05 05 017 U
124-48-1 DIBROMOCHLOROMETHANE 1 1 1 017 U
106-93-4 12-DIBROMOETHANE 1 1 1 017 U
108-90-7 CHLOROBENZENE 1 05 05 017 U
630-20-6 1112-TETRACHLOROETHANE 1 05 05 017 U
100-41-4 ETHYLBENZENE 1 05 05 017 U
136777-61-2 M+P-XYLENE 1 1 1 017 U
95-47-6 O-XYLENE 1 05 05 017 U
100-42-5 STYRENE 1 05 05 017 U
75-25-2 BROMOFORM 1 05 05 017 U
98-82-8 ~YLBENZENE 1 05 05 017 U
96-18-4 123-TRICHLOROPROPANE 1 2 2 017 U
79-34-5 1122middot TETRACHLOROETHANE 1 05 05 017 U
108-86-1 BROMOBENZENE 1 05 05 017 U
103-65-1 N-PROPYLBENZENE 1 05 05 017 U
95-49-8 2-CHLOROTOLUENE 1 05 05 017 U
108-67-8 135-TRIMETHYLBENZENE 1 05 05 017 U
106-43-4 4-CHLOROTOLUENE 1 05 05 017 U
Data Package 10 VL0911214-1
Date Printed Wednesday December n 2009 AlS Laboratory Group -- FC Page 2 of 4
lMS VeCSiOIY 6317A
9
GCMS Volatiles Method SW8260 _258
Method Blank
Lab Name ALS Laboratory Group - FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-111B09(HWB R-37 VOCs) PAR 002731703
Lab 10 VL091125-4MB Sample Matrix WATER
Moisture NIA
Prep Batch VL091125-4
QCBatchlD VL091125-4-5
Sample Aliquot
Final Volume
10 ml
10 ml
Date Collected NIA Run ID VL091125-4A Result Units UGL
Date Extracted 25-Nov-09 Cleanup NONE Clean DF 1
Date Analyzed 25-Nov-09 Basis NA
File Name 028043
CASNO Target Analyte OF Result Reporting Limit
MOL Result Qualifier
EPA Qualifier
98-06-6 TERT-BUTYLBENZENE 1 05 05 017 U
95-63-6 124-TRIMETHYLBENZENE 1 05 05 017 U
135-98-8 SEC-BUTYLBENZENE 1 05 05 017 U
541-73-1 13-DlCHLOROBENZENE 1 05 05 017 U
99-87-6 P-ISOPROPYLTOLUENE 1 05 05 017 U
106-46-7 1 A-DICHLOROBENZENE 1 05 05 017 U
104-51-8 N-BUTYLBENZENE 1 05 05 017 U
95-50-1 12-DICHLOROBENZENE 1 05 05 017 U
96-12-B 12-DIBROMO-3-CHLOROPROPANE 1 2 2 067 U
120-82-1 124-TRiCHLOROBENZENE 1 05 05 017 U
87-68-3 HEXACHLOROBUTADIENE 1 05 05 017 U
91-20-3 NAPHTHALENE 1 05 05 017 U
87-61-6 123-TRICHLOROBENZENE 1 05 05 017 U
75-05-B ACETONITRILE 1 50 50 83 U
107-05-1 ALLYL CHLORIDE 1 50 50 017 U
110-57-6 TRANS-14-DICHLORO-2-BUTENE 1 5 5 17 U
64-17-5 ETHANOL 1 200 200 78 U
97-63-2 ETHYL METHACRYLATE 1 5 5 017 U
78-83-1 ISOBUTYL ALCOHOL 1 100 100 17 U
126-98-7 METHACRYLONITRILE 1 35 35 17 U
80-62-6 METHYL METHACRYLATE 1 5 5 17 U
107-12-0 PROPIONITRILE 1 25 25 33 U
126-99-8 CHLOROPRENE 1 5 5 017 U
75-65-0 TERT-BUTANOL 1 100 100 33 U
108-20-3 ISOPROPYL ETHER 1 2 2 033 U
637-92-3 ETHYL TERT-BUTYL ETHER 1 2 2 033 U
994-05-8 TERT-AMYL METHYL ETHER 1 2 2 033 U
67-72-1 HEXACHLOROETHANE 1 2 2 033 U
Data Package 10 VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -~ Fe Page 3 of 4
LlMS Version 6317 A
10
GCMS Volatiles Method SW8260 _258
Method Blank
Lab Name ALS Laboratory Group -- FC
Work Order Number 0911214
Client Name New Mexico Envirmment Department OB
ClientProject 10 644-111809(HWB R-37 VOCs) PAR 002731703
Lab 10 VL091125-4MB Sample Matrix WATER
Moisture NIA Prep Batch VL091125-4
QCBatchlO VL091125-4-5
Sample Aliquot
Final Volume
10 m
10m Date Collected NIA Run 10 VL091125-4A Result Units UGIL Date Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Date Analyzed 25-Nov-09 BasisNIA
File Name 028043
CASNO Target Analyte Result Reporting MOL Result EPAOF Limit Qualifier Qualifier
Surrogate Recovery
CASNO Surrogate Analyte Result Flag Spike Amount
Percent Recovery
Control Limits
460-00-4 4-BROMOFLUOROBENZENE 25 25 100 82 - 121
1868-53-7 DIBROMOFLUOROMETHANE 248 25 99 80 - 123
2037-26-5 TOLUENE-D8 26 25 104 85 - 116
Data Package 10 VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- FC Page 4 of4
LlMS Version 6317A
11
GCMS Volati les Method SW8260 _258
Sample Results
Lab Name ALS Laboratory Group -- FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-111809(HWB R-37 VOCs) PAR 002731703
Field 10 Rmiddot37 Ser 2middot111809
Lab 10 0911214middot1
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml
Moisture NA QCBatchlO VL091125-4-5 Final Volume 10mi Date Collected 18-Nov-09 Run 10 VL091125-4A Result Units UGL
Date Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Analysis ReqCode 104 Date Analyzed 25-Nov-09
Prep Method SW5030 Rev C Basis As Received
File Name 028044
CASNO Target Analyte Dilution Factor
75-71-8 DICHLORODIFLUOROMETHANE 1
74middot87-3 CHLOROMETHANE 1
75-01-4 VINYL CHLORIDE 1
74-83-9 BROMOMETHANE 1
75-00-3 CHLOROETHANE 1
75-69-4 TRICHLOROFLUOROMETHANE 1
107-02-8 ACROLEIN 1
75-35-4 11middotDICHLOROETHENE 1
67-64-1 ACETONE 1
74-88-4 IODOMETHANE 1
75-15-0 CARBON DISULFIDE 1
75-09-2 METHYLENE CHLORIDE 1
156-60-5 TRANSmiddot12middotDICHLOROETHENE 1
1634-04-4 METHYL TERTIARY BUTYL ETHER 1
107-13-1 ACRYLONITRILE 1
75-34-3 1-DICHLOROETHANE 1
i 108-05-4 VINYL ACETATE 1
156-59-2 CIS-12middotDICHLOROETHENE 1
78-93-3 2-BUTANONE 1
74-97-5 BROMOCHLOROMETHANE 67-66-3 CHLOROFORM 1
71-55-6 11-TRICHLOROETHANE 594-20-7 22-DICHLOROPROPANE 56-23-5 CARBON TETRACHLORIDE 563-58-6 -DICHLOROPROPENE 107-06-2 2-DICHLOROETHANE
Result Reporting Limit
05 05
05 05
05 05
1 1
05 05
05 05
100 100
05 05
10 10
5 5
10 10
1 1
05 05
1 1
10 10
05 05
10 10
05 05
5 5
1 1
05 05
1 1
05 05
05 05
05 05
05 05
MOL Result EPA Qualifier Qualifier
017 U
017 U
017 U
017 U
017 U
017 U
17 U
017 U
33 U
017 U
017 U
017 U
017 U
017 U
17 U
017 U
067 U
017 U
17 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
Data Package ID VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- Fe Page 1 of 8
UMS Version 6317A
12
GCMS Volatiles Method SW8260_25B
Sample Results
Lab Name ALS Laboratory Group - FC
Work Order Number 0911214
Client Name New Mexico nvironment Department OB
ClientProject 10 644-111809(HWB R-37 VOCs) PAR 002731703
Field 10 R-37 Scr 2-111809
Lab 10 0911214-1
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10ml
Moisture NA QCBatchlD VL091125-4-5 Final Volume 10ml
Date Collected l8-Nov-09 Run 10 VL091125-4A Result Units UGL
Date Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Analysis ReqCode 104 Date Analyzed 25-Nov-09 Basis As Received
Prep Method SW5030 Rev C File NameD28044
CASNO Target Analyte Dilution Factor
Result Reporting Limit
MDL Result Qualifier
EPA Qualifier
I
71-43-2 BENZENE 1 05 05 017 U
79-01-6 TRICHLOROETHENE 1 05 05 017 U
78-87-5
74middot95-3
75-27-4
10061-01-5
108middot10middot1
108middot88-3
10061-02middot6
79-00-5
591-78-6
12-DICHLOROPROPANE
DIBROMOMETHANE
BROMODCHLOROMETHANE
CIS-13-DICHLOROPROPEI~E
4-METHYL-2-PENTANONE
TOLUENE
TRANS-13-DICHLOROPROPENE
112-TRICHLOROETHANE
2-HEXANONE
1
1
1
1
1
1
1
1
1
05
05
05
05
5
031
05
05
10
05
05
05
05
5
05
05
05
10
017
017
017
017
17
017
017
017
17
U
U
U
U
U
J
U
U
U
127-18-4
142-28-9
124-48-1
106-93-4
108-90-7
630-20-6
100-41-4
136777-61-2
95-47-6
100-42middot5
75-25-2
98-82middot8
96-18-4
79-34-5
108-86-1
TETRACHLOROETHENE
13-DICHLOROPROPANE
DIBROMOCHLOROMETHANE
12-DIBROMOETHANE
CHLOROBENZENE
11 12-TETRACHLOROETHANE
ETHYLBENZENE
M+PmiddotXYLENE
OmiddotXYLENE
STYRENE
BROMOFORM
ISOPRO PYLBENZENE
123middotTRICHLOROPROPANE
1122-TETRACHLOROETHANE
BROMOBENZENE
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
05
05
1
1
05
05
05
1
05
05
05
05
2
05
05
05
05
1
1
05
05
05
1
05
05
05
05
2
05
05
017
017
017
017
017
017
017
017
017
017
017
017
017
017
017
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
i
Data Package 10 VL0911214-1
Date Printed Wednesday December 022009 AlS laboratory Group bullbull Fe Page 2 of 8
UMS Version 6317A
13
GCMS Volatiles Method SW8260_258
Sample Results
Lab Name ALS Laboratory Group bullbull FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject ID 644-111809(HWB R-37 VOCs) PAR 002731703
Field 10 R-37 Sor 2-111809
Lab ID 0911214middot1
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml
Moisture NA QCBatchlD VL091125-4-5 Final Volume 10 ml
Date Collected 18-Nov-09 Run ID VL091125-4A Result Units UGL
Date Extracted 25-Nov-09 Cleanup NONE Clean DF 1
Analysis ReqCode 104 Date Analyzed 25-Nov-09 Basis As Received
Prep Method SW5030 Rev C File Name 028044
CASNO Target Analyte Dilution Factor
103-65-1 NmiddotPROPYLBENZENE 1
95-49-8 2-CHLOROTOLUENE 1
108-67-8 135-TRIMETHYLBENZENE 1
106-43-4 4-CHLOROTOLUENE 1
98-06-6 TER I-BUTYLBENZENE 1
95-63-6 124-TRIMETHYLBENZENE 1
135-98-8 SEC-BUTYLBENZENE 1
541-73-1 13-OICHLOROBENZENE 1
99-87-6 P-ISOPROPYLTOLUENE 1
106-46-7 lA-DICHLOROBENZENE 1
104-51-8 N-BUTYLBENZENE 1
95-50-1 12-DICHLOROBENZENE 1
96-12-8 l2-DIBROMOmiddot3-CHLOROPROPANE 1
120-82-1 12A-TRICHLOROBENZENE 1
187-68-3 HEXACHLOROBUTADIENE 1
91-20-3 NAPHTHALENE 1
87-61middot6 123-TRICHLOROBENZENE 1
75-05-8 ACETONITRILE 1
107middot05middot1 ALLYL CHLORIDE 1
110-57-6 TRANS-14-DICHLORO-2-BUTENE 1
164-17-5 ETHANOL 1
97-63-2 ETHYL METHACRYLATE 1
78-83-1 ISOBUTYL ALCOHOL 1
126-98-7 METHACRYLONITRILE 1
80-62-6 METHYL METHACRYLATE 1
107-12-0 PROPIONITRILE 1
Result Reporting Limit
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
2 2
05 05
05 05
05 05
05 05
50 50
50 50
5 5
200 200
5 5
100 100
35 35
5 5
25 25
MDL Result EPA Qualifier Qualifier
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
067 U
017 U
017 U
017 U
017 U
83 U
017 U
U u 78 U
017 U
17 U
17 U
17 U
33 U
Data Package 10 VL0911214-1
Date Printed Wednesday December 022009 ALS Laboratory Group MM Fe Page 3 of 8
LlMS VerSion 6317A
14
GCMS Volati las Method SW8260_258
Sample Results
Lab Name ALS Laboratory Group - FC
Work Order Number 0911214
Client Name New Mexico Environment Department 08
ClientProject 10 644-111B09(HWB R-37 VOGs) PAR 002731703
Field 10 R-37 Ser 2-111809 Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10ml
Lab 10 0911214-1 Moisture NA
Date Collected 1B-Nov-09 QCBatchlO VL091125-4-5
Run 10 VL091125-4A
Final Volume 10ml
Result Units UGIL Date Extracted 25-Nov-09 Cleanup NONE Clean OF
Analysis ReqCode 104 Date Analyzed 25-Nov-09
Prep Method SW5030 Rev G Basis As Received
File Name 028044
CASNO Target Analyte Dilution Factor
Result Reporting Limit
MDL Result Qualifier
EPA Qualifier
126-99-8 CHLOROPRENE 1 5 5 017 U
75-65-0 TERT-BUTANOL 1 100 100 33 U
108-20-3 ISOPROPYL ETHER 1 2 2 033 U
637-92-3 ETHYL TERT-BUTYL ETHER 1 2 2 033 U
994-05-8 TERT-AMYL METHYL ETHER 1 2 2 033 U
67-72-1 HEXACHLOROETHANE 1 2 2 033 U
Surrogate Recovery
CASNO Surrogate Analyte Result Flag Spike Amount
Percent Recovery
Control Limits
460-00-4 4-BROMOFLUOHOBENZENE 246 25 98 82 - 121
1868-53-7 DIBROMOFLUOHOMETHANE 248 25 99 BO - 123
2037-26-5 TOLUENE-DB 258 25 103 85middot116
Data Package 10 VL0911214-1
Date Printed Wednesday December 022009 ALS Laboratory Group bullbull FC Page 4 of 8
LIMS Version 0317 A
15
GCMS Volati les Method SW8260_25B
Sample Results
Lab Name ALS Laboratory Group -- FC
Worlt Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-111809(HWB Rmiddot37 VOCs) PAR 002731703
Field 10 Rmiddot37 Scr jmiddot111809
Lab 10 0911214-2
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml Moisture NfA QCBatchID VL091125-4middot5 Final Volume 10 ml
Date Collected 18middotNov-09 Run 10 VL091125-4A Result Units UGfL Date Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Analysis ReqCode 104 Date Analyzed 25middotNov-09 Basis As Received Prep Method SW5030 Rev C File Name 028045
CASNO Target Analyte Dilution Factor
Result Reporting Limit
MOL Result Qualifier
EPA Qualifier
75-71-8 DICHLORODIFLUOROMETHANE 1 05 05 017 U
74-87-3 CHLOROMETHANE 1 05 05 017 U
75-01middot4 VINYL CHLORIDE 1 05 05 017 U
74-83-9 BROMOMETHANE 1 1 1 017 U
75middot00middot3 CHLOROETHANE j 05 05 017 U
75-69-4 TRICHLOROFLUOROMETHANE 1 05 05 017 U
107-02-8 ACROLEIN 1 100 100 17 U
i 75-35-4 11-DICHLOROETHENE 1 05 05 017 U
67-64middot1 ACETONE 1 10 10 33 U
74-8S-4 IODOMETHANE 1 5 5 017 U
75-15-0 CARBON DISULFIDE 1 10 10 017 U
75-09-2 METHYLENE CHLORIDE 1 1 1 017 U
156-60-5 TRANS-12-DICHLOROETHENE 1 05 05 017 U
1634-04-4 METHYL TERTIARY BUTYL ETHER 1 1 1 017 U
107-13-1 ACRYLONITRILE 1 10 10 17 U
75-34middot3 11-DICHLOROETHANE 05 05 017 U
i 108-05-4 VINYL ACETATE 1 10 10 067 U
115659-2 CISmiddot 2middotDICHLOROETHENE 1 05 05 017 U
178-933 2middotBUTANONE 1 5 5 17 U
74-97middot5 BROMOCHLOROMET HANE 1 1 1 017 U
67-66-3 CHLOROFORM 1 05 05 017 U
71-55middot6 111middotTRICHLOROETHANE 1 1 1 017 U
594-20-7 22middotDICHLOROPROPANE 1 05 05 017 U
56-23-5 CARBON TETRACHLORIDE 1 05 05 017 U
563-58-6 11middotDICHLOROPROPENE 1 05 05 017 U
107-06-2 12middotDICHL OROETHANE 1 05 05 017 U
Data Package ID VL0911214-1
Date Printed Wednesday December 022009 ALS Laboratory Group -- Fe Page 5 of 8
16
GCMS Volatiles Method SW8260_25B
Sample Results
Lab Name ALS Laboratory Group -- FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-111809(HW3 R-37 VOCs) PAR 002731703
Field 10 R-37 Scr 1-11 1809
Lab 10 0911214-2
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml
Moisture NIA QCBatchlO VL091125-4-5 Final Volume 10 ml
Date Collected 18-Nov-09 Run 10 VL091125-4A Result Units UGL
[late Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Analysis ReqCode 104 Date Analyzed 25-Nov-09
Prep Method SW5030 Rev C Basis As Received
File Name 028045
CASNO Target Analyte Dilution Factor
71-43-2 BENZENE 1
79-01-6 TRICHLOROETHENE 1
78-87-5 12-DICHLOROPROPANE 1
74-95-3 DIBROMOMETHANE 1
75-27-4 BROMODICHLOROMETHANE 1
10061-01-5 CIS-13-DICHLOROPROPENE 1
108-10-1 4-METHYL-2-PtNTANON 1
108-88-3 TOLUENE 1
10061-02-6 TRANS-13-DICHLOROPROPENE 1
79-00-5 112-TRICHLOROETHANE 1
591-78-6 2-HEXANONE 1
127-18-4 TETRACHLOROETHENE 1
142-28-9 13-DICHLOROPROPANt 1
124-48-1 DI3ROMOCHLOROMETHANE 1
106-93-4 12-DIBROMOETHANE 1
108-90-7 CHLOROBENZENE 1
OETHANE 1
- 1
LENE 1
ENE 1
ENE 1
OFORM 1
OPYlBENZENE 1
96-18-4 123-TRICHLOROPROPANE 1
79-34-5 1122-TETRACHLOROETHANE 1
108-86-1 BROMOBENZENE 1
Result Reporting Limit
05 05
05 05
05 05
05 05
05 05
05 05
5 5
025 05
05 05
05 05
10 10
05 05
05 05
1 1
1 1
05 05
05 05
05 05
1 1
05 05
05 05
05 05
05 05
2 2
05 05
05 05
MDL Result EPA Qualifier Qualifier
017 U
017 U
017 U
017 U
017 U
017 U
17 U
017 J
017 U
017 U
17 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
Data Package 10 VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- Fe Page 6 of 8
317A
17
GCMS Volatiles Method SW8260 _258
Sample Results
Lab Name ALS Laboratory Group -- FC
Work Order Number 0911214
Client Name New Mexico Environment Department 08
ClientProject 10 644-11S09(HWB R-37 VOCs) PAR 002731703
Field 10 Rmiddot37 Scr 1-111809
Lab 10 0911214-2
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml Moisture NA QCBatchlD VL091125-4-5 Final Volume 10 ml
Date Collected 18-Nov-09 Run 10 VL091125-4A Result Units UGL Date Extracted 25-Nol-09 Cleanup NONE Clean OF
Analysis ReqCode 104 Date Analyzed 25-Nov-09 Basis As Received Prep Method SW5030 Rev C File Name D28045
CASNO Target Analyte Dilution Factor
103-65-1 N-PROPYLBENZENE 1
95-49-8 2-CHLOROTOLUENE 1
108-67-8 135-TRIMETHYLBENZENE 1
106-43-4 4-CHLOROTOLUENE 1
98-06-6 TERT-BUTYLBENZENE 1
95-63-6 124-TRIMETHYLBENZENE 1
135-98-8 SEC-BUTYLBENZENE 1
i 541-73-1 13middotDICHLOROBENZENE 1
99-87-6 PmiddotISOPROPYL TOLUENE 1
106-46-7 I 14-DICHLOROBENZENE 1
104-51-8 I N-BUTYLBENZENE 1
95-50-1 l2-DICHLOROBENZENE 1
96-12-8 I 12-DIBROMO-3-CHLOROPROPANE 1
120-82-1 124-TRICHLOROBENZENE 1
87-68-3 HEXACHLOROBUT ADIENE 1
91-20-3 NAPHTHALENE 1
87-61-6 123-TRICHLOROBENZENE 1
75-05-S ACETONITRILE 1
107-05-1 ALLYL CH LORIDE 1
110-57-6 TRAN S-14-DICHLORO-2-BUTENE 1
64-17-5 ETHANOL 1
97-63-2 ETHYL METHACRYLATE 1
78-83-1 ISOBUTYL ALCOHOL 1
126-98-7 METHACRYLONITRILE 1
80-62-6 METHYL METHACRYLATE 1
107-12-0 I PROPIONITRILE 1
Result Reporting Limit
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
2 2
05 05
05 05
05 05
05 05
50 50
50 50 I 5 5
200 200
5 5
100 100
35 35
5 5
25 25
MDL
017
017
017
017
017
017
017
017
017
017
017
017
067
017
017
017
017
83
017
17
78
017
17
17
17
33
Result EPA Qualifier Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
Data Package 10 VL0911214-1
Date Printed Wednesday December 022009 ALS Laboratory Group -- Fe Page 7 of 8
LlMS Version 6317A
18
GCMS Volatiles Method SW8260_258
Sample Results
Lab Name ALS Laboratory Group bullbull FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644middot111B09(HWB R-37 VOCs) PAR 002731703
Sample Matrix WATER Prep Batch VL091125--4 Sample Aliquot 10 mlRmiddot37 Ser 1-111809 Moisture NA QCBatchlO VL091125--4-5 Final Volume 10 m
0911214-2 Date Collected 18-Nov-09 Run 10 VL091125--4A Result Units UGL Date Extracted 25-Nov-09 Cleanup NONE Clean OF 1 Date Analyzed 25-Nov-09 Basis As Received
10
Analysis ReqCode 104 Prep Method SW5030 Rev C File Name 028045
I
CASNO Target Analyte Dilution Factor
Result Reporting Limit
MDL Result Qualifier
EPA Qualifier
126-99-8 CHLOROPRENE 1 5 5 017 U
75-65-0 TERT-BUTANOL 1 100 100 33 U
108-20-3 ISOPROPYL ETHER 1 2 2 033 U
637-92-3 ETHYL TERT-BUTYL ETHER 1 2 2 033 U
994-05--8 TERT-AMYL MTHYL ETHER 1 2 2 033 U
67-72-1 HEXACHLOROETHANE 1 2 2 033 U
Surrogate Recovery
CASNO Surrogate Analyte Result Flag Spike Amount
Percent Control Recovery Limits
460-00-4 4middotBROMOFLUOROBENZENE 247 25 99 1
1868-53-7 DIBROMOFLUOROMETHANE 248 25 99 80 123
2037-26-5 TOLUENEmiddotDB 255 25 102 85 - 116
Data Package 10 VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- FC Page B of 8
LlMS Version 6317A
19
GCMS Volatiles Method SW8260_258
Laboratory Control Sample and Laboratory Control Sample Duplicate
Lab Name ALS Laboratory Group - FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-111809(HWB R-37 VOCs) PAR 002731703
Lab 10 VL091125-4LCS Sample Matrix WATER
Moisture NA Prep Batch VL091125-4
QCBatchlD VL091125-4-5
Sample Aliquot
Final Volume
10ml
10ml Date Collected NA Run 10 VL091125-4A Result Units UGIL Date Extracted 111252009 Cleanup NONE Clean OF 1 Date Analyzed 11252009 Basis NA
Prep Method SW5030C File Name 028040
CASNO
74-87-3
75-01-4
74-83-9
75-69-4
75-35-4
75-15-0
156-60-5
75-34-3
108-05-4
156-59-2
78-93-3
67 -66-3
71-55-6
i 56-23-5
107-06-2
71-43-2
79-01-6
78-87-5
75-27-4
108-88-3
79-00-5
591-78-6
127-18-4
106-93-4
108-90-7
63Q20-6
Target Analyte Spike Added
CHLOROMETHANE 10
VINYL CHLORIDE 10
BROMOMETHANE 10
TRICHLOROFLUOROMETHANE 10
11-DICHLOROETHENE 10
CARBON DISULFIDE 10
TRANS-12-DICHLOROETHENE 10
11-DICHLOROETHANE 10
VINYL ACETATE 10
CIS-12-DICHLOROETHENE 10
2middotBUTANONE 40
CHLOROFORM 10
111-TRICHL ORO ETHANE 10
CARBON TETRACHLORIDE 10
12-DICHLOROETHANE 10
BENZENE 10
TRICHLOROETHENE 10
12-DICHLOROPROPANE 10
BROMODICHLOROMETHANE 10
TOLUENE 10
112-TRICHLOROETHANE 10
2-HEXANONE 40
TETRACHLOROETHENE 10
12-DIBROMOETHANE 10
CHLOROBENZENE 10
1112-TETRACHLOROETHANE 10
LCS Reporting Result Result Limit Qualifier
932 05
863 05
943 1
908 05
96 05
95 10 J
996 05
992 05
10 10
102 05
412 5
993 05
974 1
943 05
106 05
983 05
962 05
10 05
988 05
974 05
989 05
409 10
956 05
991 1
984 05
101 05
LCS Control Rec Limits
93 49 -129
86 46 134
94 32-121
91 67 -152
96 61 -135
95 61 -140
100 70 -122
99 76 -119
100 62 182
102 75 126
103 61 -137
99 79 120
97 76 - 114
94 58middot135
106 75middot132
98 70 shy 125
96 74 121
100 81 -119
99 79 - 123
97 76 - 120
99 81 -126
102 45 168
96 56 -128
99 79 -123
98 75 -120
101 82 - 123
Data Package 10 VL0911214middot1
-Date Printed Wednesday December 02 2009 ALS Laboratory Group -- Fe Page 1 of 4
LiMS Version 6317A
20
GCMS Volatiles Method SW8260_25B
Laboratory Control Sample and Laboratory Control Sample Duplicate
Lab Name ALS Laboratory Group - FC
Work Order Number 0911214
Client Name New Mexico Envircnment Department OB
ClientProject 10 644-111809(HWB R-37 VOes) PAR 002731703
Lab 10 VL091125-4LCS Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml
Moisture NIA QCBatchlO VL091125-4-5 Final Volume 10 mi
Date Collected NA Run 10 VL091125-4A Result Units UGL Date Extracted 11252009 Cleanup NONE Clean OF 1 Date Analyzed 111252009 Basis NA
Prep Method SW5030e File Name 028040
CASNO Target Analyte Spike Added
LCS Result
Reporting Limit
Result Qualifier
LCS Rec
Control Limits
100-41-4 ETHYLBENZENE 10 981 05 98 79 -114
136777-61-2 M+P-XYLENE 20 197 1 98 81-115
95-47-6 O-XYLENE 10 101 05 101 81 -115
95-49-8 2-CHLOROTOLUENE 10 97 05 97 80 -128
541-73-1 13-DICHLOROBENZiNt 10 977 05 98 81-116
106-46-7 14-DICHLOROBENZENE 10 979 05 98 81 -119
95-50-1 12-DICHLOROBENZENE 10 987 05 99 79 - 116
91-20-3 NAPHTHALENE 10 993 05 99 69 -126
87-61-6 123-TRICHLOROBENZENE 10 999 05 100 60 -137
Data Package ID VL0911214-1
Date Printed Wecnesday December 02 2009 ALS Laboratory Group -- Fe Page 2 of 4
21
GCMS Volatiles Method SW8260_25B
Laboratory Control Sample and Laboratory Control Sample Duplicate
Lab Name ALS Laboratory Group bullbull FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-11 1809(HWB R-37 VOCs) PAR 002731703
Lab 10 VL091125middot4LCSD Sample Matrix WATER
Moisture NIA Prep Batch VL091125-4
QCBatchlD VL091125-4-5
Sample Aliquot
Final Volume
10 ml
10ml Date Collected NIA Run ID VL091125-4A Result Units UGIL Date Extracted 112512009 Cleanup NONE Clean DF 1 Date Analyzed 1112512009 Basis NIA
Prep Method SW5030C File Name 028041
CASNO Target Analyte Spike Added
LCSD Result
Reporting Limit
Result Qualifier
LCSD Rec
RPD Limit
RPD
74-87-3 CHLOROMETHANE 10 897 05 90 30 4
75-01-4 VINYL CHLORIDE 10 831 05 83 25 4
74-83-9 BROMO METHANE 10 945 1 94 25 0
75-69-4 TRICHLOROFLUOROMETHANE 10 873 05 87 22 4
75-35-4 11-DICHLOROETHENE 10 909 05 91 18 5
75-15-0 CARBON DISULFIDE 10 941 10 J 94 20 1
156-60middot5 TRANS-l2middotDICHLOROETHENE 10 961 05 96 25 4
75middot34middot3 11-DICHLOROETHANE 10 977 05 98 25 2
108-05-4 VINYL ACETATE 10 993 10 J 99 20 1
156middot59-2 CIS-12-DlCHLOROETHENE 10 995 05 99 25 3
i 78-93-3 2-BUTANONE 40 419 5 105 30 2
67-66-3 CHLOROFORM 10 985 05 99 25 1
71-55-6 lll-TRICHLOROETHANE 10 942 1 94 25 3
56-23-5 CARBON TETRACHLORIDE 10 922 05 92 25 2
107middot06-2 12middotDICHLOROETHANE 10 106 05 106 25 0
71-43middot2 BENZENE 10 971 05 97 10 1
79middot01middot6 TRICHLOROETHENE 10 939 05 94 10 2
78middot87middot5 l2middotDICHLOROPROPANE 10 101 05 101 25 1
i 75middot27-4 BROMODICHLOROMETHANE 10 992 05 99 25 0
1108-88-3 TOLUENE 10 962 05 96 9 1
I 79005 112middotTRICHLOROETHANE 10 986 05 99 25 0
591middot78middot6 2-HEXANONE 40 418 10 104 20 2
127middot18-4 TETRACHLOROETHENE 10 918 05 92 25 4
106-93-4 12middotDIBROMOETHANE 10 999 1 100 15 1
108middot90-7 CHLOROBENZENE 10 997 05 100 11 1
630-20middot6 1112-TETRACHLOROETHANE 10 101 05 101 15 0
100-41-4 ETHYLBENZENE 10 968 05 97 25 1
Data Package ID VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- FC Page 3 of 4
lIMS Version 6317 A
22
GCMS Volatiles Method SW8260_25B
Laboratory Control Sample and Laboratory Control Sample Duplicate
Lab Name ALS Laboratory 13roup -- FC
Work Order Number 0911214
Client Name New Mexico Environment Department OS
ClientProject 10 644-11 1809(HWB R-37 VOCs) PAR 002731703
Lab 10 VL091125-4LCSD Sample Matrix WATER
Moisture NA Prep Batch VL091125-4
QCBatchlO VL091125-4-5
Sample Aliquot
Final Volume
10 ml
10ml Date Collected NA Run 10 VL091125-4A Result Units UGL Date Extracted 11252009 Cleanup NONE Clean OF Date Analyzed 11252009 Basis NIA
Prep Method SW5030C File Name 028041
CASNO Target Analyte Spike Added
LCSD Result
Reporting Limit
Result Qualifier
LCSD Rec
RPD Limit
RPD
136777-61-2 M+P-XYLENE 20 193 1 97 25 2
95-47-6 O-XYLENE 10 983 05 98 25 2
95-49-8 2middotCHLOROTOLUENE 10 9A9 05 95 15 2
541-73-1 13middotDICHLOROBENZENE 10 997 05 100 25 2
106-46-7 14-DICHLOROBeNZENE 10 974 05 97 25 1
95-50middot1 12middotDICHLOROBENZeNE 10 101 05 101 25 2
91middot20-3 NAPHTHALENe 10 105 05 105 24 6
87-61-6 123-TRICHLOROBENZENE 10 102 05 102 33 3
Surrogate Recovery LCSLCSD
CASNO Target Analyte Spike Added
LCS Rec
LCS Flag
LCSD Rec
LCSD Flag
Control Limits
460middot00-4 4-BROMOFLUOROBeNZENE 25 100 100 82 - 121
1868-53middot7 DIBROMOFLUOROMeTHANE 25 101 100 80middot 123
2037middot26-5 TOLUENEmiddotD8 25 102 100 85middot 116
Data Package 10 VL0911214-
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- Fe Page 4 of 4
UMS Verslmt 6317A
23
ALS Laboratory Group -- Fe Sample Number(s) Cross-Reference Table
Paragon OrderNum 0911214 Client Name New Mexico Environment Department OB
Client Project Name 644-111809(HWB R-37 VOCs) PAR Client Project Number 002731703
Client PO Number 06-667-55-01754
Client Sample Number
Lab Sample Number
COC Number Matrix Date Collected
Time Collected
R-37 Scr 2-1 11809 0911214-1 WATER 18-Nov-09 1555 R-37 Scr 1-111809 0911214-2 WATER 18-Nov-09 1744
Page 1 of 1 ALS Laboratory Group -- Fe Date Printed Wednesday December 02 2009 LlMS Version 6317 A
4
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Client _-=-N--M---f-=-D________ IVorkorde No D4 J I 4 --~~~~~~------
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14 Are all samples requiring no headspace (VOC GRG RSKlVIEE lb eNS radon)
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17 Were the lljIV~IOU on ice
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Additional Iuformation OVIDE DETAILS BELOW FOR A ND RESPONSE TO ANY (UESTION A80VE EXCEPT 1 ANI) 16
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7
GCMS Volatiles Method SW8260 _25B
Method Blank
Lab Name ALS Laboratory Group bullbull FC
Work Order Number 0911214
Client Name New Mexico Environment Department DB
ClientProject 10 644-111809(HWB Rmiddot37 VOCs) PAR 002731703
Lab 10 VL091125-4MB Sample Matrix WATER
Moisture NA Prep Batch VL091125-4
QCBatchlO VL091125-4-5
Sample Aliquot
Final Volume
10 ml
10 ml Date Collected NA Run 10 VL091125-4A Result Units UGL Date Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Date Analyzed 25middotNov-09 Basis NA
File Name 028043
CASNO Target Analyte DF
75-71-8 DICHLORODIFLUOROMETHANE
74-87-3 CHLOROMETHANE
75-01-4 VINYL CHLORIDE
74-83-9 BROMOMETHANE
75-00-3 CHLOROETHANE
75-69-4 TRICHLOROFLUOROMETHANE
107-02-8 ACROLEIN
75-35-4 11middotDICHLOROETHENE
67-64-1 ACETONE
74-88-4 IODOMETHANE
75-15-0 CARBON DISULFIDE
METHYLEN E CHLORIDE 75-09-2
156-60-5 TRANS-12middotDICHLOROETHENE
1634-04-4 METHYL TERTIARY BUTYL ETHER
107-13-1 ACRYLONITRILE
75-34-3 11-DICHLOROETHANE
108-05-4 VINYL ACETATE
156-59middot2 CIS-12middotDICHLOROETHENE
78-93-3 2middotBUTANONE
~ BROMOCHLOROMETHANE
67-66-3 CHLOROFORM
71-55-6 111middot TRICHLOROETHANE
594-20-7 22middotDICHLOROPROPANE
56-23-5 CARBON TETRACHLORIDE
563-58-6 11middotDICHLOROPROPENE
107-06middot2 l2middotDICHLOROETHAN E
71-43-2 BENZENE
79-01-6 TRICHLOROETHENE
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Result Reporting Limit
05 05
05 05
05 05
1 1
05 05
05 05
100 100
05 05
10 10
5 5
10 10
1 1
05 05
1 1
10 10
05 05
10 10
05 05
5 5
1 1
05 05
1 1
05 05
05 05
05 05
05 05
05 05
05 05
MDL Result EPA Qualifier Qualifier
017 U
017 U
017 U
017 U
017 U
017 U
17 U
017 U
33 U
017 U
017 U
017 U
017 U
017 U
17 U
017 U
067 U
017 U
17 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
Data Package 10 VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- Fe Page 1 of 4
llMS Version 6317 A
8
GCMS Volatiles Method SW8260 _25B
Method Blank
Lab Name ALS Laboratory Group -- FC
Work Order Number 0911214
Client Name New Mexico Environment Department 08
ClientProject 10 644-111809(HWEI R-37 voes) PAR 002731703
Lab 10 VL091125-4MB Sample Matrix WATER
Moisture NIA Prep Batch VL091125-4
QCBatchIO VL091125-4-5
Sample Aliquot
Final Volume
10 ml
10 ml Oate Collected NIA Run 10 VL091125-4A Result Units UGL Oate Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Date Analyzed 25-Nov-09 Basis NIA
File Name 028043
CASNO Target Analyte OF Result Reporting Limit
MOL Result Qualifier
EPA Qualifier
78-87-5 12middotDICHLOROPROPANE 1 05 05 017 U
74-95-3 DIBROMOMETHANE 1 05 05 017 U
75-27-4 BROMODICHLOROMETHANE 1 05 05 017 U
10061-01-5 CISmiddot13middotDICHLOROPROPENE 1 05 05 017 U
108-10-1 4-METHYL-2-PENT ANONE 1 5 5 17 U
108-88-3 TOLUENE 1 05 05 017 U
10061-02-6 TRANS-13-DICHLOROPROPENE 1 05 05 017 U
79-00-5 112-TRICHLOROETHANE 1 05 05 017 U
591-78-6 2-HEXANONE 1 10 10 17 U
127-18-4 TETRACHLOROETHENE 1 05 05 017 U
142-28-9 13-DICHLOROPROPANI 1 05 05 017 U
124-48-1 DIBROMOCHLOROMETHANE 1 1 1 017 U
106-93-4 12-DIBROMOETHANE 1 1 1 017 U
108-90-7 CHLOROBENZENE 1 05 05 017 U
630-20-6 1112-TETRACHLOROETHANE 1 05 05 017 U
100-41-4 ETHYLBENZENE 1 05 05 017 U
136777-61-2 M+P-XYLENE 1 1 1 017 U
95-47-6 O-XYLENE 1 05 05 017 U
100-42-5 STYRENE 1 05 05 017 U
75-25-2 BROMOFORM 1 05 05 017 U
98-82-8 ~YLBENZENE 1 05 05 017 U
96-18-4 123-TRICHLOROPROPANE 1 2 2 017 U
79-34-5 1122middot TETRACHLOROETHANE 1 05 05 017 U
108-86-1 BROMOBENZENE 1 05 05 017 U
103-65-1 N-PROPYLBENZENE 1 05 05 017 U
95-49-8 2-CHLOROTOLUENE 1 05 05 017 U
108-67-8 135-TRIMETHYLBENZENE 1 05 05 017 U
106-43-4 4-CHLOROTOLUENE 1 05 05 017 U
Data Package 10 VL0911214-1
Date Printed Wednesday December n 2009 AlS Laboratory Group -- FC Page 2 of 4
lMS VeCSiOIY 6317A
9
GCMS Volatiles Method SW8260 _258
Method Blank
Lab Name ALS Laboratory Group - FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-111B09(HWB R-37 VOCs) PAR 002731703
Lab 10 VL091125-4MB Sample Matrix WATER
Moisture NIA
Prep Batch VL091125-4
QCBatchlD VL091125-4-5
Sample Aliquot
Final Volume
10 ml
10 ml
Date Collected NIA Run ID VL091125-4A Result Units UGL
Date Extracted 25-Nov-09 Cleanup NONE Clean DF 1
Date Analyzed 25-Nov-09 Basis NA
File Name 028043
CASNO Target Analyte OF Result Reporting Limit
MOL Result Qualifier
EPA Qualifier
98-06-6 TERT-BUTYLBENZENE 1 05 05 017 U
95-63-6 124-TRIMETHYLBENZENE 1 05 05 017 U
135-98-8 SEC-BUTYLBENZENE 1 05 05 017 U
541-73-1 13-DlCHLOROBENZENE 1 05 05 017 U
99-87-6 P-ISOPROPYLTOLUENE 1 05 05 017 U
106-46-7 1 A-DICHLOROBENZENE 1 05 05 017 U
104-51-8 N-BUTYLBENZENE 1 05 05 017 U
95-50-1 12-DICHLOROBENZENE 1 05 05 017 U
96-12-B 12-DIBROMO-3-CHLOROPROPANE 1 2 2 067 U
120-82-1 124-TRiCHLOROBENZENE 1 05 05 017 U
87-68-3 HEXACHLOROBUTADIENE 1 05 05 017 U
91-20-3 NAPHTHALENE 1 05 05 017 U
87-61-6 123-TRICHLOROBENZENE 1 05 05 017 U
75-05-B ACETONITRILE 1 50 50 83 U
107-05-1 ALLYL CHLORIDE 1 50 50 017 U
110-57-6 TRANS-14-DICHLORO-2-BUTENE 1 5 5 17 U
64-17-5 ETHANOL 1 200 200 78 U
97-63-2 ETHYL METHACRYLATE 1 5 5 017 U
78-83-1 ISOBUTYL ALCOHOL 1 100 100 17 U
126-98-7 METHACRYLONITRILE 1 35 35 17 U
80-62-6 METHYL METHACRYLATE 1 5 5 17 U
107-12-0 PROPIONITRILE 1 25 25 33 U
126-99-8 CHLOROPRENE 1 5 5 017 U
75-65-0 TERT-BUTANOL 1 100 100 33 U
108-20-3 ISOPROPYL ETHER 1 2 2 033 U
637-92-3 ETHYL TERT-BUTYL ETHER 1 2 2 033 U
994-05-8 TERT-AMYL METHYL ETHER 1 2 2 033 U
67-72-1 HEXACHLOROETHANE 1 2 2 033 U
Data Package 10 VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -~ Fe Page 3 of 4
LlMS Version 6317 A
10
GCMS Volatiles Method SW8260 _258
Method Blank
Lab Name ALS Laboratory Group -- FC
Work Order Number 0911214
Client Name New Mexico Envirmment Department OB
ClientProject 10 644-111809(HWB R-37 VOCs) PAR 002731703
Lab 10 VL091125-4MB Sample Matrix WATER
Moisture NIA Prep Batch VL091125-4
QCBatchlO VL091125-4-5
Sample Aliquot
Final Volume
10 m
10m Date Collected NIA Run 10 VL091125-4A Result Units UGIL Date Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Date Analyzed 25-Nov-09 BasisNIA
File Name 028043
CASNO Target Analyte Result Reporting MOL Result EPAOF Limit Qualifier Qualifier
Surrogate Recovery
CASNO Surrogate Analyte Result Flag Spike Amount
Percent Recovery
Control Limits
460-00-4 4-BROMOFLUOROBENZENE 25 25 100 82 - 121
1868-53-7 DIBROMOFLUOROMETHANE 248 25 99 80 - 123
2037-26-5 TOLUENE-D8 26 25 104 85 - 116
Data Package 10 VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- FC Page 4 of4
LlMS Version 6317A
11
GCMS Volati les Method SW8260 _258
Sample Results
Lab Name ALS Laboratory Group -- FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-111809(HWB R-37 VOCs) PAR 002731703
Field 10 Rmiddot37 Ser 2middot111809
Lab 10 0911214middot1
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml
Moisture NA QCBatchlO VL091125-4-5 Final Volume 10mi Date Collected 18-Nov-09 Run 10 VL091125-4A Result Units UGL
Date Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Analysis ReqCode 104 Date Analyzed 25-Nov-09
Prep Method SW5030 Rev C Basis As Received
File Name 028044
CASNO Target Analyte Dilution Factor
75-71-8 DICHLORODIFLUOROMETHANE 1
74middot87-3 CHLOROMETHANE 1
75-01-4 VINYL CHLORIDE 1
74-83-9 BROMOMETHANE 1
75-00-3 CHLOROETHANE 1
75-69-4 TRICHLOROFLUOROMETHANE 1
107-02-8 ACROLEIN 1
75-35-4 11middotDICHLOROETHENE 1
67-64-1 ACETONE 1
74-88-4 IODOMETHANE 1
75-15-0 CARBON DISULFIDE 1
75-09-2 METHYLENE CHLORIDE 1
156-60-5 TRANSmiddot12middotDICHLOROETHENE 1
1634-04-4 METHYL TERTIARY BUTYL ETHER 1
107-13-1 ACRYLONITRILE 1
75-34-3 1-DICHLOROETHANE 1
i 108-05-4 VINYL ACETATE 1
156-59-2 CIS-12middotDICHLOROETHENE 1
78-93-3 2-BUTANONE 1
74-97-5 BROMOCHLOROMETHANE 67-66-3 CHLOROFORM 1
71-55-6 11-TRICHLOROETHANE 594-20-7 22-DICHLOROPROPANE 56-23-5 CARBON TETRACHLORIDE 563-58-6 -DICHLOROPROPENE 107-06-2 2-DICHLOROETHANE
Result Reporting Limit
05 05
05 05
05 05
1 1
05 05
05 05
100 100
05 05
10 10
5 5
10 10
1 1
05 05
1 1
10 10
05 05
10 10
05 05
5 5
1 1
05 05
1 1
05 05
05 05
05 05
05 05
MOL Result EPA Qualifier Qualifier
017 U
017 U
017 U
017 U
017 U
017 U
17 U
017 U
33 U
017 U
017 U
017 U
017 U
017 U
17 U
017 U
067 U
017 U
17 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
Data Package ID VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- Fe Page 1 of 8
UMS Version 6317A
12
GCMS Volatiles Method SW8260_25B
Sample Results
Lab Name ALS Laboratory Group - FC
Work Order Number 0911214
Client Name New Mexico nvironment Department OB
ClientProject 10 644-111809(HWB R-37 VOCs) PAR 002731703
Field 10 R-37 Scr 2-111809
Lab 10 0911214-1
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10ml
Moisture NA QCBatchlD VL091125-4-5 Final Volume 10ml
Date Collected l8-Nov-09 Run 10 VL091125-4A Result Units UGL
Date Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Analysis ReqCode 104 Date Analyzed 25-Nov-09 Basis As Received
Prep Method SW5030 Rev C File NameD28044
CASNO Target Analyte Dilution Factor
Result Reporting Limit
MDL Result Qualifier
EPA Qualifier
I
71-43-2 BENZENE 1 05 05 017 U
79-01-6 TRICHLOROETHENE 1 05 05 017 U
78-87-5
74middot95-3
75-27-4
10061-01-5
108middot10middot1
108middot88-3
10061-02middot6
79-00-5
591-78-6
12-DICHLOROPROPANE
DIBROMOMETHANE
BROMODCHLOROMETHANE
CIS-13-DICHLOROPROPEI~E
4-METHYL-2-PENTANONE
TOLUENE
TRANS-13-DICHLOROPROPENE
112-TRICHLOROETHANE
2-HEXANONE
1
1
1
1
1
1
1
1
1
05
05
05
05
5
031
05
05
10
05
05
05
05
5
05
05
05
10
017
017
017
017
17
017
017
017
17
U
U
U
U
U
J
U
U
U
127-18-4
142-28-9
124-48-1
106-93-4
108-90-7
630-20-6
100-41-4
136777-61-2
95-47-6
100-42middot5
75-25-2
98-82middot8
96-18-4
79-34-5
108-86-1
TETRACHLOROETHENE
13-DICHLOROPROPANE
DIBROMOCHLOROMETHANE
12-DIBROMOETHANE
CHLOROBENZENE
11 12-TETRACHLOROETHANE
ETHYLBENZENE
M+PmiddotXYLENE
OmiddotXYLENE
STYRENE
BROMOFORM
ISOPRO PYLBENZENE
123middotTRICHLOROPROPANE
1122-TETRACHLOROETHANE
BROMOBENZENE
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
05
05
1
1
05
05
05
1
05
05
05
05
2
05
05
05
05
1
1
05
05
05
1
05
05
05
05
2
05
05
017
017
017
017
017
017
017
017
017
017
017
017
017
017
017
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
i
Data Package 10 VL0911214-1
Date Printed Wednesday December 022009 AlS laboratory Group bullbull Fe Page 2 of 8
UMS Version 6317A
13
GCMS Volatiles Method SW8260_258
Sample Results
Lab Name ALS Laboratory Group bullbull FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject ID 644-111809(HWB R-37 VOCs) PAR 002731703
Field 10 R-37 Sor 2-111809
Lab ID 0911214middot1
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml
Moisture NA QCBatchlD VL091125-4-5 Final Volume 10 ml
Date Collected 18-Nov-09 Run ID VL091125-4A Result Units UGL
Date Extracted 25-Nov-09 Cleanup NONE Clean DF 1
Analysis ReqCode 104 Date Analyzed 25-Nov-09 Basis As Received
Prep Method SW5030 Rev C File Name 028044
CASNO Target Analyte Dilution Factor
103-65-1 NmiddotPROPYLBENZENE 1
95-49-8 2-CHLOROTOLUENE 1
108-67-8 135-TRIMETHYLBENZENE 1
106-43-4 4-CHLOROTOLUENE 1
98-06-6 TER I-BUTYLBENZENE 1
95-63-6 124-TRIMETHYLBENZENE 1
135-98-8 SEC-BUTYLBENZENE 1
541-73-1 13-OICHLOROBENZENE 1
99-87-6 P-ISOPROPYLTOLUENE 1
106-46-7 lA-DICHLOROBENZENE 1
104-51-8 N-BUTYLBENZENE 1
95-50-1 12-DICHLOROBENZENE 1
96-12-8 l2-DIBROMOmiddot3-CHLOROPROPANE 1
120-82-1 12A-TRICHLOROBENZENE 1
187-68-3 HEXACHLOROBUTADIENE 1
91-20-3 NAPHTHALENE 1
87-61middot6 123-TRICHLOROBENZENE 1
75-05-8 ACETONITRILE 1
107middot05middot1 ALLYL CHLORIDE 1
110-57-6 TRANS-14-DICHLORO-2-BUTENE 1
164-17-5 ETHANOL 1
97-63-2 ETHYL METHACRYLATE 1
78-83-1 ISOBUTYL ALCOHOL 1
126-98-7 METHACRYLONITRILE 1
80-62-6 METHYL METHACRYLATE 1
107-12-0 PROPIONITRILE 1
Result Reporting Limit
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
2 2
05 05
05 05
05 05
05 05
50 50
50 50
5 5
200 200
5 5
100 100
35 35
5 5
25 25
MDL Result EPA Qualifier Qualifier
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
067 U
017 U
017 U
017 U
017 U
83 U
017 U
U u 78 U
017 U
17 U
17 U
17 U
33 U
Data Package 10 VL0911214-1
Date Printed Wednesday December 022009 ALS Laboratory Group MM Fe Page 3 of 8
LlMS VerSion 6317A
14
GCMS Volati las Method SW8260_258
Sample Results
Lab Name ALS Laboratory Group - FC
Work Order Number 0911214
Client Name New Mexico Environment Department 08
ClientProject 10 644-111B09(HWB R-37 VOGs) PAR 002731703
Field 10 R-37 Ser 2-111809 Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10ml
Lab 10 0911214-1 Moisture NA
Date Collected 1B-Nov-09 QCBatchlO VL091125-4-5
Run 10 VL091125-4A
Final Volume 10ml
Result Units UGIL Date Extracted 25-Nov-09 Cleanup NONE Clean OF
Analysis ReqCode 104 Date Analyzed 25-Nov-09
Prep Method SW5030 Rev G Basis As Received
File Name 028044
CASNO Target Analyte Dilution Factor
Result Reporting Limit
MDL Result Qualifier
EPA Qualifier
126-99-8 CHLOROPRENE 1 5 5 017 U
75-65-0 TERT-BUTANOL 1 100 100 33 U
108-20-3 ISOPROPYL ETHER 1 2 2 033 U
637-92-3 ETHYL TERT-BUTYL ETHER 1 2 2 033 U
994-05-8 TERT-AMYL METHYL ETHER 1 2 2 033 U
67-72-1 HEXACHLOROETHANE 1 2 2 033 U
Surrogate Recovery
CASNO Surrogate Analyte Result Flag Spike Amount
Percent Recovery
Control Limits
460-00-4 4-BROMOFLUOHOBENZENE 246 25 98 82 - 121
1868-53-7 DIBROMOFLUOHOMETHANE 248 25 99 BO - 123
2037-26-5 TOLUENE-DB 258 25 103 85middot116
Data Package 10 VL0911214-1
Date Printed Wednesday December 022009 ALS Laboratory Group bullbull FC Page 4 of 8
LIMS Version 0317 A
15
GCMS Volati les Method SW8260_25B
Sample Results
Lab Name ALS Laboratory Group -- FC
Worlt Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-111809(HWB Rmiddot37 VOCs) PAR 002731703
Field 10 Rmiddot37 Scr jmiddot111809
Lab 10 0911214-2
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml Moisture NfA QCBatchID VL091125-4middot5 Final Volume 10 ml
Date Collected 18middotNov-09 Run 10 VL091125-4A Result Units UGfL Date Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Analysis ReqCode 104 Date Analyzed 25middotNov-09 Basis As Received Prep Method SW5030 Rev C File Name 028045
CASNO Target Analyte Dilution Factor
Result Reporting Limit
MOL Result Qualifier
EPA Qualifier
75-71-8 DICHLORODIFLUOROMETHANE 1 05 05 017 U
74-87-3 CHLOROMETHANE 1 05 05 017 U
75-01middot4 VINYL CHLORIDE 1 05 05 017 U
74-83-9 BROMOMETHANE 1 1 1 017 U
75middot00middot3 CHLOROETHANE j 05 05 017 U
75-69-4 TRICHLOROFLUOROMETHANE 1 05 05 017 U
107-02-8 ACROLEIN 1 100 100 17 U
i 75-35-4 11-DICHLOROETHENE 1 05 05 017 U
67-64middot1 ACETONE 1 10 10 33 U
74-8S-4 IODOMETHANE 1 5 5 017 U
75-15-0 CARBON DISULFIDE 1 10 10 017 U
75-09-2 METHYLENE CHLORIDE 1 1 1 017 U
156-60-5 TRANS-12-DICHLOROETHENE 1 05 05 017 U
1634-04-4 METHYL TERTIARY BUTYL ETHER 1 1 1 017 U
107-13-1 ACRYLONITRILE 1 10 10 17 U
75-34middot3 11-DICHLOROETHANE 05 05 017 U
i 108-05-4 VINYL ACETATE 1 10 10 067 U
115659-2 CISmiddot 2middotDICHLOROETHENE 1 05 05 017 U
178-933 2middotBUTANONE 1 5 5 17 U
74-97middot5 BROMOCHLOROMET HANE 1 1 1 017 U
67-66-3 CHLOROFORM 1 05 05 017 U
71-55middot6 111middotTRICHLOROETHANE 1 1 1 017 U
594-20-7 22middotDICHLOROPROPANE 1 05 05 017 U
56-23-5 CARBON TETRACHLORIDE 1 05 05 017 U
563-58-6 11middotDICHLOROPROPENE 1 05 05 017 U
107-06-2 12middotDICHL OROETHANE 1 05 05 017 U
Data Package ID VL0911214-1
Date Printed Wednesday December 022009 ALS Laboratory Group -- Fe Page 5 of 8
16
GCMS Volatiles Method SW8260_25B
Sample Results
Lab Name ALS Laboratory Group -- FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-111809(HW3 R-37 VOCs) PAR 002731703
Field 10 R-37 Scr 1-11 1809
Lab 10 0911214-2
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml
Moisture NIA QCBatchlO VL091125-4-5 Final Volume 10 ml
Date Collected 18-Nov-09 Run 10 VL091125-4A Result Units UGL
[late Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Analysis ReqCode 104 Date Analyzed 25-Nov-09
Prep Method SW5030 Rev C Basis As Received
File Name 028045
CASNO Target Analyte Dilution Factor
71-43-2 BENZENE 1
79-01-6 TRICHLOROETHENE 1
78-87-5 12-DICHLOROPROPANE 1
74-95-3 DIBROMOMETHANE 1
75-27-4 BROMODICHLOROMETHANE 1
10061-01-5 CIS-13-DICHLOROPROPENE 1
108-10-1 4-METHYL-2-PtNTANON 1
108-88-3 TOLUENE 1
10061-02-6 TRANS-13-DICHLOROPROPENE 1
79-00-5 112-TRICHLOROETHANE 1
591-78-6 2-HEXANONE 1
127-18-4 TETRACHLOROETHENE 1
142-28-9 13-DICHLOROPROPANt 1
124-48-1 DI3ROMOCHLOROMETHANE 1
106-93-4 12-DIBROMOETHANE 1
108-90-7 CHLOROBENZENE 1
OETHANE 1
- 1
LENE 1
ENE 1
ENE 1
OFORM 1
OPYlBENZENE 1
96-18-4 123-TRICHLOROPROPANE 1
79-34-5 1122-TETRACHLOROETHANE 1
108-86-1 BROMOBENZENE 1
Result Reporting Limit
05 05
05 05
05 05
05 05
05 05
05 05
5 5
025 05
05 05
05 05
10 10
05 05
05 05
1 1
1 1
05 05
05 05
05 05
1 1
05 05
05 05
05 05
05 05
2 2
05 05
05 05
MDL Result EPA Qualifier Qualifier
017 U
017 U
017 U
017 U
017 U
017 U
17 U
017 J
017 U
017 U
17 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
Data Package 10 VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- Fe Page 6 of 8
317A
17
GCMS Volatiles Method SW8260 _258
Sample Results
Lab Name ALS Laboratory Group -- FC
Work Order Number 0911214
Client Name New Mexico Environment Department 08
ClientProject 10 644-11S09(HWB R-37 VOCs) PAR 002731703
Field 10 Rmiddot37 Scr 1-111809
Lab 10 0911214-2
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml Moisture NA QCBatchlD VL091125-4-5 Final Volume 10 ml
Date Collected 18-Nov-09 Run 10 VL091125-4A Result Units UGL Date Extracted 25-Nol-09 Cleanup NONE Clean OF
Analysis ReqCode 104 Date Analyzed 25-Nov-09 Basis As Received Prep Method SW5030 Rev C File Name D28045
CASNO Target Analyte Dilution Factor
103-65-1 N-PROPYLBENZENE 1
95-49-8 2-CHLOROTOLUENE 1
108-67-8 135-TRIMETHYLBENZENE 1
106-43-4 4-CHLOROTOLUENE 1
98-06-6 TERT-BUTYLBENZENE 1
95-63-6 124-TRIMETHYLBENZENE 1
135-98-8 SEC-BUTYLBENZENE 1
i 541-73-1 13middotDICHLOROBENZENE 1
99-87-6 PmiddotISOPROPYL TOLUENE 1
106-46-7 I 14-DICHLOROBENZENE 1
104-51-8 I N-BUTYLBENZENE 1
95-50-1 l2-DICHLOROBENZENE 1
96-12-8 I 12-DIBROMO-3-CHLOROPROPANE 1
120-82-1 124-TRICHLOROBENZENE 1
87-68-3 HEXACHLOROBUT ADIENE 1
91-20-3 NAPHTHALENE 1
87-61-6 123-TRICHLOROBENZENE 1
75-05-S ACETONITRILE 1
107-05-1 ALLYL CH LORIDE 1
110-57-6 TRAN S-14-DICHLORO-2-BUTENE 1
64-17-5 ETHANOL 1
97-63-2 ETHYL METHACRYLATE 1
78-83-1 ISOBUTYL ALCOHOL 1
126-98-7 METHACRYLONITRILE 1
80-62-6 METHYL METHACRYLATE 1
107-12-0 I PROPIONITRILE 1
Result Reporting Limit
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
2 2
05 05
05 05
05 05
05 05
50 50
50 50 I 5 5
200 200
5 5
100 100
35 35
5 5
25 25
MDL
017
017
017
017
017
017
017
017
017
017
017
017
067
017
017
017
017
83
017
17
78
017
17
17
17
33
Result EPA Qualifier Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
Data Package 10 VL0911214-1
Date Printed Wednesday December 022009 ALS Laboratory Group -- Fe Page 7 of 8
LlMS Version 6317A
18
GCMS Volatiles Method SW8260_258
Sample Results
Lab Name ALS Laboratory Group bullbull FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644middot111B09(HWB R-37 VOCs) PAR 002731703
Sample Matrix WATER Prep Batch VL091125--4 Sample Aliquot 10 mlRmiddot37 Ser 1-111809 Moisture NA QCBatchlO VL091125--4-5 Final Volume 10 m
0911214-2 Date Collected 18-Nov-09 Run 10 VL091125--4A Result Units UGL Date Extracted 25-Nov-09 Cleanup NONE Clean OF 1 Date Analyzed 25-Nov-09 Basis As Received
10
Analysis ReqCode 104 Prep Method SW5030 Rev C File Name 028045
I
CASNO Target Analyte Dilution Factor
Result Reporting Limit
MDL Result Qualifier
EPA Qualifier
126-99-8 CHLOROPRENE 1 5 5 017 U
75-65-0 TERT-BUTANOL 1 100 100 33 U
108-20-3 ISOPROPYL ETHER 1 2 2 033 U
637-92-3 ETHYL TERT-BUTYL ETHER 1 2 2 033 U
994-05--8 TERT-AMYL MTHYL ETHER 1 2 2 033 U
67-72-1 HEXACHLOROETHANE 1 2 2 033 U
Surrogate Recovery
CASNO Surrogate Analyte Result Flag Spike Amount
Percent Control Recovery Limits
460-00-4 4middotBROMOFLUOROBENZENE 247 25 99 1
1868-53-7 DIBROMOFLUOROMETHANE 248 25 99 80 123
2037-26-5 TOLUENEmiddotDB 255 25 102 85 - 116
Data Package 10 VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- FC Page B of 8
LlMS Version 6317A
19
GCMS Volatiles Method SW8260_258
Laboratory Control Sample and Laboratory Control Sample Duplicate
Lab Name ALS Laboratory Group - FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-111809(HWB R-37 VOCs) PAR 002731703
Lab 10 VL091125-4LCS Sample Matrix WATER
Moisture NA Prep Batch VL091125-4
QCBatchlD VL091125-4-5
Sample Aliquot
Final Volume
10ml
10ml Date Collected NA Run 10 VL091125-4A Result Units UGIL Date Extracted 111252009 Cleanup NONE Clean OF 1 Date Analyzed 11252009 Basis NA
Prep Method SW5030C File Name 028040
CASNO
74-87-3
75-01-4
74-83-9
75-69-4
75-35-4
75-15-0
156-60-5
75-34-3
108-05-4
156-59-2
78-93-3
67 -66-3
71-55-6
i 56-23-5
107-06-2
71-43-2
79-01-6
78-87-5
75-27-4
108-88-3
79-00-5
591-78-6
127-18-4
106-93-4
108-90-7
63Q20-6
Target Analyte Spike Added
CHLOROMETHANE 10
VINYL CHLORIDE 10
BROMOMETHANE 10
TRICHLOROFLUOROMETHANE 10
11-DICHLOROETHENE 10
CARBON DISULFIDE 10
TRANS-12-DICHLOROETHENE 10
11-DICHLOROETHANE 10
VINYL ACETATE 10
CIS-12-DICHLOROETHENE 10
2middotBUTANONE 40
CHLOROFORM 10
111-TRICHL ORO ETHANE 10
CARBON TETRACHLORIDE 10
12-DICHLOROETHANE 10
BENZENE 10
TRICHLOROETHENE 10
12-DICHLOROPROPANE 10
BROMODICHLOROMETHANE 10
TOLUENE 10
112-TRICHLOROETHANE 10
2-HEXANONE 40
TETRACHLOROETHENE 10
12-DIBROMOETHANE 10
CHLOROBENZENE 10
1112-TETRACHLOROETHANE 10
LCS Reporting Result Result Limit Qualifier
932 05
863 05
943 1
908 05
96 05
95 10 J
996 05
992 05
10 10
102 05
412 5
993 05
974 1
943 05
106 05
983 05
962 05
10 05
988 05
974 05
989 05
409 10
956 05
991 1
984 05
101 05
LCS Control Rec Limits
93 49 -129
86 46 134
94 32-121
91 67 -152
96 61 -135
95 61 -140
100 70 -122
99 76 -119
100 62 182
102 75 126
103 61 -137
99 79 120
97 76 - 114
94 58middot135
106 75middot132
98 70 shy 125
96 74 121
100 81 -119
99 79 - 123
97 76 - 120
99 81 -126
102 45 168
96 56 -128
99 79 -123
98 75 -120
101 82 - 123
Data Package 10 VL0911214middot1
-Date Printed Wednesday December 02 2009 ALS Laboratory Group -- Fe Page 1 of 4
LiMS Version 6317A
20
GCMS Volatiles Method SW8260_25B
Laboratory Control Sample and Laboratory Control Sample Duplicate
Lab Name ALS Laboratory Group - FC
Work Order Number 0911214
Client Name New Mexico Envircnment Department OB
ClientProject 10 644-111809(HWB R-37 VOes) PAR 002731703
Lab 10 VL091125-4LCS Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml
Moisture NIA QCBatchlO VL091125-4-5 Final Volume 10 mi
Date Collected NA Run 10 VL091125-4A Result Units UGL Date Extracted 11252009 Cleanup NONE Clean OF 1 Date Analyzed 111252009 Basis NA
Prep Method SW5030e File Name 028040
CASNO Target Analyte Spike Added
LCS Result
Reporting Limit
Result Qualifier
LCS Rec
Control Limits
100-41-4 ETHYLBENZENE 10 981 05 98 79 -114
136777-61-2 M+P-XYLENE 20 197 1 98 81-115
95-47-6 O-XYLENE 10 101 05 101 81 -115
95-49-8 2-CHLOROTOLUENE 10 97 05 97 80 -128
541-73-1 13-DICHLOROBENZiNt 10 977 05 98 81-116
106-46-7 14-DICHLOROBENZENE 10 979 05 98 81 -119
95-50-1 12-DICHLOROBENZENE 10 987 05 99 79 - 116
91-20-3 NAPHTHALENE 10 993 05 99 69 -126
87-61-6 123-TRICHLOROBENZENE 10 999 05 100 60 -137
Data Package ID VL0911214-1
Date Printed Wecnesday December 02 2009 ALS Laboratory Group -- Fe Page 2 of 4
21
GCMS Volatiles Method SW8260_25B
Laboratory Control Sample and Laboratory Control Sample Duplicate
Lab Name ALS Laboratory Group bullbull FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-11 1809(HWB R-37 VOCs) PAR 002731703
Lab 10 VL091125middot4LCSD Sample Matrix WATER
Moisture NIA Prep Batch VL091125-4
QCBatchlD VL091125-4-5
Sample Aliquot
Final Volume
10 ml
10ml Date Collected NIA Run ID VL091125-4A Result Units UGIL Date Extracted 112512009 Cleanup NONE Clean DF 1 Date Analyzed 1112512009 Basis NIA
Prep Method SW5030C File Name 028041
CASNO Target Analyte Spike Added
LCSD Result
Reporting Limit
Result Qualifier
LCSD Rec
RPD Limit
RPD
74-87-3 CHLOROMETHANE 10 897 05 90 30 4
75-01-4 VINYL CHLORIDE 10 831 05 83 25 4
74-83-9 BROMO METHANE 10 945 1 94 25 0
75-69-4 TRICHLOROFLUOROMETHANE 10 873 05 87 22 4
75-35-4 11-DICHLOROETHENE 10 909 05 91 18 5
75-15-0 CARBON DISULFIDE 10 941 10 J 94 20 1
156-60middot5 TRANS-l2middotDICHLOROETHENE 10 961 05 96 25 4
75middot34middot3 11-DICHLOROETHANE 10 977 05 98 25 2
108-05-4 VINYL ACETATE 10 993 10 J 99 20 1
156middot59-2 CIS-12-DlCHLOROETHENE 10 995 05 99 25 3
i 78-93-3 2-BUTANONE 40 419 5 105 30 2
67-66-3 CHLOROFORM 10 985 05 99 25 1
71-55-6 lll-TRICHLOROETHANE 10 942 1 94 25 3
56-23-5 CARBON TETRACHLORIDE 10 922 05 92 25 2
107middot06-2 12middotDICHLOROETHANE 10 106 05 106 25 0
71-43middot2 BENZENE 10 971 05 97 10 1
79middot01middot6 TRICHLOROETHENE 10 939 05 94 10 2
78middot87middot5 l2middotDICHLOROPROPANE 10 101 05 101 25 1
i 75middot27-4 BROMODICHLOROMETHANE 10 992 05 99 25 0
1108-88-3 TOLUENE 10 962 05 96 9 1
I 79005 112middotTRICHLOROETHANE 10 986 05 99 25 0
591middot78middot6 2-HEXANONE 40 418 10 104 20 2
127middot18-4 TETRACHLOROETHENE 10 918 05 92 25 4
106-93-4 12middotDIBROMOETHANE 10 999 1 100 15 1
108middot90-7 CHLOROBENZENE 10 997 05 100 11 1
630-20middot6 1112-TETRACHLOROETHANE 10 101 05 101 15 0
100-41-4 ETHYLBENZENE 10 968 05 97 25 1
Data Package ID VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- FC Page 3 of 4
lIMS Version 6317 A
22
GCMS Volatiles Method SW8260_25B
Laboratory Control Sample and Laboratory Control Sample Duplicate
Lab Name ALS Laboratory 13roup -- FC
Work Order Number 0911214
Client Name New Mexico Environment Department OS
ClientProject 10 644-11 1809(HWB R-37 VOCs) PAR 002731703
Lab 10 VL091125-4LCSD Sample Matrix WATER
Moisture NA Prep Batch VL091125-4
QCBatchlO VL091125-4-5
Sample Aliquot
Final Volume
10 ml
10ml Date Collected NA Run 10 VL091125-4A Result Units UGL Date Extracted 11252009 Cleanup NONE Clean OF Date Analyzed 11252009 Basis NIA
Prep Method SW5030C File Name 028041
CASNO Target Analyte Spike Added
LCSD Result
Reporting Limit
Result Qualifier
LCSD Rec
RPD Limit
RPD
136777-61-2 M+P-XYLENE 20 193 1 97 25 2
95-47-6 O-XYLENE 10 983 05 98 25 2
95-49-8 2middotCHLOROTOLUENE 10 9A9 05 95 15 2
541-73-1 13middotDICHLOROBENZENE 10 997 05 100 25 2
106-46-7 14-DICHLOROBeNZENE 10 974 05 97 25 1
95-50middot1 12middotDICHLOROBENZeNE 10 101 05 101 25 2
91middot20-3 NAPHTHALENe 10 105 05 105 24 6
87-61-6 123-TRICHLOROBENZENE 10 102 05 102 33 3
Surrogate Recovery LCSLCSD
CASNO Target Analyte Spike Added
LCS Rec
LCS Flag
LCSD Rec
LCSD Flag
Control Limits
460middot00-4 4-BROMOFLUOROBeNZENE 25 100 100 82 - 121
1868-53middot7 DIBROMOFLUOROMeTHANE 25 101 100 80middot 123
2037middot26-5 TOLUENEmiddotD8 25 102 100 85middot 116
Data Package 10 VL0911214-
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- Fe Page 4 of 4
UMS Verslmt 6317A
23
Chain of Custody Record 1)11 d- I 4 SHIP To MAil REPORT TO HtitilJft BILL TO
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14 Are all samples requiring no headspace (VOC GRG RSKlVIEE lb eNS radon)
free Size of bubble lt
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NO
]6 Were samples checked for and free from the presence of residual chlorine (Appiicaole when PM has Indicated samples are from a chlonnated wat~ source note if field preservallor
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17 Were the lljIV~IOU on ice
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Additional Iuformation OVIDE DETAILS BELOW FOR A ND RESPONSE TO ANY (UESTION A80VE EXCEPT 1 ANI) 16
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GCMS Volatiles Method SW8260 _25B
Method Blank
Lab Name ALS Laboratory Group bullbull FC
Work Order Number 0911214
Client Name New Mexico Environment Department DB
ClientProject 10 644-111809(HWB Rmiddot37 VOCs) PAR 002731703
Lab 10 VL091125-4MB Sample Matrix WATER
Moisture NA Prep Batch VL091125-4
QCBatchlO VL091125-4-5
Sample Aliquot
Final Volume
10 ml
10 ml Date Collected NA Run 10 VL091125-4A Result Units UGL Date Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Date Analyzed 25middotNov-09 Basis NA
File Name 028043
CASNO Target Analyte DF
75-71-8 DICHLORODIFLUOROMETHANE
74-87-3 CHLOROMETHANE
75-01-4 VINYL CHLORIDE
74-83-9 BROMOMETHANE
75-00-3 CHLOROETHANE
75-69-4 TRICHLOROFLUOROMETHANE
107-02-8 ACROLEIN
75-35-4 11middotDICHLOROETHENE
67-64-1 ACETONE
74-88-4 IODOMETHANE
75-15-0 CARBON DISULFIDE
METHYLEN E CHLORIDE 75-09-2
156-60-5 TRANS-12middotDICHLOROETHENE
1634-04-4 METHYL TERTIARY BUTYL ETHER
107-13-1 ACRYLONITRILE
75-34-3 11-DICHLOROETHANE
108-05-4 VINYL ACETATE
156-59middot2 CIS-12middotDICHLOROETHENE
78-93-3 2middotBUTANONE
~ BROMOCHLOROMETHANE
67-66-3 CHLOROFORM
71-55-6 111middot TRICHLOROETHANE
594-20-7 22middotDICHLOROPROPANE
56-23-5 CARBON TETRACHLORIDE
563-58-6 11middotDICHLOROPROPENE
107-06middot2 l2middotDICHLOROETHAN E
71-43-2 BENZENE
79-01-6 TRICHLOROETHENE
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Result Reporting Limit
05 05
05 05
05 05
1 1
05 05
05 05
100 100
05 05
10 10
5 5
10 10
1 1
05 05
1 1
10 10
05 05
10 10
05 05
5 5
1 1
05 05
1 1
05 05
05 05
05 05
05 05
05 05
05 05
MDL Result EPA Qualifier Qualifier
017 U
017 U
017 U
017 U
017 U
017 U
17 U
017 U
33 U
017 U
017 U
017 U
017 U
017 U
17 U
017 U
067 U
017 U
17 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
Data Package 10 VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- Fe Page 1 of 4
llMS Version 6317 A
8
GCMS Volatiles Method SW8260 _25B
Method Blank
Lab Name ALS Laboratory Group -- FC
Work Order Number 0911214
Client Name New Mexico Environment Department 08
ClientProject 10 644-111809(HWEI R-37 voes) PAR 002731703
Lab 10 VL091125-4MB Sample Matrix WATER
Moisture NIA Prep Batch VL091125-4
QCBatchIO VL091125-4-5
Sample Aliquot
Final Volume
10 ml
10 ml Oate Collected NIA Run 10 VL091125-4A Result Units UGL Oate Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Date Analyzed 25-Nov-09 Basis NIA
File Name 028043
CASNO Target Analyte OF Result Reporting Limit
MOL Result Qualifier
EPA Qualifier
78-87-5 12middotDICHLOROPROPANE 1 05 05 017 U
74-95-3 DIBROMOMETHANE 1 05 05 017 U
75-27-4 BROMODICHLOROMETHANE 1 05 05 017 U
10061-01-5 CISmiddot13middotDICHLOROPROPENE 1 05 05 017 U
108-10-1 4-METHYL-2-PENT ANONE 1 5 5 17 U
108-88-3 TOLUENE 1 05 05 017 U
10061-02-6 TRANS-13-DICHLOROPROPENE 1 05 05 017 U
79-00-5 112-TRICHLOROETHANE 1 05 05 017 U
591-78-6 2-HEXANONE 1 10 10 17 U
127-18-4 TETRACHLOROETHENE 1 05 05 017 U
142-28-9 13-DICHLOROPROPANI 1 05 05 017 U
124-48-1 DIBROMOCHLOROMETHANE 1 1 1 017 U
106-93-4 12-DIBROMOETHANE 1 1 1 017 U
108-90-7 CHLOROBENZENE 1 05 05 017 U
630-20-6 1112-TETRACHLOROETHANE 1 05 05 017 U
100-41-4 ETHYLBENZENE 1 05 05 017 U
136777-61-2 M+P-XYLENE 1 1 1 017 U
95-47-6 O-XYLENE 1 05 05 017 U
100-42-5 STYRENE 1 05 05 017 U
75-25-2 BROMOFORM 1 05 05 017 U
98-82-8 ~YLBENZENE 1 05 05 017 U
96-18-4 123-TRICHLOROPROPANE 1 2 2 017 U
79-34-5 1122middot TETRACHLOROETHANE 1 05 05 017 U
108-86-1 BROMOBENZENE 1 05 05 017 U
103-65-1 N-PROPYLBENZENE 1 05 05 017 U
95-49-8 2-CHLOROTOLUENE 1 05 05 017 U
108-67-8 135-TRIMETHYLBENZENE 1 05 05 017 U
106-43-4 4-CHLOROTOLUENE 1 05 05 017 U
Data Package 10 VL0911214-1
Date Printed Wednesday December n 2009 AlS Laboratory Group -- FC Page 2 of 4
lMS VeCSiOIY 6317A
9
GCMS Volatiles Method SW8260 _258
Method Blank
Lab Name ALS Laboratory Group - FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-111B09(HWB R-37 VOCs) PAR 002731703
Lab 10 VL091125-4MB Sample Matrix WATER
Moisture NIA
Prep Batch VL091125-4
QCBatchlD VL091125-4-5
Sample Aliquot
Final Volume
10 ml
10 ml
Date Collected NIA Run ID VL091125-4A Result Units UGL
Date Extracted 25-Nov-09 Cleanup NONE Clean DF 1
Date Analyzed 25-Nov-09 Basis NA
File Name 028043
CASNO Target Analyte OF Result Reporting Limit
MOL Result Qualifier
EPA Qualifier
98-06-6 TERT-BUTYLBENZENE 1 05 05 017 U
95-63-6 124-TRIMETHYLBENZENE 1 05 05 017 U
135-98-8 SEC-BUTYLBENZENE 1 05 05 017 U
541-73-1 13-DlCHLOROBENZENE 1 05 05 017 U
99-87-6 P-ISOPROPYLTOLUENE 1 05 05 017 U
106-46-7 1 A-DICHLOROBENZENE 1 05 05 017 U
104-51-8 N-BUTYLBENZENE 1 05 05 017 U
95-50-1 12-DICHLOROBENZENE 1 05 05 017 U
96-12-B 12-DIBROMO-3-CHLOROPROPANE 1 2 2 067 U
120-82-1 124-TRiCHLOROBENZENE 1 05 05 017 U
87-68-3 HEXACHLOROBUTADIENE 1 05 05 017 U
91-20-3 NAPHTHALENE 1 05 05 017 U
87-61-6 123-TRICHLOROBENZENE 1 05 05 017 U
75-05-B ACETONITRILE 1 50 50 83 U
107-05-1 ALLYL CHLORIDE 1 50 50 017 U
110-57-6 TRANS-14-DICHLORO-2-BUTENE 1 5 5 17 U
64-17-5 ETHANOL 1 200 200 78 U
97-63-2 ETHYL METHACRYLATE 1 5 5 017 U
78-83-1 ISOBUTYL ALCOHOL 1 100 100 17 U
126-98-7 METHACRYLONITRILE 1 35 35 17 U
80-62-6 METHYL METHACRYLATE 1 5 5 17 U
107-12-0 PROPIONITRILE 1 25 25 33 U
126-99-8 CHLOROPRENE 1 5 5 017 U
75-65-0 TERT-BUTANOL 1 100 100 33 U
108-20-3 ISOPROPYL ETHER 1 2 2 033 U
637-92-3 ETHYL TERT-BUTYL ETHER 1 2 2 033 U
994-05-8 TERT-AMYL METHYL ETHER 1 2 2 033 U
67-72-1 HEXACHLOROETHANE 1 2 2 033 U
Data Package 10 VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -~ Fe Page 3 of 4
LlMS Version 6317 A
10
GCMS Volatiles Method SW8260 _258
Method Blank
Lab Name ALS Laboratory Group -- FC
Work Order Number 0911214
Client Name New Mexico Envirmment Department OB
ClientProject 10 644-111809(HWB R-37 VOCs) PAR 002731703
Lab 10 VL091125-4MB Sample Matrix WATER
Moisture NIA Prep Batch VL091125-4
QCBatchlO VL091125-4-5
Sample Aliquot
Final Volume
10 m
10m Date Collected NIA Run 10 VL091125-4A Result Units UGIL Date Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Date Analyzed 25-Nov-09 BasisNIA
File Name 028043
CASNO Target Analyte Result Reporting MOL Result EPAOF Limit Qualifier Qualifier
Surrogate Recovery
CASNO Surrogate Analyte Result Flag Spike Amount
Percent Recovery
Control Limits
460-00-4 4-BROMOFLUOROBENZENE 25 25 100 82 - 121
1868-53-7 DIBROMOFLUOROMETHANE 248 25 99 80 - 123
2037-26-5 TOLUENE-D8 26 25 104 85 - 116
Data Package 10 VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- FC Page 4 of4
LlMS Version 6317A
11
GCMS Volati les Method SW8260 _258
Sample Results
Lab Name ALS Laboratory Group -- FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-111809(HWB R-37 VOCs) PAR 002731703
Field 10 Rmiddot37 Ser 2middot111809
Lab 10 0911214middot1
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml
Moisture NA QCBatchlO VL091125-4-5 Final Volume 10mi Date Collected 18-Nov-09 Run 10 VL091125-4A Result Units UGL
Date Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Analysis ReqCode 104 Date Analyzed 25-Nov-09
Prep Method SW5030 Rev C Basis As Received
File Name 028044
CASNO Target Analyte Dilution Factor
75-71-8 DICHLORODIFLUOROMETHANE 1
74middot87-3 CHLOROMETHANE 1
75-01-4 VINYL CHLORIDE 1
74-83-9 BROMOMETHANE 1
75-00-3 CHLOROETHANE 1
75-69-4 TRICHLOROFLUOROMETHANE 1
107-02-8 ACROLEIN 1
75-35-4 11middotDICHLOROETHENE 1
67-64-1 ACETONE 1
74-88-4 IODOMETHANE 1
75-15-0 CARBON DISULFIDE 1
75-09-2 METHYLENE CHLORIDE 1
156-60-5 TRANSmiddot12middotDICHLOROETHENE 1
1634-04-4 METHYL TERTIARY BUTYL ETHER 1
107-13-1 ACRYLONITRILE 1
75-34-3 1-DICHLOROETHANE 1
i 108-05-4 VINYL ACETATE 1
156-59-2 CIS-12middotDICHLOROETHENE 1
78-93-3 2-BUTANONE 1
74-97-5 BROMOCHLOROMETHANE 67-66-3 CHLOROFORM 1
71-55-6 11-TRICHLOROETHANE 594-20-7 22-DICHLOROPROPANE 56-23-5 CARBON TETRACHLORIDE 563-58-6 -DICHLOROPROPENE 107-06-2 2-DICHLOROETHANE
Result Reporting Limit
05 05
05 05
05 05
1 1
05 05
05 05
100 100
05 05
10 10
5 5
10 10
1 1
05 05
1 1
10 10
05 05
10 10
05 05
5 5
1 1
05 05
1 1
05 05
05 05
05 05
05 05
MOL Result EPA Qualifier Qualifier
017 U
017 U
017 U
017 U
017 U
017 U
17 U
017 U
33 U
017 U
017 U
017 U
017 U
017 U
17 U
017 U
067 U
017 U
17 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
Data Package ID VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- Fe Page 1 of 8
UMS Version 6317A
12
GCMS Volatiles Method SW8260_25B
Sample Results
Lab Name ALS Laboratory Group - FC
Work Order Number 0911214
Client Name New Mexico nvironment Department OB
ClientProject 10 644-111809(HWB R-37 VOCs) PAR 002731703
Field 10 R-37 Scr 2-111809
Lab 10 0911214-1
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10ml
Moisture NA QCBatchlD VL091125-4-5 Final Volume 10ml
Date Collected l8-Nov-09 Run 10 VL091125-4A Result Units UGL
Date Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Analysis ReqCode 104 Date Analyzed 25-Nov-09 Basis As Received
Prep Method SW5030 Rev C File NameD28044
CASNO Target Analyte Dilution Factor
Result Reporting Limit
MDL Result Qualifier
EPA Qualifier
I
71-43-2 BENZENE 1 05 05 017 U
79-01-6 TRICHLOROETHENE 1 05 05 017 U
78-87-5
74middot95-3
75-27-4
10061-01-5
108middot10middot1
108middot88-3
10061-02middot6
79-00-5
591-78-6
12-DICHLOROPROPANE
DIBROMOMETHANE
BROMODCHLOROMETHANE
CIS-13-DICHLOROPROPEI~E
4-METHYL-2-PENTANONE
TOLUENE
TRANS-13-DICHLOROPROPENE
112-TRICHLOROETHANE
2-HEXANONE
1
1
1
1
1
1
1
1
1
05
05
05
05
5
031
05
05
10
05
05
05
05
5
05
05
05
10
017
017
017
017
17
017
017
017
17
U
U
U
U
U
J
U
U
U
127-18-4
142-28-9
124-48-1
106-93-4
108-90-7
630-20-6
100-41-4
136777-61-2
95-47-6
100-42middot5
75-25-2
98-82middot8
96-18-4
79-34-5
108-86-1
TETRACHLOROETHENE
13-DICHLOROPROPANE
DIBROMOCHLOROMETHANE
12-DIBROMOETHANE
CHLOROBENZENE
11 12-TETRACHLOROETHANE
ETHYLBENZENE
M+PmiddotXYLENE
OmiddotXYLENE
STYRENE
BROMOFORM
ISOPRO PYLBENZENE
123middotTRICHLOROPROPANE
1122-TETRACHLOROETHANE
BROMOBENZENE
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
05
05
1
1
05
05
05
1
05
05
05
05
2
05
05
05
05
1
1
05
05
05
1
05
05
05
05
2
05
05
017
017
017
017
017
017
017
017
017
017
017
017
017
017
017
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
i
Data Package 10 VL0911214-1
Date Printed Wednesday December 022009 AlS laboratory Group bullbull Fe Page 2 of 8
UMS Version 6317A
13
GCMS Volatiles Method SW8260_258
Sample Results
Lab Name ALS Laboratory Group bullbull FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject ID 644-111809(HWB R-37 VOCs) PAR 002731703
Field 10 R-37 Sor 2-111809
Lab ID 0911214middot1
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml
Moisture NA QCBatchlD VL091125-4-5 Final Volume 10 ml
Date Collected 18-Nov-09 Run ID VL091125-4A Result Units UGL
Date Extracted 25-Nov-09 Cleanup NONE Clean DF 1
Analysis ReqCode 104 Date Analyzed 25-Nov-09 Basis As Received
Prep Method SW5030 Rev C File Name 028044
CASNO Target Analyte Dilution Factor
103-65-1 NmiddotPROPYLBENZENE 1
95-49-8 2-CHLOROTOLUENE 1
108-67-8 135-TRIMETHYLBENZENE 1
106-43-4 4-CHLOROTOLUENE 1
98-06-6 TER I-BUTYLBENZENE 1
95-63-6 124-TRIMETHYLBENZENE 1
135-98-8 SEC-BUTYLBENZENE 1
541-73-1 13-OICHLOROBENZENE 1
99-87-6 P-ISOPROPYLTOLUENE 1
106-46-7 lA-DICHLOROBENZENE 1
104-51-8 N-BUTYLBENZENE 1
95-50-1 12-DICHLOROBENZENE 1
96-12-8 l2-DIBROMOmiddot3-CHLOROPROPANE 1
120-82-1 12A-TRICHLOROBENZENE 1
187-68-3 HEXACHLOROBUTADIENE 1
91-20-3 NAPHTHALENE 1
87-61middot6 123-TRICHLOROBENZENE 1
75-05-8 ACETONITRILE 1
107middot05middot1 ALLYL CHLORIDE 1
110-57-6 TRANS-14-DICHLORO-2-BUTENE 1
164-17-5 ETHANOL 1
97-63-2 ETHYL METHACRYLATE 1
78-83-1 ISOBUTYL ALCOHOL 1
126-98-7 METHACRYLONITRILE 1
80-62-6 METHYL METHACRYLATE 1
107-12-0 PROPIONITRILE 1
Result Reporting Limit
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
2 2
05 05
05 05
05 05
05 05
50 50
50 50
5 5
200 200
5 5
100 100
35 35
5 5
25 25
MDL Result EPA Qualifier Qualifier
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
067 U
017 U
017 U
017 U
017 U
83 U
017 U
U u 78 U
017 U
17 U
17 U
17 U
33 U
Data Package 10 VL0911214-1
Date Printed Wednesday December 022009 ALS Laboratory Group MM Fe Page 3 of 8
LlMS VerSion 6317A
14
GCMS Volati las Method SW8260_258
Sample Results
Lab Name ALS Laboratory Group - FC
Work Order Number 0911214
Client Name New Mexico Environment Department 08
ClientProject 10 644-111B09(HWB R-37 VOGs) PAR 002731703
Field 10 R-37 Ser 2-111809 Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10ml
Lab 10 0911214-1 Moisture NA
Date Collected 1B-Nov-09 QCBatchlO VL091125-4-5
Run 10 VL091125-4A
Final Volume 10ml
Result Units UGIL Date Extracted 25-Nov-09 Cleanup NONE Clean OF
Analysis ReqCode 104 Date Analyzed 25-Nov-09
Prep Method SW5030 Rev G Basis As Received
File Name 028044
CASNO Target Analyte Dilution Factor
Result Reporting Limit
MDL Result Qualifier
EPA Qualifier
126-99-8 CHLOROPRENE 1 5 5 017 U
75-65-0 TERT-BUTANOL 1 100 100 33 U
108-20-3 ISOPROPYL ETHER 1 2 2 033 U
637-92-3 ETHYL TERT-BUTYL ETHER 1 2 2 033 U
994-05-8 TERT-AMYL METHYL ETHER 1 2 2 033 U
67-72-1 HEXACHLOROETHANE 1 2 2 033 U
Surrogate Recovery
CASNO Surrogate Analyte Result Flag Spike Amount
Percent Recovery
Control Limits
460-00-4 4-BROMOFLUOHOBENZENE 246 25 98 82 - 121
1868-53-7 DIBROMOFLUOHOMETHANE 248 25 99 BO - 123
2037-26-5 TOLUENE-DB 258 25 103 85middot116
Data Package 10 VL0911214-1
Date Printed Wednesday December 022009 ALS Laboratory Group bullbull FC Page 4 of 8
LIMS Version 0317 A
15
GCMS Volati les Method SW8260_25B
Sample Results
Lab Name ALS Laboratory Group -- FC
Worlt Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-111809(HWB Rmiddot37 VOCs) PAR 002731703
Field 10 Rmiddot37 Scr jmiddot111809
Lab 10 0911214-2
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml Moisture NfA QCBatchID VL091125-4middot5 Final Volume 10 ml
Date Collected 18middotNov-09 Run 10 VL091125-4A Result Units UGfL Date Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Analysis ReqCode 104 Date Analyzed 25middotNov-09 Basis As Received Prep Method SW5030 Rev C File Name 028045
CASNO Target Analyte Dilution Factor
Result Reporting Limit
MOL Result Qualifier
EPA Qualifier
75-71-8 DICHLORODIFLUOROMETHANE 1 05 05 017 U
74-87-3 CHLOROMETHANE 1 05 05 017 U
75-01middot4 VINYL CHLORIDE 1 05 05 017 U
74-83-9 BROMOMETHANE 1 1 1 017 U
75middot00middot3 CHLOROETHANE j 05 05 017 U
75-69-4 TRICHLOROFLUOROMETHANE 1 05 05 017 U
107-02-8 ACROLEIN 1 100 100 17 U
i 75-35-4 11-DICHLOROETHENE 1 05 05 017 U
67-64middot1 ACETONE 1 10 10 33 U
74-8S-4 IODOMETHANE 1 5 5 017 U
75-15-0 CARBON DISULFIDE 1 10 10 017 U
75-09-2 METHYLENE CHLORIDE 1 1 1 017 U
156-60-5 TRANS-12-DICHLOROETHENE 1 05 05 017 U
1634-04-4 METHYL TERTIARY BUTYL ETHER 1 1 1 017 U
107-13-1 ACRYLONITRILE 1 10 10 17 U
75-34middot3 11-DICHLOROETHANE 05 05 017 U
i 108-05-4 VINYL ACETATE 1 10 10 067 U
115659-2 CISmiddot 2middotDICHLOROETHENE 1 05 05 017 U
178-933 2middotBUTANONE 1 5 5 17 U
74-97middot5 BROMOCHLOROMET HANE 1 1 1 017 U
67-66-3 CHLOROFORM 1 05 05 017 U
71-55middot6 111middotTRICHLOROETHANE 1 1 1 017 U
594-20-7 22middotDICHLOROPROPANE 1 05 05 017 U
56-23-5 CARBON TETRACHLORIDE 1 05 05 017 U
563-58-6 11middotDICHLOROPROPENE 1 05 05 017 U
107-06-2 12middotDICHL OROETHANE 1 05 05 017 U
Data Package ID VL0911214-1
Date Printed Wednesday December 022009 ALS Laboratory Group -- Fe Page 5 of 8
16
GCMS Volatiles Method SW8260_25B
Sample Results
Lab Name ALS Laboratory Group -- FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-111809(HW3 R-37 VOCs) PAR 002731703
Field 10 R-37 Scr 1-11 1809
Lab 10 0911214-2
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml
Moisture NIA QCBatchlO VL091125-4-5 Final Volume 10 ml
Date Collected 18-Nov-09 Run 10 VL091125-4A Result Units UGL
[late Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Analysis ReqCode 104 Date Analyzed 25-Nov-09
Prep Method SW5030 Rev C Basis As Received
File Name 028045
CASNO Target Analyte Dilution Factor
71-43-2 BENZENE 1
79-01-6 TRICHLOROETHENE 1
78-87-5 12-DICHLOROPROPANE 1
74-95-3 DIBROMOMETHANE 1
75-27-4 BROMODICHLOROMETHANE 1
10061-01-5 CIS-13-DICHLOROPROPENE 1
108-10-1 4-METHYL-2-PtNTANON 1
108-88-3 TOLUENE 1
10061-02-6 TRANS-13-DICHLOROPROPENE 1
79-00-5 112-TRICHLOROETHANE 1
591-78-6 2-HEXANONE 1
127-18-4 TETRACHLOROETHENE 1
142-28-9 13-DICHLOROPROPANt 1
124-48-1 DI3ROMOCHLOROMETHANE 1
106-93-4 12-DIBROMOETHANE 1
108-90-7 CHLOROBENZENE 1
OETHANE 1
- 1
LENE 1
ENE 1
ENE 1
OFORM 1
OPYlBENZENE 1
96-18-4 123-TRICHLOROPROPANE 1
79-34-5 1122-TETRACHLOROETHANE 1
108-86-1 BROMOBENZENE 1
Result Reporting Limit
05 05
05 05
05 05
05 05
05 05
05 05
5 5
025 05
05 05
05 05
10 10
05 05
05 05
1 1
1 1
05 05
05 05
05 05
1 1
05 05
05 05
05 05
05 05
2 2
05 05
05 05
MDL Result EPA Qualifier Qualifier
017 U
017 U
017 U
017 U
017 U
017 U
17 U
017 J
017 U
017 U
17 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
Data Package 10 VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- Fe Page 6 of 8
317A
17
GCMS Volatiles Method SW8260 _258
Sample Results
Lab Name ALS Laboratory Group -- FC
Work Order Number 0911214
Client Name New Mexico Environment Department 08
ClientProject 10 644-11S09(HWB R-37 VOCs) PAR 002731703
Field 10 Rmiddot37 Scr 1-111809
Lab 10 0911214-2
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml Moisture NA QCBatchlD VL091125-4-5 Final Volume 10 ml
Date Collected 18-Nov-09 Run 10 VL091125-4A Result Units UGL Date Extracted 25-Nol-09 Cleanup NONE Clean OF
Analysis ReqCode 104 Date Analyzed 25-Nov-09 Basis As Received Prep Method SW5030 Rev C File Name D28045
CASNO Target Analyte Dilution Factor
103-65-1 N-PROPYLBENZENE 1
95-49-8 2-CHLOROTOLUENE 1
108-67-8 135-TRIMETHYLBENZENE 1
106-43-4 4-CHLOROTOLUENE 1
98-06-6 TERT-BUTYLBENZENE 1
95-63-6 124-TRIMETHYLBENZENE 1
135-98-8 SEC-BUTYLBENZENE 1
i 541-73-1 13middotDICHLOROBENZENE 1
99-87-6 PmiddotISOPROPYL TOLUENE 1
106-46-7 I 14-DICHLOROBENZENE 1
104-51-8 I N-BUTYLBENZENE 1
95-50-1 l2-DICHLOROBENZENE 1
96-12-8 I 12-DIBROMO-3-CHLOROPROPANE 1
120-82-1 124-TRICHLOROBENZENE 1
87-68-3 HEXACHLOROBUT ADIENE 1
91-20-3 NAPHTHALENE 1
87-61-6 123-TRICHLOROBENZENE 1
75-05-S ACETONITRILE 1
107-05-1 ALLYL CH LORIDE 1
110-57-6 TRAN S-14-DICHLORO-2-BUTENE 1
64-17-5 ETHANOL 1
97-63-2 ETHYL METHACRYLATE 1
78-83-1 ISOBUTYL ALCOHOL 1
126-98-7 METHACRYLONITRILE 1
80-62-6 METHYL METHACRYLATE 1
107-12-0 I PROPIONITRILE 1
Result Reporting Limit
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
2 2
05 05
05 05
05 05
05 05
50 50
50 50 I 5 5
200 200
5 5
100 100
35 35
5 5
25 25
MDL
017
017
017
017
017
017
017
017
017
017
017
017
067
017
017
017
017
83
017
17
78
017
17
17
17
33
Result EPA Qualifier Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
Data Package 10 VL0911214-1
Date Printed Wednesday December 022009 ALS Laboratory Group -- Fe Page 7 of 8
LlMS Version 6317A
18
GCMS Volatiles Method SW8260_258
Sample Results
Lab Name ALS Laboratory Group bullbull FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644middot111B09(HWB R-37 VOCs) PAR 002731703
Sample Matrix WATER Prep Batch VL091125--4 Sample Aliquot 10 mlRmiddot37 Ser 1-111809 Moisture NA QCBatchlO VL091125--4-5 Final Volume 10 m
0911214-2 Date Collected 18-Nov-09 Run 10 VL091125--4A Result Units UGL Date Extracted 25-Nov-09 Cleanup NONE Clean OF 1 Date Analyzed 25-Nov-09 Basis As Received
10
Analysis ReqCode 104 Prep Method SW5030 Rev C File Name 028045
I
CASNO Target Analyte Dilution Factor
Result Reporting Limit
MDL Result Qualifier
EPA Qualifier
126-99-8 CHLOROPRENE 1 5 5 017 U
75-65-0 TERT-BUTANOL 1 100 100 33 U
108-20-3 ISOPROPYL ETHER 1 2 2 033 U
637-92-3 ETHYL TERT-BUTYL ETHER 1 2 2 033 U
994-05--8 TERT-AMYL MTHYL ETHER 1 2 2 033 U
67-72-1 HEXACHLOROETHANE 1 2 2 033 U
Surrogate Recovery
CASNO Surrogate Analyte Result Flag Spike Amount
Percent Control Recovery Limits
460-00-4 4middotBROMOFLUOROBENZENE 247 25 99 1
1868-53-7 DIBROMOFLUOROMETHANE 248 25 99 80 123
2037-26-5 TOLUENEmiddotDB 255 25 102 85 - 116
Data Package 10 VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- FC Page B of 8
LlMS Version 6317A
19
GCMS Volatiles Method SW8260_258
Laboratory Control Sample and Laboratory Control Sample Duplicate
Lab Name ALS Laboratory Group - FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-111809(HWB R-37 VOCs) PAR 002731703
Lab 10 VL091125-4LCS Sample Matrix WATER
Moisture NA Prep Batch VL091125-4
QCBatchlD VL091125-4-5
Sample Aliquot
Final Volume
10ml
10ml Date Collected NA Run 10 VL091125-4A Result Units UGIL Date Extracted 111252009 Cleanup NONE Clean OF 1 Date Analyzed 11252009 Basis NA
Prep Method SW5030C File Name 028040
CASNO
74-87-3
75-01-4
74-83-9
75-69-4
75-35-4
75-15-0
156-60-5
75-34-3
108-05-4
156-59-2
78-93-3
67 -66-3
71-55-6
i 56-23-5
107-06-2
71-43-2
79-01-6
78-87-5
75-27-4
108-88-3
79-00-5
591-78-6
127-18-4
106-93-4
108-90-7
63Q20-6
Target Analyte Spike Added
CHLOROMETHANE 10
VINYL CHLORIDE 10
BROMOMETHANE 10
TRICHLOROFLUOROMETHANE 10
11-DICHLOROETHENE 10
CARBON DISULFIDE 10
TRANS-12-DICHLOROETHENE 10
11-DICHLOROETHANE 10
VINYL ACETATE 10
CIS-12-DICHLOROETHENE 10
2middotBUTANONE 40
CHLOROFORM 10
111-TRICHL ORO ETHANE 10
CARBON TETRACHLORIDE 10
12-DICHLOROETHANE 10
BENZENE 10
TRICHLOROETHENE 10
12-DICHLOROPROPANE 10
BROMODICHLOROMETHANE 10
TOLUENE 10
112-TRICHLOROETHANE 10
2-HEXANONE 40
TETRACHLOROETHENE 10
12-DIBROMOETHANE 10
CHLOROBENZENE 10
1112-TETRACHLOROETHANE 10
LCS Reporting Result Result Limit Qualifier
932 05
863 05
943 1
908 05
96 05
95 10 J
996 05
992 05
10 10
102 05
412 5
993 05
974 1
943 05
106 05
983 05
962 05
10 05
988 05
974 05
989 05
409 10
956 05
991 1
984 05
101 05
LCS Control Rec Limits
93 49 -129
86 46 134
94 32-121
91 67 -152
96 61 -135
95 61 -140
100 70 -122
99 76 -119
100 62 182
102 75 126
103 61 -137
99 79 120
97 76 - 114
94 58middot135
106 75middot132
98 70 shy 125
96 74 121
100 81 -119
99 79 - 123
97 76 - 120
99 81 -126
102 45 168
96 56 -128
99 79 -123
98 75 -120
101 82 - 123
Data Package 10 VL0911214middot1
-Date Printed Wednesday December 02 2009 ALS Laboratory Group -- Fe Page 1 of 4
LiMS Version 6317A
20
GCMS Volatiles Method SW8260_25B
Laboratory Control Sample and Laboratory Control Sample Duplicate
Lab Name ALS Laboratory Group - FC
Work Order Number 0911214
Client Name New Mexico Envircnment Department OB
ClientProject 10 644-111809(HWB R-37 VOes) PAR 002731703
Lab 10 VL091125-4LCS Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml
Moisture NIA QCBatchlO VL091125-4-5 Final Volume 10 mi
Date Collected NA Run 10 VL091125-4A Result Units UGL Date Extracted 11252009 Cleanup NONE Clean OF 1 Date Analyzed 111252009 Basis NA
Prep Method SW5030e File Name 028040
CASNO Target Analyte Spike Added
LCS Result
Reporting Limit
Result Qualifier
LCS Rec
Control Limits
100-41-4 ETHYLBENZENE 10 981 05 98 79 -114
136777-61-2 M+P-XYLENE 20 197 1 98 81-115
95-47-6 O-XYLENE 10 101 05 101 81 -115
95-49-8 2-CHLOROTOLUENE 10 97 05 97 80 -128
541-73-1 13-DICHLOROBENZiNt 10 977 05 98 81-116
106-46-7 14-DICHLOROBENZENE 10 979 05 98 81 -119
95-50-1 12-DICHLOROBENZENE 10 987 05 99 79 - 116
91-20-3 NAPHTHALENE 10 993 05 99 69 -126
87-61-6 123-TRICHLOROBENZENE 10 999 05 100 60 -137
Data Package ID VL0911214-1
Date Printed Wecnesday December 02 2009 ALS Laboratory Group -- Fe Page 2 of 4
21
GCMS Volatiles Method SW8260_25B
Laboratory Control Sample and Laboratory Control Sample Duplicate
Lab Name ALS Laboratory Group bullbull FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-11 1809(HWB R-37 VOCs) PAR 002731703
Lab 10 VL091125middot4LCSD Sample Matrix WATER
Moisture NIA Prep Batch VL091125-4
QCBatchlD VL091125-4-5
Sample Aliquot
Final Volume
10 ml
10ml Date Collected NIA Run ID VL091125-4A Result Units UGIL Date Extracted 112512009 Cleanup NONE Clean DF 1 Date Analyzed 1112512009 Basis NIA
Prep Method SW5030C File Name 028041
CASNO Target Analyte Spike Added
LCSD Result
Reporting Limit
Result Qualifier
LCSD Rec
RPD Limit
RPD
74-87-3 CHLOROMETHANE 10 897 05 90 30 4
75-01-4 VINYL CHLORIDE 10 831 05 83 25 4
74-83-9 BROMO METHANE 10 945 1 94 25 0
75-69-4 TRICHLOROFLUOROMETHANE 10 873 05 87 22 4
75-35-4 11-DICHLOROETHENE 10 909 05 91 18 5
75-15-0 CARBON DISULFIDE 10 941 10 J 94 20 1
156-60middot5 TRANS-l2middotDICHLOROETHENE 10 961 05 96 25 4
75middot34middot3 11-DICHLOROETHANE 10 977 05 98 25 2
108-05-4 VINYL ACETATE 10 993 10 J 99 20 1
156middot59-2 CIS-12-DlCHLOROETHENE 10 995 05 99 25 3
i 78-93-3 2-BUTANONE 40 419 5 105 30 2
67-66-3 CHLOROFORM 10 985 05 99 25 1
71-55-6 lll-TRICHLOROETHANE 10 942 1 94 25 3
56-23-5 CARBON TETRACHLORIDE 10 922 05 92 25 2
107middot06-2 12middotDICHLOROETHANE 10 106 05 106 25 0
71-43middot2 BENZENE 10 971 05 97 10 1
79middot01middot6 TRICHLOROETHENE 10 939 05 94 10 2
78middot87middot5 l2middotDICHLOROPROPANE 10 101 05 101 25 1
i 75middot27-4 BROMODICHLOROMETHANE 10 992 05 99 25 0
1108-88-3 TOLUENE 10 962 05 96 9 1
I 79005 112middotTRICHLOROETHANE 10 986 05 99 25 0
591middot78middot6 2-HEXANONE 40 418 10 104 20 2
127middot18-4 TETRACHLOROETHENE 10 918 05 92 25 4
106-93-4 12middotDIBROMOETHANE 10 999 1 100 15 1
108middot90-7 CHLOROBENZENE 10 997 05 100 11 1
630-20middot6 1112-TETRACHLOROETHANE 10 101 05 101 15 0
100-41-4 ETHYLBENZENE 10 968 05 97 25 1
Data Package ID VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- FC Page 3 of 4
lIMS Version 6317 A
22
GCMS Volatiles Method SW8260_25B
Laboratory Control Sample and Laboratory Control Sample Duplicate
Lab Name ALS Laboratory 13roup -- FC
Work Order Number 0911214
Client Name New Mexico Environment Department OS
ClientProject 10 644-11 1809(HWB R-37 VOCs) PAR 002731703
Lab 10 VL091125-4LCSD Sample Matrix WATER
Moisture NA Prep Batch VL091125-4
QCBatchlO VL091125-4-5
Sample Aliquot
Final Volume
10 ml
10ml Date Collected NA Run 10 VL091125-4A Result Units UGL Date Extracted 11252009 Cleanup NONE Clean OF Date Analyzed 11252009 Basis NIA
Prep Method SW5030C File Name 028041
CASNO Target Analyte Spike Added
LCSD Result
Reporting Limit
Result Qualifier
LCSD Rec
RPD Limit
RPD
136777-61-2 M+P-XYLENE 20 193 1 97 25 2
95-47-6 O-XYLENE 10 983 05 98 25 2
95-49-8 2middotCHLOROTOLUENE 10 9A9 05 95 15 2
541-73-1 13middotDICHLOROBENZENE 10 997 05 100 25 2
106-46-7 14-DICHLOROBeNZENE 10 974 05 97 25 1
95-50middot1 12middotDICHLOROBENZeNE 10 101 05 101 25 2
91middot20-3 NAPHTHALENe 10 105 05 105 24 6
87-61-6 123-TRICHLOROBENZENE 10 102 05 102 33 3
Surrogate Recovery LCSLCSD
CASNO Target Analyte Spike Added
LCS Rec
LCS Flag
LCSD Rec
LCSD Flag
Control Limits
460middot00-4 4-BROMOFLUOROBeNZENE 25 100 100 82 - 121
1868-53middot7 DIBROMOFLUOROMeTHANE 25 101 100 80middot 123
2037middot26-5 TOLUENEmiddotD8 25 102 100 85middot 116
Data Package 10 VL0911214-
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- Fe Page 4 of 4
UMS Verslmt 6317A
23
---- ---- ---
ALS Laboratory GrouP - Fort Collins
CONDITIO] OF SAMPLE UPO) RECEIPT FORM
Client _-=-N--M---f-=-D________ IVorkorde No D4 J I 4 --~~~~~~------
PrO1 cc Manager L 5 lnitiais C D Date 1 -) ()- () C --~~~---------------------
1 there a cae Are the coe and bottle labels
Is the coe in agreement with samples received) of containers matrix requested anaiyses etc)
documents presen1 andor removable)
Are all aqueous samples requiring preservation preserved correctly ~- ----~-~~--- -~ -~-- ----~~~---------
volatiles)
14 Are all samples requiring no headspace (VOC GRG RSKlVIEE lb eNS radon)
free Size of bubble lt
$ Do perchlorate LCMS-MS samples have headspace (a~ least ]3 of container required)
NO
]6 Were samples checked for and free from the presence of residual chlorine (Appiicaole when PM has Indicated samples are from a chlonnated wat~ source note if field preservallor
witb sodIUm tlllosulfate wa not observed)
17 Were the lljIV~IOU on ice
IS Were cooler temperatures measured at 01-60degC IR ~Illl used 2
Coole I---
Temperature (C) 3 ~
NO
NO
NO
NO
NO
NO
NO
No of custodv seals Ol~ cooler 0 OOT ---- --- --- --l Surveyl EXlemlli flRhr n~ading I i AcceplanCfiltnforma tlon Background ulJhr reading 3 Were eX lema uRhf readl1lf5 tW(l tm bnckl1Ound and withllllxyr acceptance criterill
Additional Iuformation OVIDE DETAILS BELOW FOR A ND RESPONSE TO ANY (UESTION A80VE EXCEPT 1 ANI) 16
If applicable was the clienl contacted) YES i NO I
Project Manager Signature I Date
(1 Gun 112 Oaktoll SN 2992250020 jmiddot0066 lR Gun lie Oakton S~ 23n220101middot0(J02
Form 201r22gt15 (61109) Page 1 of _1
6
4a Express Package Service _ FadEx Pnority OvernightLJ ==lr-~MClncU1
lSlIIQSATUIIDAYlltIrwIlyis$Mf(1J
middot10_ FadEx SlaMard Ovemioht fMtRallw6ftIlfTampCI v
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FecEx~ US Airbill Express
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9439 4324
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~~oalleJl =1~~ImOt $AUROAY ftlEdOeyF1tlitNbiDrnJtin
5 Packaging -1itIcIrme-- FadEgt r- FedEgt fak FedEx Box
kt1UoorFdrStNil~~Your Internal Billing Reference Enveiope Pol _
TD
Address Wa clMOfdeiinrto POlwuscrPo ZIP CGlJla
Address
6 Special Handlmlllilld Delivery SignalUlll Options
~~~l~__Iint_dUSabulld)IjhL Indirect Sianarurc ttMtrttISMIllFtdlHrtS ~~tlltl~ eeelMllnllrl$ICIIltctdeiMv-kll lt_noaIllaIMInt$ ~
OrvlceL- OtyiclItUN186 ___ ___
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8700 9439 4324 ~rtl1~l__bPnD USA SRI
_____-----------~bull---~----- -------~~-------------------
7
GCMS Volatiles Method SW8260 _25B
Method Blank
Lab Name ALS Laboratory Group bullbull FC
Work Order Number 0911214
Client Name New Mexico Environment Department DB
ClientProject 10 644-111809(HWB Rmiddot37 VOCs) PAR 002731703
Lab 10 VL091125-4MB Sample Matrix WATER
Moisture NA Prep Batch VL091125-4
QCBatchlO VL091125-4-5
Sample Aliquot
Final Volume
10 ml
10 ml Date Collected NA Run 10 VL091125-4A Result Units UGL Date Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Date Analyzed 25middotNov-09 Basis NA
File Name 028043
CASNO Target Analyte DF
75-71-8 DICHLORODIFLUOROMETHANE
74-87-3 CHLOROMETHANE
75-01-4 VINYL CHLORIDE
74-83-9 BROMOMETHANE
75-00-3 CHLOROETHANE
75-69-4 TRICHLOROFLUOROMETHANE
107-02-8 ACROLEIN
75-35-4 11middotDICHLOROETHENE
67-64-1 ACETONE
74-88-4 IODOMETHANE
75-15-0 CARBON DISULFIDE
METHYLEN E CHLORIDE 75-09-2
156-60-5 TRANS-12middotDICHLOROETHENE
1634-04-4 METHYL TERTIARY BUTYL ETHER
107-13-1 ACRYLONITRILE
75-34-3 11-DICHLOROETHANE
108-05-4 VINYL ACETATE
156-59middot2 CIS-12middotDICHLOROETHENE
78-93-3 2middotBUTANONE
~ BROMOCHLOROMETHANE
67-66-3 CHLOROFORM
71-55-6 111middot TRICHLOROETHANE
594-20-7 22middotDICHLOROPROPANE
56-23-5 CARBON TETRACHLORIDE
563-58-6 11middotDICHLOROPROPENE
107-06middot2 l2middotDICHLOROETHAN E
71-43-2 BENZENE
79-01-6 TRICHLOROETHENE
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Result Reporting Limit
05 05
05 05
05 05
1 1
05 05
05 05
100 100
05 05
10 10
5 5
10 10
1 1
05 05
1 1
10 10
05 05
10 10
05 05
5 5
1 1
05 05
1 1
05 05
05 05
05 05
05 05
05 05
05 05
MDL Result EPA Qualifier Qualifier
017 U
017 U
017 U
017 U
017 U
017 U
17 U
017 U
33 U
017 U
017 U
017 U
017 U
017 U
17 U
017 U
067 U
017 U
17 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
Data Package 10 VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- Fe Page 1 of 4
llMS Version 6317 A
8
GCMS Volatiles Method SW8260 _25B
Method Blank
Lab Name ALS Laboratory Group -- FC
Work Order Number 0911214
Client Name New Mexico Environment Department 08
ClientProject 10 644-111809(HWEI R-37 voes) PAR 002731703
Lab 10 VL091125-4MB Sample Matrix WATER
Moisture NIA Prep Batch VL091125-4
QCBatchIO VL091125-4-5
Sample Aliquot
Final Volume
10 ml
10 ml Oate Collected NIA Run 10 VL091125-4A Result Units UGL Oate Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Date Analyzed 25-Nov-09 Basis NIA
File Name 028043
CASNO Target Analyte OF Result Reporting Limit
MOL Result Qualifier
EPA Qualifier
78-87-5 12middotDICHLOROPROPANE 1 05 05 017 U
74-95-3 DIBROMOMETHANE 1 05 05 017 U
75-27-4 BROMODICHLOROMETHANE 1 05 05 017 U
10061-01-5 CISmiddot13middotDICHLOROPROPENE 1 05 05 017 U
108-10-1 4-METHYL-2-PENT ANONE 1 5 5 17 U
108-88-3 TOLUENE 1 05 05 017 U
10061-02-6 TRANS-13-DICHLOROPROPENE 1 05 05 017 U
79-00-5 112-TRICHLOROETHANE 1 05 05 017 U
591-78-6 2-HEXANONE 1 10 10 17 U
127-18-4 TETRACHLOROETHENE 1 05 05 017 U
142-28-9 13-DICHLOROPROPANI 1 05 05 017 U
124-48-1 DIBROMOCHLOROMETHANE 1 1 1 017 U
106-93-4 12-DIBROMOETHANE 1 1 1 017 U
108-90-7 CHLOROBENZENE 1 05 05 017 U
630-20-6 1112-TETRACHLOROETHANE 1 05 05 017 U
100-41-4 ETHYLBENZENE 1 05 05 017 U
136777-61-2 M+P-XYLENE 1 1 1 017 U
95-47-6 O-XYLENE 1 05 05 017 U
100-42-5 STYRENE 1 05 05 017 U
75-25-2 BROMOFORM 1 05 05 017 U
98-82-8 ~YLBENZENE 1 05 05 017 U
96-18-4 123-TRICHLOROPROPANE 1 2 2 017 U
79-34-5 1122middot TETRACHLOROETHANE 1 05 05 017 U
108-86-1 BROMOBENZENE 1 05 05 017 U
103-65-1 N-PROPYLBENZENE 1 05 05 017 U
95-49-8 2-CHLOROTOLUENE 1 05 05 017 U
108-67-8 135-TRIMETHYLBENZENE 1 05 05 017 U
106-43-4 4-CHLOROTOLUENE 1 05 05 017 U
Data Package 10 VL0911214-1
Date Printed Wednesday December n 2009 AlS Laboratory Group -- FC Page 2 of 4
lMS VeCSiOIY 6317A
9
GCMS Volatiles Method SW8260 _258
Method Blank
Lab Name ALS Laboratory Group - FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-111B09(HWB R-37 VOCs) PAR 002731703
Lab 10 VL091125-4MB Sample Matrix WATER
Moisture NIA
Prep Batch VL091125-4
QCBatchlD VL091125-4-5
Sample Aliquot
Final Volume
10 ml
10 ml
Date Collected NIA Run ID VL091125-4A Result Units UGL
Date Extracted 25-Nov-09 Cleanup NONE Clean DF 1
Date Analyzed 25-Nov-09 Basis NA
File Name 028043
CASNO Target Analyte OF Result Reporting Limit
MOL Result Qualifier
EPA Qualifier
98-06-6 TERT-BUTYLBENZENE 1 05 05 017 U
95-63-6 124-TRIMETHYLBENZENE 1 05 05 017 U
135-98-8 SEC-BUTYLBENZENE 1 05 05 017 U
541-73-1 13-DlCHLOROBENZENE 1 05 05 017 U
99-87-6 P-ISOPROPYLTOLUENE 1 05 05 017 U
106-46-7 1 A-DICHLOROBENZENE 1 05 05 017 U
104-51-8 N-BUTYLBENZENE 1 05 05 017 U
95-50-1 12-DICHLOROBENZENE 1 05 05 017 U
96-12-B 12-DIBROMO-3-CHLOROPROPANE 1 2 2 067 U
120-82-1 124-TRiCHLOROBENZENE 1 05 05 017 U
87-68-3 HEXACHLOROBUTADIENE 1 05 05 017 U
91-20-3 NAPHTHALENE 1 05 05 017 U
87-61-6 123-TRICHLOROBENZENE 1 05 05 017 U
75-05-B ACETONITRILE 1 50 50 83 U
107-05-1 ALLYL CHLORIDE 1 50 50 017 U
110-57-6 TRANS-14-DICHLORO-2-BUTENE 1 5 5 17 U
64-17-5 ETHANOL 1 200 200 78 U
97-63-2 ETHYL METHACRYLATE 1 5 5 017 U
78-83-1 ISOBUTYL ALCOHOL 1 100 100 17 U
126-98-7 METHACRYLONITRILE 1 35 35 17 U
80-62-6 METHYL METHACRYLATE 1 5 5 17 U
107-12-0 PROPIONITRILE 1 25 25 33 U
126-99-8 CHLOROPRENE 1 5 5 017 U
75-65-0 TERT-BUTANOL 1 100 100 33 U
108-20-3 ISOPROPYL ETHER 1 2 2 033 U
637-92-3 ETHYL TERT-BUTYL ETHER 1 2 2 033 U
994-05-8 TERT-AMYL METHYL ETHER 1 2 2 033 U
67-72-1 HEXACHLOROETHANE 1 2 2 033 U
Data Package 10 VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -~ Fe Page 3 of 4
LlMS Version 6317 A
10
GCMS Volatiles Method SW8260 _258
Method Blank
Lab Name ALS Laboratory Group -- FC
Work Order Number 0911214
Client Name New Mexico Envirmment Department OB
ClientProject 10 644-111809(HWB R-37 VOCs) PAR 002731703
Lab 10 VL091125-4MB Sample Matrix WATER
Moisture NIA Prep Batch VL091125-4
QCBatchlO VL091125-4-5
Sample Aliquot
Final Volume
10 m
10m Date Collected NIA Run 10 VL091125-4A Result Units UGIL Date Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Date Analyzed 25-Nov-09 BasisNIA
File Name 028043
CASNO Target Analyte Result Reporting MOL Result EPAOF Limit Qualifier Qualifier
Surrogate Recovery
CASNO Surrogate Analyte Result Flag Spike Amount
Percent Recovery
Control Limits
460-00-4 4-BROMOFLUOROBENZENE 25 25 100 82 - 121
1868-53-7 DIBROMOFLUOROMETHANE 248 25 99 80 - 123
2037-26-5 TOLUENE-D8 26 25 104 85 - 116
Data Package 10 VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- FC Page 4 of4
LlMS Version 6317A
11
GCMS Volati les Method SW8260 _258
Sample Results
Lab Name ALS Laboratory Group -- FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-111809(HWB R-37 VOCs) PAR 002731703
Field 10 Rmiddot37 Ser 2middot111809
Lab 10 0911214middot1
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml
Moisture NA QCBatchlO VL091125-4-5 Final Volume 10mi Date Collected 18-Nov-09 Run 10 VL091125-4A Result Units UGL
Date Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Analysis ReqCode 104 Date Analyzed 25-Nov-09
Prep Method SW5030 Rev C Basis As Received
File Name 028044
CASNO Target Analyte Dilution Factor
75-71-8 DICHLORODIFLUOROMETHANE 1
74middot87-3 CHLOROMETHANE 1
75-01-4 VINYL CHLORIDE 1
74-83-9 BROMOMETHANE 1
75-00-3 CHLOROETHANE 1
75-69-4 TRICHLOROFLUOROMETHANE 1
107-02-8 ACROLEIN 1
75-35-4 11middotDICHLOROETHENE 1
67-64-1 ACETONE 1
74-88-4 IODOMETHANE 1
75-15-0 CARBON DISULFIDE 1
75-09-2 METHYLENE CHLORIDE 1
156-60-5 TRANSmiddot12middotDICHLOROETHENE 1
1634-04-4 METHYL TERTIARY BUTYL ETHER 1
107-13-1 ACRYLONITRILE 1
75-34-3 1-DICHLOROETHANE 1
i 108-05-4 VINYL ACETATE 1
156-59-2 CIS-12middotDICHLOROETHENE 1
78-93-3 2-BUTANONE 1
74-97-5 BROMOCHLOROMETHANE 67-66-3 CHLOROFORM 1
71-55-6 11-TRICHLOROETHANE 594-20-7 22-DICHLOROPROPANE 56-23-5 CARBON TETRACHLORIDE 563-58-6 -DICHLOROPROPENE 107-06-2 2-DICHLOROETHANE
Result Reporting Limit
05 05
05 05
05 05
1 1
05 05
05 05
100 100
05 05
10 10
5 5
10 10
1 1
05 05
1 1
10 10
05 05
10 10
05 05
5 5
1 1
05 05
1 1
05 05
05 05
05 05
05 05
MOL Result EPA Qualifier Qualifier
017 U
017 U
017 U
017 U
017 U
017 U
17 U
017 U
33 U
017 U
017 U
017 U
017 U
017 U
17 U
017 U
067 U
017 U
17 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
Data Package ID VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- Fe Page 1 of 8
UMS Version 6317A
12
GCMS Volatiles Method SW8260_25B
Sample Results
Lab Name ALS Laboratory Group - FC
Work Order Number 0911214
Client Name New Mexico nvironment Department OB
ClientProject 10 644-111809(HWB R-37 VOCs) PAR 002731703
Field 10 R-37 Scr 2-111809
Lab 10 0911214-1
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10ml
Moisture NA QCBatchlD VL091125-4-5 Final Volume 10ml
Date Collected l8-Nov-09 Run 10 VL091125-4A Result Units UGL
Date Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Analysis ReqCode 104 Date Analyzed 25-Nov-09 Basis As Received
Prep Method SW5030 Rev C File NameD28044
CASNO Target Analyte Dilution Factor
Result Reporting Limit
MDL Result Qualifier
EPA Qualifier
I
71-43-2 BENZENE 1 05 05 017 U
79-01-6 TRICHLOROETHENE 1 05 05 017 U
78-87-5
74middot95-3
75-27-4
10061-01-5
108middot10middot1
108middot88-3
10061-02middot6
79-00-5
591-78-6
12-DICHLOROPROPANE
DIBROMOMETHANE
BROMODCHLOROMETHANE
CIS-13-DICHLOROPROPEI~E
4-METHYL-2-PENTANONE
TOLUENE
TRANS-13-DICHLOROPROPENE
112-TRICHLOROETHANE
2-HEXANONE
1
1
1
1
1
1
1
1
1
05
05
05
05
5
031
05
05
10
05
05
05
05
5
05
05
05
10
017
017
017
017
17
017
017
017
17
U
U
U
U
U
J
U
U
U
127-18-4
142-28-9
124-48-1
106-93-4
108-90-7
630-20-6
100-41-4
136777-61-2
95-47-6
100-42middot5
75-25-2
98-82middot8
96-18-4
79-34-5
108-86-1
TETRACHLOROETHENE
13-DICHLOROPROPANE
DIBROMOCHLOROMETHANE
12-DIBROMOETHANE
CHLOROBENZENE
11 12-TETRACHLOROETHANE
ETHYLBENZENE
M+PmiddotXYLENE
OmiddotXYLENE
STYRENE
BROMOFORM
ISOPRO PYLBENZENE
123middotTRICHLOROPROPANE
1122-TETRACHLOROETHANE
BROMOBENZENE
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
05
05
1
1
05
05
05
1
05
05
05
05
2
05
05
05
05
1
1
05
05
05
1
05
05
05
05
2
05
05
017
017
017
017
017
017
017
017
017
017
017
017
017
017
017
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
i
Data Package 10 VL0911214-1
Date Printed Wednesday December 022009 AlS laboratory Group bullbull Fe Page 2 of 8
UMS Version 6317A
13
GCMS Volatiles Method SW8260_258
Sample Results
Lab Name ALS Laboratory Group bullbull FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject ID 644-111809(HWB R-37 VOCs) PAR 002731703
Field 10 R-37 Sor 2-111809
Lab ID 0911214middot1
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml
Moisture NA QCBatchlD VL091125-4-5 Final Volume 10 ml
Date Collected 18-Nov-09 Run ID VL091125-4A Result Units UGL
Date Extracted 25-Nov-09 Cleanup NONE Clean DF 1
Analysis ReqCode 104 Date Analyzed 25-Nov-09 Basis As Received
Prep Method SW5030 Rev C File Name 028044
CASNO Target Analyte Dilution Factor
103-65-1 NmiddotPROPYLBENZENE 1
95-49-8 2-CHLOROTOLUENE 1
108-67-8 135-TRIMETHYLBENZENE 1
106-43-4 4-CHLOROTOLUENE 1
98-06-6 TER I-BUTYLBENZENE 1
95-63-6 124-TRIMETHYLBENZENE 1
135-98-8 SEC-BUTYLBENZENE 1
541-73-1 13-OICHLOROBENZENE 1
99-87-6 P-ISOPROPYLTOLUENE 1
106-46-7 lA-DICHLOROBENZENE 1
104-51-8 N-BUTYLBENZENE 1
95-50-1 12-DICHLOROBENZENE 1
96-12-8 l2-DIBROMOmiddot3-CHLOROPROPANE 1
120-82-1 12A-TRICHLOROBENZENE 1
187-68-3 HEXACHLOROBUTADIENE 1
91-20-3 NAPHTHALENE 1
87-61middot6 123-TRICHLOROBENZENE 1
75-05-8 ACETONITRILE 1
107middot05middot1 ALLYL CHLORIDE 1
110-57-6 TRANS-14-DICHLORO-2-BUTENE 1
164-17-5 ETHANOL 1
97-63-2 ETHYL METHACRYLATE 1
78-83-1 ISOBUTYL ALCOHOL 1
126-98-7 METHACRYLONITRILE 1
80-62-6 METHYL METHACRYLATE 1
107-12-0 PROPIONITRILE 1
Result Reporting Limit
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
2 2
05 05
05 05
05 05
05 05
50 50
50 50
5 5
200 200
5 5
100 100
35 35
5 5
25 25
MDL Result EPA Qualifier Qualifier
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
067 U
017 U
017 U
017 U
017 U
83 U
017 U
U u 78 U
017 U
17 U
17 U
17 U
33 U
Data Package 10 VL0911214-1
Date Printed Wednesday December 022009 ALS Laboratory Group MM Fe Page 3 of 8
LlMS VerSion 6317A
14
GCMS Volati las Method SW8260_258
Sample Results
Lab Name ALS Laboratory Group - FC
Work Order Number 0911214
Client Name New Mexico Environment Department 08
ClientProject 10 644-111B09(HWB R-37 VOGs) PAR 002731703
Field 10 R-37 Ser 2-111809 Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10ml
Lab 10 0911214-1 Moisture NA
Date Collected 1B-Nov-09 QCBatchlO VL091125-4-5
Run 10 VL091125-4A
Final Volume 10ml
Result Units UGIL Date Extracted 25-Nov-09 Cleanup NONE Clean OF
Analysis ReqCode 104 Date Analyzed 25-Nov-09
Prep Method SW5030 Rev G Basis As Received
File Name 028044
CASNO Target Analyte Dilution Factor
Result Reporting Limit
MDL Result Qualifier
EPA Qualifier
126-99-8 CHLOROPRENE 1 5 5 017 U
75-65-0 TERT-BUTANOL 1 100 100 33 U
108-20-3 ISOPROPYL ETHER 1 2 2 033 U
637-92-3 ETHYL TERT-BUTYL ETHER 1 2 2 033 U
994-05-8 TERT-AMYL METHYL ETHER 1 2 2 033 U
67-72-1 HEXACHLOROETHANE 1 2 2 033 U
Surrogate Recovery
CASNO Surrogate Analyte Result Flag Spike Amount
Percent Recovery
Control Limits
460-00-4 4-BROMOFLUOHOBENZENE 246 25 98 82 - 121
1868-53-7 DIBROMOFLUOHOMETHANE 248 25 99 BO - 123
2037-26-5 TOLUENE-DB 258 25 103 85middot116
Data Package 10 VL0911214-1
Date Printed Wednesday December 022009 ALS Laboratory Group bullbull FC Page 4 of 8
LIMS Version 0317 A
15
GCMS Volati les Method SW8260_25B
Sample Results
Lab Name ALS Laboratory Group -- FC
Worlt Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-111809(HWB Rmiddot37 VOCs) PAR 002731703
Field 10 Rmiddot37 Scr jmiddot111809
Lab 10 0911214-2
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml Moisture NfA QCBatchID VL091125-4middot5 Final Volume 10 ml
Date Collected 18middotNov-09 Run 10 VL091125-4A Result Units UGfL Date Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Analysis ReqCode 104 Date Analyzed 25middotNov-09 Basis As Received Prep Method SW5030 Rev C File Name 028045
CASNO Target Analyte Dilution Factor
Result Reporting Limit
MOL Result Qualifier
EPA Qualifier
75-71-8 DICHLORODIFLUOROMETHANE 1 05 05 017 U
74-87-3 CHLOROMETHANE 1 05 05 017 U
75-01middot4 VINYL CHLORIDE 1 05 05 017 U
74-83-9 BROMOMETHANE 1 1 1 017 U
75middot00middot3 CHLOROETHANE j 05 05 017 U
75-69-4 TRICHLOROFLUOROMETHANE 1 05 05 017 U
107-02-8 ACROLEIN 1 100 100 17 U
i 75-35-4 11-DICHLOROETHENE 1 05 05 017 U
67-64middot1 ACETONE 1 10 10 33 U
74-8S-4 IODOMETHANE 1 5 5 017 U
75-15-0 CARBON DISULFIDE 1 10 10 017 U
75-09-2 METHYLENE CHLORIDE 1 1 1 017 U
156-60-5 TRANS-12-DICHLOROETHENE 1 05 05 017 U
1634-04-4 METHYL TERTIARY BUTYL ETHER 1 1 1 017 U
107-13-1 ACRYLONITRILE 1 10 10 17 U
75-34middot3 11-DICHLOROETHANE 05 05 017 U
i 108-05-4 VINYL ACETATE 1 10 10 067 U
115659-2 CISmiddot 2middotDICHLOROETHENE 1 05 05 017 U
178-933 2middotBUTANONE 1 5 5 17 U
74-97middot5 BROMOCHLOROMET HANE 1 1 1 017 U
67-66-3 CHLOROFORM 1 05 05 017 U
71-55middot6 111middotTRICHLOROETHANE 1 1 1 017 U
594-20-7 22middotDICHLOROPROPANE 1 05 05 017 U
56-23-5 CARBON TETRACHLORIDE 1 05 05 017 U
563-58-6 11middotDICHLOROPROPENE 1 05 05 017 U
107-06-2 12middotDICHL OROETHANE 1 05 05 017 U
Data Package ID VL0911214-1
Date Printed Wednesday December 022009 ALS Laboratory Group -- Fe Page 5 of 8
16
GCMS Volatiles Method SW8260_25B
Sample Results
Lab Name ALS Laboratory Group -- FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-111809(HW3 R-37 VOCs) PAR 002731703
Field 10 R-37 Scr 1-11 1809
Lab 10 0911214-2
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml
Moisture NIA QCBatchlO VL091125-4-5 Final Volume 10 ml
Date Collected 18-Nov-09 Run 10 VL091125-4A Result Units UGL
[late Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Analysis ReqCode 104 Date Analyzed 25-Nov-09
Prep Method SW5030 Rev C Basis As Received
File Name 028045
CASNO Target Analyte Dilution Factor
71-43-2 BENZENE 1
79-01-6 TRICHLOROETHENE 1
78-87-5 12-DICHLOROPROPANE 1
74-95-3 DIBROMOMETHANE 1
75-27-4 BROMODICHLOROMETHANE 1
10061-01-5 CIS-13-DICHLOROPROPENE 1
108-10-1 4-METHYL-2-PtNTANON 1
108-88-3 TOLUENE 1
10061-02-6 TRANS-13-DICHLOROPROPENE 1
79-00-5 112-TRICHLOROETHANE 1
591-78-6 2-HEXANONE 1
127-18-4 TETRACHLOROETHENE 1
142-28-9 13-DICHLOROPROPANt 1
124-48-1 DI3ROMOCHLOROMETHANE 1
106-93-4 12-DIBROMOETHANE 1
108-90-7 CHLOROBENZENE 1
OETHANE 1
- 1
LENE 1
ENE 1
ENE 1
OFORM 1
OPYlBENZENE 1
96-18-4 123-TRICHLOROPROPANE 1
79-34-5 1122-TETRACHLOROETHANE 1
108-86-1 BROMOBENZENE 1
Result Reporting Limit
05 05
05 05
05 05
05 05
05 05
05 05
5 5
025 05
05 05
05 05
10 10
05 05
05 05
1 1
1 1
05 05
05 05
05 05
1 1
05 05
05 05
05 05
05 05
2 2
05 05
05 05
MDL Result EPA Qualifier Qualifier
017 U
017 U
017 U
017 U
017 U
017 U
17 U
017 J
017 U
017 U
17 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
Data Package 10 VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- Fe Page 6 of 8
317A
17
GCMS Volatiles Method SW8260 _258
Sample Results
Lab Name ALS Laboratory Group -- FC
Work Order Number 0911214
Client Name New Mexico Environment Department 08
ClientProject 10 644-11S09(HWB R-37 VOCs) PAR 002731703
Field 10 Rmiddot37 Scr 1-111809
Lab 10 0911214-2
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml Moisture NA QCBatchlD VL091125-4-5 Final Volume 10 ml
Date Collected 18-Nov-09 Run 10 VL091125-4A Result Units UGL Date Extracted 25-Nol-09 Cleanup NONE Clean OF
Analysis ReqCode 104 Date Analyzed 25-Nov-09 Basis As Received Prep Method SW5030 Rev C File Name D28045
CASNO Target Analyte Dilution Factor
103-65-1 N-PROPYLBENZENE 1
95-49-8 2-CHLOROTOLUENE 1
108-67-8 135-TRIMETHYLBENZENE 1
106-43-4 4-CHLOROTOLUENE 1
98-06-6 TERT-BUTYLBENZENE 1
95-63-6 124-TRIMETHYLBENZENE 1
135-98-8 SEC-BUTYLBENZENE 1
i 541-73-1 13middotDICHLOROBENZENE 1
99-87-6 PmiddotISOPROPYL TOLUENE 1
106-46-7 I 14-DICHLOROBENZENE 1
104-51-8 I N-BUTYLBENZENE 1
95-50-1 l2-DICHLOROBENZENE 1
96-12-8 I 12-DIBROMO-3-CHLOROPROPANE 1
120-82-1 124-TRICHLOROBENZENE 1
87-68-3 HEXACHLOROBUT ADIENE 1
91-20-3 NAPHTHALENE 1
87-61-6 123-TRICHLOROBENZENE 1
75-05-S ACETONITRILE 1
107-05-1 ALLYL CH LORIDE 1
110-57-6 TRAN S-14-DICHLORO-2-BUTENE 1
64-17-5 ETHANOL 1
97-63-2 ETHYL METHACRYLATE 1
78-83-1 ISOBUTYL ALCOHOL 1
126-98-7 METHACRYLONITRILE 1
80-62-6 METHYL METHACRYLATE 1
107-12-0 I PROPIONITRILE 1
Result Reporting Limit
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
2 2
05 05
05 05
05 05
05 05
50 50
50 50 I 5 5
200 200
5 5
100 100
35 35
5 5
25 25
MDL
017
017
017
017
017
017
017
017
017
017
017
017
067
017
017
017
017
83
017
17
78
017
17
17
17
33
Result EPA Qualifier Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
Data Package 10 VL0911214-1
Date Printed Wednesday December 022009 ALS Laboratory Group -- Fe Page 7 of 8
LlMS Version 6317A
18
GCMS Volatiles Method SW8260_258
Sample Results
Lab Name ALS Laboratory Group bullbull FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644middot111B09(HWB R-37 VOCs) PAR 002731703
Sample Matrix WATER Prep Batch VL091125--4 Sample Aliquot 10 mlRmiddot37 Ser 1-111809 Moisture NA QCBatchlO VL091125--4-5 Final Volume 10 m
0911214-2 Date Collected 18-Nov-09 Run 10 VL091125--4A Result Units UGL Date Extracted 25-Nov-09 Cleanup NONE Clean OF 1 Date Analyzed 25-Nov-09 Basis As Received
10
Analysis ReqCode 104 Prep Method SW5030 Rev C File Name 028045
I
CASNO Target Analyte Dilution Factor
Result Reporting Limit
MDL Result Qualifier
EPA Qualifier
126-99-8 CHLOROPRENE 1 5 5 017 U
75-65-0 TERT-BUTANOL 1 100 100 33 U
108-20-3 ISOPROPYL ETHER 1 2 2 033 U
637-92-3 ETHYL TERT-BUTYL ETHER 1 2 2 033 U
994-05--8 TERT-AMYL MTHYL ETHER 1 2 2 033 U
67-72-1 HEXACHLOROETHANE 1 2 2 033 U
Surrogate Recovery
CASNO Surrogate Analyte Result Flag Spike Amount
Percent Control Recovery Limits
460-00-4 4middotBROMOFLUOROBENZENE 247 25 99 1
1868-53-7 DIBROMOFLUOROMETHANE 248 25 99 80 123
2037-26-5 TOLUENEmiddotDB 255 25 102 85 - 116
Data Package 10 VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- FC Page B of 8
LlMS Version 6317A
19
GCMS Volatiles Method SW8260_258
Laboratory Control Sample and Laboratory Control Sample Duplicate
Lab Name ALS Laboratory Group - FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-111809(HWB R-37 VOCs) PAR 002731703
Lab 10 VL091125-4LCS Sample Matrix WATER
Moisture NA Prep Batch VL091125-4
QCBatchlD VL091125-4-5
Sample Aliquot
Final Volume
10ml
10ml Date Collected NA Run 10 VL091125-4A Result Units UGIL Date Extracted 111252009 Cleanup NONE Clean OF 1 Date Analyzed 11252009 Basis NA
Prep Method SW5030C File Name 028040
CASNO
74-87-3
75-01-4
74-83-9
75-69-4
75-35-4
75-15-0
156-60-5
75-34-3
108-05-4
156-59-2
78-93-3
67 -66-3
71-55-6
i 56-23-5
107-06-2
71-43-2
79-01-6
78-87-5
75-27-4
108-88-3
79-00-5
591-78-6
127-18-4
106-93-4
108-90-7
63Q20-6
Target Analyte Spike Added
CHLOROMETHANE 10
VINYL CHLORIDE 10
BROMOMETHANE 10
TRICHLOROFLUOROMETHANE 10
11-DICHLOROETHENE 10
CARBON DISULFIDE 10
TRANS-12-DICHLOROETHENE 10
11-DICHLOROETHANE 10
VINYL ACETATE 10
CIS-12-DICHLOROETHENE 10
2middotBUTANONE 40
CHLOROFORM 10
111-TRICHL ORO ETHANE 10
CARBON TETRACHLORIDE 10
12-DICHLOROETHANE 10
BENZENE 10
TRICHLOROETHENE 10
12-DICHLOROPROPANE 10
BROMODICHLOROMETHANE 10
TOLUENE 10
112-TRICHLOROETHANE 10
2-HEXANONE 40
TETRACHLOROETHENE 10
12-DIBROMOETHANE 10
CHLOROBENZENE 10
1112-TETRACHLOROETHANE 10
LCS Reporting Result Result Limit Qualifier
932 05
863 05
943 1
908 05
96 05
95 10 J
996 05
992 05
10 10
102 05
412 5
993 05
974 1
943 05
106 05
983 05
962 05
10 05
988 05
974 05
989 05
409 10
956 05
991 1
984 05
101 05
LCS Control Rec Limits
93 49 -129
86 46 134
94 32-121
91 67 -152
96 61 -135
95 61 -140
100 70 -122
99 76 -119
100 62 182
102 75 126
103 61 -137
99 79 120
97 76 - 114
94 58middot135
106 75middot132
98 70 shy 125
96 74 121
100 81 -119
99 79 - 123
97 76 - 120
99 81 -126
102 45 168
96 56 -128
99 79 -123
98 75 -120
101 82 - 123
Data Package 10 VL0911214middot1
-Date Printed Wednesday December 02 2009 ALS Laboratory Group -- Fe Page 1 of 4
LiMS Version 6317A
20
GCMS Volatiles Method SW8260_25B
Laboratory Control Sample and Laboratory Control Sample Duplicate
Lab Name ALS Laboratory Group - FC
Work Order Number 0911214
Client Name New Mexico Envircnment Department OB
ClientProject 10 644-111809(HWB R-37 VOes) PAR 002731703
Lab 10 VL091125-4LCS Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml
Moisture NIA QCBatchlO VL091125-4-5 Final Volume 10 mi
Date Collected NA Run 10 VL091125-4A Result Units UGL Date Extracted 11252009 Cleanup NONE Clean OF 1 Date Analyzed 111252009 Basis NA
Prep Method SW5030e File Name 028040
CASNO Target Analyte Spike Added
LCS Result
Reporting Limit
Result Qualifier
LCS Rec
Control Limits
100-41-4 ETHYLBENZENE 10 981 05 98 79 -114
136777-61-2 M+P-XYLENE 20 197 1 98 81-115
95-47-6 O-XYLENE 10 101 05 101 81 -115
95-49-8 2-CHLOROTOLUENE 10 97 05 97 80 -128
541-73-1 13-DICHLOROBENZiNt 10 977 05 98 81-116
106-46-7 14-DICHLOROBENZENE 10 979 05 98 81 -119
95-50-1 12-DICHLOROBENZENE 10 987 05 99 79 - 116
91-20-3 NAPHTHALENE 10 993 05 99 69 -126
87-61-6 123-TRICHLOROBENZENE 10 999 05 100 60 -137
Data Package ID VL0911214-1
Date Printed Wecnesday December 02 2009 ALS Laboratory Group -- Fe Page 2 of 4
21
GCMS Volatiles Method SW8260_25B
Laboratory Control Sample and Laboratory Control Sample Duplicate
Lab Name ALS Laboratory Group bullbull FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-11 1809(HWB R-37 VOCs) PAR 002731703
Lab 10 VL091125middot4LCSD Sample Matrix WATER
Moisture NIA Prep Batch VL091125-4
QCBatchlD VL091125-4-5
Sample Aliquot
Final Volume
10 ml
10ml Date Collected NIA Run ID VL091125-4A Result Units UGIL Date Extracted 112512009 Cleanup NONE Clean DF 1 Date Analyzed 1112512009 Basis NIA
Prep Method SW5030C File Name 028041
CASNO Target Analyte Spike Added
LCSD Result
Reporting Limit
Result Qualifier
LCSD Rec
RPD Limit
RPD
74-87-3 CHLOROMETHANE 10 897 05 90 30 4
75-01-4 VINYL CHLORIDE 10 831 05 83 25 4
74-83-9 BROMO METHANE 10 945 1 94 25 0
75-69-4 TRICHLOROFLUOROMETHANE 10 873 05 87 22 4
75-35-4 11-DICHLOROETHENE 10 909 05 91 18 5
75-15-0 CARBON DISULFIDE 10 941 10 J 94 20 1
156-60middot5 TRANS-l2middotDICHLOROETHENE 10 961 05 96 25 4
75middot34middot3 11-DICHLOROETHANE 10 977 05 98 25 2
108-05-4 VINYL ACETATE 10 993 10 J 99 20 1
156middot59-2 CIS-12-DlCHLOROETHENE 10 995 05 99 25 3
i 78-93-3 2-BUTANONE 40 419 5 105 30 2
67-66-3 CHLOROFORM 10 985 05 99 25 1
71-55-6 lll-TRICHLOROETHANE 10 942 1 94 25 3
56-23-5 CARBON TETRACHLORIDE 10 922 05 92 25 2
107middot06-2 12middotDICHLOROETHANE 10 106 05 106 25 0
71-43middot2 BENZENE 10 971 05 97 10 1
79middot01middot6 TRICHLOROETHENE 10 939 05 94 10 2
78middot87middot5 l2middotDICHLOROPROPANE 10 101 05 101 25 1
i 75middot27-4 BROMODICHLOROMETHANE 10 992 05 99 25 0
1108-88-3 TOLUENE 10 962 05 96 9 1
I 79005 112middotTRICHLOROETHANE 10 986 05 99 25 0
591middot78middot6 2-HEXANONE 40 418 10 104 20 2
127middot18-4 TETRACHLOROETHENE 10 918 05 92 25 4
106-93-4 12middotDIBROMOETHANE 10 999 1 100 15 1
108middot90-7 CHLOROBENZENE 10 997 05 100 11 1
630-20middot6 1112-TETRACHLOROETHANE 10 101 05 101 15 0
100-41-4 ETHYLBENZENE 10 968 05 97 25 1
Data Package ID VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- FC Page 3 of 4
lIMS Version 6317 A
22
GCMS Volatiles Method SW8260_25B
Laboratory Control Sample and Laboratory Control Sample Duplicate
Lab Name ALS Laboratory 13roup -- FC
Work Order Number 0911214
Client Name New Mexico Environment Department OS
ClientProject 10 644-11 1809(HWB R-37 VOCs) PAR 002731703
Lab 10 VL091125-4LCSD Sample Matrix WATER
Moisture NA Prep Batch VL091125-4
QCBatchlO VL091125-4-5
Sample Aliquot
Final Volume
10 ml
10ml Date Collected NA Run 10 VL091125-4A Result Units UGL Date Extracted 11252009 Cleanup NONE Clean OF Date Analyzed 11252009 Basis NIA
Prep Method SW5030C File Name 028041
CASNO Target Analyte Spike Added
LCSD Result
Reporting Limit
Result Qualifier
LCSD Rec
RPD Limit
RPD
136777-61-2 M+P-XYLENE 20 193 1 97 25 2
95-47-6 O-XYLENE 10 983 05 98 25 2
95-49-8 2middotCHLOROTOLUENE 10 9A9 05 95 15 2
541-73-1 13middotDICHLOROBENZENE 10 997 05 100 25 2
106-46-7 14-DICHLOROBeNZENE 10 974 05 97 25 1
95-50middot1 12middotDICHLOROBENZeNE 10 101 05 101 25 2
91middot20-3 NAPHTHALENe 10 105 05 105 24 6
87-61-6 123-TRICHLOROBENZENE 10 102 05 102 33 3
Surrogate Recovery LCSLCSD
CASNO Target Analyte Spike Added
LCS Rec
LCS Flag
LCSD Rec
LCSD Flag
Control Limits
460middot00-4 4-BROMOFLUOROBeNZENE 25 100 100 82 - 121
1868-53middot7 DIBROMOFLUOROMeTHANE 25 101 100 80middot 123
2037middot26-5 TOLUENEmiddotD8 25 102 100 85middot 116
Data Package 10 VL0911214-
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- Fe Page 4 of 4
UMS Verslmt 6317A
23
4a Express Package Service _ FadEx Pnority OvernightLJ ==lr-~MClncU1
lSlIIQSATUIIDAYlltIrwIlyis$Mf(1J
middot10_ FadEx SlaMard Ovemioht fMtRallw6ftIlfTampCI v
Stun1I1V OlIwtrlN01IMlIIbU1 PtnIttlgas IIfI ro 150lbs FedEx First OV1lmigtr ~Mmnm~rnollnll onwy9Itetlncalklfl bull SIItlmiIlYDNOTaBItOifi
FecEx~ US Airbill Express
Rate
9439 4324
~ FadEx2Dav FadEx ExDress Saver ~ 5leoMlMmmdayenlh~ TlifaoIUillltrtalllmiddot L ~wqb9di1l~flKlonMool8V SatuIOIyDdillllYldIT~
unRISSSAl1JRDAYOeilwrvI$Mde~
4b ExpressfreightService - __ C0T1llanv
~~oalleJl =1~~ImOt $AUROAY ftlEdOeyF1tlitNbiDrnJtin
5 Packaging -1itIcIrme-- FadEgt r- FedEgt fak FedEx Box
kt1UoorFdrStNil~~Your Internal Billing Reference Enveiope Pol _
TD
Address Wa clMOfdeiinrto POlwuscrPo ZIP CGlJla
Address
6 Special Handlmlllilld Delivery SignalUlll Options
~~~l~__Iint_dUSabulld)IjhL Indirect Sianarurc ttMtrttISMIllFtdlHrtS ~~tlltl~ eeelMllnllrl$ICIIltctdeiMv-kll lt_noaIllaIMInt$ ~
OrvlceL- OtyiclItUN186 ___ ___
[ CaflO Aircraft Oniy
8700 9439 4324 ~rtl1~l__bPnD USA SRI
_____-----------~bull---~----- -------~~-------------------
7
GCMS Volatiles Method SW8260 _25B
Method Blank
Lab Name ALS Laboratory Group bullbull FC
Work Order Number 0911214
Client Name New Mexico Environment Department DB
ClientProject 10 644-111809(HWB Rmiddot37 VOCs) PAR 002731703
Lab 10 VL091125-4MB Sample Matrix WATER
Moisture NA Prep Batch VL091125-4
QCBatchlO VL091125-4-5
Sample Aliquot
Final Volume
10 ml
10 ml Date Collected NA Run 10 VL091125-4A Result Units UGL Date Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Date Analyzed 25middotNov-09 Basis NA
File Name 028043
CASNO Target Analyte DF
75-71-8 DICHLORODIFLUOROMETHANE
74-87-3 CHLOROMETHANE
75-01-4 VINYL CHLORIDE
74-83-9 BROMOMETHANE
75-00-3 CHLOROETHANE
75-69-4 TRICHLOROFLUOROMETHANE
107-02-8 ACROLEIN
75-35-4 11middotDICHLOROETHENE
67-64-1 ACETONE
74-88-4 IODOMETHANE
75-15-0 CARBON DISULFIDE
METHYLEN E CHLORIDE 75-09-2
156-60-5 TRANS-12middotDICHLOROETHENE
1634-04-4 METHYL TERTIARY BUTYL ETHER
107-13-1 ACRYLONITRILE
75-34-3 11-DICHLOROETHANE
108-05-4 VINYL ACETATE
156-59middot2 CIS-12middotDICHLOROETHENE
78-93-3 2middotBUTANONE
~ BROMOCHLOROMETHANE
67-66-3 CHLOROFORM
71-55-6 111middot TRICHLOROETHANE
594-20-7 22middotDICHLOROPROPANE
56-23-5 CARBON TETRACHLORIDE
563-58-6 11middotDICHLOROPROPENE
107-06middot2 l2middotDICHLOROETHAN E
71-43-2 BENZENE
79-01-6 TRICHLOROETHENE
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Result Reporting Limit
05 05
05 05
05 05
1 1
05 05
05 05
100 100
05 05
10 10
5 5
10 10
1 1
05 05
1 1
10 10
05 05
10 10
05 05
5 5
1 1
05 05
1 1
05 05
05 05
05 05
05 05
05 05
05 05
MDL Result EPA Qualifier Qualifier
017 U
017 U
017 U
017 U
017 U
017 U
17 U
017 U
33 U
017 U
017 U
017 U
017 U
017 U
17 U
017 U
067 U
017 U
17 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
Data Package 10 VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- Fe Page 1 of 4
llMS Version 6317 A
8
GCMS Volatiles Method SW8260 _25B
Method Blank
Lab Name ALS Laboratory Group -- FC
Work Order Number 0911214
Client Name New Mexico Environment Department 08
ClientProject 10 644-111809(HWEI R-37 voes) PAR 002731703
Lab 10 VL091125-4MB Sample Matrix WATER
Moisture NIA Prep Batch VL091125-4
QCBatchIO VL091125-4-5
Sample Aliquot
Final Volume
10 ml
10 ml Oate Collected NIA Run 10 VL091125-4A Result Units UGL Oate Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Date Analyzed 25-Nov-09 Basis NIA
File Name 028043
CASNO Target Analyte OF Result Reporting Limit
MOL Result Qualifier
EPA Qualifier
78-87-5 12middotDICHLOROPROPANE 1 05 05 017 U
74-95-3 DIBROMOMETHANE 1 05 05 017 U
75-27-4 BROMODICHLOROMETHANE 1 05 05 017 U
10061-01-5 CISmiddot13middotDICHLOROPROPENE 1 05 05 017 U
108-10-1 4-METHYL-2-PENT ANONE 1 5 5 17 U
108-88-3 TOLUENE 1 05 05 017 U
10061-02-6 TRANS-13-DICHLOROPROPENE 1 05 05 017 U
79-00-5 112-TRICHLOROETHANE 1 05 05 017 U
591-78-6 2-HEXANONE 1 10 10 17 U
127-18-4 TETRACHLOROETHENE 1 05 05 017 U
142-28-9 13-DICHLOROPROPANI 1 05 05 017 U
124-48-1 DIBROMOCHLOROMETHANE 1 1 1 017 U
106-93-4 12-DIBROMOETHANE 1 1 1 017 U
108-90-7 CHLOROBENZENE 1 05 05 017 U
630-20-6 1112-TETRACHLOROETHANE 1 05 05 017 U
100-41-4 ETHYLBENZENE 1 05 05 017 U
136777-61-2 M+P-XYLENE 1 1 1 017 U
95-47-6 O-XYLENE 1 05 05 017 U
100-42-5 STYRENE 1 05 05 017 U
75-25-2 BROMOFORM 1 05 05 017 U
98-82-8 ~YLBENZENE 1 05 05 017 U
96-18-4 123-TRICHLOROPROPANE 1 2 2 017 U
79-34-5 1122middot TETRACHLOROETHANE 1 05 05 017 U
108-86-1 BROMOBENZENE 1 05 05 017 U
103-65-1 N-PROPYLBENZENE 1 05 05 017 U
95-49-8 2-CHLOROTOLUENE 1 05 05 017 U
108-67-8 135-TRIMETHYLBENZENE 1 05 05 017 U
106-43-4 4-CHLOROTOLUENE 1 05 05 017 U
Data Package 10 VL0911214-1
Date Printed Wednesday December n 2009 AlS Laboratory Group -- FC Page 2 of 4
lMS VeCSiOIY 6317A
9
GCMS Volatiles Method SW8260 _258
Method Blank
Lab Name ALS Laboratory Group - FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-111B09(HWB R-37 VOCs) PAR 002731703
Lab 10 VL091125-4MB Sample Matrix WATER
Moisture NIA
Prep Batch VL091125-4
QCBatchlD VL091125-4-5
Sample Aliquot
Final Volume
10 ml
10 ml
Date Collected NIA Run ID VL091125-4A Result Units UGL
Date Extracted 25-Nov-09 Cleanup NONE Clean DF 1
Date Analyzed 25-Nov-09 Basis NA
File Name 028043
CASNO Target Analyte OF Result Reporting Limit
MOL Result Qualifier
EPA Qualifier
98-06-6 TERT-BUTYLBENZENE 1 05 05 017 U
95-63-6 124-TRIMETHYLBENZENE 1 05 05 017 U
135-98-8 SEC-BUTYLBENZENE 1 05 05 017 U
541-73-1 13-DlCHLOROBENZENE 1 05 05 017 U
99-87-6 P-ISOPROPYLTOLUENE 1 05 05 017 U
106-46-7 1 A-DICHLOROBENZENE 1 05 05 017 U
104-51-8 N-BUTYLBENZENE 1 05 05 017 U
95-50-1 12-DICHLOROBENZENE 1 05 05 017 U
96-12-B 12-DIBROMO-3-CHLOROPROPANE 1 2 2 067 U
120-82-1 124-TRiCHLOROBENZENE 1 05 05 017 U
87-68-3 HEXACHLOROBUTADIENE 1 05 05 017 U
91-20-3 NAPHTHALENE 1 05 05 017 U
87-61-6 123-TRICHLOROBENZENE 1 05 05 017 U
75-05-B ACETONITRILE 1 50 50 83 U
107-05-1 ALLYL CHLORIDE 1 50 50 017 U
110-57-6 TRANS-14-DICHLORO-2-BUTENE 1 5 5 17 U
64-17-5 ETHANOL 1 200 200 78 U
97-63-2 ETHYL METHACRYLATE 1 5 5 017 U
78-83-1 ISOBUTYL ALCOHOL 1 100 100 17 U
126-98-7 METHACRYLONITRILE 1 35 35 17 U
80-62-6 METHYL METHACRYLATE 1 5 5 17 U
107-12-0 PROPIONITRILE 1 25 25 33 U
126-99-8 CHLOROPRENE 1 5 5 017 U
75-65-0 TERT-BUTANOL 1 100 100 33 U
108-20-3 ISOPROPYL ETHER 1 2 2 033 U
637-92-3 ETHYL TERT-BUTYL ETHER 1 2 2 033 U
994-05-8 TERT-AMYL METHYL ETHER 1 2 2 033 U
67-72-1 HEXACHLOROETHANE 1 2 2 033 U
Data Package 10 VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -~ Fe Page 3 of 4
LlMS Version 6317 A
10
GCMS Volatiles Method SW8260 _258
Method Blank
Lab Name ALS Laboratory Group -- FC
Work Order Number 0911214
Client Name New Mexico Envirmment Department OB
ClientProject 10 644-111809(HWB R-37 VOCs) PAR 002731703
Lab 10 VL091125-4MB Sample Matrix WATER
Moisture NIA Prep Batch VL091125-4
QCBatchlO VL091125-4-5
Sample Aliquot
Final Volume
10 m
10m Date Collected NIA Run 10 VL091125-4A Result Units UGIL Date Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Date Analyzed 25-Nov-09 BasisNIA
File Name 028043
CASNO Target Analyte Result Reporting MOL Result EPAOF Limit Qualifier Qualifier
Surrogate Recovery
CASNO Surrogate Analyte Result Flag Spike Amount
Percent Recovery
Control Limits
460-00-4 4-BROMOFLUOROBENZENE 25 25 100 82 - 121
1868-53-7 DIBROMOFLUOROMETHANE 248 25 99 80 - 123
2037-26-5 TOLUENE-D8 26 25 104 85 - 116
Data Package 10 VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- FC Page 4 of4
LlMS Version 6317A
11
GCMS Volati les Method SW8260 _258
Sample Results
Lab Name ALS Laboratory Group -- FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-111809(HWB R-37 VOCs) PAR 002731703
Field 10 Rmiddot37 Ser 2middot111809
Lab 10 0911214middot1
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml
Moisture NA QCBatchlO VL091125-4-5 Final Volume 10mi Date Collected 18-Nov-09 Run 10 VL091125-4A Result Units UGL
Date Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Analysis ReqCode 104 Date Analyzed 25-Nov-09
Prep Method SW5030 Rev C Basis As Received
File Name 028044
CASNO Target Analyte Dilution Factor
75-71-8 DICHLORODIFLUOROMETHANE 1
74middot87-3 CHLOROMETHANE 1
75-01-4 VINYL CHLORIDE 1
74-83-9 BROMOMETHANE 1
75-00-3 CHLOROETHANE 1
75-69-4 TRICHLOROFLUOROMETHANE 1
107-02-8 ACROLEIN 1
75-35-4 11middotDICHLOROETHENE 1
67-64-1 ACETONE 1
74-88-4 IODOMETHANE 1
75-15-0 CARBON DISULFIDE 1
75-09-2 METHYLENE CHLORIDE 1
156-60-5 TRANSmiddot12middotDICHLOROETHENE 1
1634-04-4 METHYL TERTIARY BUTYL ETHER 1
107-13-1 ACRYLONITRILE 1
75-34-3 1-DICHLOROETHANE 1
i 108-05-4 VINYL ACETATE 1
156-59-2 CIS-12middotDICHLOROETHENE 1
78-93-3 2-BUTANONE 1
74-97-5 BROMOCHLOROMETHANE 67-66-3 CHLOROFORM 1
71-55-6 11-TRICHLOROETHANE 594-20-7 22-DICHLOROPROPANE 56-23-5 CARBON TETRACHLORIDE 563-58-6 -DICHLOROPROPENE 107-06-2 2-DICHLOROETHANE
Result Reporting Limit
05 05
05 05
05 05
1 1
05 05
05 05
100 100
05 05
10 10
5 5
10 10
1 1
05 05
1 1
10 10
05 05
10 10
05 05
5 5
1 1
05 05
1 1
05 05
05 05
05 05
05 05
MOL Result EPA Qualifier Qualifier
017 U
017 U
017 U
017 U
017 U
017 U
17 U
017 U
33 U
017 U
017 U
017 U
017 U
017 U
17 U
017 U
067 U
017 U
17 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
Data Package ID VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- Fe Page 1 of 8
UMS Version 6317A
12
GCMS Volatiles Method SW8260_25B
Sample Results
Lab Name ALS Laboratory Group - FC
Work Order Number 0911214
Client Name New Mexico nvironment Department OB
ClientProject 10 644-111809(HWB R-37 VOCs) PAR 002731703
Field 10 R-37 Scr 2-111809
Lab 10 0911214-1
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10ml
Moisture NA QCBatchlD VL091125-4-5 Final Volume 10ml
Date Collected l8-Nov-09 Run 10 VL091125-4A Result Units UGL
Date Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Analysis ReqCode 104 Date Analyzed 25-Nov-09 Basis As Received
Prep Method SW5030 Rev C File NameD28044
CASNO Target Analyte Dilution Factor
Result Reporting Limit
MDL Result Qualifier
EPA Qualifier
I
71-43-2 BENZENE 1 05 05 017 U
79-01-6 TRICHLOROETHENE 1 05 05 017 U
78-87-5
74middot95-3
75-27-4
10061-01-5
108middot10middot1
108middot88-3
10061-02middot6
79-00-5
591-78-6
12-DICHLOROPROPANE
DIBROMOMETHANE
BROMODCHLOROMETHANE
CIS-13-DICHLOROPROPEI~E
4-METHYL-2-PENTANONE
TOLUENE
TRANS-13-DICHLOROPROPENE
112-TRICHLOROETHANE
2-HEXANONE
1
1
1
1
1
1
1
1
1
05
05
05
05
5
031
05
05
10
05
05
05
05
5
05
05
05
10
017
017
017
017
17
017
017
017
17
U
U
U
U
U
J
U
U
U
127-18-4
142-28-9
124-48-1
106-93-4
108-90-7
630-20-6
100-41-4
136777-61-2
95-47-6
100-42middot5
75-25-2
98-82middot8
96-18-4
79-34-5
108-86-1
TETRACHLOROETHENE
13-DICHLOROPROPANE
DIBROMOCHLOROMETHANE
12-DIBROMOETHANE
CHLOROBENZENE
11 12-TETRACHLOROETHANE
ETHYLBENZENE
M+PmiddotXYLENE
OmiddotXYLENE
STYRENE
BROMOFORM
ISOPRO PYLBENZENE
123middotTRICHLOROPROPANE
1122-TETRACHLOROETHANE
BROMOBENZENE
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
05
05
1
1
05
05
05
1
05
05
05
05
2
05
05
05
05
1
1
05
05
05
1
05
05
05
05
2
05
05
017
017
017
017
017
017
017
017
017
017
017
017
017
017
017
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
i
Data Package 10 VL0911214-1
Date Printed Wednesday December 022009 AlS laboratory Group bullbull Fe Page 2 of 8
UMS Version 6317A
13
GCMS Volatiles Method SW8260_258
Sample Results
Lab Name ALS Laboratory Group bullbull FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject ID 644-111809(HWB R-37 VOCs) PAR 002731703
Field 10 R-37 Sor 2-111809
Lab ID 0911214middot1
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml
Moisture NA QCBatchlD VL091125-4-5 Final Volume 10 ml
Date Collected 18-Nov-09 Run ID VL091125-4A Result Units UGL
Date Extracted 25-Nov-09 Cleanup NONE Clean DF 1
Analysis ReqCode 104 Date Analyzed 25-Nov-09 Basis As Received
Prep Method SW5030 Rev C File Name 028044
CASNO Target Analyte Dilution Factor
103-65-1 NmiddotPROPYLBENZENE 1
95-49-8 2-CHLOROTOLUENE 1
108-67-8 135-TRIMETHYLBENZENE 1
106-43-4 4-CHLOROTOLUENE 1
98-06-6 TER I-BUTYLBENZENE 1
95-63-6 124-TRIMETHYLBENZENE 1
135-98-8 SEC-BUTYLBENZENE 1
541-73-1 13-OICHLOROBENZENE 1
99-87-6 P-ISOPROPYLTOLUENE 1
106-46-7 lA-DICHLOROBENZENE 1
104-51-8 N-BUTYLBENZENE 1
95-50-1 12-DICHLOROBENZENE 1
96-12-8 l2-DIBROMOmiddot3-CHLOROPROPANE 1
120-82-1 12A-TRICHLOROBENZENE 1
187-68-3 HEXACHLOROBUTADIENE 1
91-20-3 NAPHTHALENE 1
87-61middot6 123-TRICHLOROBENZENE 1
75-05-8 ACETONITRILE 1
107middot05middot1 ALLYL CHLORIDE 1
110-57-6 TRANS-14-DICHLORO-2-BUTENE 1
164-17-5 ETHANOL 1
97-63-2 ETHYL METHACRYLATE 1
78-83-1 ISOBUTYL ALCOHOL 1
126-98-7 METHACRYLONITRILE 1
80-62-6 METHYL METHACRYLATE 1
107-12-0 PROPIONITRILE 1
Result Reporting Limit
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
2 2
05 05
05 05
05 05
05 05
50 50
50 50
5 5
200 200
5 5
100 100
35 35
5 5
25 25
MDL Result EPA Qualifier Qualifier
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
067 U
017 U
017 U
017 U
017 U
83 U
017 U
U u 78 U
017 U
17 U
17 U
17 U
33 U
Data Package 10 VL0911214-1
Date Printed Wednesday December 022009 ALS Laboratory Group MM Fe Page 3 of 8
LlMS VerSion 6317A
14
GCMS Volati las Method SW8260_258
Sample Results
Lab Name ALS Laboratory Group - FC
Work Order Number 0911214
Client Name New Mexico Environment Department 08
ClientProject 10 644-111B09(HWB R-37 VOGs) PAR 002731703
Field 10 R-37 Ser 2-111809 Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10ml
Lab 10 0911214-1 Moisture NA
Date Collected 1B-Nov-09 QCBatchlO VL091125-4-5
Run 10 VL091125-4A
Final Volume 10ml
Result Units UGIL Date Extracted 25-Nov-09 Cleanup NONE Clean OF
Analysis ReqCode 104 Date Analyzed 25-Nov-09
Prep Method SW5030 Rev G Basis As Received
File Name 028044
CASNO Target Analyte Dilution Factor
Result Reporting Limit
MDL Result Qualifier
EPA Qualifier
126-99-8 CHLOROPRENE 1 5 5 017 U
75-65-0 TERT-BUTANOL 1 100 100 33 U
108-20-3 ISOPROPYL ETHER 1 2 2 033 U
637-92-3 ETHYL TERT-BUTYL ETHER 1 2 2 033 U
994-05-8 TERT-AMYL METHYL ETHER 1 2 2 033 U
67-72-1 HEXACHLOROETHANE 1 2 2 033 U
Surrogate Recovery
CASNO Surrogate Analyte Result Flag Spike Amount
Percent Recovery
Control Limits
460-00-4 4-BROMOFLUOHOBENZENE 246 25 98 82 - 121
1868-53-7 DIBROMOFLUOHOMETHANE 248 25 99 BO - 123
2037-26-5 TOLUENE-DB 258 25 103 85middot116
Data Package 10 VL0911214-1
Date Printed Wednesday December 022009 ALS Laboratory Group bullbull FC Page 4 of 8
LIMS Version 0317 A
15
GCMS Volati les Method SW8260_25B
Sample Results
Lab Name ALS Laboratory Group -- FC
Worlt Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-111809(HWB Rmiddot37 VOCs) PAR 002731703
Field 10 Rmiddot37 Scr jmiddot111809
Lab 10 0911214-2
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml Moisture NfA QCBatchID VL091125-4middot5 Final Volume 10 ml
Date Collected 18middotNov-09 Run 10 VL091125-4A Result Units UGfL Date Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Analysis ReqCode 104 Date Analyzed 25middotNov-09 Basis As Received Prep Method SW5030 Rev C File Name 028045
CASNO Target Analyte Dilution Factor
Result Reporting Limit
MOL Result Qualifier
EPA Qualifier
75-71-8 DICHLORODIFLUOROMETHANE 1 05 05 017 U
74-87-3 CHLOROMETHANE 1 05 05 017 U
75-01middot4 VINYL CHLORIDE 1 05 05 017 U
74-83-9 BROMOMETHANE 1 1 1 017 U
75middot00middot3 CHLOROETHANE j 05 05 017 U
75-69-4 TRICHLOROFLUOROMETHANE 1 05 05 017 U
107-02-8 ACROLEIN 1 100 100 17 U
i 75-35-4 11-DICHLOROETHENE 1 05 05 017 U
67-64middot1 ACETONE 1 10 10 33 U
74-8S-4 IODOMETHANE 1 5 5 017 U
75-15-0 CARBON DISULFIDE 1 10 10 017 U
75-09-2 METHYLENE CHLORIDE 1 1 1 017 U
156-60-5 TRANS-12-DICHLOROETHENE 1 05 05 017 U
1634-04-4 METHYL TERTIARY BUTYL ETHER 1 1 1 017 U
107-13-1 ACRYLONITRILE 1 10 10 17 U
75-34middot3 11-DICHLOROETHANE 05 05 017 U
i 108-05-4 VINYL ACETATE 1 10 10 067 U
115659-2 CISmiddot 2middotDICHLOROETHENE 1 05 05 017 U
178-933 2middotBUTANONE 1 5 5 17 U
74-97middot5 BROMOCHLOROMET HANE 1 1 1 017 U
67-66-3 CHLOROFORM 1 05 05 017 U
71-55middot6 111middotTRICHLOROETHANE 1 1 1 017 U
594-20-7 22middotDICHLOROPROPANE 1 05 05 017 U
56-23-5 CARBON TETRACHLORIDE 1 05 05 017 U
563-58-6 11middotDICHLOROPROPENE 1 05 05 017 U
107-06-2 12middotDICHL OROETHANE 1 05 05 017 U
Data Package ID VL0911214-1
Date Printed Wednesday December 022009 ALS Laboratory Group -- Fe Page 5 of 8
16
GCMS Volatiles Method SW8260_25B
Sample Results
Lab Name ALS Laboratory Group -- FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-111809(HW3 R-37 VOCs) PAR 002731703
Field 10 R-37 Scr 1-11 1809
Lab 10 0911214-2
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml
Moisture NIA QCBatchlO VL091125-4-5 Final Volume 10 ml
Date Collected 18-Nov-09 Run 10 VL091125-4A Result Units UGL
[late Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Analysis ReqCode 104 Date Analyzed 25-Nov-09
Prep Method SW5030 Rev C Basis As Received
File Name 028045
CASNO Target Analyte Dilution Factor
71-43-2 BENZENE 1
79-01-6 TRICHLOROETHENE 1
78-87-5 12-DICHLOROPROPANE 1
74-95-3 DIBROMOMETHANE 1
75-27-4 BROMODICHLOROMETHANE 1
10061-01-5 CIS-13-DICHLOROPROPENE 1
108-10-1 4-METHYL-2-PtNTANON 1
108-88-3 TOLUENE 1
10061-02-6 TRANS-13-DICHLOROPROPENE 1
79-00-5 112-TRICHLOROETHANE 1
591-78-6 2-HEXANONE 1
127-18-4 TETRACHLOROETHENE 1
142-28-9 13-DICHLOROPROPANt 1
124-48-1 DI3ROMOCHLOROMETHANE 1
106-93-4 12-DIBROMOETHANE 1
108-90-7 CHLOROBENZENE 1
OETHANE 1
- 1
LENE 1
ENE 1
ENE 1
OFORM 1
OPYlBENZENE 1
96-18-4 123-TRICHLOROPROPANE 1
79-34-5 1122-TETRACHLOROETHANE 1
108-86-1 BROMOBENZENE 1
Result Reporting Limit
05 05
05 05
05 05
05 05
05 05
05 05
5 5
025 05
05 05
05 05
10 10
05 05
05 05
1 1
1 1
05 05
05 05
05 05
1 1
05 05
05 05
05 05
05 05
2 2
05 05
05 05
MDL Result EPA Qualifier Qualifier
017 U
017 U
017 U
017 U
017 U
017 U
17 U
017 J
017 U
017 U
17 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
Data Package 10 VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- Fe Page 6 of 8
317A
17
GCMS Volatiles Method SW8260 _258
Sample Results
Lab Name ALS Laboratory Group -- FC
Work Order Number 0911214
Client Name New Mexico Environment Department 08
ClientProject 10 644-11S09(HWB R-37 VOCs) PAR 002731703
Field 10 Rmiddot37 Scr 1-111809
Lab 10 0911214-2
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml Moisture NA QCBatchlD VL091125-4-5 Final Volume 10 ml
Date Collected 18-Nov-09 Run 10 VL091125-4A Result Units UGL Date Extracted 25-Nol-09 Cleanup NONE Clean OF
Analysis ReqCode 104 Date Analyzed 25-Nov-09 Basis As Received Prep Method SW5030 Rev C File Name D28045
CASNO Target Analyte Dilution Factor
103-65-1 N-PROPYLBENZENE 1
95-49-8 2-CHLOROTOLUENE 1
108-67-8 135-TRIMETHYLBENZENE 1
106-43-4 4-CHLOROTOLUENE 1
98-06-6 TERT-BUTYLBENZENE 1
95-63-6 124-TRIMETHYLBENZENE 1
135-98-8 SEC-BUTYLBENZENE 1
i 541-73-1 13middotDICHLOROBENZENE 1
99-87-6 PmiddotISOPROPYL TOLUENE 1
106-46-7 I 14-DICHLOROBENZENE 1
104-51-8 I N-BUTYLBENZENE 1
95-50-1 l2-DICHLOROBENZENE 1
96-12-8 I 12-DIBROMO-3-CHLOROPROPANE 1
120-82-1 124-TRICHLOROBENZENE 1
87-68-3 HEXACHLOROBUT ADIENE 1
91-20-3 NAPHTHALENE 1
87-61-6 123-TRICHLOROBENZENE 1
75-05-S ACETONITRILE 1
107-05-1 ALLYL CH LORIDE 1
110-57-6 TRAN S-14-DICHLORO-2-BUTENE 1
64-17-5 ETHANOL 1
97-63-2 ETHYL METHACRYLATE 1
78-83-1 ISOBUTYL ALCOHOL 1
126-98-7 METHACRYLONITRILE 1
80-62-6 METHYL METHACRYLATE 1
107-12-0 I PROPIONITRILE 1
Result Reporting Limit
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
2 2
05 05
05 05
05 05
05 05
50 50
50 50 I 5 5
200 200
5 5
100 100
35 35
5 5
25 25
MDL
017
017
017
017
017
017
017
017
017
017
017
017
067
017
017
017
017
83
017
17
78
017
17
17
17
33
Result EPA Qualifier Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
Data Package 10 VL0911214-1
Date Printed Wednesday December 022009 ALS Laboratory Group -- Fe Page 7 of 8
LlMS Version 6317A
18
GCMS Volatiles Method SW8260_258
Sample Results
Lab Name ALS Laboratory Group bullbull FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644middot111B09(HWB R-37 VOCs) PAR 002731703
Sample Matrix WATER Prep Batch VL091125--4 Sample Aliquot 10 mlRmiddot37 Ser 1-111809 Moisture NA QCBatchlO VL091125--4-5 Final Volume 10 m
0911214-2 Date Collected 18-Nov-09 Run 10 VL091125--4A Result Units UGL Date Extracted 25-Nov-09 Cleanup NONE Clean OF 1 Date Analyzed 25-Nov-09 Basis As Received
10
Analysis ReqCode 104 Prep Method SW5030 Rev C File Name 028045
I
CASNO Target Analyte Dilution Factor
Result Reporting Limit
MDL Result Qualifier
EPA Qualifier
126-99-8 CHLOROPRENE 1 5 5 017 U
75-65-0 TERT-BUTANOL 1 100 100 33 U
108-20-3 ISOPROPYL ETHER 1 2 2 033 U
637-92-3 ETHYL TERT-BUTYL ETHER 1 2 2 033 U
994-05--8 TERT-AMYL MTHYL ETHER 1 2 2 033 U
67-72-1 HEXACHLOROETHANE 1 2 2 033 U
Surrogate Recovery
CASNO Surrogate Analyte Result Flag Spike Amount
Percent Control Recovery Limits
460-00-4 4middotBROMOFLUOROBENZENE 247 25 99 1
1868-53-7 DIBROMOFLUOROMETHANE 248 25 99 80 123
2037-26-5 TOLUENEmiddotDB 255 25 102 85 - 116
Data Package 10 VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- FC Page B of 8
LlMS Version 6317A
19
GCMS Volatiles Method SW8260_258
Laboratory Control Sample and Laboratory Control Sample Duplicate
Lab Name ALS Laboratory Group - FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-111809(HWB R-37 VOCs) PAR 002731703
Lab 10 VL091125-4LCS Sample Matrix WATER
Moisture NA Prep Batch VL091125-4
QCBatchlD VL091125-4-5
Sample Aliquot
Final Volume
10ml
10ml Date Collected NA Run 10 VL091125-4A Result Units UGIL Date Extracted 111252009 Cleanup NONE Clean OF 1 Date Analyzed 11252009 Basis NA
Prep Method SW5030C File Name 028040
CASNO
74-87-3
75-01-4
74-83-9
75-69-4
75-35-4
75-15-0
156-60-5
75-34-3
108-05-4
156-59-2
78-93-3
67 -66-3
71-55-6
i 56-23-5
107-06-2
71-43-2
79-01-6
78-87-5
75-27-4
108-88-3
79-00-5
591-78-6
127-18-4
106-93-4
108-90-7
63Q20-6
Target Analyte Spike Added
CHLOROMETHANE 10
VINYL CHLORIDE 10
BROMOMETHANE 10
TRICHLOROFLUOROMETHANE 10
11-DICHLOROETHENE 10
CARBON DISULFIDE 10
TRANS-12-DICHLOROETHENE 10
11-DICHLOROETHANE 10
VINYL ACETATE 10
CIS-12-DICHLOROETHENE 10
2middotBUTANONE 40
CHLOROFORM 10
111-TRICHL ORO ETHANE 10
CARBON TETRACHLORIDE 10
12-DICHLOROETHANE 10
BENZENE 10
TRICHLOROETHENE 10
12-DICHLOROPROPANE 10
BROMODICHLOROMETHANE 10
TOLUENE 10
112-TRICHLOROETHANE 10
2-HEXANONE 40
TETRACHLOROETHENE 10
12-DIBROMOETHANE 10
CHLOROBENZENE 10
1112-TETRACHLOROETHANE 10
LCS Reporting Result Result Limit Qualifier
932 05
863 05
943 1
908 05
96 05
95 10 J
996 05
992 05
10 10
102 05
412 5
993 05
974 1
943 05
106 05
983 05
962 05
10 05
988 05
974 05
989 05
409 10
956 05
991 1
984 05
101 05
LCS Control Rec Limits
93 49 -129
86 46 134
94 32-121
91 67 -152
96 61 -135
95 61 -140
100 70 -122
99 76 -119
100 62 182
102 75 126
103 61 -137
99 79 120
97 76 - 114
94 58middot135
106 75middot132
98 70 shy 125
96 74 121
100 81 -119
99 79 - 123
97 76 - 120
99 81 -126
102 45 168
96 56 -128
99 79 -123
98 75 -120
101 82 - 123
Data Package 10 VL0911214middot1
-Date Printed Wednesday December 02 2009 ALS Laboratory Group -- Fe Page 1 of 4
LiMS Version 6317A
20
GCMS Volatiles Method SW8260_25B
Laboratory Control Sample and Laboratory Control Sample Duplicate
Lab Name ALS Laboratory Group - FC
Work Order Number 0911214
Client Name New Mexico Envircnment Department OB
ClientProject 10 644-111809(HWB R-37 VOes) PAR 002731703
Lab 10 VL091125-4LCS Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml
Moisture NIA QCBatchlO VL091125-4-5 Final Volume 10 mi
Date Collected NA Run 10 VL091125-4A Result Units UGL Date Extracted 11252009 Cleanup NONE Clean OF 1 Date Analyzed 111252009 Basis NA
Prep Method SW5030e File Name 028040
CASNO Target Analyte Spike Added
LCS Result
Reporting Limit
Result Qualifier
LCS Rec
Control Limits
100-41-4 ETHYLBENZENE 10 981 05 98 79 -114
136777-61-2 M+P-XYLENE 20 197 1 98 81-115
95-47-6 O-XYLENE 10 101 05 101 81 -115
95-49-8 2-CHLOROTOLUENE 10 97 05 97 80 -128
541-73-1 13-DICHLOROBENZiNt 10 977 05 98 81-116
106-46-7 14-DICHLOROBENZENE 10 979 05 98 81 -119
95-50-1 12-DICHLOROBENZENE 10 987 05 99 79 - 116
91-20-3 NAPHTHALENE 10 993 05 99 69 -126
87-61-6 123-TRICHLOROBENZENE 10 999 05 100 60 -137
Data Package ID VL0911214-1
Date Printed Wecnesday December 02 2009 ALS Laboratory Group -- Fe Page 2 of 4
21
GCMS Volatiles Method SW8260_25B
Laboratory Control Sample and Laboratory Control Sample Duplicate
Lab Name ALS Laboratory Group bullbull FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-11 1809(HWB R-37 VOCs) PAR 002731703
Lab 10 VL091125middot4LCSD Sample Matrix WATER
Moisture NIA Prep Batch VL091125-4
QCBatchlD VL091125-4-5
Sample Aliquot
Final Volume
10 ml
10ml Date Collected NIA Run ID VL091125-4A Result Units UGIL Date Extracted 112512009 Cleanup NONE Clean DF 1 Date Analyzed 1112512009 Basis NIA
Prep Method SW5030C File Name 028041
CASNO Target Analyte Spike Added
LCSD Result
Reporting Limit
Result Qualifier
LCSD Rec
RPD Limit
RPD
74-87-3 CHLOROMETHANE 10 897 05 90 30 4
75-01-4 VINYL CHLORIDE 10 831 05 83 25 4
74-83-9 BROMO METHANE 10 945 1 94 25 0
75-69-4 TRICHLOROFLUOROMETHANE 10 873 05 87 22 4
75-35-4 11-DICHLOROETHENE 10 909 05 91 18 5
75-15-0 CARBON DISULFIDE 10 941 10 J 94 20 1
156-60middot5 TRANS-l2middotDICHLOROETHENE 10 961 05 96 25 4
75middot34middot3 11-DICHLOROETHANE 10 977 05 98 25 2
108-05-4 VINYL ACETATE 10 993 10 J 99 20 1
156middot59-2 CIS-12-DlCHLOROETHENE 10 995 05 99 25 3
i 78-93-3 2-BUTANONE 40 419 5 105 30 2
67-66-3 CHLOROFORM 10 985 05 99 25 1
71-55-6 lll-TRICHLOROETHANE 10 942 1 94 25 3
56-23-5 CARBON TETRACHLORIDE 10 922 05 92 25 2
107middot06-2 12middotDICHLOROETHANE 10 106 05 106 25 0
71-43middot2 BENZENE 10 971 05 97 10 1
79middot01middot6 TRICHLOROETHENE 10 939 05 94 10 2
78middot87middot5 l2middotDICHLOROPROPANE 10 101 05 101 25 1
i 75middot27-4 BROMODICHLOROMETHANE 10 992 05 99 25 0
1108-88-3 TOLUENE 10 962 05 96 9 1
I 79005 112middotTRICHLOROETHANE 10 986 05 99 25 0
591middot78middot6 2-HEXANONE 40 418 10 104 20 2
127middot18-4 TETRACHLOROETHENE 10 918 05 92 25 4
106-93-4 12middotDIBROMOETHANE 10 999 1 100 15 1
108middot90-7 CHLOROBENZENE 10 997 05 100 11 1
630-20middot6 1112-TETRACHLOROETHANE 10 101 05 101 15 0
100-41-4 ETHYLBENZENE 10 968 05 97 25 1
Data Package ID VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- FC Page 3 of 4
lIMS Version 6317 A
22
GCMS Volatiles Method SW8260_25B
Laboratory Control Sample and Laboratory Control Sample Duplicate
Lab Name ALS Laboratory 13roup -- FC
Work Order Number 0911214
Client Name New Mexico Environment Department OS
ClientProject 10 644-11 1809(HWB R-37 VOCs) PAR 002731703
Lab 10 VL091125-4LCSD Sample Matrix WATER
Moisture NA Prep Batch VL091125-4
QCBatchlO VL091125-4-5
Sample Aliquot
Final Volume
10 ml
10ml Date Collected NA Run 10 VL091125-4A Result Units UGL Date Extracted 11252009 Cleanup NONE Clean OF Date Analyzed 11252009 Basis NIA
Prep Method SW5030C File Name 028041
CASNO Target Analyte Spike Added
LCSD Result
Reporting Limit
Result Qualifier
LCSD Rec
RPD Limit
RPD
136777-61-2 M+P-XYLENE 20 193 1 97 25 2
95-47-6 O-XYLENE 10 983 05 98 25 2
95-49-8 2middotCHLOROTOLUENE 10 9A9 05 95 15 2
541-73-1 13middotDICHLOROBENZENE 10 997 05 100 25 2
106-46-7 14-DICHLOROBeNZENE 10 974 05 97 25 1
95-50middot1 12middotDICHLOROBENZeNE 10 101 05 101 25 2
91middot20-3 NAPHTHALENe 10 105 05 105 24 6
87-61-6 123-TRICHLOROBENZENE 10 102 05 102 33 3
Surrogate Recovery LCSLCSD
CASNO Target Analyte Spike Added
LCS Rec
LCS Flag
LCSD Rec
LCSD Flag
Control Limits
460middot00-4 4-BROMOFLUOROBeNZENE 25 100 100 82 - 121
1868-53middot7 DIBROMOFLUOROMeTHANE 25 101 100 80middot 123
2037middot26-5 TOLUENEmiddotD8 25 102 100 85middot 116
Data Package 10 VL0911214-
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- Fe Page 4 of 4
UMS Verslmt 6317A
23
GCMS Volatiles Method SW8260 _25B
Method Blank
Lab Name ALS Laboratory Group bullbull FC
Work Order Number 0911214
Client Name New Mexico Environment Department DB
ClientProject 10 644-111809(HWB Rmiddot37 VOCs) PAR 002731703
Lab 10 VL091125-4MB Sample Matrix WATER
Moisture NA Prep Batch VL091125-4
QCBatchlO VL091125-4-5
Sample Aliquot
Final Volume
10 ml
10 ml Date Collected NA Run 10 VL091125-4A Result Units UGL Date Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Date Analyzed 25middotNov-09 Basis NA
File Name 028043
CASNO Target Analyte DF
75-71-8 DICHLORODIFLUOROMETHANE
74-87-3 CHLOROMETHANE
75-01-4 VINYL CHLORIDE
74-83-9 BROMOMETHANE
75-00-3 CHLOROETHANE
75-69-4 TRICHLOROFLUOROMETHANE
107-02-8 ACROLEIN
75-35-4 11middotDICHLOROETHENE
67-64-1 ACETONE
74-88-4 IODOMETHANE
75-15-0 CARBON DISULFIDE
METHYLEN E CHLORIDE 75-09-2
156-60-5 TRANS-12middotDICHLOROETHENE
1634-04-4 METHYL TERTIARY BUTYL ETHER
107-13-1 ACRYLONITRILE
75-34-3 11-DICHLOROETHANE
108-05-4 VINYL ACETATE
156-59middot2 CIS-12middotDICHLOROETHENE
78-93-3 2middotBUTANONE
~ BROMOCHLOROMETHANE
67-66-3 CHLOROFORM
71-55-6 111middot TRICHLOROETHANE
594-20-7 22middotDICHLOROPROPANE
56-23-5 CARBON TETRACHLORIDE
563-58-6 11middotDICHLOROPROPENE
107-06middot2 l2middotDICHLOROETHAN E
71-43-2 BENZENE
79-01-6 TRICHLOROETHENE
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Result Reporting Limit
05 05
05 05
05 05
1 1
05 05
05 05
100 100
05 05
10 10
5 5
10 10
1 1
05 05
1 1
10 10
05 05
10 10
05 05
5 5
1 1
05 05
1 1
05 05
05 05
05 05
05 05
05 05
05 05
MDL Result EPA Qualifier Qualifier
017 U
017 U
017 U
017 U
017 U
017 U
17 U
017 U
33 U
017 U
017 U
017 U
017 U
017 U
17 U
017 U
067 U
017 U
17 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
Data Package 10 VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- Fe Page 1 of 4
llMS Version 6317 A
8
GCMS Volatiles Method SW8260 _25B
Method Blank
Lab Name ALS Laboratory Group -- FC
Work Order Number 0911214
Client Name New Mexico Environment Department 08
ClientProject 10 644-111809(HWEI R-37 voes) PAR 002731703
Lab 10 VL091125-4MB Sample Matrix WATER
Moisture NIA Prep Batch VL091125-4
QCBatchIO VL091125-4-5
Sample Aliquot
Final Volume
10 ml
10 ml Oate Collected NIA Run 10 VL091125-4A Result Units UGL Oate Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Date Analyzed 25-Nov-09 Basis NIA
File Name 028043
CASNO Target Analyte OF Result Reporting Limit
MOL Result Qualifier
EPA Qualifier
78-87-5 12middotDICHLOROPROPANE 1 05 05 017 U
74-95-3 DIBROMOMETHANE 1 05 05 017 U
75-27-4 BROMODICHLOROMETHANE 1 05 05 017 U
10061-01-5 CISmiddot13middotDICHLOROPROPENE 1 05 05 017 U
108-10-1 4-METHYL-2-PENT ANONE 1 5 5 17 U
108-88-3 TOLUENE 1 05 05 017 U
10061-02-6 TRANS-13-DICHLOROPROPENE 1 05 05 017 U
79-00-5 112-TRICHLOROETHANE 1 05 05 017 U
591-78-6 2-HEXANONE 1 10 10 17 U
127-18-4 TETRACHLOROETHENE 1 05 05 017 U
142-28-9 13-DICHLOROPROPANI 1 05 05 017 U
124-48-1 DIBROMOCHLOROMETHANE 1 1 1 017 U
106-93-4 12-DIBROMOETHANE 1 1 1 017 U
108-90-7 CHLOROBENZENE 1 05 05 017 U
630-20-6 1112-TETRACHLOROETHANE 1 05 05 017 U
100-41-4 ETHYLBENZENE 1 05 05 017 U
136777-61-2 M+P-XYLENE 1 1 1 017 U
95-47-6 O-XYLENE 1 05 05 017 U
100-42-5 STYRENE 1 05 05 017 U
75-25-2 BROMOFORM 1 05 05 017 U
98-82-8 ~YLBENZENE 1 05 05 017 U
96-18-4 123-TRICHLOROPROPANE 1 2 2 017 U
79-34-5 1122middot TETRACHLOROETHANE 1 05 05 017 U
108-86-1 BROMOBENZENE 1 05 05 017 U
103-65-1 N-PROPYLBENZENE 1 05 05 017 U
95-49-8 2-CHLOROTOLUENE 1 05 05 017 U
108-67-8 135-TRIMETHYLBENZENE 1 05 05 017 U
106-43-4 4-CHLOROTOLUENE 1 05 05 017 U
Data Package 10 VL0911214-1
Date Printed Wednesday December n 2009 AlS Laboratory Group -- FC Page 2 of 4
lMS VeCSiOIY 6317A
9
GCMS Volatiles Method SW8260 _258
Method Blank
Lab Name ALS Laboratory Group - FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-111B09(HWB R-37 VOCs) PAR 002731703
Lab 10 VL091125-4MB Sample Matrix WATER
Moisture NIA
Prep Batch VL091125-4
QCBatchlD VL091125-4-5
Sample Aliquot
Final Volume
10 ml
10 ml
Date Collected NIA Run ID VL091125-4A Result Units UGL
Date Extracted 25-Nov-09 Cleanup NONE Clean DF 1
Date Analyzed 25-Nov-09 Basis NA
File Name 028043
CASNO Target Analyte OF Result Reporting Limit
MOL Result Qualifier
EPA Qualifier
98-06-6 TERT-BUTYLBENZENE 1 05 05 017 U
95-63-6 124-TRIMETHYLBENZENE 1 05 05 017 U
135-98-8 SEC-BUTYLBENZENE 1 05 05 017 U
541-73-1 13-DlCHLOROBENZENE 1 05 05 017 U
99-87-6 P-ISOPROPYLTOLUENE 1 05 05 017 U
106-46-7 1 A-DICHLOROBENZENE 1 05 05 017 U
104-51-8 N-BUTYLBENZENE 1 05 05 017 U
95-50-1 12-DICHLOROBENZENE 1 05 05 017 U
96-12-B 12-DIBROMO-3-CHLOROPROPANE 1 2 2 067 U
120-82-1 124-TRiCHLOROBENZENE 1 05 05 017 U
87-68-3 HEXACHLOROBUTADIENE 1 05 05 017 U
91-20-3 NAPHTHALENE 1 05 05 017 U
87-61-6 123-TRICHLOROBENZENE 1 05 05 017 U
75-05-B ACETONITRILE 1 50 50 83 U
107-05-1 ALLYL CHLORIDE 1 50 50 017 U
110-57-6 TRANS-14-DICHLORO-2-BUTENE 1 5 5 17 U
64-17-5 ETHANOL 1 200 200 78 U
97-63-2 ETHYL METHACRYLATE 1 5 5 017 U
78-83-1 ISOBUTYL ALCOHOL 1 100 100 17 U
126-98-7 METHACRYLONITRILE 1 35 35 17 U
80-62-6 METHYL METHACRYLATE 1 5 5 17 U
107-12-0 PROPIONITRILE 1 25 25 33 U
126-99-8 CHLOROPRENE 1 5 5 017 U
75-65-0 TERT-BUTANOL 1 100 100 33 U
108-20-3 ISOPROPYL ETHER 1 2 2 033 U
637-92-3 ETHYL TERT-BUTYL ETHER 1 2 2 033 U
994-05-8 TERT-AMYL METHYL ETHER 1 2 2 033 U
67-72-1 HEXACHLOROETHANE 1 2 2 033 U
Data Package 10 VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -~ Fe Page 3 of 4
LlMS Version 6317 A
10
GCMS Volatiles Method SW8260 _258
Method Blank
Lab Name ALS Laboratory Group -- FC
Work Order Number 0911214
Client Name New Mexico Envirmment Department OB
ClientProject 10 644-111809(HWB R-37 VOCs) PAR 002731703
Lab 10 VL091125-4MB Sample Matrix WATER
Moisture NIA Prep Batch VL091125-4
QCBatchlO VL091125-4-5
Sample Aliquot
Final Volume
10 m
10m Date Collected NIA Run 10 VL091125-4A Result Units UGIL Date Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Date Analyzed 25-Nov-09 BasisNIA
File Name 028043
CASNO Target Analyte Result Reporting MOL Result EPAOF Limit Qualifier Qualifier
Surrogate Recovery
CASNO Surrogate Analyte Result Flag Spike Amount
Percent Recovery
Control Limits
460-00-4 4-BROMOFLUOROBENZENE 25 25 100 82 - 121
1868-53-7 DIBROMOFLUOROMETHANE 248 25 99 80 - 123
2037-26-5 TOLUENE-D8 26 25 104 85 - 116
Data Package 10 VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- FC Page 4 of4
LlMS Version 6317A
11
GCMS Volati les Method SW8260 _258
Sample Results
Lab Name ALS Laboratory Group -- FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-111809(HWB R-37 VOCs) PAR 002731703
Field 10 Rmiddot37 Ser 2middot111809
Lab 10 0911214middot1
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml
Moisture NA QCBatchlO VL091125-4-5 Final Volume 10mi Date Collected 18-Nov-09 Run 10 VL091125-4A Result Units UGL
Date Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Analysis ReqCode 104 Date Analyzed 25-Nov-09
Prep Method SW5030 Rev C Basis As Received
File Name 028044
CASNO Target Analyte Dilution Factor
75-71-8 DICHLORODIFLUOROMETHANE 1
74middot87-3 CHLOROMETHANE 1
75-01-4 VINYL CHLORIDE 1
74-83-9 BROMOMETHANE 1
75-00-3 CHLOROETHANE 1
75-69-4 TRICHLOROFLUOROMETHANE 1
107-02-8 ACROLEIN 1
75-35-4 11middotDICHLOROETHENE 1
67-64-1 ACETONE 1
74-88-4 IODOMETHANE 1
75-15-0 CARBON DISULFIDE 1
75-09-2 METHYLENE CHLORIDE 1
156-60-5 TRANSmiddot12middotDICHLOROETHENE 1
1634-04-4 METHYL TERTIARY BUTYL ETHER 1
107-13-1 ACRYLONITRILE 1
75-34-3 1-DICHLOROETHANE 1
i 108-05-4 VINYL ACETATE 1
156-59-2 CIS-12middotDICHLOROETHENE 1
78-93-3 2-BUTANONE 1
74-97-5 BROMOCHLOROMETHANE 67-66-3 CHLOROFORM 1
71-55-6 11-TRICHLOROETHANE 594-20-7 22-DICHLOROPROPANE 56-23-5 CARBON TETRACHLORIDE 563-58-6 -DICHLOROPROPENE 107-06-2 2-DICHLOROETHANE
Result Reporting Limit
05 05
05 05
05 05
1 1
05 05
05 05
100 100
05 05
10 10
5 5
10 10
1 1
05 05
1 1
10 10
05 05
10 10
05 05
5 5
1 1
05 05
1 1
05 05
05 05
05 05
05 05
MOL Result EPA Qualifier Qualifier
017 U
017 U
017 U
017 U
017 U
017 U
17 U
017 U
33 U
017 U
017 U
017 U
017 U
017 U
17 U
017 U
067 U
017 U
17 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
Data Package ID VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- Fe Page 1 of 8
UMS Version 6317A
12
GCMS Volatiles Method SW8260_25B
Sample Results
Lab Name ALS Laboratory Group - FC
Work Order Number 0911214
Client Name New Mexico nvironment Department OB
ClientProject 10 644-111809(HWB R-37 VOCs) PAR 002731703
Field 10 R-37 Scr 2-111809
Lab 10 0911214-1
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10ml
Moisture NA QCBatchlD VL091125-4-5 Final Volume 10ml
Date Collected l8-Nov-09 Run 10 VL091125-4A Result Units UGL
Date Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Analysis ReqCode 104 Date Analyzed 25-Nov-09 Basis As Received
Prep Method SW5030 Rev C File NameD28044
CASNO Target Analyte Dilution Factor
Result Reporting Limit
MDL Result Qualifier
EPA Qualifier
I
71-43-2 BENZENE 1 05 05 017 U
79-01-6 TRICHLOROETHENE 1 05 05 017 U
78-87-5
74middot95-3
75-27-4
10061-01-5
108middot10middot1
108middot88-3
10061-02middot6
79-00-5
591-78-6
12-DICHLOROPROPANE
DIBROMOMETHANE
BROMODCHLOROMETHANE
CIS-13-DICHLOROPROPEI~E
4-METHYL-2-PENTANONE
TOLUENE
TRANS-13-DICHLOROPROPENE
112-TRICHLOROETHANE
2-HEXANONE
1
1
1
1
1
1
1
1
1
05
05
05
05
5
031
05
05
10
05
05
05
05
5
05
05
05
10
017
017
017
017
17
017
017
017
17
U
U
U
U
U
J
U
U
U
127-18-4
142-28-9
124-48-1
106-93-4
108-90-7
630-20-6
100-41-4
136777-61-2
95-47-6
100-42middot5
75-25-2
98-82middot8
96-18-4
79-34-5
108-86-1
TETRACHLOROETHENE
13-DICHLOROPROPANE
DIBROMOCHLOROMETHANE
12-DIBROMOETHANE
CHLOROBENZENE
11 12-TETRACHLOROETHANE
ETHYLBENZENE
M+PmiddotXYLENE
OmiddotXYLENE
STYRENE
BROMOFORM
ISOPRO PYLBENZENE
123middotTRICHLOROPROPANE
1122-TETRACHLOROETHANE
BROMOBENZENE
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
05
05
1
1
05
05
05
1
05
05
05
05
2
05
05
05
05
1
1
05
05
05
1
05
05
05
05
2
05
05
017
017
017
017
017
017
017
017
017
017
017
017
017
017
017
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
i
Data Package 10 VL0911214-1
Date Printed Wednesday December 022009 AlS laboratory Group bullbull Fe Page 2 of 8
UMS Version 6317A
13
GCMS Volatiles Method SW8260_258
Sample Results
Lab Name ALS Laboratory Group bullbull FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject ID 644-111809(HWB R-37 VOCs) PAR 002731703
Field 10 R-37 Sor 2-111809
Lab ID 0911214middot1
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml
Moisture NA QCBatchlD VL091125-4-5 Final Volume 10 ml
Date Collected 18-Nov-09 Run ID VL091125-4A Result Units UGL
Date Extracted 25-Nov-09 Cleanup NONE Clean DF 1
Analysis ReqCode 104 Date Analyzed 25-Nov-09 Basis As Received
Prep Method SW5030 Rev C File Name 028044
CASNO Target Analyte Dilution Factor
103-65-1 NmiddotPROPYLBENZENE 1
95-49-8 2-CHLOROTOLUENE 1
108-67-8 135-TRIMETHYLBENZENE 1
106-43-4 4-CHLOROTOLUENE 1
98-06-6 TER I-BUTYLBENZENE 1
95-63-6 124-TRIMETHYLBENZENE 1
135-98-8 SEC-BUTYLBENZENE 1
541-73-1 13-OICHLOROBENZENE 1
99-87-6 P-ISOPROPYLTOLUENE 1
106-46-7 lA-DICHLOROBENZENE 1
104-51-8 N-BUTYLBENZENE 1
95-50-1 12-DICHLOROBENZENE 1
96-12-8 l2-DIBROMOmiddot3-CHLOROPROPANE 1
120-82-1 12A-TRICHLOROBENZENE 1
187-68-3 HEXACHLOROBUTADIENE 1
91-20-3 NAPHTHALENE 1
87-61middot6 123-TRICHLOROBENZENE 1
75-05-8 ACETONITRILE 1
107middot05middot1 ALLYL CHLORIDE 1
110-57-6 TRANS-14-DICHLORO-2-BUTENE 1
164-17-5 ETHANOL 1
97-63-2 ETHYL METHACRYLATE 1
78-83-1 ISOBUTYL ALCOHOL 1
126-98-7 METHACRYLONITRILE 1
80-62-6 METHYL METHACRYLATE 1
107-12-0 PROPIONITRILE 1
Result Reporting Limit
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
2 2
05 05
05 05
05 05
05 05
50 50
50 50
5 5
200 200
5 5
100 100
35 35
5 5
25 25
MDL Result EPA Qualifier Qualifier
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
067 U
017 U
017 U
017 U
017 U
83 U
017 U
U u 78 U
017 U
17 U
17 U
17 U
33 U
Data Package 10 VL0911214-1
Date Printed Wednesday December 022009 ALS Laboratory Group MM Fe Page 3 of 8
LlMS VerSion 6317A
14
GCMS Volati las Method SW8260_258
Sample Results
Lab Name ALS Laboratory Group - FC
Work Order Number 0911214
Client Name New Mexico Environment Department 08
ClientProject 10 644-111B09(HWB R-37 VOGs) PAR 002731703
Field 10 R-37 Ser 2-111809 Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10ml
Lab 10 0911214-1 Moisture NA
Date Collected 1B-Nov-09 QCBatchlO VL091125-4-5
Run 10 VL091125-4A
Final Volume 10ml
Result Units UGIL Date Extracted 25-Nov-09 Cleanup NONE Clean OF
Analysis ReqCode 104 Date Analyzed 25-Nov-09
Prep Method SW5030 Rev G Basis As Received
File Name 028044
CASNO Target Analyte Dilution Factor
Result Reporting Limit
MDL Result Qualifier
EPA Qualifier
126-99-8 CHLOROPRENE 1 5 5 017 U
75-65-0 TERT-BUTANOL 1 100 100 33 U
108-20-3 ISOPROPYL ETHER 1 2 2 033 U
637-92-3 ETHYL TERT-BUTYL ETHER 1 2 2 033 U
994-05-8 TERT-AMYL METHYL ETHER 1 2 2 033 U
67-72-1 HEXACHLOROETHANE 1 2 2 033 U
Surrogate Recovery
CASNO Surrogate Analyte Result Flag Spike Amount
Percent Recovery
Control Limits
460-00-4 4-BROMOFLUOHOBENZENE 246 25 98 82 - 121
1868-53-7 DIBROMOFLUOHOMETHANE 248 25 99 BO - 123
2037-26-5 TOLUENE-DB 258 25 103 85middot116
Data Package 10 VL0911214-1
Date Printed Wednesday December 022009 ALS Laboratory Group bullbull FC Page 4 of 8
LIMS Version 0317 A
15
GCMS Volati les Method SW8260_25B
Sample Results
Lab Name ALS Laboratory Group -- FC
Worlt Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-111809(HWB Rmiddot37 VOCs) PAR 002731703
Field 10 Rmiddot37 Scr jmiddot111809
Lab 10 0911214-2
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml Moisture NfA QCBatchID VL091125-4middot5 Final Volume 10 ml
Date Collected 18middotNov-09 Run 10 VL091125-4A Result Units UGfL Date Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Analysis ReqCode 104 Date Analyzed 25middotNov-09 Basis As Received Prep Method SW5030 Rev C File Name 028045
CASNO Target Analyte Dilution Factor
Result Reporting Limit
MOL Result Qualifier
EPA Qualifier
75-71-8 DICHLORODIFLUOROMETHANE 1 05 05 017 U
74-87-3 CHLOROMETHANE 1 05 05 017 U
75-01middot4 VINYL CHLORIDE 1 05 05 017 U
74-83-9 BROMOMETHANE 1 1 1 017 U
75middot00middot3 CHLOROETHANE j 05 05 017 U
75-69-4 TRICHLOROFLUOROMETHANE 1 05 05 017 U
107-02-8 ACROLEIN 1 100 100 17 U
i 75-35-4 11-DICHLOROETHENE 1 05 05 017 U
67-64middot1 ACETONE 1 10 10 33 U
74-8S-4 IODOMETHANE 1 5 5 017 U
75-15-0 CARBON DISULFIDE 1 10 10 017 U
75-09-2 METHYLENE CHLORIDE 1 1 1 017 U
156-60-5 TRANS-12-DICHLOROETHENE 1 05 05 017 U
1634-04-4 METHYL TERTIARY BUTYL ETHER 1 1 1 017 U
107-13-1 ACRYLONITRILE 1 10 10 17 U
75-34middot3 11-DICHLOROETHANE 05 05 017 U
i 108-05-4 VINYL ACETATE 1 10 10 067 U
115659-2 CISmiddot 2middotDICHLOROETHENE 1 05 05 017 U
178-933 2middotBUTANONE 1 5 5 17 U
74-97middot5 BROMOCHLOROMET HANE 1 1 1 017 U
67-66-3 CHLOROFORM 1 05 05 017 U
71-55middot6 111middotTRICHLOROETHANE 1 1 1 017 U
594-20-7 22middotDICHLOROPROPANE 1 05 05 017 U
56-23-5 CARBON TETRACHLORIDE 1 05 05 017 U
563-58-6 11middotDICHLOROPROPENE 1 05 05 017 U
107-06-2 12middotDICHL OROETHANE 1 05 05 017 U
Data Package ID VL0911214-1
Date Printed Wednesday December 022009 ALS Laboratory Group -- Fe Page 5 of 8
16
GCMS Volatiles Method SW8260_25B
Sample Results
Lab Name ALS Laboratory Group -- FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-111809(HW3 R-37 VOCs) PAR 002731703
Field 10 R-37 Scr 1-11 1809
Lab 10 0911214-2
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml
Moisture NIA QCBatchlO VL091125-4-5 Final Volume 10 ml
Date Collected 18-Nov-09 Run 10 VL091125-4A Result Units UGL
[late Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Analysis ReqCode 104 Date Analyzed 25-Nov-09
Prep Method SW5030 Rev C Basis As Received
File Name 028045
CASNO Target Analyte Dilution Factor
71-43-2 BENZENE 1
79-01-6 TRICHLOROETHENE 1
78-87-5 12-DICHLOROPROPANE 1
74-95-3 DIBROMOMETHANE 1
75-27-4 BROMODICHLOROMETHANE 1
10061-01-5 CIS-13-DICHLOROPROPENE 1
108-10-1 4-METHYL-2-PtNTANON 1
108-88-3 TOLUENE 1
10061-02-6 TRANS-13-DICHLOROPROPENE 1
79-00-5 112-TRICHLOROETHANE 1
591-78-6 2-HEXANONE 1
127-18-4 TETRACHLOROETHENE 1
142-28-9 13-DICHLOROPROPANt 1
124-48-1 DI3ROMOCHLOROMETHANE 1
106-93-4 12-DIBROMOETHANE 1
108-90-7 CHLOROBENZENE 1
OETHANE 1
- 1
LENE 1
ENE 1
ENE 1
OFORM 1
OPYlBENZENE 1
96-18-4 123-TRICHLOROPROPANE 1
79-34-5 1122-TETRACHLOROETHANE 1
108-86-1 BROMOBENZENE 1
Result Reporting Limit
05 05
05 05
05 05
05 05
05 05
05 05
5 5
025 05
05 05
05 05
10 10
05 05
05 05
1 1
1 1
05 05
05 05
05 05
1 1
05 05
05 05
05 05
05 05
2 2
05 05
05 05
MDL Result EPA Qualifier Qualifier
017 U
017 U
017 U
017 U
017 U
017 U
17 U
017 J
017 U
017 U
17 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
Data Package 10 VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- Fe Page 6 of 8
317A
17
GCMS Volatiles Method SW8260 _258
Sample Results
Lab Name ALS Laboratory Group -- FC
Work Order Number 0911214
Client Name New Mexico Environment Department 08
ClientProject 10 644-11S09(HWB R-37 VOCs) PAR 002731703
Field 10 Rmiddot37 Scr 1-111809
Lab 10 0911214-2
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml Moisture NA QCBatchlD VL091125-4-5 Final Volume 10 ml
Date Collected 18-Nov-09 Run 10 VL091125-4A Result Units UGL Date Extracted 25-Nol-09 Cleanup NONE Clean OF
Analysis ReqCode 104 Date Analyzed 25-Nov-09 Basis As Received Prep Method SW5030 Rev C File Name D28045
CASNO Target Analyte Dilution Factor
103-65-1 N-PROPYLBENZENE 1
95-49-8 2-CHLOROTOLUENE 1
108-67-8 135-TRIMETHYLBENZENE 1
106-43-4 4-CHLOROTOLUENE 1
98-06-6 TERT-BUTYLBENZENE 1
95-63-6 124-TRIMETHYLBENZENE 1
135-98-8 SEC-BUTYLBENZENE 1
i 541-73-1 13middotDICHLOROBENZENE 1
99-87-6 PmiddotISOPROPYL TOLUENE 1
106-46-7 I 14-DICHLOROBENZENE 1
104-51-8 I N-BUTYLBENZENE 1
95-50-1 l2-DICHLOROBENZENE 1
96-12-8 I 12-DIBROMO-3-CHLOROPROPANE 1
120-82-1 124-TRICHLOROBENZENE 1
87-68-3 HEXACHLOROBUT ADIENE 1
91-20-3 NAPHTHALENE 1
87-61-6 123-TRICHLOROBENZENE 1
75-05-S ACETONITRILE 1
107-05-1 ALLYL CH LORIDE 1
110-57-6 TRAN S-14-DICHLORO-2-BUTENE 1
64-17-5 ETHANOL 1
97-63-2 ETHYL METHACRYLATE 1
78-83-1 ISOBUTYL ALCOHOL 1
126-98-7 METHACRYLONITRILE 1
80-62-6 METHYL METHACRYLATE 1
107-12-0 I PROPIONITRILE 1
Result Reporting Limit
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
2 2
05 05
05 05
05 05
05 05
50 50
50 50 I 5 5
200 200
5 5
100 100
35 35
5 5
25 25
MDL
017
017
017
017
017
017
017
017
017
017
017
017
067
017
017
017
017
83
017
17
78
017
17
17
17
33
Result EPA Qualifier Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
Data Package 10 VL0911214-1
Date Printed Wednesday December 022009 ALS Laboratory Group -- Fe Page 7 of 8
LlMS Version 6317A
18
GCMS Volatiles Method SW8260_258
Sample Results
Lab Name ALS Laboratory Group bullbull FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644middot111B09(HWB R-37 VOCs) PAR 002731703
Sample Matrix WATER Prep Batch VL091125--4 Sample Aliquot 10 mlRmiddot37 Ser 1-111809 Moisture NA QCBatchlO VL091125--4-5 Final Volume 10 m
0911214-2 Date Collected 18-Nov-09 Run 10 VL091125--4A Result Units UGL Date Extracted 25-Nov-09 Cleanup NONE Clean OF 1 Date Analyzed 25-Nov-09 Basis As Received
10
Analysis ReqCode 104 Prep Method SW5030 Rev C File Name 028045
I
CASNO Target Analyte Dilution Factor
Result Reporting Limit
MDL Result Qualifier
EPA Qualifier
126-99-8 CHLOROPRENE 1 5 5 017 U
75-65-0 TERT-BUTANOL 1 100 100 33 U
108-20-3 ISOPROPYL ETHER 1 2 2 033 U
637-92-3 ETHYL TERT-BUTYL ETHER 1 2 2 033 U
994-05--8 TERT-AMYL MTHYL ETHER 1 2 2 033 U
67-72-1 HEXACHLOROETHANE 1 2 2 033 U
Surrogate Recovery
CASNO Surrogate Analyte Result Flag Spike Amount
Percent Control Recovery Limits
460-00-4 4middotBROMOFLUOROBENZENE 247 25 99 1
1868-53-7 DIBROMOFLUOROMETHANE 248 25 99 80 123
2037-26-5 TOLUENEmiddotDB 255 25 102 85 - 116
Data Package 10 VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- FC Page B of 8
LlMS Version 6317A
19
GCMS Volatiles Method SW8260_258
Laboratory Control Sample and Laboratory Control Sample Duplicate
Lab Name ALS Laboratory Group - FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-111809(HWB R-37 VOCs) PAR 002731703
Lab 10 VL091125-4LCS Sample Matrix WATER
Moisture NA Prep Batch VL091125-4
QCBatchlD VL091125-4-5
Sample Aliquot
Final Volume
10ml
10ml Date Collected NA Run 10 VL091125-4A Result Units UGIL Date Extracted 111252009 Cleanup NONE Clean OF 1 Date Analyzed 11252009 Basis NA
Prep Method SW5030C File Name 028040
CASNO
74-87-3
75-01-4
74-83-9
75-69-4
75-35-4
75-15-0
156-60-5
75-34-3
108-05-4
156-59-2
78-93-3
67 -66-3
71-55-6
i 56-23-5
107-06-2
71-43-2
79-01-6
78-87-5
75-27-4
108-88-3
79-00-5
591-78-6
127-18-4
106-93-4
108-90-7
63Q20-6
Target Analyte Spike Added
CHLOROMETHANE 10
VINYL CHLORIDE 10
BROMOMETHANE 10
TRICHLOROFLUOROMETHANE 10
11-DICHLOROETHENE 10
CARBON DISULFIDE 10
TRANS-12-DICHLOROETHENE 10
11-DICHLOROETHANE 10
VINYL ACETATE 10
CIS-12-DICHLOROETHENE 10
2middotBUTANONE 40
CHLOROFORM 10
111-TRICHL ORO ETHANE 10
CARBON TETRACHLORIDE 10
12-DICHLOROETHANE 10
BENZENE 10
TRICHLOROETHENE 10
12-DICHLOROPROPANE 10
BROMODICHLOROMETHANE 10
TOLUENE 10
112-TRICHLOROETHANE 10
2-HEXANONE 40
TETRACHLOROETHENE 10
12-DIBROMOETHANE 10
CHLOROBENZENE 10
1112-TETRACHLOROETHANE 10
LCS Reporting Result Result Limit Qualifier
932 05
863 05
943 1
908 05
96 05
95 10 J
996 05
992 05
10 10
102 05
412 5
993 05
974 1
943 05
106 05
983 05
962 05
10 05
988 05
974 05
989 05
409 10
956 05
991 1
984 05
101 05
LCS Control Rec Limits
93 49 -129
86 46 134
94 32-121
91 67 -152
96 61 -135
95 61 -140
100 70 -122
99 76 -119
100 62 182
102 75 126
103 61 -137
99 79 120
97 76 - 114
94 58middot135
106 75middot132
98 70 shy 125
96 74 121
100 81 -119
99 79 - 123
97 76 - 120
99 81 -126
102 45 168
96 56 -128
99 79 -123
98 75 -120
101 82 - 123
Data Package 10 VL0911214middot1
-Date Printed Wednesday December 02 2009 ALS Laboratory Group -- Fe Page 1 of 4
LiMS Version 6317A
20
GCMS Volatiles Method SW8260_25B
Laboratory Control Sample and Laboratory Control Sample Duplicate
Lab Name ALS Laboratory Group - FC
Work Order Number 0911214
Client Name New Mexico Envircnment Department OB
ClientProject 10 644-111809(HWB R-37 VOes) PAR 002731703
Lab 10 VL091125-4LCS Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml
Moisture NIA QCBatchlO VL091125-4-5 Final Volume 10 mi
Date Collected NA Run 10 VL091125-4A Result Units UGL Date Extracted 11252009 Cleanup NONE Clean OF 1 Date Analyzed 111252009 Basis NA
Prep Method SW5030e File Name 028040
CASNO Target Analyte Spike Added
LCS Result
Reporting Limit
Result Qualifier
LCS Rec
Control Limits
100-41-4 ETHYLBENZENE 10 981 05 98 79 -114
136777-61-2 M+P-XYLENE 20 197 1 98 81-115
95-47-6 O-XYLENE 10 101 05 101 81 -115
95-49-8 2-CHLOROTOLUENE 10 97 05 97 80 -128
541-73-1 13-DICHLOROBENZiNt 10 977 05 98 81-116
106-46-7 14-DICHLOROBENZENE 10 979 05 98 81 -119
95-50-1 12-DICHLOROBENZENE 10 987 05 99 79 - 116
91-20-3 NAPHTHALENE 10 993 05 99 69 -126
87-61-6 123-TRICHLOROBENZENE 10 999 05 100 60 -137
Data Package ID VL0911214-1
Date Printed Wecnesday December 02 2009 ALS Laboratory Group -- Fe Page 2 of 4
21
GCMS Volatiles Method SW8260_25B
Laboratory Control Sample and Laboratory Control Sample Duplicate
Lab Name ALS Laboratory Group bullbull FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-11 1809(HWB R-37 VOCs) PAR 002731703
Lab 10 VL091125middot4LCSD Sample Matrix WATER
Moisture NIA Prep Batch VL091125-4
QCBatchlD VL091125-4-5
Sample Aliquot
Final Volume
10 ml
10ml Date Collected NIA Run ID VL091125-4A Result Units UGIL Date Extracted 112512009 Cleanup NONE Clean DF 1 Date Analyzed 1112512009 Basis NIA
Prep Method SW5030C File Name 028041
CASNO Target Analyte Spike Added
LCSD Result
Reporting Limit
Result Qualifier
LCSD Rec
RPD Limit
RPD
74-87-3 CHLOROMETHANE 10 897 05 90 30 4
75-01-4 VINYL CHLORIDE 10 831 05 83 25 4
74-83-9 BROMO METHANE 10 945 1 94 25 0
75-69-4 TRICHLOROFLUOROMETHANE 10 873 05 87 22 4
75-35-4 11-DICHLOROETHENE 10 909 05 91 18 5
75-15-0 CARBON DISULFIDE 10 941 10 J 94 20 1
156-60middot5 TRANS-l2middotDICHLOROETHENE 10 961 05 96 25 4
75middot34middot3 11-DICHLOROETHANE 10 977 05 98 25 2
108-05-4 VINYL ACETATE 10 993 10 J 99 20 1
156middot59-2 CIS-12-DlCHLOROETHENE 10 995 05 99 25 3
i 78-93-3 2-BUTANONE 40 419 5 105 30 2
67-66-3 CHLOROFORM 10 985 05 99 25 1
71-55-6 lll-TRICHLOROETHANE 10 942 1 94 25 3
56-23-5 CARBON TETRACHLORIDE 10 922 05 92 25 2
107middot06-2 12middotDICHLOROETHANE 10 106 05 106 25 0
71-43middot2 BENZENE 10 971 05 97 10 1
79middot01middot6 TRICHLOROETHENE 10 939 05 94 10 2
78middot87middot5 l2middotDICHLOROPROPANE 10 101 05 101 25 1
i 75middot27-4 BROMODICHLOROMETHANE 10 992 05 99 25 0
1108-88-3 TOLUENE 10 962 05 96 9 1
I 79005 112middotTRICHLOROETHANE 10 986 05 99 25 0
591middot78middot6 2-HEXANONE 40 418 10 104 20 2
127middot18-4 TETRACHLOROETHENE 10 918 05 92 25 4
106-93-4 12middotDIBROMOETHANE 10 999 1 100 15 1
108middot90-7 CHLOROBENZENE 10 997 05 100 11 1
630-20middot6 1112-TETRACHLOROETHANE 10 101 05 101 15 0
100-41-4 ETHYLBENZENE 10 968 05 97 25 1
Data Package ID VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- FC Page 3 of 4
lIMS Version 6317 A
22
GCMS Volatiles Method SW8260_25B
Laboratory Control Sample and Laboratory Control Sample Duplicate
Lab Name ALS Laboratory 13roup -- FC
Work Order Number 0911214
Client Name New Mexico Environment Department OS
ClientProject 10 644-11 1809(HWB R-37 VOCs) PAR 002731703
Lab 10 VL091125-4LCSD Sample Matrix WATER
Moisture NA Prep Batch VL091125-4
QCBatchlO VL091125-4-5
Sample Aliquot
Final Volume
10 ml
10ml Date Collected NA Run 10 VL091125-4A Result Units UGL Date Extracted 11252009 Cleanup NONE Clean OF Date Analyzed 11252009 Basis NIA
Prep Method SW5030C File Name 028041
CASNO Target Analyte Spike Added
LCSD Result
Reporting Limit
Result Qualifier
LCSD Rec
RPD Limit
RPD
136777-61-2 M+P-XYLENE 20 193 1 97 25 2
95-47-6 O-XYLENE 10 983 05 98 25 2
95-49-8 2middotCHLOROTOLUENE 10 9A9 05 95 15 2
541-73-1 13middotDICHLOROBENZENE 10 997 05 100 25 2
106-46-7 14-DICHLOROBeNZENE 10 974 05 97 25 1
95-50middot1 12middotDICHLOROBENZeNE 10 101 05 101 25 2
91middot20-3 NAPHTHALENe 10 105 05 105 24 6
87-61-6 123-TRICHLOROBENZENE 10 102 05 102 33 3
Surrogate Recovery LCSLCSD
CASNO Target Analyte Spike Added
LCS Rec
LCS Flag
LCSD Rec
LCSD Flag
Control Limits
460middot00-4 4-BROMOFLUOROBeNZENE 25 100 100 82 - 121
1868-53middot7 DIBROMOFLUOROMeTHANE 25 101 100 80middot 123
2037middot26-5 TOLUENEmiddotD8 25 102 100 85middot 116
Data Package 10 VL0911214-
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- Fe Page 4 of 4
UMS Verslmt 6317A
23
GCMS Volatiles Method SW8260 _25B
Method Blank
Lab Name ALS Laboratory Group -- FC
Work Order Number 0911214
Client Name New Mexico Environment Department 08
ClientProject 10 644-111809(HWEI R-37 voes) PAR 002731703
Lab 10 VL091125-4MB Sample Matrix WATER
Moisture NIA Prep Batch VL091125-4
QCBatchIO VL091125-4-5
Sample Aliquot
Final Volume
10 ml
10 ml Oate Collected NIA Run 10 VL091125-4A Result Units UGL Oate Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Date Analyzed 25-Nov-09 Basis NIA
File Name 028043
CASNO Target Analyte OF Result Reporting Limit
MOL Result Qualifier
EPA Qualifier
78-87-5 12middotDICHLOROPROPANE 1 05 05 017 U
74-95-3 DIBROMOMETHANE 1 05 05 017 U
75-27-4 BROMODICHLOROMETHANE 1 05 05 017 U
10061-01-5 CISmiddot13middotDICHLOROPROPENE 1 05 05 017 U
108-10-1 4-METHYL-2-PENT ANONE 1 5 5 17 U
108-88-3 TOLUENE 1 05 05 017 U
10061-02-6 TRANS-13-DICHLOROPROPENE 1 05 05 017 U
79-00-5 112-TRICHLOROETHANE 1 05 05 017 U
591-78-6 2-HEXANONE 1 10 10 17 U
127-18-4 TETRACHLOROETHENE 1 05 05 017 U
142-28-9 13-DICHLOROPROPANI 1 05 05 017 U
124-48-1 DIBROMOCHLOROMETHANE 1 1 1 017 U
106-93-4 12-DIBROMOETHANE 1 1 1 017 U
108-90-7 CHLOROBENZENE 1 05 05 017 U
630-20-6 1112-TETRACHLOROETHANE 1 05 05 017 U
100-41-4 ETHYLBENZENE 1 05 05 017 U
136777-61-2 M+P-XYLENE 1 1 1 017 U
95-47-6 O-XYLENE 1 05 05 017 U
100-42-5 STYRENE 1 05 05 017 U
75-25-2 BROMOFORM 1 05 05 017 U
98-82-8 ~YLBENZENE 1 05 05 017 U
96-18-4 123-TRICHLOROPROPANE 1 2 2 017 U
79-34-5 1122middot TETRACHLOROETHANE 1 05 05 017 U
108-86-1 BROMOBENZENE 1 05 05 017 U
103-65-1 N-PROPYLBENZENE 1 05 05 017 U
95-49-8 2-CHLOROTOLUENE 1 05 05 017 U
108-67-8 135-TRIMETHYLBENZENE 1 05 05 017 U
106-43-4 4-CHLOROTOLUENE 1 05 05 017 U
Data Package 10 VL0911214-1
Date Printed Wednesday December n 2009 AlS Laboratory Group -- FC Page 2 of 4
lMS VeCSiOIY 6317A
9
GCMS Volatiles Method SW8260 _258
Method Blank
Lab Name ALS Laboratory Group - FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-111B09(HWB R-37 VOCs) PAR 002731703
Lab 10 VL091125-4MB Sample Matrix WATER
Moisture NIA
Prep Batch VL091125-4
QCBatchlD VL091125-4-5
Sample Aliquot
Final Volume
10 ml
10 ml
Date Collected NIA Run ID VL091125-4A Result Units UGL
Date Extracted 25-Nov-09 Cleanup NONE Clean DF 1
Date Analyzed 25-Nov-09 Basis NA
File Name 028043
CASNO Target Analyte OF Result Reporting Limit
MOL Result Qualifier
EPA Qualifier
98-06-6 TERT-BUTYLBENZENE 1 05 05 017 U
95-63-6 124-TRIMETHYLBENZENE 1 05 05 017 U
135-98-8 SEC-BUTYLBENZENE 1 05 05 017 U
541-73-1 13-DlCHLOROBENZENE 1 05 05 017 U
99-87-6 P-ISOPROPYLTOLUENE 1 05 05 017 U
106-46-7 1 A-DICHLOROBENZENE 1 05 05 017 U
104-51-8 N-BUTYLBENZENE 1 05 05 017 U
95-50-1 12-DICHLOROBENZENE 1 05 05 017 U
96-12-B 12-DIBROMO-3-CHLOROPROPANE 1 2 2 067 U
120-82-1 124-TRiCHLOROBENZENE 1 05 05 017 U
87-68-3 HEXACHLOROBUTADIENE 1 05 05 017 U
91-20-3 NAPHTHALENE 1 05 05 017 U
87-61-6 123-TRICHLOROBENZENE 1 05 05 017 U
75-05-B ACETONITRILE 1 50 50 83 U
107-05-1 ALLYL CHLORIDE 1 50 50 017 U
110-57-6 TRANS-14-DICHLORO-2-BUTENE 1 5 5 17 U
64-17-5 ETHANOL 1 200 200 78 U
97-63-2 ETHYL METHACRYLATE 1 5 5 017 U
78-83-1 ISOBUTYL ALCOHOL 1 100 100 17 U
126-98-7 METHACRYLONITRILE 1 35 35 17 U
80-62-6 METHYL METHACRYLATE 1 5 5 17 U
107-12-0 PROPIONITRILE 1 25 25 33 U
126-99-8 CHLOROPRENE 1 5 5 017 U
75-65-0 TERT-BUTANOL 1 100 100 33 U
108-20-3 ISOPROPYL ETHER 1 2 2 033 U
637-92-3 ETHYL TERT-BUTYL ETHER 1 2 2 033 U
994-05-8 TERT-AMYL METHYL ETHER 1 2 2 033 U
67-72-1 HEXACHLOROETHANE 1 2 2 033 U
Data Package 10 VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -~ Fe Page 3 of 4
LlMS Version 6317 A
10
GCMS Volatiles Method SW8260 _258
Method Blank
Lab Name ALS Laboratory Group -- FC
Work Order Number 0911214
Client Name New Mexico Envirmment Department OB
ClientProject 10 644-111809(HWB R-37 VOCs) PAR 002731703
Lab 10 VL091125-4MB Sample Matrix WATER
Moisture NIA Prep Batch VL091125-4
QCBatchlO VL091125-4-5
Sample Aliquot
Final Volume
10 m
10m Date Collected NIA Run 10 VL091125-4A Result Units UGIL Date Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Date Analyzed 25-Nov-09 BasisNIA
File Name 028043
CASNO Target Analyte Result Reporting MOL Result EPAOF Limit Qualifier Qualifier
Surrogate Recovery
CASNO Surrogate Analyte Result Flag Spike Amount
Percent Recovery
Control Limits
460-00-4 4-BROMOFLUOROBENZENE 25 25 100 82 - 121
1868-53-7 DIBROMOFLUOROMETHANE 248 25 99 80 - 123
2037-26-5 TOLUENE-D8 26 25 104 85 - 116
Data Package 10 VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- FC Page 4 of4
LlMS Version 6317A
11
GCMS Volati les Method SW8260 _258
Sample Results
Lab Name ALS Laboratory Group -- FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-111809(HWB R-37 VOCs) PAR 002731703
Field 10 Rmiddot37 Ser 2middot111809
Lab 10 0911214middot1
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml
Moisture NA QCBatchlO VL091125-4-5 Final Volume 10mi Date Collected 18-Nov-09 Run 10 VL091125-4A Result Units UGL
Date Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Analysis ReqCode 104 Date Analyzed 25-Nov-09
Prep Method SW5030 Rev C Basis As Received
File Name 028044
CASNO Target Analyte Dilution Factor
75-71-8 DICHLORODIFLUOROMETHANE 1
74middot87-3 CHLOROMETHANE 1
75-01-4 VINYL CHLORIDE 1
74-83-9 BROMOMETHANE 1
75-00-3 CHLOROETHANE 1
75-69-4 TRICHLOROFLUOROMETHANE 1
107-02-8 ACROLEIN 1
75-35-4 11middotDICHLOROETHENE 1
67-64-1 ACETONE 1
74-88-4 IODOMETHANE 1
75-15-0 CARBON DISULFIDE 1
75-09-2 METHYLENE CHLORIDE 1
156-60-5 TRANSmiddot12middotDICHLOROETHENE 1
1634-04-4 METHYL TERTIARY BUTYL ETHER 1
107-13-1 ACRYLONITRILE 1
75-34-3 1-DICHLOROETHANE 1
i 108-05-4 VINYL ACETATE 1
156-59-2 CIS-12middotDICHLOROETHENE 1
78-93-3 2-BUTANONE 1
74-97-5 BROMOCHLOROMETHANE 67-66-3 CHLOROFORM 1
71-55-6 11-TRICHLOROETHANE 594-20-7 22-DICHLOROPROPANE 56-23-5 CARBON TETRACHLORIDE 563-58-6 -DICHLOROPROPENE 107-06-2 2-DICHLOROETHANE
Result Reporting Limit
05 05
05 05
05 05
1 1
05 05
05 05
100 100
05 05
10 10
5 5
10 10
1 1
05 05
1 1
10 10
05 05
10 10
05 05
5 5
1 1
05 05
1 1
05 05
05 05
05 05
05 05
MOL Result EPA Qualifier Qualifier
017 U
017 U
017 U
017 U
017 U
017 U
17 U
017 U
33 U
017 U
017 U
017 U
017 U
017 U
17 U
017 U
067 U
017 U
17 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
Data Package ID VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- Fe Page 1 of 8
UMS Version 6317A
12
GCMS Volatiles Method SW8260_25B
Sample Results
Lab Name ALS Laboratory Group - FC
Work Order Number 0911214
Client Name New Mexico nvironment Department OB
ClientProject 10 644-111809(HWB R-37 VOCs) PAR 002731703
Field 10 R-37 Scr 2-111809
Lab 10 0911214-1
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10ml
Moisture NA QCBatchlD VL091125-4-5 Final Volume 10ml
Date Collected l8-Nov-09 Run 10 VL091125-4A Result Units UGL
Date Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Analysis ReqCode 104 Date Analyzed 25-Nov-09 Basis As Received
Prep Method SW5030 Rev C File NameD28044
CASNO Target Analyte Dilution Factor
Result Reporting Limit
MDL Result Qualifier
EPA Qualifier
I
71-43-2 BENZENE 1 05 05 017 U
79-01-6 TRICHLOROETHENE 1 05 05 017 U
78-87-5
74middot95-3
75-27-4
10061-01-5
108middot10middot1
108middot88-3
10061-02middot6
79-00-5
591-78-6
12-DICHLOROPROPANE
DIBROMOMETHANE
BROMODCHLOROMETHANE
CIS-13-DICHLOROPROPEI~E
4-METHYL-2-PENTANONE
TOLUENE
TRANS-13-DICHLOROPROPENE
112-TRICHLOROETHANE
2-HEXANONE
1
1
1
1
1
1
1
1
1
05
05
05
05
5
031
05
05
10
05
05
05
05
5
05
05
05
10
017
017
017
017
17
017
017
017
17
U
U
U
U
U
J
U
U
U
127-18-4
142-28-9
124-48-1
106-93-4
108-90-7
630-20-6
100-41-4
136777-61-2
95-47-6
100-42middot5
75-25-2
98-82middot8
96-18-4
79-34-5
108-86-1
TETRACHLOROETHENE
13-DICHLOROPROPANE
DIBROMOCHLOROMETHANE
12-DIBROMOETHANE
CHLOROBENZENE
11 12-TETRACHLOROETHANE
ETHYLBENZENE
M+PmiddotXYLENE
OmiddotXYLENE
STYRENE
BROMOFORM
ISOPRO PYLBENZENE
123middotTRICHLOROPROPANE
1122-TETRACHLOROETHANE
BROMOBENZENE
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
05
05
1
1
05
05
05
1
05
05
05
05
2
05
05
05
05
1
1
05
05
05
1
05
05
05
05
2
05
05
017
017
017
017
017
017
017
017
017
017
017
017
017
017
017
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
i
Data Package 10 VL0911214-1
Date Printed Wednesday December 022009 AlS laboratory Group bullbull Fe Page 2 of 8
UMS Version 6317A
13
GCMS Volatiles Method SW8260_258
Sample Results
Lab Name ALS Laboratory Group bullbull FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject ID 644-111809(HWB R-37 VOCs) PAR 002731703
Field 10 R-37 Sor 2-111809
Lab ID 0911214middot1
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml
Moisture NA QCBatchlD VL091125-4-5 Final Volume 10 ml
Date Collected 18-Nov-09 Run ID VL091125-4A Result Units UGL
Date Extracted 25-Nov-09 Cleanup NONE Clean DF 1
Analysis ReqCode 104 Date Analyzed 25-Nov-09 Basis As Received
Prep Method SW5030 Rev C File Name 028044
CASNO Target Analyte Dilution Factor
103-65-1 NmiddotPROPYLBENZENE 1
95-49-8 2-CHLOROTOLUENE 1
108-67-8 135-TRIMETHYLBENZENE 1
106-43-4 4-CHLOROTOLUENE 1
98-06-6 TER I-BUTYLBENZENE 1
95-63-6 124-TRIMETHYLBENZENE 1
135-98-8 SEC-BUTYLBENZENE 1
541-73-1 13-OICHLOROBENZENE 1
99-87-6 P-ISOPROPYLTOLUENE 1
106-46-7 lA-DICHLOROBENZENE 1
104-51-8 N-BUTYLBENZENE 1
95-50-1 12-DICHLOROBENZENE 1
96-12-8 l2-DIBROMOmiddot3-CHLOROPROPANE 1
120-82-1 12A-TRICHLOROBENZENE 1
187-68-3 HEXACHLOROBUTADIENE 1
91-20-3 NAPHTHALENE 1
87-61middot6 123-TRICHLOROBENZENE 1
75-05-8 ACETONITRILE 1
107middot05middot1 ALLYL CHLORIDE 1
110-57-6 TRANS-14-DICHLORO-2-BUTENE 1
164-17-5 ETHANOL 1
97-63-2 ETHYL METHACRYLATE 1
78-83-1 ISOBUTYL ALCOHOL 1
126-98-7 METHACRYLONITRILE 1
80-62-6 METHYL METHACRYLATE 1
107-12-0 PROPIONITRILE 1
Result Reporting Limit
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
2 2
05 05
05 05
05 05
05 05
50 50
50 50
5 5
200 200
5 5
100 100
35 35
5 5
25 25
MDL Result EPA Qualifier Qualifier
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
067 U
017 U
017 U
017 U
017 U
83 U
017 U
U u 78 U
017 U
17 U
17 U
17 U
33 U
Data Package 10 VL0911214-1
Date Printed Wednesday December 022009 ALS Laboratory Group MM Fe Page 3 of 8
LlMS VerSion 6317A
14
GCMS Volati las Method SW8260_258
Sample Results
Lab Name ALS Laboratory Group - FC
Work Order Number 0911214
Client Name New Mexico Environment Department 08
ClientProject 10 644-111B09(HWB R-37 VOGs) PAR 002731703
Field 10 R-37 Ser 2-111809 Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10ml
Lab 10 0911214-1 Moisture NA
Date Collected 1B-Nov-09 QCBatchlO VL091125-4-5
Run 10 VL091125-4A
Final Volume 10ml
Result Units UGIL Date Extracted 25-Nov-09 Cleanup NONE Clean OF
Analysis ReqCode 104 Date Analyzed 25-Nov-09
Prep Method SW5030 Rev G Basis As Received
File Name 028044
CASNO Target Analyte Dilution Factor
Result Reporting Limit
MDL Result Qualifier
EPA Qualifier
126-99-8 CHLOROPRENE 1 5 5 017 U
75-65-0 TERT-BUTANOL 1 100 100 33 U
108-20-3 ISOPROPYL ETHER 1 2 2 033 U
637-92-3 ETHYL TERT-BUTYL ETHER 1 2 2 033 U
994-05-8 TERT-AMYL METHYL ETHER 1 2 2 033 U
67-72-1 HEXACHLOROETHANE 1 2 2 033 U
Surrogate Recovery
CASNO Surrogate Analyte Result Flag Spike Amount
Percent Recovery
Control Limits
460-00-4 4-BROMOFLUOHOBENZENE 246 25 98 82 - 121
1868-53-7 DIBROMOFLUOHOMETHANE 248 25 99 BO - 123
2037-26-5 TOLUENE-DB 258 25 103 85middot116
Data Package 10 VL0911214-1
Date Printed Wednesday December 022009 ALS Laboratory Group bullbull FC Page 4 of 8
LIMS Version 0317 A
15
GCMS Volati les Method SW8260_25B
Sample Results
Lab Name ALS Laboratory Group -- FC
Worlt Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-111809(HWB Rmiddot37 VOCs) PAR 002731703
Field 10 Rmiddot37 Scr jmiddot111809
Lab 10 0911214-2
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml Moisture NfA QCBatchID VL091125-4middot5 Final Volume 10 ml
Date Collected 18middotNov-09 Run 10 VL091125-4A Result Units UGfL Date Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Analysis ReqCode 104 Date Analyzed 25middotNov-09 Basis As Received Prep Method SW5030 Rev C File Name 028045
CASNO Target Analyte Dilution Factor
Result Reporting Limit
MOL Result Qualifier
EPA Qualifier
75-71-8 DICHLORODIFLUOROMETHANE 1 05 05 017 U
74-87-3 CHLOROMETHANE 1 05 05 017 U
75-01middot4 VINYL CHLORIDE 1 05 05 017 U
74-83-9 BROMOMETHANE 1 1 1 017 U
75middot00middot3 CHLOROETHANE j 05 05 017 U
75-69-4 TRICHLOROFLUOROMETHANE 1 05 05 017 U
107-02-8 ACROLEIN 1 100 100 17 U
i 75-35-4 11-DICHLOROETHENE 1 05 05 017 U
67-64middot1 ACETONE 1 10 10 33 U
74-8S-4 IODOMETHANE 1 5 5 017 U
75-15-0 CARBON DISULFIDE 1 10 10 017 U
75-09-2 METHYLENE CHLORIDE 1 1 1 017 U
156-60-5 TRANS-12-DICHLOROETHENE 1 05 05 017 U
1634-04-4 METHYL TERTIARY BUTYL ETHER 1 1 1 017 U
107-13-1 ACRYLONITRILE 1 10 10 17 U
75-34middot3 11-DICHLOROETHANE 05 05 017 U
i 108-05-4 VINYL ACETATE 1 10 10 067 U
115659-2 CISmiddot 2middotDICHLOROETHENE 1 05 05 017 U
178-933 2middotBUTANONE 1 5 5 17 U
74-97middot5 BROMOCHLOROMET HANE 1 1 1 017 U
67-66-3 CHLOROFORM 1 05 05 017 U
71-55middot6 111middotTRICHLOROETHANE 1 1 1 017 U
594-20-7 22middotDICHLOROPROPANE 1 05 05 017 U
56-23-5 CARBON TETRACHLORIDE 1 05 05 017 U
563-58-6 11middotDICHLOROPROPENE 1 05 05 017 U
107-06-2 12middotDICHL OROETHANE 1 05 05 017 U
Data Package ID VL0911214-1
Date Printed Wednesday December 022009 ALS Laboratory Group -- Fe Page 5 of 8
16
GCMS Volatiles Method SW8260_25B
Sample Results
Lab Name ALS Laboratory Group -- FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-111809(HW3 R-37 VOCs) PAR 002731703
Field 10 R-37 Scr 1-11 1809
Lab 10 0911214-2
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml
Moisture NIA QCBatchlO VL091125-4-5 Final Volume 10 ml
Date Collected 18-Nov-09 Run 10 VL091125-4A Result Units UGL
[late Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Analysis ReqCode 104 Date Analyzed 25-Nov-09
Prep Method SW5030 Rev C Basis As Received
File Name 028045
CASNO Target Analyte Dilution Factor
71-43-2 BENZENE 1
79-01-6 TRICHLOROETHENE 1
78-87-5 12-DICHLOROPROPANE 1
74-95-3 DIBROMOMETHANE 1
75-27-4 BROMODICHLOROMETHANE 1
10061-01-5 CIS-13-DICHLOROPROPENE 1
108-10-1 4-METHYL-2-PtNTANON 1
108-88-3 TOLUENE 1
10061-02-6 TRANS-13-DICHLOROPROPENE 1
79-00-5 112-TRICHLOROETHANE 1
591-78-6 2-HEXANONE 1
127-18-4 TETRACHLOROETHENE 1
142-28-9 13-DICHLOROPROPANt 1
124-48-1 DI3ROMOCHLOROMETHANE 1
106-93-4 12-DIBROMOETHANE 1
108-90-7 CHLOROBENZENE 1
OETHANE 1
- 1
LENE 1
ENE 1
ENE 1
OFORM 1
OPYlBENZENE 1
96-18-4 123-TRICHLOROPROPANE 1
79-34-5 1122-TETRACHLOROETHANE 1
108-86-1 BROMOBENZENE 1
Result Reporting Limit
05 05
05 05
05 05
05 05
05 05
05 05
5 5
025 05
05 05
05 05
10 10
05 05
05 05
1 1
1 1
05 05
05 05
05 05
1 1
05 05
05 05
05 05
05 05
2 2
05 05
05 05
MDL Result EPA Qualifier Qualifier
017 U
017 U
017 U
017 U
017 U
017 U
17 U
017 J
017 U
017 U
17 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
Data Package 10 VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- Fe Page 6 of 8
317A
17
GCMS Volatiles Method SW8260 _258
Sample Results
Lab Name ALS Laboratory Group -- FC
Work Order Number 0911214
Client Name New Mexico Environment Department 08
ClientProject 10 644-11S09(HWB R-37 VOCs) PAR 002731703
Field 10 Rmiddot37 Scr 1-111809
Lab 10 0911214-2
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml Moisture NA QCBatchlD VL091125-4-5 Final Volume 10 ml
Date Collected 18-Nov-09 Run 10 VL091125-4A Result Units UGL Date Extracted 25-Nol-09 Cleanup NONE Clean OF
Analysis ReqCode 104 Date Analyzed 25-Nov-09 Basis As Received Prep Method SW5030 Rev C File Name D28045
CASNO Target Analyte Dilution Factor
103-65-1 N-PROPYLBENZENE 1
95-49-8 2-CHLOROTOLUENE 1
108-67-8 135-TRIMETHYLBENZENE 1
106-43-4 4-CHLOROTOLUENE 1
98-06-6 TERT-BUTYLBENZENE 1
95-63-6 124-TRIMETHYLBENZENE 1
135-98-8 SEC-BUTYLBENZENE 1
i 541-73-1 13middotDICHLOROBENZENE 1
99-87-6 PmiddotISOPROPYL TOLUENE 1
106-46-7 I 14-DICHLOROBENZENE 1
104-51-8 I N-BUTYLBENZENE 1
95-50-1 l2-DICHLOROBENZENE 1
96-12-8 I 12-DIBROMO-3-CHLOROPROPANE 1
120-82-1 124-TRICHLOROBENZENE 1
87-68-3 HEXACHLOROBUT ADIENE 1
91-20-3 NAPHTHALENE 1
87-61-6 123-TRICHLOROBENZENE 1
75-05-S ACETONITRILE 1
107-05-1 ALLYL CH LORIDE 1
110-57-6 TRAN S-14-DICHLORO-2-BUTENE 1
64-17-5 ETHANOL 1
97-63-2 ETHYL METHACRYLATE 1
78-83-1 ISOBUTYL ALCOHOL 1
126-98-7 METHACRYLONITRILE 1
80-62-6 METHYL METHACRYLATE 1
107-12-0 I PROPIONITRILE 1
Result Reporting Limit
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
2 2
05 05
05 05
05 05
05 05
50 50
50 50 I 5 5
200 200
5 5
100 100
35 35
5 5
25 25
MDL
017
017
017
017
017
017
017
017
017
017
017
017
067
017
017
017
017
83
017
17
78
017
17
17
17
33
Result EPA Qualifier Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
Data Package 10 VL0911214-1
Date Printed Wednesday December 022009 ALS Laboratory Group -- Fe Page 7 of 8
LlMS Version 6317A
18
GCMS Volatiles Method SW8260_258
Sample Results
Lab Name ALS Laboratory Group bullbull FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644middot111B09(HWB R-37 VOCs) PAR 002731703
Sample Matrix WATER Prep Batch VL091125--4 Sample Aliquot 10 mlRmiddot37 Ser 1-111809 Moisture NA QCBatchlO VL091125--4-5 Final Volume 10 m
0911214-2 Date Collected 18-Nov-09 Run 10 VL091125--4A Result Units UGL Date Extracted 25-Nov-09 Cleanup NONE Clean OF 1 Date Analyzed 25-Nov-09 Basis As Received
10
Analysis ReqCode 104 Prep Method SW5030 Rev C File Name 028045
I
CASNO Target Analyte Dilution Factor
Result Reporting Limit
MDL Result Qualifier
EPA Qualifier
126-99-8 CHLOROPRENE 1 5 5 017 U
75-65-0 TERT-BUTANOL 1 100 100 33 U
108-20-3 ISOPROPYL ETHER 1 2 2 033 U
637-92-3 ETHYL TERT-BUTYL ETHER 1 2 2 033 U
994-05--8 TERT-AMYL MTHYL ETHER 1 2 2 033 U
67-72-1 HEXACHLOROETHANE 1 2 2 033 U
Surrogate Recovery
CASNO Surrogate Analyte Result Flag Spike Amount
Percent Control Recovery Limits
460-00-4 4middotBROMOFLUOROBENZENE 247 25 99 1
1868-53-7 DIBROMOFLUOROMETHANE 248 25 99 80 123
2037-26-5 TOLUENEmiddotDB 255 25 102 85 - 116
Data Package 10 VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- FC Page B of 8
LlMS Version 6317A
19
GCMS Volatiles Method SW8260_258
Laboratory Control Sample and Laboratory Control Sample Duplicate
Lab Name ALS Laboratory Group - FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-111809(HWB R-37 VOCs) PAR 002731703
Lab 10 VL091125-4LCS Sample Matrix WATER
Moisture NA Prep Batch VL091125-4
QCBatchlD VL091125-4-5
Sample Aliquot
Final Volume
10ml
10ml Date Collected NA Run 10 VL091125-4A Result Units UGIL Date Extracted 111252009 Cleanup NONE Clean OF 1 Date Analyzed 11252009 Basis NA
Prep Method SW5030C File Name 028040
CASNO
74-87-3
75-01-4
74-83-9
75-69-4
75-35-4
75-15-0
156-60-5
75-34-3
108-05-4
156-59-2
78-93-3
67 -66-3
71-55-6
i 56-23-5
107-06-2
71-43-2
79-01-6
78-87-5
75-27-4
108-88-3
79-00-5
591-78-6
127-18-4
106-93-4
108-90-7
63Q20-6
Target Analyte Spike Added
CHLOROMETHANE 10
VINYL CHLORIDE 10
BROMOMETHANE 10
TRICHLOROFLUOROMETHANE 10
11-DICHLOROETHENE 10
CARBON DISULFIDE 10
TRANS-12-DICHLOROETHENE 10
11-DICHLOROETHANE 10
VINYL ACETATE 10
CIS-12-DICHLOROETHENE 10
2middotBUTANONE 40
CHLOROFORM 10
111-TRICHL ORO ETHANE 10
CARBON TETRACHLORIDE 10
12-DICHLOROETHANE 10
BENZENE 10
TRICHLOROETHENE 10
12-DICHLOROPROPANE 10
BROMODICHLOROMETHANE 10
TOLUENE 10
112-TRICHLOROETHANE 10
2-HEXANONE 40
TETRACHLOROETHENE 10
12-DIBROMOETHANE 10
CHLOROBENZENE 10
1112-TETRACHLOROETHANE 10
LCS Reporting Result Result Limit Qualifier
932 05
863 05
943 1
908 05
96 05
95 10 J
996 05
992 05
10 10
102 05
412 5
993 05
974 1
943 05
106 05
983 05
962 05
10 05
988 05
974 05
989 05
409 10
956 05
991 1
984 05
101 05
LCS Control Rec Limits
93 49 -129
86 46 134
94 32-121
91 67 -152
96 61 -135
95 61 -140
100 70 -122
99 76 -119
100 62 182
102 75 126
103 61 -137
99 79 120
97 76 - 114
94 58middot135
106 75middot132
98 70 shy 125
96 74 121
100 81 -119
99 79 - 123
97 76 - 120
99 81 -126
102 45 168
96 56 -128
99 79 -123
98 75 -120
101 82 - 123
Data Package 10 VL0911214middot1
-Date Printed Wednesday December 02 2009 ALS Laboratory Group -- Fe Page 1 of 4
LiMS Version 6317A
20
GCMS Volatiles Method SW8260_25B
Laboratory Control Sample and Laboratory Control Sample Duplicate
Lab Name ALS Laboratory Group - FC
Work Order Number 0911214
Client Name New Mexico Envircnment Department OB
ClientProject 10 644-111809(HWB R-37 VOes) PAR 002731703
Lab 10 VL091125-4LCS Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml
Moisture NIA QCBatchlO VL091125-4-5 Final Volume 10 mi
Date Collected NA Run 10 VL091125-4A Result Units UGL Date Extracted 11252009 Cleanup NONE Clean OF 1 Date Analyzed 111252009 Basis NA
Prep Method SW5030e File Name 028040
CASNO Target Analyte Spike Added
LCS Result
Reporting Limit
Result Qualifier
LCS Rec
Control Limits
100-41-4 ETHYLBENZENE 10 981 05 98 79 -114
136777-61-2 M+P-XYLENE 20 197 1 98 81-115
95-47-6 O-XYLENE 10 101 05 101 81 -115
95-49-8 2-CHLOROTOLUENE 10 97 05 97 80 -128
541-73-1 13-DICHLOROBENZiNt 10 977 05 98 81-116
106-46-7 14-DICHLOROBENZENE 10 979 05 98 81 -119
95-50-1 12-DICHLOROBENZENE 10 987 05 99 79 - 116
91-20-3 NAPHTHALENE 10 993 05 99 69 -126
87-61-6 123-TRICHLOROBENZENE 10 999 05 100 60 -137
Data Package ID VL0911214-1
Date Printed Wecnesday December 02 2009 ALS Laboratory Group -- Fe Page 2 of 4
21
GCMS Volatiles Method SW8260_25B
Laboratory Control Sample and Laboratory Control Sample Duplicate
Lab Name ALS Laboratory Group bullbull FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-11 1809(HWB R-37 VOCs) PAR 002731703
Lab 10 VL091125middot4LCSD Sample Matrix WATER
Moisture NIA Prep Batch VL091125-4
QCBatchlD VL091125-4-5
Sample Aliquot
Final Volume
10 ml
10ml Date Collected NIA Run ID VL091125-4A Result Units UGIL Date Extracted 112512009 Cleanup NONE Clean DF 1 Date Analyzed 1112512009 Basis NIA
Prep Method SW5030C File Name 028041
CASNO Target Analyte Spike Added
LCSD Result
Reporting Limit
Result Qualifier
LCSD Rec
RPD Limit
RPD
74-87-3 CHLOROMETHANE 10 897 05 90 30 4
75-01-4 VINYL CHLORIDE 10 831 05 83 25 4
74-83-9 BROMO METHANE 10 945 1 94 25 0
75-69-4 TRICHLOROFLUOROMETHANE 10 873 05 87 22 4
75-35-4 11-DICHLOROETHENE 10 909 05 91 18 5
75-15-0 CARBON DISULFIDE 10 941 10 J 94 20 1
156-60middot5 TRANS-l2middotDICHLOROETHENE 10 961 05 96 25 4
75middot34middot3 11-DICHLOROETHANE 10 977 05 98 25 2
108-05-4 VINYL ACETATE 10 993 10 J 99 20 1
156middot59-2 CIS-12-DlCHLOROETHENE 10 995 05 99 25 3
i 78-93-3 2-BUTANONE 40 419 5 105 30 2
67-66-3 CHLOROFORM 10 985 05 99 25 1
71-55-6 lll-TRICHLOROETHANE 10 942 1 94 25 3
56-23-5 CARBON TETRACHLORIDE 10 922 05 92 25 2
107middot06-2 12middotDICHLOROETHANE 10 106 05 106 25 0
71-43middot2 BENZENE 10 971 05 97 10 1
79middot01middot6 TRICHLOROETHENE 10 939 05 94 10 2
78middot87middot5 l2middotDICHLOROPROPANE 10 101 05 101 25 1
i 75middot27-4 BROMODICHLOROMETHANE 10 992 05 99 25 0
1108-88-3 TOLUENE 10 962 05 96 9 1
I 79005 112middotTRICHLOROETHANE 10 986 05 99 25 0
591middot78middot6 2-HEXANONE 40 418 10 104 20 2
127middot18-4 TETRACHLOROETHENE 10 918 05 92 25 4
106-93-4 12middotDIBROMOETHANE 10 999 1 100 15 1
108middot90-7 CHLOROBENZENE 10 997 05 100 11 1
630-20middot6 1112-TETRACHLOROETHANE 10 101 05 101 15 0
100-41-4 ETHYLBENZENE 10 968 05 97 25 1
Data Package ID VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- FC Page 3 of 4
lIMS Version 6317 A
22
GCMS Volatiles Method SW8260_25B
Laboratory Control Sample and Laboratory Control Sample Duplicate
Lab Name ALS Laboratory 13roup -- FC
Work Order Number 0911214
Client Name New Mexico Environment Department OS
ClientProject 10 644-11 1809(HWB R-37 VOCs) PAR 002731703
Lab 10 VL091125-4LCSD Sample Matrix WATER
Moisture NA Prep Batch VL091125-4
QCBatchlO VL091125-4-5
Sample Aliquot
Final Volume
10 ml
10ml Date Collected NA Run 10 VL091125-4A Result Units UGL Date Extracted 11252009 Cleanup NONE Clean OF Date Analyzed 11252009 Basis NIA
Prep Method SW5030C File Name 028041
CASNO Target Analyte Spike Added
LCSD Result
Reporting Limit
Result Qualifier
LCSD Rec
RPD Limit
RPD
136777-61-2 M+P-XYLENE 20 193 1 97 25 2
95-47-6 O-XYLENE 10 983 05 98 25 2
95-49-8 2middotCHLOROTOLUENE 10 9A9 05 95 15 2
541-73-1 13middotDICHLOROBENZENE 10 997 05 100 25 2
106-46-7 14-DICHLOROBeNZENE 10 974 05 97 25 1
95-50middot1 12middotDICHLOROBENZeNE 10 101 05 101 25 2
91middot20-3 NAPHTHALENe 10 105 05 105 24 6
87-61-6 123-TRICHLOROBENZENE 10 102 05 102 33 3
Surrogate Recovery LCSLCSD
CASNO Target Analyte Spike Added
LCS Rec
LCS Flag
LCSD Rec
LCSD Flag
Control Limits
460middot00-4 4-BROMOFLUOROBeNZENE 25 100 100 82 - 121
1868-53middot7 DIBROMOFLUOROMeTHANE 25 101 100 80middot 123
2037middot26-5 TOLUENEmiddotD8 25 102 100 85middot 116
Data Package 10 VL0911214-
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- Fe Page 4 of 4
UMS Verslmt 6317A
23
GCMS Volatiles Method SW8260 _258
Method Blank
Lab Name ALS Laboratory Group - FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-111B09(HWB R-37 VOCs) PAR 002731703
Lab 10 VL091125-4MB Sample Matrix WATER
Moisture NIA
Prep Batch VL091125-4
QCBatchlD VL091125-4-5
Sample Aliquot
Final Volume
10 ml
10 ml
Date Collected NIA Run ID VL091125-4A Result Units UGL
Date Extracted 25-Nov-09 Cleanup NONE Clean DF 1
Date Analyzed 25-Nov-09 Basis NA
File Name 028043
CASNO Target Analyte OF Result Reporting Limit
MOL Result Qualifier
EPA Qualifier
98-06-6 TERT-BUTYLBENZENE 1 05 05 017 U
95-63-6 124-TRIMETHYLBENZENE 1 05 05 017 U
135-98-8 SEC-BUTYLBENZENE 1 05 05 017 U
541-73-1 13-DlCHLOROBENZENE 1 05 05 017 U
99-87-6 P-ISOPROPYLTOLUENE 1 05 05 017 U
106-46-7 1 A-DICHLOROBENZENE 1 05 05 017 U
104-51-8 N-BUTYLBENZENE 1 05 05 017 U
95-50-1 12-DICHLOROBENZENE 1 05 05 017 U
96-12-B 12-DIBROMO-3-CHLOROPROPANE 1 2 2 067 U
120-82-1 124-TRiCHLOROBENZENE 1 05 05 017 U
87-68-3 HEXACHLOROBUTADIENE 1 05 05 017 U
91-20-3 NAPHTHALENE 1 05 05 017 U
87-61-6 123-TRICHLOROBENZENE 1 05 05 017 U
75-05-B ACETONITRILE 1 50 50 83 U
107-05-1 ALLYL CHLORIDE 1 50 50 017 U
110-57-6 TRANS-14-DICHLORO-2-BUTENE 1 5 5 17 U
64-17-5 ETHANOL 1 200 200 78 U
97-63-2 ETHYL METHACRYLATE 1 5 5 017 U
78-83-1 ISOBUTYL ALCOHOL 1 100 100 17 U
126-98-7 METHACRYLONITRILE 1 35 35 17 U
80-62-6 METHYL METHACRYLATE 1 5 5 17 U
107-12-0 PROPIONITRILE 1 25 25 33 U
126-99-8 CHLOROPRENE 1 5 5 017 U
75-65-0 TERT-BUTANOL 1 100 100 33 U
108-20-3 ISOPROPYL ETHER 1 2 2 033 U
637-92-3 ETHYL TERT-BUTYL ETHER 1 2 2 033 U
994-05-8 TERT-AMYL METHYL ETHER 1 2 2 033 U
67-72-1 HEXACHLOROETHANE 1 2 2 033 U
Data Package 10 VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -~ Fe Page 3 of 4
LlMS Version 6317 A
10
GCMS Volatiles Method SW8260 _258
Method Blank
Lab Name ALS Laboratory Group -- FC
Work Order Number 0911214
Client Name New Mexico Envirmment Department OB
ClientProject 10 644-111809(HWB R-37 VOCs) PAR 002731703
Lab 10 VL091125-4MB Sample Matrix WATER
Moisture NIA Prep Batch VL091125-4
QCBatchlO VL091125-4-5
Sample Aliquot
Final Volume
10 m
10m Date Collected NIA Run 10 VL091125-4A Result Units UGIL Date Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Date Analyzed 25-Nov-09 BasisNIA
File Name 028043
CASNO Target Analyte Result Reporting MOL Result EPAOF Limit Qualifier Qualifier
Surrogate Recovery
CASNO Surrogate Analyte Result Flag Spike Amount
Percent Recovery
Control Limits
460-00-4 4-BROMOFLUOROBENZENE 25 25 100 82 - 121
1868-53-7 DIBROMOFLUOROMETHANE 248 25 99 80 - 123
2037-26-5 TOLUENE-D8 26 25 104 85 - 116
Data Package 10 VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- FC Page 4 of4
LlMS Version 6317A
11
GCMS Volati les Method SW8260 _258
Sample Results
Lab Name ALS Laboratory Group -- FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-111809(HWB R-37 VOCs) PAR 002731703
Field 10 Rmiddot37 Ser 2middot111809
Lab 10 0911214middot1
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml
Moisture NA QCBatchlO VL091125-4-5 Final Volume 10mi Date Collected 18-Nov-09 Run 10 VL091125-4A Result Units UGL
Date Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Analysis ReqCode 104 Date Analyzed 25-Nov-09
Prep Method SW5030 Rev C Basis As Received
File Name 028044
CASNO Target Analyte Dilution Factor
75-71-8 DICHLORODIFLUOROMETHANE 1
74middot87-3 CHLOROMETHANE 1
75-01-4 VINYL CHLORIDE 1
74-83-9 BROMOMETHANE 1
75-00-3 CHLOROETHANE 1
75-69-4 TRICHLOROFLUOROMETHANE 1
107-02-8 ACROLEIN 1
75-35-4 11middotDICHLOROETHENE 1
67-64-1 ACETONE 1
74-88-4 IODOMETHANE 1
75-15-0 CARBON DISULFIDE 1
75-09-2 METHYLENE CHLORIDE 1
156-60-5 TRANSmiddot12middotDICHLOROETHENE 1
1634-04-4 METHYL TERTIARY BUTYL ETHER 1
107-13-1 ACRYLONITRILE 1
75-34-3 1-DICHLOROETHANE 1
i 108-05-4 VINYL ACETATE 1
156-59-2 CIS-12middotDICHLOROETHENE 1
78-93-3 2-BUTANONE 1
74-97-5 BROMOCHLOROMETHANE 67-66-3 CHLOROFORM 1
71-55-6 11-TRICHLOROETHANE 594-20-7 22-DICHLOROPROPANE 56-23-5 CARBON TETRACHLORIDE 563-58-6 -DICHLOROPROPENE 107-06-2 2-DICHLOROETHANE
Result Reporting Limit
05 05
05 05
05 05
1 1
05 05
05 05
100 100
05 05
10 10
5 5
10 10
1 1
05 05
1 1
10 10
05 05
10 10
05 05
5 5
1 1
05 05
1 1
05 05
05 05
05 05
05 05
MOL Result EPA Qualifier Qualifier
017 U
017 U
017 U
017 U
017 U
017 U
17 U
017 U
33 U
017 U
017 U
017 U
017 U
017 U
17 U
017 U
067 U
017 U
17 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
Data Package ID VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- Fe Page 1 of 8
UMS Version 6317A
12
GCMS Volatiles Method SW8260_25B
Sample Results
Lab Name ALS Laboratory Group - FC
Work Order Number 0911214
Client Name New Mexico nvironment Department OB
ClientProject 10 644-111809(HWB R-37 VOCs) PAR 002731703
Field 10 R-37 Scr 2-111809
Lab 10 0911214-1
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10ml
Moisture NA QCBatchlD VL091125-4-5 Final Volume 10ml
Date Collected l8-Nov-09 Run 10 VL091125-4A Result Units UGL
Date Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Analysis ReqCode 104 Date Analyzed 25-Nov-09 Basis As Received
Prep Method SW5030 Rev C File NameD28044
CASNO Target Analyte Dilution Factor
Result Reporting Limit
MDL Result Qualifier
EPA Qualifier
I
71-43-2 BENZENE 1 05 05 017 U
79-01-6 TRICHLOROETHENE 1 05 05 017 U
78-87-5
74middot95-3
75-27-4
10061-01-5
108middot10middot1
108middot88-3
10061-02middot6
79-00-5
591-78-6
12-DICHLOROPROPANE
DIBROMOMETHANE
BROMODCHLOROMETHANE
CIS-13-DICHLOROPROPEI~E
4-METHYL-2-PENTANONE
TOLUENE
TRANS-13-DICHLOROPROPENE
112-TRICHLOROETHANE
2-HEXANONE
1
1
1
1
1
1
1
1
1
05
05
05
05
5
031
05
05
10
05
05
05
05
5
05
05
05
10
017
017
017
017
17
017
017
017
17
U
U
U
U
U
J
U
U
U
127-18-4
142-28-9
124-48-1
106-93-4
108-90-7
630-20-6
100-41-4
136777-61-2
95-47-6
100-42middot5
75-25-2
98-82middot8
96-18-4
79-34-5
108-86-1
TETRACHLOROETHENE
13-DICHLOROPROPANE
DIBROMOCHLOROMETHANE
12-DIBROMOETHANE
CHLOROBENZENE
11 12-TETRACHLOROETHANE
ETHYLBENZENE
M+PmiddotXYLENE
OmiddotXYLENE
STYRENE
BROMOFORM
ISOPRO PYLBENZENE
123middotTRICHLOROPROPANE
1122-TETRACHLOROETHANE
BROMOBENZENE
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
05
05
1
1
05
05
05
1
05
05
05
05
2
05
05
05
05
1
1
05
05
05
1
05
05
05
05
2
05
05
017
017
017
017
017
017
017
017
017
017
017
017
017
017
017
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
i
Data Package 10 VL0911214-1
Date Printed Wednesday December 022009 AlS laboratory Group bullbull Fe Page 2 of 8
UMS Version 6317A
13
GCMS Volatiles Method SW8260_258
Sample Results
Lab Name ALS Laboratory Group bullbull FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject ID 644-111809(HWB R-37 VOCs) PAR 002731703
Field 10 R-37 Sor 2-111809
Lab ID 0911214middot1
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml
Moisture NA QCBatchlD VL091125-4-5 Final Volume 10 ml
Date Collected 18-Nov-09 Run ID VL091125-4A Result Units UGL
Date Extracted 25-Nov-09 Cleanup NONE Clean DF 1
Analysis ReqCode 104 Date Analyzed 25-Nov-09 Basis As Received
Prep Method SW5030 Rev C File Name 028044
CASNO Target Analyte Dilution Factor
103-65-1 NmiddotPROPYLBENZENE 1
95-49-8 2-CHLOROTOLUENE 1
108-67-8 135-TRIMETHYLBENZENE 1
106-43-4 4-CHLOROTOLUENE 1
98-06-6 TER I-BUTYLBENZENE 1
95-63-6 124-TRIMETHYLBENZENE 1
135-98-8 SEC-BUTYLBENZENE 1
541-73-1 13-OICHLOROBENZENE 1
99-87-6 P-ISOPROPYLTOLUENE 1
106-46-7 lA-DICHLOROBENZENE 1
104-51-8 N-BUTYLBENZENE 1
95-50-1 12-DICHLOROBENZENE 1
96-12-8 l2-DIBROMOmiddot3-CHLOROPROPANE 1
120-82-1 12A-TRICHLOROBENZENE 1
187-68-3 HEXACHLOROBUTADIENE 1
91-20-3 NAPHTHALENE 1
87-61middot6 123-TRICHLOROBENZENE 1
75-05-8 ACETONITRILE 1
107middot05middot1 ALLYL CHLORIDE 1
110-57-6 TRANS-14-DICHLORO-2-BUTENE 1
164-17-5 ETHANOL 1
97-63-2 ETHYL METHACRYLATE 1
78-83-1 ISOBUTYL ALCOHOL 1
126-98-7 METHACRYLONITRILE 1
80-62-6 METHYL METHACRYLATE 1
107-12-0 PROPIONITRILE 1
Result Reporting Limit
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
2 2
05 05
05 05
05 05
05 05
50 50
50 50
5 5
200 200
5 5
100 100
35 35
5 5
25 25
MDL Result EPA Qualifier Qualifier
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
067 U
017 U
017 U
017 U
017 U
83 U
017 U
U u 78 U
017 U
17 U
17 U
17 U
33 U
Data Package 10 VL0911214-1
Date Printed Wednesday December 022009 ALS Laboratory Group MM Fe Page 3 of 8
LlMS VerSion 6317A
14
GCMS Volati las Method SW8260_258
Sample Results
Lab Name ALS Laboratory Group - FC
Work Order Number 0911214
Client Name New Mexico Environment Department 08
ClientProject 10 644-111B09(HWB R-37 VOGs) PAR 002731703
Field 10 R-37 Ser 2-111809 Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10ml
Lab 10 0911214-1 Moisture NA
Date Collected 1B-Nov-09 QCBatchlO VL091125-4-5
Run 10 VL091125-4A
Final Volume 10ml
Result Units UGIL Date Extracted 25-Nov-09 Cleanup NONE Clean OF
Analysis ReqCode 104 Date Analyzed 25-Nov-09
Prep Method SW5030 Rev G Basis As Received
File Name 028044
CASNO Target Analyte Dilution Factor
Result Reporting Limit
MDL Result Qualifier
EPA Qualifier
126-99-8 CHLOROPRENE 1 5 5 017 U
75-65-0 TERT-BUTANOL 1 100 100 33 U
108-20-3 ISOPROPYL ETHER 1 2 2 033 U
637-92-3 ETHYL TERT-BUTYL ETHER 1 2 2 033 U
994-05-8 TERT-AMYL METHYL ETHER 1 2 2 033 U
67-72-1 HEXACHLOROETHANE 1 2 2 033 U
Surrogate Recovery
CASNO Surrogate Analyte Result Flag Spike Amount
Percent Recovery
Control Limits
460-00-4 4-BROMOFLUOHOBENZENE 246 25 98 82 - 121
1868-53-7 DIBROMOFLUOHOMETHANE 248 25 99 BO - 123
2037-26-5 TOLUENE-DB 258 25 103 85middot116
Data Package 10 VL0911214-1
Date Printed Wednesday December 022009 ALS Laboratory Group bullbull FC Page 4 of 8
LIMS Version 0317 A
15
GCMS Volati les Method SW8260_25B
Sample Results
Lab Name ALS Laboratory Group -- FC
Worlt Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-111809(HWB Rmiddot37 VOCs) PAR 002731703
Field 10 Rmiddot37 Scr jmiddot111809
Lab 10 0911214-2
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml Moisture NfA QCBatchID VL091125-4middot5 Final Volume 10 ml
Date Collected 18middotNov-09 Run 10 VL091125-4A Result Units UGfL Date Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Analysis ReqCode 104 Date Analyzed 25middotNov-09 Basis As Received Prep Method SW5030 Rev C File Name 028045
CASNO Target Analyte Dilution Factor
Result Reporting Limit
MOL Result Qualifier
EPA Qualifier
75-71-8 DICHLORODIFLUOROMETHANE 1 05 05 017 U
74-87-3 CHLOROMETHANE 1 05 05 017 U
75-01middot4 VINYL CHLORIDE 1 05 05 017 U
74-83-9 BROMOMETHANE 1 1 1 017 U
75middot00middot3 CHLOROETHANE j 05 05 017 U
75-69-4 TRICHLOROFLUOROMETHANE 1 05 05 017 U
107-02-8 ACROLEIN 1 100 100 17 U
i 75-35-4 11-DICHLOROETHENE 1 05 05 017 U
67-64middot1 ACETONE 1 10 10 33 U
74-8S-4 IODOMETHANE 1 5 5 017 U
75-15-0 CARBON DISULFIDE 1 10 10 017 U
75-09-2 METHYLENE CHLORIDE 1 1 1 017 U
156-60-5 TRANS-12-DICHLOROETHENE 1 05 05 017 U
1634-04-4 METHYL TERTIARY BUTYL ETHER 1 1 1 017 U
107-13-1 ACRYLONITRILE 1 10 10 17 U
75-34middot3 11-DICHLOROETHANE 05 05 017 U
i 108-05-4 VINYL ACETATE 1 10 10 067 U
115659-2 CISmiddot 2middotDICHLOROETHENE 1 05 05 017 U
178-933 2middotBUTANONE 1 5 5 17 U
74-97middot5 BROMOCHLOROMET HANE 1 1 1 017 U
67-66-3 CHLOROFORM 1 05 05 017 U
71-55middot6 111middotTRICHLOROETHANE 1 1 1 017 U
594-20-7 22middotDICHLOROPROPANE 1 05 05 017 U
56-23-5 CARBON TETRACHLORIDE 1 05 05 017 U
563-58-6 11middotDICHLOROPROPENE 1 05 05 017 U
107-06-2 12middotDICHL OROETHANE 1 05 05 017 U
Data Package ID VL0911214-1
Date Printed Wednesday December 022009 ALS Laboratory Group -- Fe Page 5 of 8
16
GCMS Volatiles Method SW8260_25B
Sample Results
Lab Name ALS Laboratory Group -- FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-111809(HW3 R-37 VOCs) PAR 002731703
Field 10 R-37 Scr 1-11 1809
Lab 10 0911214-2
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml
Moisture NIA QCBatchlO VL091125-4-5 Final Volume 10 ml
Date Collected 18-Nov-09 Run 10 VL091125-4A Result Units UGL
[late Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Analysis ReqCode 104 Date Analyzed 25-Nov-09
Prep Method SW5030 Rev C Basis As Received
File Name 028045
CASNO Target Analyte Dilution Factor
71-43-2 BENZENE 1
79-01-6 TRICHLOROETHENE 1
78-87-5 12-DICHLOROPROPANE 1
74-95-3 DIBROMOMETHANE 1
75-27-4 BROMODICHLOROMETHANE 1
10061-01-5 CIS-13-DICHLOROPROPENE 1
108-10-1 4-METHYL-2-PtNTANON 1
108-88-3 TOLUENE 1
10061-02-6 TRANS-13-DICHLOROPROPENE 1
79-00-5 112-TRICHLOROETHANE 1
591-78-6 2-HEXANONE 1
127-18-4 TETRACHLOROETHENE 1
142-28-9 13-DICHLOROPROPANt 1
124-48-1 DI3ROMOCHLOROMETHANE 1
106-93-4 12-DIBROMOETHANE 1
108-90-7 CHLOROBENZENE 1
OETHANE 1
- 1
LENE 1
ENE 1
ENE 1
OFORM 1
OPYlBENZENE 1
96-18-4 123-TRICHLOROPROPANE 1
79-34-5 1122-TETRACHLOROETHANE 1
108-86-1 BROMOBENZENE 1
Result Reporting Limit
05 05
05 05
05 05
05 05
05 05
05 05
5 5
025 05
05 05
05 05
10 10
05 05
05 05
1 1
1 1
05 05
05 05
05 05
1 1
05 05
05 05
05 05
05 05
2 2
05 05
05 05
MDL Result EPA Qualifier Qualifier
017 U
017 U
017 U
017 U
017 U
017 U
17 U
017 J
017 U
017 U
17 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
Data Package 10 VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- Fe Page 6 of 8
317A
17
GCMS Volatiles Method SW8260 _258
Sample Results
Lab Name ALS Laboratory Group -- FC
Work Order Number 0911214
Client Name New Mexico Environment Department 08
ClientProject 10 644-11S09(HWB R-37 VOCs) PAR 002731703
Field 10 Rmiddot37 Scr 1-111809
Lab 10 0911214-2
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml Moisture NA QCBatchlD VL091125-4-5 Final Volume 10 ml
Date Collected 18-Nov-09 Run 10 VL091125-4A Result Units UGL Date Extracted 25-Nol-09 Cleanup NONE Clean OF
Analysis ReqCode 104 Date Analyzed 25-Nov-09 Basis As Received Prep Method SW5030 Rev C File Name D28045
CASNO Target Analyte Dilution Factor
103-65-1 N-PROPYLBENZENE 1
95-49-8 2-CHLOROTOLUENE 1
108-67-8 135-TRIMETHYLBENZENE 1
106-43-4 4-CHLOROTOLUENE 1
98-06-6 TERT-BUTYLBENZENE 1
95-63-6 124-TRIMETHYLBENZENE 1
135-98-8 SEC-BUTYLBENZENE 1
i 541-73-1 13middotDICHLOROBENZENE 1
99-87-6 PmiddotISOPROPYL TOLUENE 1
106-46-7 I 14-DICHLOROBENZENE 1
104-51-8 I N-BUTYLBENZENE 1
95-50-1 l2-DICHLOROBENZENE 1
96-12-8 I 12-DIBROMO-3-CHLOROPROPANE 1
120-82-1 124-TRICHLOROBENZENE 1
87-68-3 HEXACHLOROBUT ADIENE 1
91-20-3 NAPHTHALENE 1
87-61-6 123-TRICHLOROBENZENE 1
75-05-S ACETONITRILE 1
107-05-1 ALLYL CH LORIDE 1
110-57-6 TRAN S-14-DICHLORO-2-BUTENE 1
64-17-5 ETHANOL 1
97-63-2 ETHYL METHACRYLATE 1
78-83-1 ISOBUTYL ALCOHOL 1
126-98-7 METHACRYLONITRILE 1
80-62-6 METHYL METHACRYLATE 1
107-12-0 I PROPIONITRILE 1
Result Reporting Limit
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
2 2
05 05
05 05
05 05
05 05
50 50
50 50 I 5 5
200 200
5 5
100 100
35 35
5 5
25 25
MDL
017
017
017
017
017
017
017
017
017
017
017
017
067
017
017
017
017
83
017
17
78
017
17
17
17
33
Result EPA Qualifier Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
Data Package 10 VL0911214-1
Date Printed Wednesday December 022009 ALS Laboratory Group -- Fe Page 7 of 8
LlMS Version 6317A
18
GCMS Volatiles Method SW8260_258
Sample Results
Lab Name ALS Laboratory Group bullbull FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644middot111B09(HWB R-37 VOCs) PAR 002731703
Sample Matrix WATER Prep Batch VL091125--4 Sample Aliquot 10 mlRmiddot37 Ser 1-111809 Moisture NA QCBatchlO VL091125--4-5 Final Volume 10 m
0911214-2 Date Collected 18-Nov-09 Run 10 VL091125--4A Result Units UGL Date Extracted 25-Nov-09 Cleanup NONE Clean OF 1 Date Analyzed 25-Nov-09 Basis As Received
10
Analysis ReqCode 104 Prep Method SW5030 Rev C File Name 028045
I
CASNO Target Analyte Dilution Factor
Result Reporting Limit
MDL Result Qualifier
EPA Qualifier
126-99-8 CHLOROPRENE 1 5 5 017 U
75-65-0 TERT-BUTANOL 1 100 100 33 U
108-20-3 ISOPROPYL ETHER 1 2 2 033 U
637-92-3 ETHYL TERT-BUTYL ETHER 1 2 2 033 U
994-05--8 TERT-AMYL MTHYL ETHER 1 2 2 033 U
67-72-1 HEXACHLOROETHANE 1 2 2 033 U
Surrogate Recovery
CASNO Surrogate Analyte Result Flag Spike Amount
Percent Control Recovery Limits
460-00-4 4middotBROMOFLUOROBENZENE 247 25 99 1
1868-53-7 DIBROMOFLUOROMETHANE 248 25 99 80 123
2037-26-5 TOLUENEmiddotDB 255 25 102 85 - 116
Data Package 10 VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- FC Page B of 8
LlMS Version 6317A
19
GCMS Volatiles Method SW8260_258
Laboratory Control Sample and Laboratory Control Sample Duplicate
Lab Name ALS Laboratory Group - FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-111809(HWB R-37 VOCs) PAR 002731703
Lab 10 VL091125-4LCS Sample Matrix WATER
Moisture NA Prep Batch VL091125-4
QCBatchlD VL091125-4-5
Sample Aliquot
Final Volume
10ml
10ml Date Collected NA Run 10 VL091125-4A Result Units UGIL Date Extracted 111252009 Cleanup NONE Clean OF 1 Date Analyzed 11252009 Basis NA
Prep Method SW5030C File Name 028040
CASNO
74-87-3
75-01-4
74-83-9
75-69-4
75-35-4
75-15-0
156-60-5
75-34-3
108-05-4
156-59-2
78-93-3
67 -66-3
71-55-6
i 56-23-5
107-06-2
71-43-2
79-01-6
78-87-5
75-27-4
108-88-3
79-00-5
591-78-6
127-18-4
106-93-4
108-90-7
63Q20-6
Target Analyte Spike Added
CHLOROMETHANE 10
VINYL CHLORIDE 10
BROMOMETHANE 10
TRICHLOROFLUOROMETHANE 10
11-DICHLOROETHENE 10
CARBON DISULFIDE 10
TRANS-12-DICHLOROETHENE 10
11-DICHLOROETHANE 10
VINYL ACETATE 10
CIS-12-DICHLOROETHENE 10
2middotBUTANONE 40
CHLOROFORM 10
111-TRICHL ORO ETHANE 10
CARBON TETRACHLORIDE 10
12-DICHLOROETHANE 10
BENZENE 10
TRICHLOROETHENE 10
12-DICHLOROPROPANE 10
BROMODICHLOROMETHANE 10
TOLUENE 10
112-TRICHLOROETHANE 10
2-HEXANONE 40
TETRACHLOROETHENE 10
12-DIBROMOETHANE 10
CHLOROBENZENE 10
1112-TETRACHLOROETHANE 10
LCS Reporting Result Result Limit Qualifier
932 05
863 05
943 1
908 05
96 05
95 10 J
996 05
992 05
10 10
102 05
412 5
993 05
974 1
943 05
106 05
983 05
962 05
10 05
988 05
974 05
989 05
409 10
956 05
991 1
984 05
101 05
LCS Control Rec Limits
93 49 -129
86 46 134
94 32-121
91 67 -152
96 61 -135
95 61 -140
100 70 -122
99 76 -119
100 62 182
102 75 126
103 61 -137
99 79 120
97 76 - 114
94 58middot135
106 75middot132
98 70 shy 125
96 74 121
100 81 -119
99 79 - 123
97 76 - 120
99 81 -126
102 45 168
96 56 -128
99 79 -123
98 75 -120
101 82 - 123
Data Package 10 VL0911214middot1
-Date Printed Wednesday December 02 2009 ALS Laboratory Group -- Fe Page 1 of 4
LiMS Version 6317A
20
GCMS Volatiles Method SW8260_25B
Laboratory Control Sample and Laboratory Control Sample Duplicate
Lab Name ALS Laboratory Group - FC
Work Order Number 0911214
Client Name New Mexico Envircnment Department OB
ClientProject 10 644-111809(HWB R-37 VOes) PAR 002731703
Lab 10 VL091125-4LCS Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml
Moisture NIA QCBatchlO VL091125-4-5 Final Volume 10 mi
Date Collected NA Run 10 VL091125-4A Result Units UGL Date Extracted 11252009 Cleanup NONE Clean OF 1 Date Analyzed 111252009 Basis NA
Prep Method SW5030e File Name 028040
CASNO Target Analyte Spike Added
LCS Result
Reporting Limit
Result Qualifier
LCS Rec
Control Limits
100-41-4 ETHYLBENZENE 10 981 05 98 79 -114
136777-61-2 M+P-XYLENE 20 197 1 98 81-115
95-47-6 O-XYLENE 10 101 05 101 81 -115
95-49-8 2-CHLOROTOLUENE 10 97 05 97 80 -128
541-73-1 13-DICHLOROBENZiNt 10 977 05 98 81-116
106-46-7 14-DICHLOROBENZENE 10 979 05 98 81 -119
95-50-1 12-DICHLOROBENZENE 10 987 05 99 79 - 116
91-20-3 NAPHTHALENE 10 993 05 99 69 -126
87-61-6 123-TRICHLOROBENZENE 10 999 05 100 60 -137
Data Package ID VL0911214-1
Date Printed Wecnesday December 02 2009 ALS Laboratory Group -- Fe Page 2 of 4
21
GCMS Volatiles Method SW8260_25B
Laboratory Control Sample and Laboratory Control Sample Duplicate
Lab Name ALS Laboratory Group bullbull FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-11 1809(HWB R-37 VOCs) PAR 002731703
Lab 10 VL091125middot4LCSD Sample Matrix WATER
Moisture NIA Prep Batch VL091125-4
QCBatchlD VL091125-4-5
Sample Aliquot
Final Volume
10 ml
10ml Date Collected NIA Run ID VL091125-4A Result Units UGIL Date Extracted 112512009 Cleanup NONE Clean DF 1 Date Analyzed 1112512009 Basis NIA
Prep Method SW5030C File Name 028041
CASNO Target Analyte Spike Added
LCSD Result
Reporting Limit
Result Qualifier
LCSD Rec
RPD Limit
RPD
74-87-3 CHLOROMETHANE 10 897 05 90 30 4
75-01-4 VINYL CHLORIDE 10 831 05 83 25 4
74-83-9 BROMO METHANE 10 945 1 94 25 0
75-69-4 TRICHLOROFLUOROMETHANE 10 873 05 87 22 4
75-35-4 11-DICHLOROETHENE 10 909 05 91 18 5
75-15-0 CARBON DISULFIDE 10 941 10 J 94 20 1
156-60middot5 TRANS-l2middotDICHLOROETHENE 10 961 05 96 25 4
75middot34middot3 11-DICHLOROETHANE 10 977 05 98 25 2
108-05-4 VINYL ACETATE 10 993 10 J 99 20 1
156middot59-2 CIS-12-DlCHLOROETHENE 10 995 05 99 25 3
i 78-93-3 2-BUTANONE 40 419 5 105 30 2
67-66-3 CHLOROFORM 10 985 05 99 25 1
71-55-6 lll-TRICHLOROETHANE 10 942 1 94 25 3
56-23-5 CARBON TETRACHLORIDE 10 922 05 92 25 2
107middot06-2 12middotDICHLOROETHANE 10 106 05 106 25 0
71-43middot2 BENZENE 10 971 05 97 10 1
79middot01middot6 TRICHLOROETHENE 10 939 05 94 10 2
78middot87middot5 l2middotDICHLOROPROPANE 10 101 05 101 25 1
i 75middot27-4 BROMODICHLOROMETHANE 10 992 05 99 25 0
1108-88-3 TOLUENE 10 962 05 96 9 1
I 79005 112middotTRICHLOROETHANE 10 986 05 99 25 0
591middot78middot6 2-HEXANONE 40 418 10 104 20 2
127middot18-4 TETRACHLOROETHENE 10 918 05 92 25 4
106-93-4 12middotDIBROMOETHANE 10 999 1 100 15 1
108middot90-7 CHLOROBENZENE 10 997 05 100 11 1
630-20middot6 1112-TETRACHLOROETHANE 10 101 05 101 15 0
100-41-4 ETHYLBENZENE 10 968 05 97 25 1
Data Package ID VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- FC Page 3 of 4
lIMS Version 6317 A
22
GCMS Volatiles Method SW8260_25B
Laboratory Control Sample and Laboratory Control Sample Duplicate
Lab Name ALS Laboratory 13roup -- FC
Work Order Number 0911214
Client Name New Mexico Environment Department OS
ClientProject 10 644-11 1809(HWB R-37 VOCs) PAR 002731703
Lab 10 VL091125-4LCSD Sample Matrix WATER
Moisture NA Prep Batch VL091125-4
QCBatchlO VL091125-4-5
Sample Aliquot
Final Volume
10 ml
10ml Date Collected NA Run 10 VL091125-4A Result Units UGL Date Extracted 11252009 Cleanup NONE Clean OF Date Analyzed 11252009 Basis NIA
Prep Method SW5030C File Name 028041
CASNO Target Analyte Spike Added
LCSD Result
Reporting Limit
Result Qualifier
LCSD Rec
RPD Limit
RPD
136777-61-2 M+P-XYLENE 20 193 1 97 25 2
95-47-6 O-XYLENE 10 983 05 98 25 2
95-49-8 2middotCHLOROTOLUENE 10 9A9 05 95 15 2
541-73-1 13middotDICHLOROBENZENE 10 997 05 100 25 2
106-46-7 14-DICHLOROBeNZENE 10 974 05 97 25 1
95-50middot1 12middotDICHLOROBENZeNE 10 101 05 101 25 2
91middot20-3 NAPHTHALENe 10 105 05 105 24 6
87-61-6 123-TRICHLOROBENZENE 10 102 05 102 33 3
Surrogate Recovery LCSLCSD
CASNO Target Analyte Spike Added
LCS Rec
LCS Flag
LCSD Rec
LCSD Flag
Control Limits
460middot00-4 4-BROMOFLUOROBeNZENE 25 100 100 82 - 121
1868-53middot7 DIBROMOFLUOROMeTHANE 25 101 100 80middot 123
2037middot26-5 TOLUENEmiddotD8 25 102 100 85middot 116
Data Package 10 VL0911214-
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- Fe Page 4 of 4
UMS Verslmt 6317A
23
GCMS Volatiles Method SW8260 _258
Method Blank
Lab Name ALS Laboratory Group -- FC
Work Order Number 0911214
Client Name New Mexico Envirmment Department OB
ClientProject 10 644-111809(HWB R-37 VOCs) PAR 002731703
Lab 10 VL091125-4MB Sample Matrix WATER
Moisture NIA Prep Batch VL091125-4
QCBatchlO VL091125-4-5
Sample Aliquot
Final Volume
10 m
10m Date Collected NIA Run 10 VL091125-4A Result Units UGIL Date Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Date Analyzed 25-Nov-09 BasisNIA
File Name 028043
CASNO Target Analyte Result Reporting MOL Result EPAOF Limit Qualifier Qualifier
Surrogate Recovery
CASNO Surrogate Analyte Result Flag Spike Amount
Percent Recovery
Control Limits
460-00-4 4-BROMOFLUOROBENZENE 25 25 100 82 - 121
1868-53-7 DIBROMOFLUOROMETHANE 248 25 99 80 - 123
2037-26-5 TOLUENE-D8 26 25 104 85 - 116
Data Package 10 VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- FC Page 4 of4
LlMS Version 6317A
11
GCMS Volati les Method SW8260 _258
Sample Results
Lab Name ALS Laboratory Group -- FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-111809(HWB R-37 VOCs) PAR 002731703
Field 10 Rmiddot37 Ser 2middot111809
Lab 10 0911214middot1
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml
Moisture NA QCBatchlO VL091125-4-5 Final Volume 10mi Date Collected 18-Nov-09 Run 10 VL091125-4A Result Units UGL
Date Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Analysis ReqCode 104 Date Analyzed 25-Nov-09
Prep Method SW5030 Rev C Basis As Received
File Name 028044
CASNO Target Analyte Dilution Factor
75-71-8 DICHLORODIFLUOROMETHANE 1
74middot87-3 CHLOROMETHANE 1
75-01-4 VINYL CHLORIDE 1
74-83-9 BROMOMETHANE 1
75-00-3 CHLOROETHANE 1
75-69-4 TRICHLOROFLUOROMETHANE 1
107-02-8 ACROLEIN 1
75-35-4 11middotDICHLOROETHENE 1
67-64-1 ACETONE 1
74-88-4 IODOMETHANE 1
75-15-0 CARBON DISULFIDE 1
75-09-2 METHYLENE CHLORIDE 1
156-60-5 TRANSmiddot12middotDICHLOROETHENE 1
1634-04-4 METHYL TERTIARY BUTYL ETHER 1
107-13-1 ACRYLONITRILE 1
75-34-3 1-DICHLOROETHANE 1
i 108-05-4 VINYL ACETATE 1
156-59-2 CIS-12middotDICHLOROETHENE 1
78-93-3 2-BUTANONE 1
74-97-5 BROMOCHLOROMETHANE 67-66-3 CHLOROFORM 1
71-55-6 11-TRICHLOROETHANE 594-20-7 22-DICHLOROPROPANE 56-23-5 CARBON TETRACHLORIDE 563-58-6 -DICHLOROPROPENE 107-06-2 2-DICHLOROETHANE
Result Reporting Limit
05 05
05 05
05 05
1 1
05 05
05 05
100 100
05 05
10 10
5 5
10 10
1 1
05 05
1 1
10 10
05 05
10 10
05 05
5 5
1 1
05 05
1 1
05 05
05 05
05 05
05 05
MOL Result EPA Qualifier Qualifier
017 U
017 U
017 U
017 U
017 U
017 U
17 U
017 U
33 U
017 U
017 U
017 U
017 U
017 U
17 U
017 U
067 U
017 U
17 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
Data Package ID VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- Fe Page 1 of 8
UMS Version 6317A
12
GCMS Volatiles Method SW8260_25B
Sample Results
Lab Name ALS Laboratory Group - FC
Work Order Number 0911214
Client Name New Mexico nvironment Department OB
ClientProject 10 644-111809(HWB R-37 VOCs) PAR 002731703
Field 10 R-37 Scr 2-111809
Lab 10 0911214-1
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10ml
Moisture NA QCBatchlD VL091125-4-5 Final Volume 10ml
Date Collected l8-Nov-09 Run 10 VL091125-4A Result Units UGL
Date Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Analysis ReqCode 104 Date Analyzed 25-Nov-09 Basis As Received
Prep Method SW5030 Rev C File NameD28044
CASNO Target Analyte Dilution Factor
Result Reporting Limit
MDL Result Qualifier
EPA Qualifier
I
71-43-2 BENZENE 1 05 05 017 U
79-01-6 TRICHLOROETHENE 1 05 05 017 U
78-87-5
74middot95-3
75-27-4
10061-01-5
108middot10middot1
108middot88-3
10061-02middot6
79-00-5
591-78-6
12-DICHLOROPROPANE
DIBROMOMETHANE
BROMODCHLOROMETHANE
CIS-13-DICHLOROPROPEI~E
4-METHYL-2-PENTANONE
TOLUENE
TRANS-13-DICHLOROPROPENE
112-TRICHLOROETHANE
2-HEXANONE
1
1
1
1
1
1
1
1
1
05
05
05
05
5
031
05
05
10
05
05
05
05
5
05
05
05
10
017
017
017
017
17
017
017
017
17
U
U
U
U
U
J
U
U
U
127-18-4
142-28-9
124-48-1
106-93-4
108-90-7
630-20-6
100-41-4
136777-61-2
95-47-6
100-42middot5
75-25-2
98-82middot8
96-18-4
79-34-5
108-86-1
TETRACHLOROETHENE
13-DICHLOROPROPANE
DIBROMOCHLOROMETHANE
12-DIBROMOETHANE
CHLOROBENZENE
11 12-TETRACHLOROETHANE
ETHYLBENZENE
M+PmiddotXYLENE
OmiddotXYLENE
STYRENE
BROMOFORM
ISOPRO PYLBENZENE
123middotTRICHLOROPROPANE
1122-TETRACHLOROETHANE
BROMOBENZENE
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
05
05
1
1
05
05
05
1
05
05
05
05
2
05
05
05
05
1
1
05
05
05
1
05
05
05
05
2
05
05
017
017
017
017
017
017
017
017
017
017
017
017
017
017
017
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
i
Data Package 10 VL0911214-1
Date Printed Wednesday December 022009 AlS laboratory Group bullbull Fe Page 2 of 8
UMS Version 6317A
13
GCMS Volatiles Method SW8260_258
Sample Results
Lab Name ALS Laboratory Group bullbull FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject ID 644-111809(HWB R-37 VOCs) PAR 002731703
Field 10 R-37 Sor 2-111809
Lab ID 0911214middot1
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml
Moisture NA QCBatchlD VL091125-4-5 Final Volume 10 ml
Date Collected 18-Nov-09 Run ID VL091125-4A Result Units UGL
Date Extracted 25-Nov-09 Cleanup NONE Clean DF 1
Analysis ReqCode 104 Date Analyzed 25-Nov-09 Basis As Received
Prep Method SW5030 Rev C File Name 028044
CASNO Target Analyte Dilution Factor
103-65-1 NmiddotPROPYLBENZENE 1
95-49-8 2-CHLOROTOLUENE 1
108-67-8 135-TRIMETHYLBENZENE 1
106-43-4 4-CHLOROTOLUENE 1
98-06-6 TER I-BUTYLBENZENE 1
95-63-6 124-TRIMETHYLBENZENE 1
135-98-8 SEC-BUTYLBENZENE 1
541-73-1 13-OICHLOROBENZENE 1
99-87-6 P-ISOPROPYLTOLUENE 1
106-46-7 lA-DICHLOROBENZENE 1
104-51-8 N-BUTYLBENZENE 1
95-50-1 12-DICHLOROBENZENE 1
96-12-8 l2-DIBROMOmiddot3-CHLOROPROPANE 1
120-82-1 12A-TRICHLOROBENZENE 1
187-68-3 HEXACHLOROBUTADIENE 1
91-20-3 NAPHTHALENE 1
87-61middot6 123-TRICHLOROBENZENE 1
75-05-8 ACETONITRILE 1
107middot05middot1 ALLYL CHLORIDE 1
110-57-6 TRANS-14-DICHLORO-2-BUTENE 1
164-17-5 ETHANOL 1
97-63-2 ETHYL METHACRYLATE 1
78-83-1 ISOBUTYL ALCOHOL 1
126-98-7 METHACRYLONITRILE 1
80-62-6 METHYL METHACRYLATE 1
107-12-0 PROPIONITRILE 1
Result Reporting Limit
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
2 2
05 05
05 05
05 05
05 05
50 50
50 50
5 5
200 200
5 5
100 100
35 35
5 5
25 25
MDL Result EPA Qualifier Qualifier
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
067 U
017 U
017 U
017 U
017 U
83 U
017 U
U u 78 U
017 U
17 U
17 U
17 U
33 U
Data Package 10 VL0911214-1
Date Printed Wednesday December 022009 ALS Laboratory Group MM Fe Page 3 of 8
LlMS VerSion 6317A
14
GCMS Volati las Method SW8260_258
Sample Results
Lab Name ALS Laboratory Group - FC
Work Order Number 0911214
Client Name New Mexico Environment Department 08
ClientProject 10 644-111B09(HWB R-37 VOGs) PAR 002731703
Field 10 R-37 Ser 2-111809 Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10ml
Lab 10 0911214-1 Moisture NA
Date Collected 1B-Nov-09 QCBatchlO VL091125-4-5
Run 10 VL091125-4A
Final Volume 10ml
Result Units UGIL Date Extracted 25-Nov-09 Cleanup NONE Clean OF
Analysis ReqCode 104 Date Analyzed 25-Nov-09
Prep Method SW5030 Rev G Basis As Received
File Name 028044
CASNO Target Analyte Dilution Factor
Result Reporting Limit
MDL Result Qualifier
EPA Qualifier
126-99-8 CHLOROPRENE 1 5 5 017 U
75-65-0 TERT-BUTANOL 1 100 100 33 U
108-20-3 ISOPROPYL ETHER 1 2 2 033 U
637-92-3 ETHYL TERT-BUTYL ETHER 1 2 2 033 U
994-05-8 TERT-AMYL METHYL ETHER 1 2 2 033 U
67-72-1 HEXACHLOROETHANE 1 2 2 033 U
Surrogate Recovery
CASNO Surrogate Analyte Result Flag Spike Amount
Percent Recovery
Control Limits
460-00-4 4-BROMOFLUOHOBENZENE 246 25 98 82 - 121
1868-53-7 DIBROMOFLUOHOMETHANE 248 25 99 BO - 123
2037-26-5 TOLUENE-DB 258 25 103 85middot116
Data Package 10 VL0911214-1
Date Printed Wednesday December 022009 ALS Laboratory Group bullbull FC Page 4 of 8
LIMS Version 0317 A
15
GCMS Volati les Method SW8260_25B
Sample Results
Lab Name ALS Laboratory Group -- FC
Worlt Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-111809(HWB Rmiddot37 VOCs) PAR 002731703
Field 10 Rmiddot37 Scr jmiddot111809
Lab 10 0911214-2
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml Moisture NfA QCBatchID VL091125-4middot5 Final Volume 10 ml
Date Collected 18middotNov-09 Run 10 VL091125-4A Result Units UGfL Date Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Analysis ReqCode 104 Date Analyzed 25middotNov-09 Basis As Received Prep Method SW5030 Rev C File Name 028045
CASNO Target Analyte Dilution Factor
Result Reporting Limit
MOL Result Qualifier
EPA Qualifier
75-71-8 DICHLORODIFLUOROMETHANE 1 05 05 017 U
74-87-3 CHLOROMETHANE 1 05 05 017 U
75-01middot4 VINYL CHLORIDE 1 05 05 017 U
74-83-9 BROMOMETHANE 1 1 1 017 U
75middot00middot3 CHLOROETHANE j 05 05 017 U
75-69-4 TRICHLOROFLUOROMETHANE 1 05 05 017 U
107-02-8 ACROLEIN 1 100 100 17 U
i 75-35-4 11-DICHLOROETHENE 1 05 05 017 U
67-64middot1 ACETONE 1 10 10 33 U
74-8S-4 IODOMETHANE 1 5 5 017 U
75-15-0 CARBON DISULFIDE 1 10 10 017 U
75-09-2 METHYLENE CHLORIDE 1 1 1 017 U
156-60-5 TRANS-12-DICHLOROETHENE 1 05 05 017 U
1634-04-4 METHYL TERTIARY BUTYL ETHER 1 1 1 017 U
107-13-1 ACRYLONITRILE 1 10 10 17 U
75-34middot3 11-DICHLOROETHANE 05 05 017 U
i 108-05-4 VINYL ACETATE 1 10 10 067 U
115659-2 CISmiddot 2middotDICHLOROETHENE 1 05 05 017 U
178-933 2middotBUTANONE 1 5 5 17 U
74-97middot5 BROMOCHLOROMET HANE 1 1 1 017 U
67-66-3 CHLOROFORM 1 05 05 017 U
71-55middot6 111middotTRICHLOROETHANE 1 1 1 017 U
594-20-7 22middotDICHLOROPROPANE 1 05 05 017 U
56-23-5 CARBON TETRACHLORIDE 1 05 05 017 U
563-58-6 11middotDICHLOROPROPENE 1 05 05 017 U
107-06-2 12middotDICHL OROETHANE 1 05 05 017 U
Data Package ID VL0911214-1
Date Printed Wednesday December 022009 ALS Laboratory Group -- Fe Page 5 of 8
16
GCMS Volatiles Method SW8260_25B
Sample Results
Lab Name ALS Laboratory Group -- FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-111809(HW3 R-37 VOCs) PAR 002731703
Field 10 R-37 Scr 1-11 1809
Lab 10 0911214-2
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml
Moisture NIA QCBatchlO VL091125-4-5 Final Volume 10 ml
Date Collected 18-Nov-09 Run 10 VL091125-4A Result Units UGL
[late Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Analysis ReqCode 104 Date Analyzed 25-Nov-09
Prep Method SW5030 Rev C Basis As Received
File Name 028045
CASNO Target Analyte Dilution Factor
71-43-2 BENZENE 1
79-01-6 TRICHLOROETHENE 1
78-87-5 12-DICHLOROPROPANE 1
74-95-3 DIBROMOMETHANE 1
75-27-4 BROMODICHLOROMETHANE 1
10061-01-5 CIS-13-DICHLOROPROPENE 1
108-10-1 4-METHYL-2-PtNTANON 1
108-88-3 TOLUENE 1
10061-02-6 TRANS-13-DICHLOROPROPENE 1
79-00-5 112-TRICHLOROETHANE 1
591-78-6 2-HEXANONE 1
127-18-4 TETRACHLOROETHENE 1
142-28-9 13-DICHLOROPROPANt 1
124-48-1 DI3ROMOCHLOROMETHANE 1
106-93-4 12-DIBROMOETHANE 1
108-90-7 CHLOROBENZENE 1
OETHANE 1
- 1
LENE 1
ENE 1
ENE 1
OFORM 1
OPYlBENZENE 1
96-18-4 123-TRICHLOROPROPANE 1
79-34-5 1122-TETRACHLOROETHANE 1
108-86-1 BROMOBENZENE 1
Result Reporting Limit
05 05
05 05
05 05
05 05
05 05
05 05
5 5
025 05
05 05
05 05
10 10
05 05
05 05
1 1
1 1
05 05
05 05
05 05
1 1
05 05
05 05
05 05
05 05
2 2
05 05
05 05
MDL Result EPA Qualifier Qualifier
017 U
017 U
017 U
017 U
017 U
017 U
17 U
017 J
017 U
017 U
17 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
Data Package 10 VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- Fe Page 6 of 8
317A
17
GCMS Volatiles Method SW8260 _258
Sample Results
Lab Name ALS Laboratory Group -- FC
Work Order Number 0911214
Client Name New Mexico Environment Department 08
ClientProject 10 644-11S09(HWB R-37 VOCs) PAR 002731703
Field 10 Rmiddot37 Scr 1-111809
Lab 10 0911214-2
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml Moisture NA QCBatchlD VL091125-4-5 Final Volume 10 ml
Date Collected 18-Nov-09 Run 10 VL091125-4A Result Units UGL Date Extracted 25-Nol-09 Cleanup NONE Clean OF
Analysis ReqCode 104 Date Analyzed 25-Nov-09 Basis As Received Prep Method SW5030 Rev C File Name D28045
CASNO Target Analyte Dilution Factor
103-65-1 N-PROPYLBENZENE 1
95-49-8 2-CHLOROTOLUENE 1
108-67-8 135-TRIMETHYLBENZENE 1
106-43-4 4-CHLOROTOLUENE 1
98-06-6 TERT-BUTYLBENZENE 1
95-63-6 124-TRIMETHYLBENZENE 1
135-98-8 SEC-BUTYLBENZENE 1
i 541-73-1 13middotDICHLOROBENZENE 1
99-87-6 PmiddotISOPROPYL TOLUENE 1
106-46-7 I 14-DICHLOROBENZENE 1
104-51-8 I N-BUTYLBENZENE 1
95-50-1 l2-DICHLOROBENZENE 1
96-12-8 I 12-DIBROMO-3-CHLOROPROPANE 1
120-82-1 124-TRICHLOROBENZENE 1
87-68-3 HEXACHLOROBUT ADIENE 1
91-20-3 NAPHTHALENE 1
87-61-6 123-TRICHLOROBENZENE 1
75-05-S ACETONITRILE 1
107-05-1 ALLYL CH LORIDE 1
110-57-6 TRAN S-14-DICHLORO-2-BUTENE 1
64-17-5 ETHANOL 1
97-63-2 ETHYL METHACRYLATE 1
78-83-1 ISOBUTYL ALCOHOL 1
126-98-7 METHACRYLONITRILE 1
80-62-6 METHYL METHACRYLATE 1
107-12-0 I PROPIONITRILE 1
Result Reporting Limit
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
2 2
05 05
05 05
05 05
05 05
50 50
50 50 I 5 5
200 200
5 5
100 100
35 35
5 5
25 25
MDL
017
017
017
017
017
017
017
017
017
017
017
017
067
017
017
017
017
83
017
17
78
017
17
17
17
33
Result EPA Qualifier Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
Data Package 10 VL0911214-1
Date Printed Wednesday December 022009 ALS Laboratory Group -- Fe Page 7 of 8
LlMS Version 6317A
18
GCMS Volatiles Method SW8260_258
Sample Results
Lab Name ALS Laboratory Group bullbull FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644middot111B09(HWB R-37 VOCs) PAR 002731703
Sample Matrix WATER Prep Batch VL091125--4 Sample Aliquot 10 mlRmiddot37 Ser 1-111809 Moisture NA QCBatchlO VL091125--4-5 Final Volume 10 m
0911214-2 Date Collected 18-Nov-09 Run 10 VL091125--4A Result Units UGL Date Extracted 25-Nov-09 Cleanup NONE Clean OF 1 Date Analyzed 25-Nov-09 Basis As Received
10
Analysis ReqCode 104 Prep Method SW5030 Rev C File Name 028045
I
CASNO Target Analyte Dilution Factor
Result Reporting Limit
MDL Result Qualifier
EPA Qualifier
126-99-8 CHLOROPRENE 1 5 5 017 U
75-65-0 TERT-BUTANOL 1 100 100 33 U
108-20-3 ISOPROPYL ETHER 1 2 2 033 U
637-92-3 ETHYL TERT-BUTYL ETHER 1 2 2 033 U
994-05--8 TERT-AMYL MTHYL ETHER 1 2 2 033 U
67-72-1 HEXACHLOROETHANE 1 2 2 033 U
Surrogate Recovery
CASNO Surrogate Analyte Result Flag Spike Amount
Percent Control Recovery Limits
460-00-4 4middotBROMOFLUOROBENZENE 247 25 99 1
1868-53-7 DIBROMOFLUOROMETHANE 248 25 99 80 123
2037-26-5 TOLUENEmiddotDB 255 25 102 85 - 116
Data Package 10 VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- FC Page B of 8
LlMS Version 6317A
19
GCMS Volatiles Method SW8260_258
Laboratory Control Sample and Laboratory Control Sample Duplicate
Lab Name ALS Laboratory Group - FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-111809(HWB R-37 VOCs) PAR 002731703
Lab 10 VL091125-4LCS Sample Matrix WATER
Moisture NA Prep Batch VL091125-4
QCBatchlD VL091125-4-5
Sample Aliquot
Final Volume
10ml
10ml Date Collected NA Run 10 VL091125-4A Result Units UGIL Date Extracted 111252009 Cleanup NONE Clean OF 1 Date Analyzed 11252009 Basis NA
Prep Method SW5030C File Name 028040
CASNO
74-87-3
75-01-4
74-83-9
75-69-4
75-35-4
75-15-0
156-60-5
75-34-3
108-05-4
156-59-2
78-93-3
67 -66-3
71-55-6
i 56-23-5
107-06-2
71-43-2
79-01-6
78-87-5
75-27-4
108-88-3
79-00-5
591-78-6
127-18-4
106-93-4
108-90-7
63Q20-6
Target Analyte Spike Added
CHLOROMETHANE 10
VINYL CHLORIDE 10
BROMOMETHANE 10
TRICHLOROFLUOROMETHANE 10
11-DICHLOROETHENE 10
CARBON DISULFIDE 10
TRANS-12-DICHLOROETHENE 10
11-DICHLOROETHANE 10
VINYL ACETATE 10
CIS-12-DICHLOROETHENE 10
2middotBUTANONE 40
CHLOROFORM 10
111-TRICHL ORO ETHANE 10
CARBON TETRACHLORIDE 10
12-DICHLOROETHANE 10
BENZENE 10
TRICHLOROETHENE 10
12-DICHLOROPROPANE 10
BROMODICHLOROMETHANE 10
TOLUENE 10
112-TRICHLOROETHANE 10
2-HEXANONE 40
TETRACHLOROETHENE 10
12-DIBROMOETHANE 10
CHLOROBENZENE 10
1112-TETRACHLOROETHANE 10
LCS Reporting Result Result Limit Qualifier
932 05
863 05
943 1
908 05
96 05
95 10 J
996 05
992 05
10 10
102 05
412 5
993 05
974 1
943 05
106 05
983 05
962 05
10 05
988 05
974 05
989 05
409 10
956 05
991 1
984 05
101 05
LCS Control Rec Limits
93 49 -129
86 46 134
94 32-121
91 67 -152
96 61 -135
95 61 -140
100 70 -122
99 76 -119
100 62 182
102 75 126
103 61 -137
99 79 120
97 76 - 114
94 58middot135
106 75middot132
98 70 shy 125
96 74 121
100 81 -119
99 79 - 123
97 76 - 120
99 81 -126
102 45 168
96 56 -128
99 79 -123
98 75 -120
101 82 - 123
Data Package 10 VL0911214middot1
-Date Printed Wednesday December 02 2009 ALS Laboratory Group -- Fe Page 1 of 4
LiMS Version 6317A
20
GCMS Volatiles Method SW8260_25B
Laboratory Control Sample and Laboratory Control Sample Duplicate
Lab Name ALS Laboratory Group - FC
Work Order Number 0911214
Client Name New Mexico Envircnment Department OB
ClientProject 10 644-111809(HWB R-37 VOes) PAR 002731703
Lab 10 VL091125-4LCS Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml
Moisture NIA QCBatchlO VL091125-4-5 Final Volume 10 mi
Date Collected NA Run 10 VL091125-4A Result Units UGL Date Extracted 11252009 Cleanup NONE Clean OF 1 Date Analyzed 111252009 Basis NA
Prep Method SW5030e File Name 028040
CASNO Target Analyte Spike Added
LCS Result
Reporting Limit
Result Qualifier
LCS Rec
Control Limits
100-41-4 ETHYLBENZENE 10 981 05 98 79 -114
136777-61-2 M+P-XYLENE 20 197 1 98 81-115
95-47-6 O-XYLENE 10 101 05 101 81 -115
95-49-8 2-CHLOROTOLUENE 10 97 05 97 80 -128
541-73-1 13-DICHLOROBENZiNt 10 977 05 98 81-116
106-46-7 14-DICHLOROBENZENE 10 979 05 98 81 -119
95-50-1 12-DICHLOROBENZENE 10 987 05 99 79 - 116
91-20-3 NAPHTHALENE 10 993 05 99 69 -126
87-61-6 123-TRICHLOROBENZENE 10 999 05 100 60 -137
Data Package ID VL0911214-1
Date Printed Wecnesday December 02 2009 ALS Laboratory Group -- Fe Page 2 of 4
21
GCMS Volatiles Method SW8260_25B
Laboratory Control Sample and Laboratory Control Sample Duplicate
Lab Name ALS Laboratory Group bullbull FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-11 1809(HWB R-37 VOCs) PAR 002731703
Lab 10 VL091125middot4LCSD Sample Matrix WATER
Moisture NIA Prep Batch VL091125-4
QCBatchlD VL091125-4-5
Sample Aliquot
Final Volume
10 ml
10ml Date Collected NIA Run ID VL091125-4A Result Units UGIL Date Extracted 112512009 Cleanup NONE Clean DF 1 Date Analyzed 1112512009 Basis NIA
Prep Method SW5030C File Name 028041
CASNO Target Analyte Spike Added
LCSD Result
Reporting Limit
Result Qualifier
LCSD Rec
RPD Limit
RPD
74-87-3 CHLOROMETHANE 10 897 05 90 30 4
75-01-4 VINYL CHLORIDE 10 831 05 83 25 4
74-83-9 BROMO METHANE 10 945 1 94 25 0
75-69-4 TRICHLOROFLUOROMETHANE 10 873 05 87 22 4
75-35-4 11-DICHLOROETHENE 10 909 05 91 18 5
75-15-0 CARBON DISULFIDE 10 941 10 J 94 20 1
156-60middot5 TRANS-l2middotDICHLOROETHENE 10 961 05 96 25 4
75middot34middot3 11-DICHLOROETHANE 10 977 05 98 25 2
108-05-4 VINYL ACETATE 10 993 10 J 99 20 1
156middot59-2 CIS-12-DlCHLOROETHENE 10 995 05 99 25 3
i 78-93-3 2-BUTANONE 40 419 5 105 30 2
67-66-3 CHLOROFORM 10 985 05 99 25 1
71-55-6 lll-TRICHLOROETHANE 10 942 1 94 25 3
56-23-5 CARBON TETRACHLORIDE 10 922 05 92 25 2
107middot06-2 12middotDICHLOROETHANE 10 106 05 106 25 0
71-43middot2 BENZENE 10 971 05 97 10 1
79middot01middot6 TRICHLOROETHENE 10 939 05 94 10 2
78middot87middot5 l2middotDICHLOROPROPANE 10 101 05 101 25 1
i 75middot27-4 BROMODICHLOROMETHANE 10 992 05 99 25 0
1108-88-3 TOLUENE 10 962 05 96 9 1
I 79005 112middotTRICHLOROETHANE 10 986 05 99 25 0
591middot78middot6 2-HEXANONE 40 418 10 104 20 2
127middot18-4 TETRACHLOROETHENE 10 918 05 92 25 4
106-93-4 12middotDIBROMOETHANE 10 999 1 100 15 1
108middot90-7 CHLOROBENZENE 10 997 05 100 11 1
630-20middot6 1112-TETRACHLOROETHANE 10 101 05 101 15 0
100-41-4 ETHYLBENZENE 10 968 05 97 25 1
Data Package ID VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- FC Page 3 of 4
lIMS Version 6317 A
22
GCMS Volatiles Method SW8260_25B
Laboratory Control Sample and Laboratory Control Sample Duplicate
Lab Name ALS Laboratory 13roup -- FC
Work Order Number 0911214
Client Name New Mexico Environment Department OS
ClientProject 10 644-11 1809(HWB R-37 VOCs) PAR 002731703
Lab 10 VL091125-4LCSD Sample Matrix WATER
Moisture NA Prep Batch VL091125-4
QCBatchlO VL091125-4-5
Sample Aliquot
Final Volume
10 ml
10ml Date Collected NA Run 10 VL091125-4A Result Units UGL Date Extracted 11252009 Cleanup NONE Clean OF Date Analyzed 11252009 Basis NIA
Prep Method SW5030C File Name 028041
CASNO Target Analyte Spike Added
LCSD Result
Reporting Limit
Result Qualifier
LCSD Rec
RPD Limit
RPD
136777-61-2 M+P-XYLENE 20 193 1 97 25 2
95-47-6 O-XYLENE 10 983 05 98 25 2
95-49-8 2middotCHLOROTOLUENE 10 9A9 05 95 15 2
541-73-1 13middotDICHLOROBENZENE 10 997 05 100 25 2
106-46-7 14-DICHLOROBeNZENE 10 974 05 97 25 1
95-50middot1 12middotDICHLOROBENZeNE 10 101 05 101 25 2
91middot20-3 NAPHTHALENe 10 105 05 105 24 6
87-61-6 123-TRICHLOROBENZENE 10 102 05 102 33 3
Surrogate Recovery LCSLCSD
CASNO Target Analyte Spike Added
LCS Rec
LCS Flag
LCSD Rec
LCSD Flag
Control Limits
460middot00-4 4-BROMOFLUOROBeNZENE 25 100 100 82 - 121
1868-53middot7 DIBROMOFLUOROMeTHANE 25 101 100 80middot 123
2037middot26-5 TOLUENEmiddotD8 25 102 100 85middot 116
Data Package 10 VL0911214-
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- Fe Page 4 of 4
UMS Verslmt 6317A
23
GCMS Volati les Method SW8260 _258
Sample Results
Lab Name ALS Laboratory Group -- FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-111809(HWB R-37 VOCs) PAR 002731703
Field 10 Rmiddot37 Ser 2middot111809
Lab 10 0911214middot1
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml
Moisture NA QCBatchlO VL091125-4-5 Final Volume 10mi Date Collected 18-Nov-09 Run 10 VL091125-4A Result Units UGL
Date Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Analysis ReqCode 104 Date Analyzed 25-Nov-09
Prep Method SW5030 Rev C Basis As Received
File Name 028044
CASNO Target Analyte Dilution Factor
75-71-8 DICHLORODIFLUOROMETHANE 1
74middot87-3 CHLOROMETHANE 1
75-01-4 VINYL CHLORIDE 1
74-83-9 BROMOMETHANE 1
75-00-3 CHLOROETHANE 1
75-69-4 TRICHLOROFLUOROMETHANE 1
107-02-8 ACROLEIN 1
75-35-4 11middotDICHLOROETHENE 1
67-64-1 ACETONE 1
74-88-4 IODOMETHANE 1
75-15-0 CARBON DISULFIDE 1
75-09-2 METHYLENE CHLORIDE 1
156-60-5 TRANSmiddot12middotDICHLOROETHENE 1
1634-04-4 METHYL TERTIARY BUTYL ETHER 1
107-13-1 ACRYLONITRILE 1
75-34-3 1-DICHLOROETHANE 1
i 108-05-4 VINYL ACETATE 1
156-59-2 CIS-12middotDICHLOROETHENE 1
78-93-3 2-BUTANONE 1
74-97-5 BROMOCHLOROMETHANE 67-66-3 CHLOROFORM 1
71-55-6 11-TRICHLOROETHANE 594-20-7 22-DICHLOROPROPANE 56-23-5 CARBON TETRACHLORIDE 563-58-6 -DICHLOROPROPENE 107-06-2 2-DICHLOROETHANE
Result Reporting Limit
05 05
05 05
05 05
1 1
05 05
05 05
100 100
05 05
10 10
5 5
10 10
1 1
05 05
1 1
10 10
05 05
10 10
05 05
5 5
1 1
05 05
1 1
05 05
05 05
05 05
05 05
MOL Result EPA Qualifier Qualifier
017 U
017 U
017 U
017 U
017 U
017 U
17 U
017 U
33 U
017 U
017 U
017 U
017 U
017 U
17 U
017 U
067 U
017 U
17 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
Data Package ID VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- Fe Page 1 of 8
UMS Version 6317A
12
GCMS Volatiles Method SW8260_25B
Sample Results
Lab Name ALS Laboratory Group - FC
Work Order Number 0911214
Client Name New Mexico nvironment Department OB
ClientProject 10 644-111809(HWB R-37 VOCs) PAR 002731703
Field 10 R-37 Scr 2-111809
Lab 10 0911214-1
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10ml
Moisture NA QCBatchlD VL091125-4-5 Final Volume 10ml
Date Collected l8-Nov-09 Run 10 VL091125-4A Result Units UGL
Date Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Analysis ReqCode 104 Date Analyzed 25-Nov-09 Basis As Received
Prep Method SW5030 Rev C File NameD28044
CASNO Target Analyte Dilution Factor
Result Reporting Limit
MDL Result Qualifier
EPA Qualifier
I
71-43-2 BENZENE 1 05 05 017 U
79-01-6 TRICHLOROETHENE 1 05 05 017 U
78-87-5
74middot95-3
75-27-4
10061-01-5
108middot10middot1
108middot88-3
10061-02middot6
79-00-5
591-78-6
12-DICHLOROPROPANE
DIBROMOMETHANE
BROMODCHLOROMETHANE
CIS-13-DICHLOROPROPEI~E
4-METHYL-2-PENTANONE
TOLUENE
TRANS-13-DICHLOROPROPENE
112-TRICHLOROETHANE
2-HEXANONE
1
1
1
1
1
1
1
1
1
05
05
05
05
5
031
05
05
10
05
05
05
05
5
05
05
05
10
017
017
017
017
17
017
017
017
17
U
U
U
U
U
J
U
U
U
127-18-4
142-28-9
124-48-1
106-93-4
108-90-7
630-20-6
100-41-4
136777-61-2
95-47-6
100-42middot5
75-25-2
98-82middot8
96-18-4
79-34-5
108-86-1
TETRACHLOROETHENE
13-DICHLOROPROPANE
DIBROMOCHLOROMETHANE
12-DIBROMOETHANE
CHLOROBENZENE
11 12-TETRACHLOROETHANE
ETHYLBENZENE
M+PmiddotXYLENE
OmiddotXYLENE
STYRENE
BROMOFORM
ISOPRO PYLBENZENE
123middotTRICHLOROPROPANE
1122-TETRACHLOROETHANE
BROMOBENZENE
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
05
05
1
1
05
05
05
1
05
05
05
05
2
05
05
05
05
1
1
05
05
05
1
05
05
05
05
2
05
05
017
017
017
017
017
017
017
017
017
017
017
017
017
017
017
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
i
Data Package 10 VL0911214-1
Date Printed Wednesday December 022009 AlS laboratory Group bullbull Fe Page 2 of 8
UMS Version 6317A
13
GCMS Volatiles Method SW8260_258
Sample Results
Lab Name ALS Laboratory Group bullbull FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject ID 644-111809(HWB R-37 VOCs) PAR 002731703
Field 10 R-37 Sor 2-111809
Lab ID 0911214middot1
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml
Moisture NA QCBatchlD VL091125-4-5 Final Volume 10 ml
Date Collected 18-Nov-09 Run ID VL091125-4A Result Units UGL
Date Extracted 25-Nov-09 Cleanup NONE Clean DF 1
Analysis ReqCode 104 Date Analyzed 25-Nov-09 Basis As Received
Prep Method SW5030 Rev C File Name 028044
CASNO Target Analyte Dilution Factor
103-65-1 NmiddotPROPYLBENZENE 1
95-49-8 2-CHLOROTOLUENE 1
108-67-8 135-TRIMETHYLBENZENE 1
106-43-4 4-CHLOROTOLUENE 1
98-06-6 TER I-BUTYLBENZENE 1
95-63-6 124-TRIMETHYLBENZENE 1
135-98-8 SEC-BUTYLBENZENE 1
541-73-1 13-OICHLOROBENZENE 1
99-87-6 P-ISOPROPYLTOLUENE 1
106-46-7 lA-DICHLOROBENZENE 1
104-51-8 N-BUTYLBENZENE 1
95-50-1 12-DICHLOROBENZENE 1
96-12-8 l2-DIBROMOmiddot3-CHLOROPROPANE 1
120-82-1 12A-TRICHLOROBENZENE 1
187-68-3 HEXACHLOROBUTADIENE 1
91-20-3 NAPHTHALENE 1
87-61middot6 123-TRICHLOROBENZENE 1
75-05-8 ACETONITRILE 1
107middot05middot1 ALLYL CHLORIDE 1
110-57-6 TRANS-14-DICHLORO-2-BUTENE 1
164-17-5 ETHANOL 1
97-63-2 ETHYL METHACRYLATE 1
78-83-1 ISOBUTYL ALCOHOL 1
126-98-7 METHACRYLONITRILE 1
80-62-6 METHYL METHACRYLATE 1
107-12-0 PROPIONITRILE 1
Result Reporting Limit
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
2 2
05 05
05 05
05 05
05 05
50 50
50 50
5 5
200 200
5 5
100 100
35 35
5 5
25 25
MDL Result EPA Qualifier Qualifier
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
067 U
017 U
017 U
017 U
017 U
83 U
017 U
U u 78 U
017 U
17 U
17 U
17 U
33 U
Data Package 10 VL0911214-1
Date Printed Wednesday December 022009 ALS Laboratory Group MM Fe Page 3 of 8
LlMS VerSion 6317A
14
GCMS Volati las Method SW8260_258
Sample Results
Lab Name ALS Laboratory Group - FC
Work Order Number 0911214
Client Name New Mexico Environment Department 08
ClientProject 10 644-111B09(HWB R-37 VOGs) PAR 002731703
Field 10 R-37 Ser 2-111809 Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10ml
Lab 10 0911214-1 Moisture NA
Date Collected 1B-Nov-09 QCBatchlO VL091125-4-5
Run 10 VL091125-4A
Final Volume 10ml
Result Units UGIL Date Extracted 25-Nov-09 Cleanup NONE Clean OF
Analysis ReqCode 104 Date Analyzed 25-Nov-09
Prep Method SW5030 Rev G Basis As Received
File Name 028044
CASNO Target Analyte Dilution Factor
Result Reporting Limit
MDL Result Qualifier
EPA Qualifier
126-99-8 CHLOROPRENE 1 5 5 017 U
75-65-0 TERT-BUTANOL 1 100 100 33 U
108-20-3 ISOPROPYL ETHER 1 2 2 033 U
637-92-3 ETHYL TERT-BUTYL ETHER 1 2 2 033 U
994-05-8 TERT-AMYL METHYL ETHER 1 2 2 033 U
67-72-1 HEXACHLOROETHANE 1 2 2 033 U
Surrogate Recovery
CASNO Surrogate Analyte Result Flag Spike Amount
Percent Recovery
Control Limits
460-00-4 4-BROMOFLUOHOBENZENE 246 25 98 82 - 121
1868-53-7 DIBROMOFLUOHOMETHANE 248 25 99 BO - 123
2037-26-5 TOLUENE-DB 258 25 103 85middot116
Data Package 10 VL0911214-1
Date Printed Wednesday December 022009 ALS Laboratory Group bullbull FC Page 4 of 8
LIMS Version 0317 A
15
GCMS Volati les Method SW8260_25B
Sample Results
Lab Name ALS Laboratory Group -- FC
Worlt Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-111809(HWB Rmiddot37 VOCs) PAR 002731703
Field 10 Rmiddot37 Scr jmiddot111809
Lab 10 0911214-2
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml Moisture NfA QCBatchID VL091125-4middot5 Final Volume 10 ml
Date Collected 18middotNov-09 Run 10 VL091125-4A Result Units UGfL Date Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Analysis ReqCode 104 Date Analyzed 25middotNov-09 Basis As Received Prep Method SW5030 Rev C File Name 028045
CASNO Target Analyte Dilution Factor
Result Reporting Limit
MOL Result Qualifier
EPA Qualifier
75-71-8 DICHLORODIFLUOROMETHANE 1 05 05 017 U
74-87-3 CHLOROMETHANE 1 05 05 017 U
75-01middot4 VINYL CHLORIDE 1 05 05 017 U
74-83-9 BROMOMETHANE 1 1 1 017 U
75middot00middot3 CHLOROETHANE j 05 05 017 U
75-69-4 TRICHLOROFLUOROMETHANE 1 05 05 017 U
107-02-8 ACROLEIN 1 100 100 17 U
i 75-35-4 11-DICHLOROETHENE 1 05 05 017 U
67-64middot1 ACETONE 1 10 10 33 U
74-8S-4 IODOMETHANE 1 5 5 017 U
75-15-0 CARBON DISULFIDE 1 10 10 017 U
75-09-2 METHYLENE CHLORIDE 1 1 1 017 U
156-60-5 TRANS-12-DICHLOROETHENE 1 05 05 017 U
1634-04-4 METHYL TERTIARY BUTYL ETHER 1 1 1 017 U
107-13-1 ACRYLONITRILE 1 10 10 17 U
75-34middot3 11-DICHLOROETHANE 05 05 017 U
i 108-05-4 VINYL ACETATE 1 10 10 067 U
115659-2 CISmiddot 2middotDICHLOROETHENE 1 05 05 017 U
178-933 2middotBUTANONE 1 5 5 17 U
74-97middot5 BROMOCHLOROMET HANE 1 1 1 017 U
67-66-3 CHLOROFORM 1 05 05 017 U
71-55middot6 111middotTRICHLOROETHANE 1 1 1 017 U
594-20-7 22middotDICHLOROPROPANE 1 05 05 017 U
56-23-5 CARBON TETRACHLORIDE 1 05 05 017 U
563-58-6 11middotDICHLOROPROPENE 1 05 05 017 U
107-06-2 12middotDICHL OROETHANE 1 05 05 017 U
Data Package ID VL0911214-1
Date Printed Wednesday December 022009 ALS Laboratory Group -- Fe Page 5 of 8
16
GCMS Volatiles Method SW8260_25B
Sample Results
Lab Name ALS Laboratory Group -- FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-111809(HW3 R-37 VOCs) PAR 002731703
Field 10 R-37 Scr 1-11 1809
Lab 10 0911214-2
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml
Moisture NIA QCBatchlO VL091125-4-5 Final Volume 10 ml
Date Collected 18-Nov-09 Run 10 VL091125-4A Result Units UGL
[late Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Analysis ReqCode 104 Date Analyzed 25-Nov-09
Prep Method SW5030 Rev C Basis As Received
File Name 028045
CASNO Target Analyte Dilution Factor
71-43-2 BENZENE 1
79-01-6 TRICHLOROETHENE 1
78-87-5 12-DICHLOROPROPANE 1
74-95-3 DIBROMOMETHANE 1
75-27-4 BROMODICHLOROMETHANE 1
10061-01-5 CIS-13-DICHLOROPROPENE 1
108-10-1 4-METHYL-2-PtNTANON 1
108-88-3 TOLUENE 1
10061-02-6 TRANS-13-DICHLOROPROPENE 1
79-00-5 112-TRICHLOROETHANE 1
591-78-6 2-HEXANONE 1
127-18-4 TETRACHLOROETHENE 1
142-28-9 13-DICHLOROPROPANt 1
124-48-1 DI3ROMOCHLOROMETHANE 1
106-93-4 12-DIBROMOETHANE 1
108-90-7 CHLOROBENZENE 1
OETHANE 1
- 1
LENE 1
ENE 1
ENE 1
OFORM 1
OPYlBENZENE 1
96-18-4 123-TRICHLOROPROPANE 1
79-34-5 1122-TETRACHLOROETHANE 1
108-86-1 BROMOBENZENE 1
Result Reporting Limit
05 05
05 05
05 05
05 05
05 05
05 05
5 5
025 05
05 05
05 05
10 10
05 05
05 05
1 1
1 1
05 05
05 05
05 05
1 1
05 05
05 05
05 05
05 05
2 2
05 05
05 05
MDL Result EPA Qualifier Qualifier
017 U
017 U
017 U
017 U
017 U
017 U
17 U
017 J
017 U
017 U
17 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
Data Package 10 VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- Fe Page 6 of 8
317A
17
GCMS Volatiles Method SW8260 _258
Sample Results
Lab Name ALS Laboratory Group -- FC
Work Order Number 0911214
Client Name New Mexico Environment Department 08
ClientProject 10 644-11S09(HWB R-37 VOCs) PAR 002731703
Field 10 Rmiddot37 Scr 1-111809
Lab 10 0911214-2
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml Moisture NA QCBatchlD VL091125-4-5 Final Volume 10 ml
Date Collected 18-Nov-09 Run 10 VL091125-4A Result Units UGL Date Extracted 25-Nol-09 Cleanup NONE Clean OF
Analysis ReqCode 104 Date Analyzed 25-Nov-09 Basis As Received Prep Method SW5030 Rev C File Name D28045
CASNO Target Analyte Dilution Factor
103-65-1 N-PROPYLBENZENE 1
95-49-8 2-CHLOROTOLUENE 1
108-67-8 135-TRIMETHYLBENZENE 1
106-43-4 4-CHLOROTOLUENE 1
98-06-6 TERT-BUTYLBENZENE 1
95-63-6 124-TRIMETHYLBENZENE 1
135-98-8 SEC-BUTYLBENZENE 1
i 541-73-1 13middotDICHLOROBENZENE 1
99-87-6 PmiddotISOPROPYL TOLUENE 1
106-46-7 I 14-DICHLOROBENZENE 1
104-51-8 I N-BUTYLBENZENE 1
95-50-1 l2-DICHLOROBENZENE 1
96-12-8 I 12-DIBROMO-3-CHLOROPROPANE 1
120-82-1 124-TRICHLOROBENZENE 1
87-68-3 HEXACHLOROBUT ADIENE 1
91-20-3 NAPHTHALENE 1
87-61-6 123-TRICHLOROBENZENE 1
75-05-S ACETONITRILE 1
107-05-1 ALLYL CH LORIDE 1
110-57-6 TRAN S-14-DICHLORO-2-BUTENE 1
64-17-5 ETHANOL 1
97-63-2 ETHYL METHACRYLATE 1
78-83-1 ISOBUTYL ALCOHOL 1
126-98-7 METHACRYLONITRILE 1
80-62-6 METHYL METHACRYLATE 1
107-12-0 I PROPIONITRILE 1
Result Reporting Limit
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
2 2
05 05
05 05
05 05
05 05
50 50
50 50 I 5 5
200 200
5 5
100 100
35 35
5 5
25 25
MDL
017
017
017
017
017
017
017
017
017
017
017
017
067
017
017
017
017
83
017
17
78
017
17
17
17
33
Result EPA Qualifier Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
Data Package 10 VL0911214-1
Date Printed Wednesday December 022009 ALS Laboratory Group -- Fe Page 7 of 8
LlMS Version 6317A
18
GCMS Volatiles Method SW8260_258
Sample Results
Lab Name ALS Laboratory Group bullbull FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644middot111B09(HWB R-37 VOCs) PAR 002731703
Sample Matrix WATER Prep Batch VL091125--4 Sample Aliquot 10 mlRmiddot37 Ser 1-111809 Moisture NA QCBatchlO VL091125--4-5 Final Volume 10 m
0911214-2 Date Collected 18-Nov-09 Run 10 VL091125--4A Result Units UGL Date Extracted 25-Nov-09 Cleanup NONE Clean OF 1 Date Analyzed 25-Nov-09 Basis As Received
10
Analysis ReqCode 104 Prep Method SW5030 Rev C File Name 028045
I
CASNO Target Analyte Dilution Factor
Result Reporting Limit
MDL Result Qualifier
EPA Qualifier
126-99-8 CHLOROPRENE 1 5 5 017 U
75-65-0 TERT-BUTANOL 1 100 100 33 U
108-20-3 ISOPROPYL ETHER 1 2 2 033 U
637-92-3 ETHYL TERT-BUTYL ETHER 1 2 2 033 U
994-05--8 TERT-AMYL MTHYL ETHER 1 2 2 033 U
67-72-1 HEXACHLOROETHANE 1 2 2 033 U
Surrogate Recovery
CASNO Surrogate Analyte Result Flag Spike Amount
Percent Control Recovery Limits
460-00-4 4middotBROMOFLUOROBENZENE 247 25 99 1
1868-53-7 DIBROMOFLUOROMETHANE 248 25 99 80 123
2037-26-5 TOLUENEmiddotDB 255 25 102 85 - 116
Data Package 10 VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- FC Page B of 8
LlMS Version 6317A
19
GCMS Volatiles Method SW8260_258
Laboratory Control Sample and Laboratory Control Sample Duplicate
Lab Name ALS Laboratory Group - FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-111809(HWB R-37 VOCs) PAR 002731703
Lab 10 VL091125-4LCS Sample Matrix WATER
Moisture NA Prep Batch VL091125-4
QCBatchlD VL091125-4-5
Sample Aliquot
Final Volume
10ml
10ml Date Collected NA Run 10 VL091125-4A Result Units UGIL Date Extracted 111252009 Cleanup NONE Clean OF 1 Date Analyzed 11252009 Basis NA
Prep Method SW5030C File Name 028040
CASNO
74-87-3
75-01-4
74-83-9
75-69-4
75-35-4
75-15-0
156-60-5
75-34-3
108-05-4
156-59-2
78-93-3
67 -66-3
71-55-6
i 56-23-5
107-06-2
71-43-2
79-01-6
78-87-5
75-27-4
108-88-3
79-00-5
591-78-6
127-18-4
106-93-4
108-90-7
63Q20-6
Target Analyte Spike Added
CHLOROMETHANE 10
VINYL CHLORIDE 10
BROMOMETHANE 10
TRICHLOROFLUOROMETHANE 10
11-DICHLOROETHENE 10
CARBON DISULFIDE 10
TRANS-12-DICHLOROETHENE 10
11-DICHLOROETHANE 10
VINYL ACETATE 10
CIS-12-DICHLOROETHENE 10
2middotBUTANONE 40
CHLOROFORM 10
111-TRICHL ORO ETHANE 10
CARBON TETRACHLORIDE 10
12-DICHLOROETHANE 10
BENZENE 10
TRICHLOROETHENE 10
12-DICHLOROPROPANE 10
BROMODICHLOROMETHANE 10
TOLUENE 10
112-TRICHLOROETHANE 10
2-HEXANONE 40
TETRACHLOROETHENE 10
12-DIBROMOETHANE 10
CHLOROBENZENE 10
1112-TETRACHLOROETHANE 10
LCS Reporting Result Result Limit Qualifier
932 05
863 05
943 1
908 05
96 05
95 10 J
996 05
992 05
10 10
102 05
412 5
993 05
974 1
943 05
106 05
983 05
962 05
10 05
988 05
974 05
989 05
409 10
956 05
991 1
984 05
101 05
LCS Control Rec Limits
93 49 -129
86 46 134
94 32-121
91 67 -152
96 61 -135
95 61 -140
100 70 -122
99 76 -119
100 62 182
102 75 126
103 61 -137
99 79 120
97 76 - 114
94 58middot135
106 75middot132
98 70 shy 125
96 74 121
100 81 -119
99 79 - 123
97 76 - 120
99 81 -126
102 45 168
96 56 -128
99 79 -123
98 75 -120
101 82 - 123
Data Package 10 VL0911214middot1
-Date Printed Wednesday December 02 2009 ALS Laboratory Group -- Fe Page 1 of 4
LiMS Version 6317A
20
GCMS Volatiles Method SW8260_25B
Laboratory Control Sample and Laboratory Control Sample Duplicate
Lab Name ALS Laboratory Group - FC
Work Order Number 0911214
Client Name New Mexico Envircnment Department OB
ClientProject 10 644-111809(HWB R-37 VOes) PAR 002731703
Lab 10 VL091125-4LCS Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml
Moisture NIA QCBatchlO VL091125-4-5 Final Volume 10 mi
Date Collected NA Run 10 VL091125-4A Result Units UGL Date Extracted 11252009 Cleanup NONE Clean OF 1 Date Analyzed 111252009 Basis NA
Prep Method SW5030e File Name 028040
CASNO Target Analyte Spike Added
LCS Result
Reporting Limit
Result Qualifier
LCS Rec
Control Limits
100-41-4 ETHYLBENZENE 10 981 05 98 79 -114
136777-61-2 M+P-XYLENE 20 197 1 98 81-115
95-47-6 O-XYLENE 10 101 05 101 81 -115
95-49-8 2-CHLOROTOLUENE 10 97 05 97 80 -128
541-73-1 13-DICHLOROBENZiNt 10 977 05 98 81-116
106-46-7 14-DICHLOROBENZENE 10 979 05 98 81 -119
95-50-1 12-DICHLOROBENZENE 10 987 05 99 79 - 116
91-20-3 NAPHTHALENE 10 993 05 99 69 -126
87-61-6 123-TRICHLOROBENZENE 10 999 05 100 60 -137
Data Package ID VL0911214-1
Date Printed Wecnesday December 02 2009 ALS Laboratory Group -- Fe Page 2 of 4
21
GCMS Volatiles Method SW8260_25B
Laboratory Control Sample and Laboratory Control Sample Duplicate
Lab Name ALS Laboratory Group bullbull FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-11 1809(HWB R-37 VOCs) PAR 002731703
Lab 10 VL091125middot4LCSD Sample Matrix WATER
Moisture NIA Prep Batch VL091125-4
QCBatchlD VL091125-4-5
Sample Aliquot
Final Volume
10 ml
10ml Date Collected NIA Run ID VL091125-4A Result Units UGIL Date Extracted 112512009 Cleanup NONE Clean DF 1 Date Analyzed 1112512009 Basis NIA
Prep Method SW5030C File Name 028041
CASNO Target Analyte Spike Added
LCSD Result
Reporting Limit
Result Qualifier
LCSD Rec
RPD Limit
RPD
74-87-3 CHLOROMETHANE 10 897 05 90 30 4
75-01-4 VINYL CHLORIDE 10 831 05 83 25 4
74-83-9 BROMO METHANE 10 945 1 94 25 0
75-69-4 TRICHLOROFLUOROMETHANE 10 873 05 87 22 4
75-35-4 11-DICHLOROETHENE 10 909 05 91 18 5
75-15-0 CARBON DISULFIDE 10 941 10 J 94 20 1
156-60middot5 TRANS-l2middotDICHLOROETHENE 10 961 05 96 25 4
75middot34middot3 11-DICHLOROETHANE 10 977 05 98 25 2
108-05-4 VINYL ACETATE 10 993 10 J 99 20 1
156middot59-2 CIS-12-DlCHLOROETHENE 10 995 05 99 25 3
i 78-93-3 2-BUTANONE 40 419 5 105 30 2
67-66-3 CHLOROFORM 10 985 05 99 25 1
71-55-6 lll-TRICHLOROETHANE 10 942 1 94 25 3
56-23-5 CARBON TETRACHLORIDE 10 922 05 92 25 2
107middot06-2 12middotDICHLOROETHANE 10 106 05 106 25 0
71-43middot2 BENZENE 10 971 05 97 10 1
79middot01middot6 TRICHLOROETHENE 10 939 05 94 10 2
78middot87middot5 l2middotDICHLOROPROPANE 10 101 05 101 25 1
i 75middot27-4 BROMODICHLOROMETHANE 10 992 05 99 25 0
1108-88-3 TOLUENE 10 962 05 96 9 1
I 79005 112middotTRICHLOROETHANE 10 986 05 99 25 0
591middot78middot6 2-HEXANONE 40 418 10 104 20 2
127middot18-4 TETRACHLOROETHENE 10 918 05 92 25 4
106-93-4 12middotDIBROMOETHANE 10 999 1 100 15 1
108middot90-7 CHLOROBENZENE 10 997 05 100 11 1
630-20middot6 1112-TETRACHLOROETHANE 10 101 05 101 15 0
100-41-4 ETHYLBENZENE 10 968 05 97 25 1
Data Package ID VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- FC Page 3 of 4
lIMS Version 6317 A
22
GCMS Volatiles Method SW8260_25B
Laboratory Control Sample and Laboratory Control Sample Duplicate
Lab Name ALS Laboratory 13roup -- FC
Work Order Number 0911214
Client Name New Mexico Environment Department OS
ClientProject 10 644-11 1809(HWB R-37 VOCs) PAR 002731703
Lab 10 VL091125-4LCSD Sample Matrix WATER
Moisture NA Prep Batch VL091125-4
QCBatchlO VL091125-4-5
Sample Aliquot
Final Volume
10 ml
10ml Date Collected NA Run 10 VL091125-4A Result Units UGL Date Extracted 11252009 Cleanup NONE Clean OF Date Analyzed 11252009 Basis NIA
Prep Method SW5030C File Name 028041
CASNO Target Analyte Spike Added
LCSD Result
Reporting Limit
Result Qualifier
LCSD Rec
RPD Limit
RPD
136777-61-2 M+P-XYLENE 20 193 1 97 25 2
95-47-6 O-XYLENE 10 983 05 98 25 2
95-49-8 2middotCHLOROTOLUENE 10 9A9 05 95 15 2
541-73-1 13middotDICHLOROBENZENE 10 997 05 100 25 2
106-46-7 14-DICHLOROBeNZENE 10 974 05 97 25 1
95-50middot1 12middotDICHLOROBENZeNE 10 101 05 101 25 2
91middot20-3 NAPHTHALENe 10 105 05 105 24 6
87-61-6 123-TRICHLOROBENZENE 10 102 05 102 33 3
Surrogate Recovery LCSLCSD
CASNO Target Analyte Spike Added
LCS Rec
LCS Flag
LCSD Rec
LCSD Flag
Control Limits
460middot00-4 4-BROMOFLUOROBeNZENE 25 100 100 82 - 121
1868-53middot7 DIBROMOFLUOROMeTHANE 25 101 100 80middot 123
2037middot26-5 TOLUENEmiddotD8 25 102 100 85middot 116
Data Package 10 VL0911214-
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- Fe Page 4 of 4
UMS Verslmt 6317A
23
GCMS Volatiles Method SW8260_25B
Sample Results
Lab Name ALS Laboratory Group - FC
Work Order Number 0911214
Client Name New Mexico nvironment Department OB
ClientProject 10 644-111809(HWB R-37 VOCs) PAR 002731703
Field 10 R-37 Scr 2-111809
Lab 10 0911214-1
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10ml
Moisture NA QCBatchlD VL091125-4-5 Final Volume 10ml
Date Collected l8-Nov-09 Run 10 VL091125-4A Result Units UGL
Date Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Analysis ReqCode 104 Date Analyzed 25-Nov-09 Basis As Received
Prep Method SW5030 Rev C File NameD28044
CASNO Target Analyte Dilution Factor
Result Reporting Limit
MDL Result Qualifier
EPA Qualifier
I
71-43-2 BENZENE 1 05 05 017 U
79-01-6 TRICHLOROETHENE 1 05 05 017 U
78-87-5
74middot95-3
75-27-4
10061-01-5
108middot10middot1
108middot88-3
10061-02middot6
79-00-5
591-78-6
12-DICHLOROPROPANE
DIBROMOMETHANE
BROMODCHLOROMETHANE
CIS-13-DICHLOROPROPEI~E
4-METHYL-2-PENTANONE
TOLUENE
TRANS-13-DICHLOROPROPENE
112-TRICHLOROETHANE
2-HEXANONE
1
1
1
1
1
1
1
1
1
05
05
05
05
5
031
05
05
10
05
05
05
05
5
05
05
05
10
017
017
017
017
17
017
017
017
17
U
U
U
U
U
J
U
U
U
127-18-4
142-28-9
124-48-1
106-93-4
108-90-7
630-20-6
100-41-4
136777-61-2
95-47-6
100-42middot5
75-25-2
98-82middot8
96-18-4
79-34-5
108-86-1
TETRACHLOROETHENE
13-DICHLOROPROPANE
DIBROMOCHLOROMETHANE
12-DIBROMOETHANE
CHLOROBENZENE
11 12-TETRACHLOROETHANE
ETHYLBENZENE
M+PmiddotXYLENE
OmiddotXYLENE
STYRENE
BROMOFORM
ISOPRO PYLBENZENE
123middotTRICHLOROPROPANE
1122-TETRACHLOROETHANE
BROMOBENZENE
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
05
05
1
1
05
05
05
1
05
05
05
05
2
05
05
05
05
1
1
05
05
05
1
05
05
05
05
2
05
05
017
017
017
017
017
017
017
017
017
017
017
017
017
017
017
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
i
Data Package 10 VL0911214-1
Date Printed Wednesday December 022009 AlS laboratory Group bullbull Fe Page 2 of 8
UMS Version 6317A
13
GCMS Volatiles Method SW8260_258
Sample Results
Lab Name ALS Laboratory Group bullbull FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject ID 644-111809(HWB R-37 VOCs) PAR 002731703
Field 10 R-37 Sor 2-111809
Lab ID 0911214middot1
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml
Moisture NA QCBatchlD VL091125-4-5 Final Volume 10 ml
Date Collected 18-Nov-09 Run ID VL091125-4A Result Units UGL
Date Extracted 25-Nov-09 Cleanup NONE Clean DF 1
Analysis ReqCode 104 Date Analyzed 25-Nov-09 Basis As Received
Prep Method SW5030 Rev C File Name 028044
CASNO Target Analyte Dilution Factor
103-65-1 NmiddotPROPYLBENZENE 1
95-49-8 2-CHLOROTOLUENE 1
108-67-8 135-TRIMETHYLBENZENE 1
106-43-4 4-CHLOROTOLUENE 1
98-06-6 TER I-BUTYLBENZENE 1
95-63-6 124-TRIMETHYLBENZENE 1
135-98-8 SEC-BUTYLBENZENE 1
541-73-1 13-OICHLOROBENZENE 1
99-87-6 P-ISOPROPYLTOLUENE 1
106-46-7 lA-DICHLOROBENZENE 1
104-51-8 N-BUTYLBENZENE 1
95-50-1 12-DICHLOROBENZENE 1
96-12-8 l2-DIBROMOmiddot3-CHLOROPROPANE 1
120-82-1 12A-TRICHLOROBENZENE 1
187-68-3 HEXACHLOROBUTADIENE 1
91-20-3 NAPHTHALENE 1
87-61middot6 123-TRICHLOROBENZENE 1
75-05-8 ACETONITRILE 1
107middot05middot1 ALLYL CHLORIDE 1
110-57-6 TRANS-14-DICHLORO-2-BUTENE 1
164-17-5 ETHANOL 1
97-63-2 ETHYL METHACRYLATE 1
78-83-1 ISOBUTYL ALCOHOL 1
126-98-7 METHACRYLONITRILE 1
80-62-6 METHYL METHACRYLATE 1
107-12-0 PROPIONITRILE 1
Result Reporting Limit
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
2 2
05 05
05 05
05 05
05 05
50 50
50 50
5 5
200 200
5 5
100 100
35 35
5 5
25 25
MDL Result EPA Qualifier Qualifier
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
067 U
017 U
017 U
017 U
017 U
83 U
017 U
U u 78 U
017 U
17 U
17 U
17 U
33 U
Data Package 10 VL0911214-1
Date Printed Wednesday December 022009 ALS Laboratory Group MM Fe Page 3 of 8
LlMS VerSion 6317A
14
GCMS Volati las Method SW8260_258
Sample Results
Lab Name ALS Laboratory Group - FC
Work Order Number 0911214
Client Name New Mexico Environment Department 08
ClientProject 10 644-111B09(HWB R-37 VOGs) PAR 002731703
Field 10 R-37 Ser 2-111809 Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10ml
Lab 10 0911214-1 Moisture NA
Date Collected 1B-Nov-09 QCBatchlO VL091125-4-5
Run 10 VL091125-4A
Final Volume 10ml
Result Units UGIL Date Extracted 25-Nov-09 Cleanup NONE Clean OF
Analysis ReqCode 104 Date Analyzed 25-Nov-09
Prep Method SW5030 Rev G Basis As Received
File Name 028044
CASNO Target Analyte Dilution Factor
Result Reporting Limit
MDL Result Qualifier
EPA Qualifier
126-99-8 CHLOROPRENE 1 5 5 017 U
75-65-0 TERT-BUTANOL 1 100 100 33 U
108-20-3 ISOPROPYL ETHER 1 2 2 033 U
637-92-3 ETHYL TERT-BUTYL ETHER 1 2 2 033 U
994-05-8 TERT-AMYL METHYL ETHER 1 2 2 033 U
67-72-1 HEXACHLOROETHANE 1 2 2 033 U
Surrogate Recovery
CASNO Surrogate Analyte Result Flag Spike Amount
Percent Recovery
Control Limits
460-00-4 4-BROMOFLUOHOBENZENE 246 25 98 82 - 121
1868-53-7 DIBROMOFLUOHOMETHANE 248 25 99 BO - 123
2037-26-5 TOLUENE-DB 258 25 103 85middot116
Data Package 10 VL0911214-1
Date Printed Wednesday December 022009 ALS Laboratory Group bullbull FC Page 4 of 8
LIMS Version 0317 A
15
GCMS Volati les Method SW8260_25B
Sample Results
Lab Name ALS Laboratory Group -- FC
Worlt Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-111809(HWB Rmiddot37 VOCs) PAR 002731703
Field 10 Rmiddot37 Scr jmiddot111809
Lab 10 0911214-2
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml Moisture NfA QCBatchID VL091125-4middot5 Final Volume 10 ml
Date Collected 18middotNov-09 Run 10 VL091125-4A Result Units UGfL Date Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Analysis ReqCode 104 Date Analyzed 25middotNov-09 Basis As Received Prep Method SW5030 Rev C File Name 028045
CASNO Target Analyte Dilution Factor
Result Reporting Limit
MOL Result Qualifier
EPA Qualifier
75-71-8 DICHLORODIFLUOROMETHANE 1 05 05 017 U
74-87-3 CHLOROMETHANE 1 05 05 017 U
75-01middot4 VINYL CHLORIDE 1 05 05 017 U
74-83-9 BROMOMETHANE 1 1 1 017 U
75middot00middot3 CHLOROETHANE j 05 05 017 U
75-69-4 TRICHLOROFLUOROMETHANE 1 05 05 017 U
107-02-8 ACROLEIN 1 100 100 17 U
i 75-35-4 11-DICHLOROETHENE 1 05 05 017 U
67-64middot1 ACETONE 1 10 10 33 U
74-8S-4 IODOMETHANE 1 5 5 017 U
75-15-0 CARBON DISULFIDE 1 10 10 017 U
75-09-2 METHYLENE CHLORIDE 1 1 1 017 U
156-60-5 TRANS-12-DICHLOROETHENE 1 05 05 017 U
1634-04-4 METHYL TERTIARY BUTYL ETHER 1 1 1 017 U
107-13-1 ACRYLONITRILE 1 10 10 17 U
75-34middot3 11-DICHLOROETHANE 05 05 017 U
i 108-05-4 VINYL ACETATE 1 10 10 067 U
115659-2 CISmiddot 2middotDICHLOROETHENE 1 05 05 017 U
178-933 2middotBUTANONE 1 5 5 17 U
74-97middot5 BROMOCHLOROMET HANE 1 1 1 017 U
67-66-3 CHLOROFORM 1 05 05 017 U
71-55middot6 111middotTRICHLOROETHANE 1 1 1 017 U
594-20-7 22middotDICHLOROPROPANE 1 05 05 017 U
56-23-5 CARBON TETRACHLORIDE 1 05 05 017 U
563-58-6 11middotDICHLOROPROPENE 1 05 05 017 U
107-06-2 12middotDICHL OROETHANE 1 05 05 017 U
Data Package ID VL0911214-1
Date Printed Wednesday December 022009 ALS Laboratory Group -- Fe Page 5 of 8
16
GCMS Volatiles Method SW8260_25B
Sample Results
Lab Name ALS Laboratory Group -- FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-111809(HW3 R-37 VOCs) PAR 002731703
Field 10 R-37 Scr 1-11 1809
Lab 10 0911214-2
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml
Moisture NIA QCBatchlO VL091125-4-5 Final Volume 10 ml
Date Collected 18-Nov-09 Run 10 VL091125-4A Result Units UGL
[late Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Analysis ReqCode 104 Date Analyzed 25-Nov-09
Prep Method SW5030 Rev C Basis As Received
File Name 028045
CASNO Target Analyte Dilution Factor
71-43-2 BENZENE 1
79-01-6 TRICHLOROETHENE 1
78-87-5 12-DICHLOROPROPANE 1
74-95-3 DIBROMOMETHANE 1
75-27-4 BROMODICHLOROMETHANE 1
10061-01-5 CIS-13-DICHLOROPROPENE 1
108-10-1 4-METHYL-2-PtNTANON 1
108-88-3 TOLUENE 1
10061-02-6 TRANS-13-DICHLOROPROPENE 1
79-00-5 112-TRICHLOROETHANE 1
591-78-6 2-HEXANONE 1
127-18-4 TETRACHLOROETHENE 1
142-28-9 13-DICHLOROPROPANt 1
124-48-1 DI3ROMOCHLOROMETHANE 1
106-93-4 12-DIBROMOETHANE 1
108-90-7 CHLOROBENZENE 1
OETHANE 1
- 1
LENE 1
ENE 1
ENE 1
OFORM 1
OPYlBENZENE 1
96-18-4 123-TRICHLOROPROPANE 1
79-34-5 1122-TETRACHLOROETHANE 1
108-86-1 BROMOBENZENE 1
Result Reporting Limit
05 05
05 05
05 05
05 05
05 05
05 05
5 5
025 05
05 05
05 05
10 10
05 05
05 05
1 1
1 1
05 05
05 05
05 05
1 1
05 05
05 05
05 05
05 05
2 2
05 05
05 05
MDL Result EPA Qualifier Qualifier
017 U
017 U
017 U
017 U
017 U
017 U
17 U
017 J
017 U
017 U
17 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
Data Package 10 VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- Fe Page 6 of 8
317A
17
GCMS Volatiles Method SW8260 _258
Sample Results
Lab Name ALS Laboratory Group -- FC
Work Order Number 0911214
Client Name New Mexico Environment Department 08
ClientProject 10 644-11S09(HWB R-37 VOCs) PAR 002731703
Field 10 Rmiddot37 Scr 1-111809
Lab 10 0911214-2
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml Moisture NA QCBatchlD VL091125-4-5 Final Volume 10 ml
Date Collected 18-Nov-09 Run 10 VL091125-4A Result Units UGL Date Extracted 25-Nol-09 Cleanup NONE Clean OF
Analysis ReqCode 104 Date Analyzed 25-Nov-09 Basis As Received Prep Method SW5030 Rev C File Name D28045
CASNO Target Analyte Dilution Factor
103-65-1 N-PROPYLBENZENE 1
95-49-8 2-CHLOROTOLUENE 1
108-67-8 135-TRIMETHYLBENZENE 1
106-43-4 4-CHLOROTOLUENE 1
98-06-6 TERT-BUTYLBENZENE 1
95-63-6 124-TRIMETHYLBENZENE 1
135-98-8 SEC-BUTYLBENZENE 1
i 541-73-1 13middotDICHLOROBENZENE 1
99-87-6 PmiddotISOPROPYL TOLUENE 1
106-46-7 I 14-DICHLOROBENZENE 1
104-51-8 I N-BUTYLBENZENE 1
95-50-1 l2-DICHLOROBENZENE 1
96-12-8 I 12-DIBROMO-3-CHLOROPROPANE 1
120-82-1 124-TRICHLOROBENZENE 1
87-68-3 HEXACHLOROBUT ADIENE 1
91-20-3 NAPHTHALENE 1
87-61-6 123-TRICHLOROBENZENE 1
75-05-S ACETONITRILE 1
107-05-1 ALLYL CH LORIDE 1
110-57-6 TRAN S-14-DICHLORO-2-BUTENE 1
64-17-5 ETHANOL 1
97-63-2 ETHYL METHACRYLATE 1
78-83-1 ISOBUTYL ALCOHOL 1
126-98-7 METHACRYLONITRILE 1
80-62-6 METHYL METHACRYLATE 1
107-12-0 I PROPIONITRILE 1
Result Reporting Limit
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
2 2
05 05
05 05
05 05
05 05
50 50
50 50 I 5 5
200 200
5 5
100 100
35 35
5 5
25 25
MDL
017
017
017
017
017
017
017
017
017
017
017
017
067
017
017
017
017
83
017
17
78
017
17
17
17
33
Result EPA Qualifier Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
Data Package 10 VL0911214-1
Date Printed Wednesday December 022009 ALS Laboratory Group -- Fe Page 7 of 8
LlMS Version 6317A
18
GCMS Volatiles Method SW8260_258
Sample Results
Lab Name ALS Laboratory Group bullbull FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644middot111B09(HWB R-37 VOCs) PAR 002731703
Sample Matrix WATER Prep Batch VL091125--4 Sample Aliquot 10 mlRmiddot37 Ser 1-111809 Moisture NA QCBatchlO VL091125--4-5 Final Volume 10 m
0911214-2 Date Collected 18-Nov-09 Run 10 VL091125--4A Result Units UGL Date Extracted 25-Nov-09 Cleanup NONE Clean OF 1 Date Analyzed 25-Nov-09 Basis As Received
10
Analysis ReqCode 104 Prep Method SW5030 Rev C File Name 028045
I
CASNO Target Analyte Dilution Factor
Result Reporting Limit
MDL Result Qualifier
EPA Qualifier
126-99-8 CHLOROPRENE 1 5 5 017 U
75-65-0 TERT-BUTANOL 1 100 100 33 U
108-20-3 ISOPROPYL ETHER 1 2 2 033 U
637-92-3 ETHYL TERT-BUTYL ETHER 1 2 2 033 U
994-05--8 TERT-AMYL MTHYL ETHER 1 2 2 033 U
67-72-1 HEXACHLOROETHANE 1 2 2 033 U
Surrogate Recovery
CASNO Surrogate Analyte Result Flag Spike Amount
Percent Control Recovery Limits
460-00-4 4middotBROMOFLUOROBENZENE 247 25 99 1
1868-53-7 DIBROMOFLUOROMETHANE 248 25 99 80 123
2037-26-5 TOLUENEmiddotDB 255 25 102 85 - 116
Data Package 10 VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- FC Page B of 8
LlMS Version 6317A
19
GCMS Volatiles Method SW8260_258
Laboratory Control Sample and Laboratory Control Sample Duplicate
Lab Name ALS Laboratory Group - FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-111809(HWB R-37 VOCs) PAR 002731703
Lab 10 VL091125-4LCS Sample Matrix WATER
Moisture NA Prep Batch VL091125-4
QCBatchlD VL091125-4-5
Sample Aliquot
Final Volume
10ml
10ml Date Collected NA Run 10 VL091125-4A Result Units UGIL Date Extracted 111252009 Cleanup NONE Clean OF 1 Date Analyzed 11252009 Basis NA
Prep Method SW5030C File Name 028040
CASNO
74-87-3
75-01-4
74-83-9
75-69-4
75-35-4
75-15-0
156-60-5
75-34-3
108-05-4
156-59-2
78-93-3
67 -66-3
71-55-6
i 56-23-5
107-06-2
71-43-2
79-01-6
78-87-5
75-27-4
108-88-3
79-00-5
591-78-6
127-18-4
106-93-4
108-90-7
63Q20-6
Target Analyte Spike Added
CHLOROMETHANE 10
VINYL CHLORIDE 10
BROMOMETHANE 10
TRICHLOROFLUOROMETHANE 10
11-DICHLOROETHENE 10
CARBON DISULFIDE 10
TRANS-12-DICHLOROETHENE 10
11-DICHLOROETHANE 10
VINYL ACETATE 10
CIS-12-DICHLOROETHENE 10
2middotBUTANONE 40
CHLOROFORM 10
111-TRICHL ORO ETHANE 10
CARBON TETRACHLORIDE 10
12-DICHLOROETHANE 10
BENZENE 10
TRICHLOROETHENE 10
12-DICHLOROPROPANE 10
BROMODICHLOROMETHANE 10
TOLUENE 10
112-TRICHLOROETHANE 10
2-HEXANONE 40
TETRACHLOROETHENE 10
12-DIBROMOETHANE 10
CHLOROBENZENE 10
1112-TETRACHLOROETHANE 10
LCS Reporting Result Result Limit Qualifier
932 05
863 05
943 1
908 05
96 05
95 10 J
996 05
992 05
10 10
102 05
412 5
993 05
974 1
943 05
106 05
983 05
962 05
10 05
988 05
974 05
989 05
409 10
956 05
991 1
984 05
101 05
LCS Control Rec Limits
93 49 -129
86 46 134
94 32-121
91 67 -152
96 61 -135
95 61 -140
100 70 -122
99 76 -119
100 62 182
102 75 126
103 61 -137
99 79 120
97 76 - 114
94 58middot135
106 75middot132
98 70 shy 125
96 74 121
100 81 -119
99 79 - 123
97 76 - 120
99 81 -126
102 45 168
96 56 -128
99 79 -123
98 75 -120
101 82 - 123
Data Package 10 VL0911214middot1
-Date Printed Wednesday December 02 2009 ALS Laboratory Group -- Fe Page 1 of 4
LiMS Version 6317A
20
GCMS Volatiles Method SW8260_25B
Laboratory Control Sample and Laboratory Control Sample Duplicate
Lab Name ALS Laboratory Group - FC
Work Order Number 0911214
Client Name New Mexico Envircnment Department OB
ClientProject 10 644-111809(HWB R-37 VOes) PAR 002731703
Lab 10 VL091125-4LCS Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml
Moisture NIA QCBatchlO VL091125-4-5 Final Volume 10 mi
Date Collected NA Run 10 VL091125-4A Result Units UGL Date Extracted 11252009 Cleanup NONE Clean OF 1 Date Analyzed 111252009 Basis NA
Prep Method SW5030e File Name 028040
CASNO Target Analyte Spike Added
LCS Result
Reporting Limit
Result Qualifier
LCS Rec
Control Limits
100-41-4 ETHYLBENZENE 10 981 05 98 79 -114
136777-61-2 M+P-XYLENE 20 197 1 98 81-115
95-47-6 O-XYLENE 10 101 05 101 81 -115
95-49-8 2-CHLOROTOLUENE 10 97 05 97 80 -128
541-73-1 13-DICHLOROBENZiNt 10 977 05 98 81-116
106-46-7 14-DICHLOROBENZENE 10 979 05 98 81 -119
95-50-1 12-DICHLOROBENZENE 10 987 05 99 79 - 116
91-20-3 NAPHTHALENE 10 993 05 99 69 -126
87-61-6 123-TRICHLOROBENZENE 10 999 05 100 60 -137
Data Package ID VL0911214-1
Date Printed Wecnesday December 02 2009 ALS Laboratory Group -- Fe Page 2 of 4
21
GCMS Volatiles Method SW8260_25B
Laboratory Control Sample and Laboratory Control Sample Duplicate
Lab Name ALS Laboratory Group bullbull FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-11 1809(HWB R-37 VOCs) PAR 002731703
Lab 10 VL091125middot4LCSD Sample Matrix WATER
Moisture NIA Prep Batch VL091125-4
QCBatchlD VL091125-4-5
Sample Aliquot
Final Volume
10 ml
10ml Date Collected NIA Run ID VL091125-4A Result Units UGIL Date Extracted 112512009 Cleanup NONE Clean DF 1 Date Analyzed 1112512009 Basis NIA
Prep Method SW5030C File Name 028041
CASNO Target Analyte Spike Added
LCSD Result
Reporting Limit
Result Qualifier
LCSD Rec
RPD Limit
RPD
74-87-3 CHLOROMETHANE 10 897 05 90 30 4
75-01-4 VINYL CHLORIDE 10 831 05 83 25 4
74-83-9 BROMO METHANE 10 945 1 94 25 0
75-69-4 TRICHLOROFLUOROMETHANE 10 873 05 87 22 4
75-35-4 11-DICHLOROETHENE 10 909 05 91 18 5
75-15-0 CARBON DISULFIDE 10 941 10 J 94 20 1
156-60middot5 TRANS-l2middotDICHLOROETHENE 10 961 05 96 25 4
75middot34middot3 11-DICHLOROETHANE 10 977 05 98 25 2
108-05-4 VINYL ACETATE 10 993 10 J 99 20 1
156middot59-2 CIS-12-DlCHLOROETHENE 10 995 05 99 25 3
i 78-93-3 2-BUTANONE 40 419 5 105 30 2
67-66-3 CHLOROFORM 10 985 05 99 25 1
71-55-6 lll-TRICHLOROETHANE 10 942 1 94 25 3
56-23-5 CARBON TETRACHLORIDE 10 922 05 92 25 2
107middot06-2 12middotDICHLOROETHANE 10 106 05 106 25 0
71-43middot2 BENZENE 10 971 05 97 10 1
79middot01middot6 TRICHLOROETHENE 10 939 05 94 10 2
78middot87middot5 l2middotDICHLOROPROPANE 10 101 05 101 25 1
i 75middot27-4 BROMODICHLOROMETHANE 10 992 05 99 25 0
1108-88-3 TOLUENE 10 962 05 96 9 1
I 79005 112middotTRICHLOROETHANE 10 986 05 99 25 0
591middot78middot6 2-HEXANONE 40 418 10 104 20 2
127middot18-4 TETRACHLOROETHENE 10 918 05 92 25 4
106-93-4 12middotDIBROMOETHANE 10 999 1 100 15 1
108middot90-7 CHLOROBENZENE 10 997 05 100 11 1
630-20middot6 1112-TETRACHLOROETHANE 10 101 05 101 15 0
100-41-4 ETHYLBENZENE 10 968 05 97 25 1
Data Package ID VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- FC Page 3 of 4
lIMS Version 6317 A
22
GCMS Volatiles Method SW8260_25B
Laboratory Control Sample and Laboratory Control Sample Duplicate
Lab Name ALS Laboratory 13roup -- FC
Work Order Number 0911214
Client Name New Mexico Environment Department OS
ClientProject 10 644-11 1809(HWB R-37 VOCs) PAR 002731703
Lab 10 VL091125-4LCSD Sample Matrix WATER
Moisture NA Prep Batch VL091125-4
QCBatchlO VL091125-4-5
Sample Aliquot
Final Volume
10 ml
10ml Date Collected NA Run 10 VL091125-4A Result Units UGL Date Extracted 11252009 Cleanup NONE Clean OF Date Analyzed 11252009 Basis NIA
Prep Method SW5030C File Name 028041
CASNO Target Analyte Spike Added
LCSD Result
Reporting Limit
Result Qualifier
LCSD Rec
RPD Limit
RPD
136777-61-2 M+P-XYLENE 20 193 1 97 25 2
95-47-6 O-XYLENE 10 983 05 98 25 2
95-49-8 2middotCHLOROTOLUENE 10 9A9 05 95 15 2
541-73-1 13middotDICHLOROBENZENE 10 997 05 100 25 2
106-46-7 14-DICHLOROBeNZENE 10 974 05 97 25 1
95-50middot1 12middotDICHLOROBENZeNE 10 101 05 101 25 2
91middot20-3 NAPHTHALENe 10 105 05 105 24 6
87-61-6 123-TRICHLOROBENZENE 10 102 05 102 33 3
Surrogate Recovery LCSLCSD
CASNO Target Analyte Spike Added
LCS Rec
LCS Flag
LCSD Rec
LCSD Flag
Control Limits
460middot00-4 4-BROMOFLUOROBeNZENE 25 100 100 82 - 121
1868-53middot7 DIBROMOFLUOROMeTHANE 25 101 100 80middot 123
2037middot26-5 TOLUENEmiddotD8 25 102 100 85middot 116
Data Package 10 VL0911214-
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- Fe Page 4 of 4
UMS Verslmt 6317A
23
GCMS Volatiles Method SW8260_258
Sample Results
Lab Name ALS Laboratory Group bullbull FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject ID 644-111809(HWB R-37 VOCs) PAR 002731703
Field 10 R-37 Sor 2-111809
Lab ID 0911214middot1
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml
Moisture NA QCBatchlD VL091125-4-5 Final Volume 10 ml
Date Collected 18-Nov-09 Run ID VL091125-4A Result Units UGL
Date Extracted 25-Nov-09 Cleanup NONE Clean DF 1
Analysis ReqCode 104 Date Analyzed 25-Nov-09 Basis As Received
Prep Method SW5030 Rev C File Name 028044
CASNO Target Analyte Dilution Factor
103-65-1 NmiddotPROPYLBENZENE 1
95-49-8 2-CHLOROTOLUENE 1
108-67-8 135-TRIMETHYLBENZENE 1
106-43-4 4-CHLOROTOLUENE 1
98-06-6 TER I-BUTYLBENZENE 1
95-63-6 124-TRIMETHYLBENZENE 1
135-98-8 SEC-BUTYLBENZENE 1
541-73-1 13-OICHLOROBENZENE 1
99-87-6 P-ISOPROPYLTOLUENE 1
106-46-7 lA-DICHLOROBENZENE 1
104-51-8 N-BUTYLBENZENE 1
95-50-1 12-DICHLOROBENZENE 1
96-12-8 l2-DIBROMOmiddot3-CHLOROPROPANE 1
120-82-1 12A-TRICHLOROBENZENE 1
187-68-3 HEXACHLOROBUTADIENE 1
91-20-3 NAPHTHALENE 1
87-61middot6 123-TRICHLOROBENZENE 1
75-05-8 ACETONITRILE 1
107middot05middot1 ALLYL CHLORIDE 1
110-57-6 TRANS-14-DICHLORO-2-BUTENE 1
164-17-5 ETHANOL 1
97-63-2 ETHYL METHACRYLATE 1
78-83-1 ISOBUTYL ALCOHOL 1
126-98-7 METHACRYLONITRILE 1
80-62-6 METHYL METHACRYLATE 1
107-12-0 PROPIONITRILE 1
Result Reporting Limit
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
2 2
05 05
05 05
05 05
05 05
50 50
50 50
5 5
200 200
5 5
100 100
35 35
5 5
25 25
MDL Result EPA Qualifier Qualifier
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
067 U
017 U
017 U
017 U
017 U
83 U
017 U
U u 78 U
017 U
17 U
17 U
17 U
33 U
Data Package 10 VL0911214-1
Date Printed Wednesday December 022009 ALS Laboratory Group MM Fe Page 3 of 8
LlMS VerSion 6317A
14
GCMS Volati las Method SW8260_258
Sample Results
Lab Name ALS Laboratory Group - FC
Work Order Number 0911214
Client Name New Mexico Environment Department 08
ClientProject 10 644-111B09(HWB R-37 VOGs) PAR 002731703
Field 10 R-37 Ser 2-111809 Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10ml
Lab 10 0911214-1 Moisture NA
Date Collected 1B-Nov-09 QCBatchlO VL091125-4-5
Run 10 VL091125-4A
Final Volume 10ml
Result Units UGIL Date Extracted 25-Nov-09 Cleanup NONE Clean OF
Analysis ReqCode 104 Date Analyzed 25-Nov-09
Prep Method SW5030 Rev G Basis As Received
File Name 028044
CASNO Target Analyte Dilution Factor
Result Reporting Limit
MDL Result Qualifier
EPA Qualifier
126-99-8 CHLOROPRENE 1 5 5 017 U
75-65-0 TERT-BUTANOL 1 100 100 33 U
108-20-3 ISOPROPYL ETHER 1 2 2 033 U
637-92-3 ETHYL TERT-BUTYL ETHER 1 2 2 033 U
994-05-8 TERT-AMYL METHYL ETHER 1 2 2 033 U
67-72-1 HEXACHLOROETHANE 1 2 2 033 U
Surrogate Recovery
CASNO Surrogate Analyte Result Flag Spike Amount
Percent Recovery
Control Limits
460-00-4 4-BROMOFLUOHOBENZENE 246 25 98 82 - 121
1868-53-7 DIBROMOFLUOHOMETHANE 248 25 99 BO - 123
2037-26-5 TOLUENE-DB 258 25 103 85middot116
Data Package 10 VL0911214-1
Date Printed Wednesday December 022009 ALS Laboratory Group bullbull FC Page 4 of 8
LIMS Version 0317 A
15
GCMS Volati les Method SW8260_25B
Sample Results
Lab Name ALS Laboratory Group -- FC
Worlt Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-111809(HWB Rmiddot37 VOCs) PAR 002731703
Field 10 Rmiddot37 Scr jmiddot111809
Lab 10 0911214-2
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml Moisture NfA QCBatchID VL091125-4middot5 Final Volume 10 ml
Date Collected 18middotNov-09 Run 10 VL091125-4A Result Units UGfL Date Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Analysis ReqCode 104 Date Analyzed 25middotNov-09 Basis As Received Prep Method SW5030 Rev C File Name 028045
CASNO Target Analyte Dilution Factor
Result Reporting Limit
MOL Result Qualifier
EPA Qualifier
75-71-8 DICHLORODIFLUOROMETHANE 1 05 05 017 U
74-87-3 CHLOROMETHANE 1 05 05 017 U
75-01middot4 VINYL CHLORIDE 1 05 05 017 U
74-83-9 BROMOMETHANE 1 1 1 017 U
75middot00middot3 CHLOROETHANE j 05 05 017 U
75-69-4 TRICHLOROFLUOROMETHANE 1 05 05 017 U
107-02-8 ACROLEIN 1 100 100 17 U
i 75-35-4 11-DICHLOROETHENE 1 05 05 017 U
67-64middot1 ACETONE 1 10 10 33 U
74-8S-4 IODOMETHANE 1 5 5 017 U
75-15-0 CARBON DISULFIDE 1 10 10 017 U
75-09-2 METHYLENE CHLORIDE 1 1 1 017 U
156-60-5 TRANS-12-DICHLOROETHENE 1 05 05 017 U
1634-04-4 METHYL TERTIARY BUTYL ETHER 1 1 1 017 U
107-13-1 ACRYLONITRILE 1 10 10 17 U
75-34middot3 11-DICHLOROETHANE 05 05 017 U
i 108-05-4 VINYL ACETATE 1 10 10 067 U
115659-2 CISmiddot 2middotDICHLOROETHENE 1 05 05 017 U
178-933 2middotBUTANONE 1 5 5 17 U
74-97middot5 BROMOCHLOROMET HANE 1 1 1 017 U
67-66-3 CHLOROFORM 1 05 05 017 U
71-55middot6 111middotTRICHLOROETHANE 1 1 1 017 U
594-20-7 22middotDICHLOROPROPANE 1 05 05 017 U
56-23-5 CARBON TETRACHLORIDE 1 05 05 017 U
563-58-6 11middotDICHLOROPROPENE 1 05 05 017 U
107-06-2 12middotDICHL OROETHANE 1 05 05 017 U
Data Package ID VL0911214-1
Date Printed Wednesday December 022009 ALS Laboratory Group -- Fe Page 5 of 8
16
GCMS Volatiles Method SW8260_25B
Sample Results
Lab Name ALS Laboratory Group -- FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-111809(HW3 R-37 VOCs) PAR 002731703
Field 10 R-37 Scr 1-11 1809
Lab 10 0911214-2
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml
Moisture NIA QCBatchlO VL091125-4-5 Final Volume 10 ml
Date Collected 18-Nov-09 Run 10 VL091125-4A Result Units UGL
[late Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Analysis ReqCode 104 Date Analyzed 25-Nov-09
Prep Method SW5030 Rev C Basis As Received
File Name 028045
CASNO Target Analyte Dilution Factor
71-43-2 BENZENE 1
79-01-6 TRICHLOROETHENE 1
78-87-5 12-DICHLOROPROPANE 1
74-95-3 DIBROMOMETHANE 1
75-27-4 BROMODICHLOROMETHANE 1
10061-01-5 CIS-13-DICHLOROPROPENE 1
108-10-1 4-METHYL-2-PtNTANON 1
108-88-3 TOLUENE 1
10061-02-6 TRANS-13-DICHLOROPROPENE 1
79-00-5 112-TRICHLOROETHANE 1
591-78-6 2-HEXANONE 1
127-18-4 TETRACHLOROETHENE 1
142-28-9 13-DICHLOROPROPANt 1
124-48-1 DI3ROMOCHLOROMETHANE 1
106-93-4 12-DIBROMOETHANE 1
108-90-7 CHLOROBENZENE 1
OETHANE 1
- 1
LENE 1
ENE 1
ENE 1
OFORM 1
OPYlBENZENE 1
96-18-4 123-TRICHLOROPROPANE 1
79-34-5 1122-TETRACHLOROETHANE 1
108-86-1 BROMOBENZENE 1
Result Reporting Limit
05 05
05 05
05 05
05 05
05 05
05 05
5 5
025 05
05 05
05 05
10 10
05 05
05 05
1 1
1 1
05 05
05 05
05 05
1 1
05 05
05 05
05 05
05 05
2 2
05 05
05 05
MDL Result EPA Qualifier Qualifier
017 U
017 U
017 U
017 U
017 U
017 U
17 U
017 J
017 U
017 U
17 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
Data Package 10 VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- Fe Page 6 of 8
317A
17
GCMS Volatiles Method SW8260 _258
Sample Results
Lab Name ALS Laboratory Group -- FC
Work Order Number 0911214
Client Name New Mexico Environment Department 08
ClientProject 10 644-11S09(HWB R-37 VOCs) PAR 002731703
Field 10 Rmiddot37 Scr 1-111809
Lab 10 0911214-2
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml Moisture NA QCBatchlD VL091125-4-5 Final Volume 10 ml
Date Collected 18-Nov-09 Run 10 VL091125-4A Result Units UGL Date Extracted 25-Nol-09 Cleanup NONE Clean OF
Analysis ReqCode 104 Date Analyzed 25-Nov-09 Basis As Received Prep Method SW5030 Rev C File Name D28045
CASNO Target Analyte Dilution Factor
103-65-1 N-PROPYLBENZENE 1
95-49-8 2-CHLOROTOLUENE 1
108-67-8 135-TRIMETHYLBENZENE 1
106-43-4 4-CHLOROTOLUENE 1
98-06-6 TERT-BUTYLBENZENE 1
95-63-6 124-TRIMETHYLBENZENE 1
135-98-8 SEC-BUTYLBENZENE 1
i 541-73-1 13middotDICHLOROBENZENE 1
99-87-6 PmiddotISOPROPYL TOLUENE 1
106-46-7 I 14-DICHLOROBENZENE 1
104-51-8 I N-BUTYLBENZENE 1
95-50-1 l2-DICHLOROBENZENE 1
96-12-8 I 12-DIBROMO-3-CHLOROPROPANE 1
120-82-1 124-TRICHLOROBENZENE 1
87-68-3 HEXACHLOROBUT ADIENE 1
91-20-3 NAPHTHALENE 1
87-61-6 123-TRICHLOROBENZENE 1
75-05-S ACETONITRILE 1
107-05-1 ALLYL CH LORIDE 1
110-57-6 TRAN S-14-DICHLORO-2-BUTENE 1
64-17-5 ETHANOL 1
97-63-2 ETHYL METHACRYLATE 1
78-83-1 ISOBUTYL ALCOHOL 1
126-98-7 METHACRYLONITRILE 1
80-62-6 METHYL METHACRYLATE 1
107-12-0 I PROPIONITRILE 1
Result Reporting Limit
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
2 2
05 05
05 05
05 05
05 05
50 50
50 50 I 5 5
200 200
5 5
100 100
35 35
5 5
25 25
MDL
017
017
017
017
017
017
017
017
017
017
017
017
067
017
017
017
017
83
017
17
78
017
17
17
17
33
Result EPA Qualifier Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
Data Package 10 VL0911214-1
Date Printed Wednesday December 022009 ALS Laboratory Group -- Fe Page 7 of 8
LlMS Version 6317A
18
GCMS Volatiles Method SW8260_258
Sample Results
Lab Name ALS Laboratory Group bullbull FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644middot111B09(HWB R-37 VOCs) PAR 002731703
Sample Matrix WATER Prep Batch VL091125--4 Sample Aliquot 10 mlRmiddot37 Ser 1-111809 Moisture NA QCBatchlO VL091125--4-5 Final Volume 10 m
0911214-2 Date Collected 18-Nov-09 Run 10 VL091125--4A Result Units UGL Date Extracted 25-Nov-09 Cleanup NONE Clean OF 1 Date Analyzed 25-Nov-09 Basis As Received
10
Analysis ReqCode 104 Prep Method SW5030 Rev C File Name 028045
I
CASNO Target Analyte Dilution Factor
Result Reporting Limit
MDL Result Qualifier
EPA Qualifier
126-99-8 CHLOROPRENE 1 5 5 017 U
75-65-0 TERT-BUTANOL 1 100 100 33 U
108-20-3 ISOPROPYL ETHER 1 2 2 033 U
637-92-3 ETHYL TERT-BUTYL ETHER 1 2 2 033 U
994-05--8 TERT-AMYL MTHYL ETHER 1 2 2 033 U
67-72-1 HEXACHLOROETHANE 1 2 2 033 U
Surrogate Recovery
CASNO Surrogate Analyte Result Flag Spike Amount
Percent Control Recovery Limits
460-00-4 4middotBROMOFLUOROBENZENE 247 25 99 1
1868-53-7 DIBROMOFLUOROMETHANE 248 25 99 80 123
2037-26-5 TOLUENEmiddotDB 255 25 102 85 - 116
Data Package 10 VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- FC Page B of 8
LlMS Version 6317A
19
GCMS Volatiles Method SW8260_258
Laboratory Control Sample and Laboratory Control Sample Duplicate
Lab Name ALS Laboratory Group - FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-111809(HWB R-37 VOCs) PAR 002731703
Lab 10 VL091125-4LCS Sample Matrix WATER
Moisture NA Prep Batch VL091125-4
QCBatchlD VL091125-4-5
Sample Aliquot
Final Volume
10ml
10ml Date Collected NA Run 10 VL091125-4A Result Units UGIL Date Extracted 111252009 Cleanup NONE Clean OF 1 Date Analyzed 11252009 Basis NA
Prep Method SW5030C File Name 028040
CASNO
74-87-3
75-01-4
74-83-9
75-69-4
75-35-4
75-15-0
156-60-5
75-34-3
108-05-4
156-59-2
78-93-3
67 -66-3
71-55-6
i 56-23-5
107-06-2
71-43-2
79-01-6
78-87-5
75-27-4
108-88-3
79-00-5
591-78-6
127-18-4
106-93-4
108-90-7
63Q20-6
Target Analyte Spike Added
CHLOROMETHANE 10
VINYL CHLORIDE 10
BROMOMETHANE 10
TRICHLOROFLUOROMETHANE 10
11-DICHLOROETHENE 10
CARBON DISULFIDE 10
TRANS-12-DICHLOROETHENE 10
11-DICHLOROETHANE 10
VINYL ACETATE 10
CIS-12-DICHLOROETHENE 10
2middotBUTANONE 40
CHLOROFORM 10
111-TRICHL ORO ETHANE 10
CARBON TETRACHLORIDE 10
12-DICHLOROETHANE 10
BENZENE 10
TRICHLOROETHENE 10
12-DICHLOROPROPANE 10
BROMODICHLOROMETHANE 10
TOLUENE 10
112-TRICHLOROETHANE 10
2-HEXANONE 40
TETRACHLOROETHENE 10
12-DIBROMOETHANE 10
CHLOROBENZENE 10
1112-TETRACHLOROETHANE 10
LCS Reporting Result Result Limit Qualifier
932 05
863 05
943 1
908 05
96 05
95 10 J
996 05
992 05
10 10
102 05
412 5
993 05
974 1
943 05
106 05
983 05
962 05
10 05
988 05
974 05
989 05
409 10
956 05
991 1
984 05
101 05
LCS Control Rec Limits
93 49 -129
86 46 134
94 32-121
91 67 -152
96 61 -135
95 61 -140
100 70 -122
99 76 -119
100 62 182
102 75 126
103 61 -137
99 79 120
97 76 - 114
94 58middot135
106 75middot132
98 70 shy 125
96 74 121
100 81 -119
99 79 - 123
97 76 - 120
99 81 -126
102 45 168
96 56 -128
99 79 -123
98 75 -120
101 82 - 123
Data Package 10 VL0911214middot1
-Date Printed Wednesday December 02 2009 ALS Laboratory Group -- Fe Page 1 of 4
LiMS Version 6317A
20
GCMS Volatiles Method SW8260_25B
Laboratory Control Sample and Laboratory Control Sample Duplicate
Lab Name ALS Laboratory Group - FC
Work Order Number 0911214
Client Name New Mexico Envircnment Department OB
ClientProject 10 644-111809(HWB R-37 VOes) PAR 002731703
Lab 10 VL091125-4LCS Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml
Moisture NIA QCBatchlO VL091125-4-5 Final Volume 10 mi
Date Collected NA Run 10 VL091125-4A Result Units UGL Date Extracted 11252009 Cleanup NONE Clean OF 1 Date Analyzed 111252009 Basis NA
Prep Method SW5030e File Name 028040
CASNO Target Analyte Spike Added
LCS Result
Reporting Limit
Result Qualifier
LCS Rec
Control Limits
100-41-4 ETHYLBENZENE 10 981 05 98 79 -114
136777-61-2 M+P-XYLENE 20 197 1 98 81-115
95-47-6 O-XYLENE 10 101 05 101 81 -115
95-49-8 2-CHLOROTOLUENE 10 97 05 97 80 -128
541-73-1 13-DICHLOROBENZiNt 10 977 05 98 81-116
106-46-7 14-DICHLOROBENZENE 10 979 05 98 81 -119
95-50-1 12-DICHLOROBENZENE 10 987 05 99 79 - 116
91-20-3 NAPHTHALENE 10 993 05 99 69 -126
87-61-6 123-TRICHLOROBENZENE 10 999 05 100 60 -137
Data Package ID VL0911214-1
Date Printed Wecnesday December 02 2009 ALS Laboratory Group -- Fe Page 2 of 4
21
GCMS Volatiles Method SW8260_25B
Laboratory Control Sample and Laboratory Control Sample Duplicate
Lab Name ALS Laboratory Group bullbull FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-11 1809(HWB R-37 VOCs) PAR 002731703
Lab 10 VL091125middot4LCSD Sample Matrix WATER
Moisture NIA Prep Batch VL091125-4
QCBatchlD VL091125-4-5
Sample Aliquot
Final Volume
10 ml
10ml Date Collected NIA Run ID VL091125-4A Result Units UGIL Date Extracted 112512009 Cleanup NONE Clean DF 1 Date Analyzed 1112512009 Basis NIA
Prep Method SW5030C File Name 028041
CASNO Target Analyte Spike Added
LCSD Result
Reporting Limit
Result Qualifier
LCSD Rec
RPD Limit
RPD
74-87-3 CHLOROMETHANE 10 897 05 90 30 4
75-01-4 VINYL CHLORIDE 10 831 05 83 25 4
74-83-9 BROMO METHANE 10 945 1 94 25 0
75-69-4 TRICHLOROFLUOROMETHANE 10 873 05 87 22 4
75-35-4 11-DICHLOROETHENE 10 909 05 91 18 5
75-15-0 CARBON DISULFIDE 10 941 10 J 94 20 1
156-60middot5 TRANS-l2middotDICHLOROETHENE 10 961 05 96 25 4
75middot34middot3 11-DICHLOROETHANE 10 977 05 98 25 2
108-05-4 VINYL ACETATE 10 993 10 J 99 20 1
156middot59-2 CIS-12-DlCHLOROETHENE 10 995 05 99 25 3
i 78-93-3 2-BUTANONE 40 419 5 105 30 2
67-66-3 CHLOROFORM 10 985 05 99 25 1
71-55-6 lll-TRICHLOROETHANE 10 942 1 94 25 3
56-23-5 CARBON TETRACHLORIDE 10 922 05 92 25 2
107middot06-2 12middotDICHLOROETHANE 10 106 05 106 25 0
71-43middot2 BENZENE 10 971 05 97 10 1
79middot01middot6 TRICHLOROETHENE 10 939 05 94 10 2
78middot87middot5 l2middotDICHLOROPROPANE 10 101 05 101 25 1
i 75middot27-4 BROMODICHLOROMETHANE 10 992 05 99 25 0
1108-88-3 TOLUENE 10 962 05 96 9 1
I 79005 112middotTRICHLOROETHANE 10 986 05 99 25 0
591middot78middot6 2-HEXANONE 40 418 10 104 20 2
127middot18-4 TETRACHLOROETHENE 10 918 05 92 25 4
106-93-4 12middotDIBROMOETHANE 10 999 1 100 15 1
108middot90-7 CHLOROBENZENE 10 997 05 100 11 1
630-20middot6 1112-TETRACHLOROETHANE 10 101 05 101 15 0
100-41-4 ETHYLBENZENE 10 968 05 97 25 1
Data Package ID VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- FC Page 3 of 4
lIMS Version 6317 A
22
GCMS Volatiles Method SW8260_25B
Laboratory Control Sample and Laboratory Control Sample Duplicate
Lab Name ALS Laboratory 13roup -- FC
Work Order Number 0911214
Client Name New Mexico Environment Department OS
ClientProject 10 644-11 1809(HWB R-37 VOCs) PAR 002731703
Lab 10 VL091125-4LCSD Sample Matrix WATER
Moisture NA Prep Batch VL091125-4
QCBatchlO VL091125-4-5
Sample Aliquot
Final Volume
10 ml
10ml Date Collected NA Run 10 VL091125-4A Result Units UGL Date Extracted 11252009 Cleanup NONE Clean OF Date Analyzed 11252009 Basis NIA
Prep Method SW5030C File Name 028041
CASNO Target Analyte Spike Added
LCSD Result
Reporting Limit
Result Qualifier
LCSD Rec
RPD Limit
RPD
136777-61-2 M+P-XYLENE 20 193 1 97 25 2
95-47-6 O-XYLENE 10 983 05 98 25 2
95-49-8 2middotCHLOROTOLUENE 10 9A9 05 95 15 2
541-73-1 13middotDICHLOROBENZENE 10 997 05 100 25 2
106-46-7 14-DICHLOROBeNZENE 10 974 05 97 25 1
95-50middot1 12middotDICHLOROBENZeNE 10 101 05 101 25 2
91middot20-3 NAPHTHALENe 10 105 05 105 24 6
87-61-6 123-TRICHLOROBENZENE 10 102 05 102 33 3
Surrogate Recovery LCSLCSD
CASNO Target Analyte Spike Added
LCS Rec
LCS Flag
LCSD Rec
LCSD Flag
Control Limits
460middot00-4 4-BROMOFLUOROBeNZENE 25 100 100 82 - 121
1868-53middot7 DIBROMOFLUOROMeTHANE 25 101 100 80middot 123
2037middot26-5 TOLUENEmiddotD8 25 102 100 85middot 116
Data Package 10 VL0911214-
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- Fe Page 4 of 4
UMS Verslmt 6317A
23
GCMS Volati las Method SW8260_258
Sample Results
Lab Name ALS Laboratory Group - FC
Work Order Number 0911214
Client Name New Mexico Environment Department 08
ClientProject 10 644-111B09(HWB R-37 VOGs) PAR 002731703
Field 10 R-37 Ser 2-111809 Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10ml
Lab 10 0911214-1 Moisture NA
Date Collected 1B-Nov-09 QCBatchlO VL091125-4-5
Run 10 VL091125-4A
Final Volume 10ml
Result Units UGIL Date Extracted 25-Nov-09 Cleanup NONE Clean OF
Analysis ReqCode 104 Date Analyzed 25-Nov-09
Prep Method SW5030 Rev G Basis As Received
File Name 028044
CASNO Target Analyte Dilution Factor
Result Reporting Limit
MDL Result Qualifier
EPA Qualifier
126-99-8 CHLOROPRENE 1 5 5 017 U
75-65-0 TERT-BUTANOL 1 100 100 33 U
108-20-3 ISOPROPYL ETHER 1 2 2 033 U
637-92-3 ETHYL TERT-BUTYL ETHER 1 2 2 033 U
994-05-8 TERT-AMYL METHYL ETHER 1 2 2 033 U
67-72-1 HEXACHLOROETHANE 1 2 2 033 U
Surrogate Recovery
CASNO Surrogate Analyte Result Flag Spike Amount
Percent Recovery
Control Limits
460-00-4 4-BROMOFLUOHOBENZENE 246 25 98 82 - 121
1868-53-7 DIBROMOFLUOHOMETHANE 248 25 99 BO - 123
2037-26-5 TOLUENE-DB 258 25 103 85middot116
Data Package 10 VL0911214-1
Date Printed Wednesday December 022009 ALS Laboratory Group bullbull FC Page 4 of 8
LIMS Version 0317 A
15
GCMS Volati les Method SW8260_25B
Sample Results
Lab Name ALS Laboratory Group -- FC
Worlt Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-111809(HWB Rmiddot37 VOCs) PAR 002731703
Field 10 Rmiddot37 Scr jmiddot111809
Lab 10 0911214-2
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml Moisture NfA QCBatchID VL091125-4middot5 Final Volume 10 ml
Date Collected 18middotNov-09 Run 10 VL091125-4A Result Units UGfL Date Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Analysis ReqCode 104 Date Analyzed 25middotNov-09 Basis As Received Prep Method SW5030 Rev C File Name 028045
CASNO Target Analyte Dilution Factor
Result Reporting Limit
MOL Result Qualifier
EPA Qualifier
75-71-8 DICHLORODIFLUOROMETHANE 1 05 05 017 U
74-87-3 CHLOROMETHANE 1 05 05 017 U
75-01middot4 VINYL CHLORIDE 1 05 05 017 U
74-83-9 BROMOMETHANE 1 1 1 017 U
75middot00middot3 CHLOROETHANE j 05 05 017 U
75-69-4 TRICHLOROFLUOROMETHANE 1 05 05 017 U
107-02-8 ACROLEIN 1 100 100 17 U
i 75-35-4 11-DICHLOROETHENE 1 05 05 017 U
67-64middot1 ACETONE 1 10 10 33 U
74-8S-4 IODOMETHANE 1 5 5 017 U
75-15-0 CARBON DISULFIDE 1 10 10 017 U
75-09-2 METHYLENE CHLORIDE 1 1 1 017 U
156-60-5 TRANS-12-DICHLOROETHENE 1 05 05 017 U
1634-04-4 METHYL TERTIARY BUTYL ETHER 1 1 1 017 U
107-13-1 ACRYLONITRILE 1 10 10 17 U
75-34middot3 11-DICHLOROETHANE 05 05 017 U
i 108-05-4 VINYL ACETATE 1 10 10 067 U
115659-2 CISmiddot 2middotDICHLOROETHENE 1 05 05 017 U
178-933 2middotBUTANONE 1 5 5 17 U
74-97middot5 BROMOCHLOROMET HANE 1 1 1 017 U
67-66-3 CHLOROFORM 1 05 05 017 U
71-55middot6 111middotTRICHLOROETHANE 1 1 1 017 U
594-20-7 22middotDICHLOROPROPANE 1 05 05 017 U
56-23-5 CARBON TETRACHLORIDE 1 05 05 017 U
563-58-6 11middotDICHLOROPROPENE 1 05 05 017 U
107-06-2 12middotDICHL OROETHANE 1 05 05 017 U
Data Package ID VL0911214-1
Date Printed Wednesday December 022009 ALS Laboratory Group -- Fe Page 5 of 8
16
GCMS Volatiles Method SW8260_25B
Sample Results
Lab Name ALS Laboratory Group -- FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-111809(HW3 R-37 VOCs) PAR 002731703
Field 10 R-37 Scr 1-11 1809
Lab 10 0911214-2
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml
Moisture NIA QCBatchlO VL091125-4-5 Final Volume 10 ml
Date Collected 18-Nov-09 Run 10 VL091125-4A Result Units UGL
[late Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Analysis ReqCode 104 Date Analyzed 25-Nov-09
Prep Method SW5030 Rev C Basis As Received
File Name 028045
CASNO Target Analyte Dilution Factor
71-43-2 BENZENE 1
79-01-6 TRICHLOROETHENE 1
78-87-5 12-DICHLOROPROPANE 1
74-95-3 DIBROMOMETHANE 1
75-27-4 BROMODICHLOROMETHANE 1
10061-01-5 CIS-13-DICHLOROPROPENE 1
108-10-1 4-METHYL-2-PtNTANON 1
108-88-3 TOLUENE 1
10061-02-6 TRANS-13-DICHLOROPROPENE 1
79-00-5 112-TRICHLOROETHANE 1
591-78-6 2-HEXANONE 1
127-18-4 TETRACHLOROETHENE 1
142-28-9 13-DICHLOROPROPANt 1
124-48-1 DI3ROMOCHLOROMETHANE 1
106-93-4 12-DIBROMOETHANE 1
108-90-7 CHLOROBENZENE 1
OETHANE 1
- 1
LENE 1
ENE 1
ENE 1
OFORM 1
OPYlBENZENE 1
96-18-4 123-TRICHLOROPROPANE 1
79-34-5 1122-TETRACHLOROETHANE 1
108-86-1 BROMOBENZENE 1
Result Reporting Limit
05 05
05 05
05 05
05 05
05 05
05 05
5 5
025 05
05 05
05 05
10 10
05 05
05 05
1 1
1 1
05 05
05 05
05 05
1 1
05 05
05 05
05 05
05 05
2 2
05 05
05 05
MDL Result EPA Qualifier Qualifier
017 U
017 U
017 U
017 U
017 U
017 U
17 U
017 J
017 U
017 U
17 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
Data Package 10 VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- Fe Page 6 of 8
317A
17
GCMS Volatiles Method SW8260 _258
Sample Results
Lab Name ALS Laboratory Group -- FC
Work Order Number 0911214
Client Name New Mexico Environment Department 08
ClientProject 10 644-11S09(HWB R-37 VOCs) PAR 002731703
Field 10 Rmiddot37 Scr 1-111809
Lab 10 0911214-2
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml Moisture NA QCBatchlD VL091125-4-5 Final Volume 10 ml
Date Collected 18-Nov-09 Run 10 VL091125-4A Result Units UGL Date Extracted 25-Nol-09 Cleanup NONE Clean OF
Analysis ReqCode 104 Date Analyzed 25-Nov-09 Basis As Received Prep Method SW5030 Rev C File Name D28045
CASNO Target Analyte Dilution Factor
103-65-1 N-PROPYLBENZENE 1
95-49-8 2-CHLOROTOLUENE 1
108-67-8 135-TRIMETHYLBENZENE 1
106-43-4 4-CHLOROTOLUENE 1
98-06-6 TERT-BUTYLBENZENE 1
95-63-6 124-TRIMETHYLBENZENE 1
135-98-8 SEC-BUTYLBENZENE 1
i 541-73-1 13middotDICHLOROBENZENE 1
99-87-6 PmiddotISOPROPYL TOLUENE 1
106-46-7 I 14-DICHLOROBENZENE 1
104-51-8 I N-BUTYLBENZENE 1
95-50-1 l2-DICHLOROBENZENE 1
96-12-8 I 12-DIBROMO-3-CHLOROPROPANE 1
120-82-1 124-TRICHLOROBENZENE 1
87-68-3 HEXACHLOROBUT ADIENE 1
91-20-3 NAPHTHALENE 1
87-61-6 123-TRICHLOROBENZENE 1
75-05-S ACETONITRILE 1
107-05-1 ALLYL CH LORIDE 1
110-57-6 TRAN S-14-DICHLORO-2-BUTENE 1
64-17-5 ETHANOL 1
97-63-2 ETHYL METHACRYLATE 1
78-83-1 ISOBUTYL ALCOHOL 1
126-98-7 METHACRYLONITRILE 1
80-62-6 METHYL METHACRYLATE 1
107-12-0 I PROPIONITRILE 1
Result Reporting Limit
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
2 2
05 05
05 05
05 05
05 05
50 50
50 50 I 5 5
200 200
5 5
100 100
35 35
5 5
25 25
MDL
017
017
017
017
017
017
017
017
017
017
017
017
067
017
017
017
017
83
017
17
78
017
17
17
17
33
Result EPA Qualifier Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
Data Package 10 VL0911214-1
Date Printed Wednesday December 022009 ALS Laboratory Group -- Fe Page 7 of 8
LlMS Version 6317A
18
GCMS Volatiles Method SW8260_258
Sample Results
Lab Name ALS Laboratory Group bullbull FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644middot111B09(HWB R-37 VOCs) PAR 002731703
Sample Matrix WATER Prep Batch VL091125--4 Sample Aliquot 10 mlRmiddot37 Ser 1-111809 Moisture NA QCBatchlO VL091125--4-5 Final Volume 10 m
0911214-2 Date Collected 18-Nov-09 Run 10 VL091125--4A Result Units UGL Date Extracted 25-Nov-09 Cleanup NONE Clean OF 1 Date Analyzed 25-Nov-09 Basis As Received
10
Analysis ReqCode 104 Prep Method SW5030 Rev C File Name 028045
I
CASNO Target Analyte Dilution Factor
Result Reporting Limit
MDL Result Qualifier
EPA Qualifier
126-99-8 CHLOROPRENE 1 5 5 017 U
75-65-0 TERT-BUTANOL 1 100 100 33 U
108-20-3 ISOPROPYL ETHER 1 2 2 033 U
637-92-3 ETHYL TERT-BUTYL ETHER 1 2 2 033 U
994-05--8 TERT-AMYL MTHYL ETHER 1 2 2 033 U
67-72-1 HEXACHLOROETHANE 1 2 2 033 U
Surrogate Recovery
CASNO Surrogate Analyte Result Flag Spike Amount
Percent Control Recovery Limits
460-00-4 4middotBROMOFLUOROBENZENE 247 25 99 1
1868-53-7 DIBROMOFLUOROMETHANE 248 25 99 80 123
2037-26-5 TOLUENEmiddotDB 255 25 102 85 - 116
Data Package 10 VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- FC Page B of 8
LlMS Version 6317A
19
GCMS Volatiles Method SW8260_258
Laboratory Control Sample and Laboratory Control Sample Duplicate
Lab Name ALS Laboratory Group - FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-111809(HWB R-37 VOCs) PAR 002731703
Lab 10 VL091125-4LCS Sample Matrix WATER
Moisture NA Prep Batch VL091125-4
QCBatchlD VL091125-4-5
Sample Aliquot
Final Volume
10ml
10ml Date Collected NA Run 10 VL091125-4A Result Units UGIL Date Extracted 111252009 Cleanup NONE Clean OF 1 Date Analyzed 11252009 Basis NA
Prep Method SW5030C File Name 028040
CASNO
74-87-3
75-01-4
74-83-9
75-69-4
75-35-4
75-15-0
156-60-5
75-34-3
108-05-4
156-59-2
78-93-3
67 -66-3
71-55-6
i 56-23-5
107-06-2
71-43-2
79-01-6
78-87-5
75-27-4
108-88-3
79-00-5
591-78-6
127-18-4
106-93-4
108-90-7
63Q20-6
Target Analyte Spike Added
CHLOROMETHANE 10
VINYL CHLORIDE 10
BROMOMETHANE 10
TRICHLOROFLUOROMETHANE 10
11-DICHLOROETHENE 10
CARBON DISULFIDE 10
TRANS-12-DICHLOROETHENE 10
11-DICHLOROETHANE 10
VINYL ACETATE 10
CIS-12-DICHLOROETHENE 10
2middotBUTANONE 40
CHLOROFORM 10
111-TRICHL ORO ETHANE 10
CARBON TETRACHLORIDE 10
12-DICHLOROETHANE 10
BENZENE 10
TRICHLOROETHENE 10
12-DICHLOROPROPANE 10
BROMODICHLOROMETHANE 10
TOLUENE 10
112-TRICHLOROETHANE 10
2-HEXANONE 40
TETRACHLOROETHENE 10
12-DIBROMOETHANE 10
CHLOROBENZENE 10
1112-TETRACHLOROETHANE 10
LCS Reporting Result Result Limit Qualifier
932 05
863 05
943 1
908 05
96 05
95 10 J
996 05
992 05
10 10
102 05
412 5
993 05
974 1
943 05
106 05
983 05
962 05
10 05
988 05
974 05
989 05
409 10
956 05
991 1
984 05
101 05
LCS Control Rec Limits
93 49 -129
86 46 134
94 32-121
91 67 -152
96 61 -135
95 61 -140
100 70 -122
99 76 -119
100 62 182
102 75 126
103 61 -137
99 79 120
97 76 - 114
94 58middot135
106 75middot132
98 70 shy 125
96 74 121
100 81 -119
99 79 - 123
97 76 - 120
99 81 -126
102 45 168
96 56 -128
99 79 -123
98 75 -120
101 82 - 123
Data Package 10 VL0911214middot1
-Date Printed Wednesday December 02 2009 ALS Laboratory Group -- Fe Page 1 of 4
LiMS Version 6317A
20
GCMS Volatiles Method SW8260_25B
Laboratory Control Sample and Laboratory Control Sample Duplicate
Lab Name ALS Laboratory Group - FC
Work Order Number 0911214
Client Name New Mexico Envircnment Department OB
ClientProject 10 644-111809(HWB R-37 VOes) PAR 002731703
Lab 10 VL091125-4LCS Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml
Moisture NIA QCBatchlO VL091125-4-5 Final Volume 10 mi
Date Collected NA Run 10 VL091125-4A Result Units UGL Date Extracted 11252009 Cleanup NONE Clean OF 1 Date Analyzed 111252009 Basis NA
Prep Method SW5030e File Name 028040
CASNO Target Analyte Spike Added
LCS Result
Reporting Limit
Result Qualifier
LCS Rec
Control Limits
100-41-4 ETHYLBENZENE 10 981 05 98 79 -114
136777-61-2 M+P-XYLENE 20 197 1 98 81-115
95-47-6 O-XYLENE 10 101 05 101 81 -115
95-49-8 2-CHLOROTOLUENE 10 97 05 97 80 -128
541-73-1 13-DICHLOROBENZiNt 10 977 05 98 81-116
106-46-7 14-DICHLOROBENZENE 10 979 05 98 81 -119
95-50-1 12-DICHLOROBENZENE 10 987 05 99 79 - 116
91-20-3 NAPHTHALENE 10 993 05 99 69 -126
87-61-6 123-TRICHLOROBENZENE 10 999 05 100 60 -137
Data Package ID VL0911214-1
Date Printed Wecnesday December 02 2009 ALS Laboratory Group -- Fe Page 2 of 4
21
GCMS Volatiles Method SW8260_25B
Laboratory Control Sample and Laboratory Control Sample Duplicate
Lab Name ALS Laboratory Group bullbull FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-11 1809(HWB R-37 VOCs) PAR 002731703
Lab 10 VL091125middot4LCSD Sample Matrix WATER
Moisture NIA Prep Batch VL091125-4
QCBatchlD VL091125-4-5
Sample Aliquot
Final Volume
10 ml
10ml Date Collected NIA Run ID VL091125-4A Result Units UGIL Date Extracted 112512009 Cleanup NONE Clean DF 1 Date Analyzed 1112512009 Basis NIA
Prep Method SW5030C File Name 028041
CASNO Target Analyte Spike Added
LCSD Result
Reporting Limit
Result Qualifier
LCSD Rec
RPD Limit
RPD
74-87-3 CHLOROMETHANE 10 897 05 90 30 4
75-01-4 VINYL CHLORIDE 10 831 05 83 25 4
74-83-9 BROMO METHANE 10 945 1 94 25 0
75-69-4 TRICHLOROFLUOROMETHANE 10 873 05 87 22 4
75-35-4 11-DICHLOROETHENE 10 909 05 91 18 5
75-15-0 CARBON DISULFIDE 10 941 10 J 94 20 1
156-60middot5 TRANS-l2middotDICHLOROETHENE 10 961 05 96 25 4
75middot34middot3 11-DICHLOROETHANE 10 977 05 98 25 2
108-05-4 VINYL ACETATE 10 993 10 J 99 20 1
156middot59-2 CIS-12-DlCHLOROETHENE 10 995 05 99 25 3
i 78-93-3 2-BUTANONE 40 419 5 105 30 2
67-66-3 CHLOROFORM 10 985 05 99 25 1
71-55-6 lll-TRICHLOROETHANE 10 942 1 94 25 3
56-23-5 CARBON TETRACHLORIDE 10 922 05 92 25 2
107middot06-2 12middotDICHLOROETHANE 10 106 05 106 25 0
71-43middot2 BENZENE 10 971 05 97 10 1
79middot01middot6 TRICHLOROETHENE 10 939 05 94 10 2
78middot87middot5 l2middotDICHLOROPROPANE 10 101 05 101 25 1
i 75middot27-4 BROMODICHLOROMETHANE 10 992 05 99 25 0
1108-88-3 TOLUENE 10 962 05 96 9 1
I 79005 112middotTRICHLOROETHANE 10 986 05 99 25 0
591middot78middot6 2-HEXANONE 40 418 10 104 20 2
127middot18-4 TETRACHLOROETHENE 10 918 05 92 25 4
106-93-4 12middotDIBROMOETHANE 10 999 1 100 15 1
108middot90-7 CHLOROBENZENE 10 997 05 100 11 1
630-20middot6 1112-TETRACHLOROETHANE 10 101 05 101 15 0
100-41-4 ETHYLBENZENE 10 968 05 97 25 1
Data Package ID VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- FC Page 3 of 4
lIMS Version 6317 A
22
GCMS Volatiles Method SW8260_25B
Laboratory Control Sample and Laboratory Control Sample Duplicate
Lab Name ALS Laboratory 13roup -- FC
Work Order Number 0911214
Client Name New Mexico Environment Department OS
ClientProject 10 644-11 1809(HWB R-37 VOCs) PAR 002731703
Lab 10 VL091125-4LCSD Sample Matrix WATER
Moisture NA Prep Batch VL091125-4
QCBatchlO VL091125-4-5
Sample Aliquot
Final Volume
10 ml
10ml Date Collected NA Run 10 VL091125-4A Result Units UGL Date Extracted 11252009 Cleanup NONE Clean OF Date Analyzed 11252009 Basis NIA
Prep Method SW5030C File Name 028041
CASNO Target Analyte Spike Added
LCSD Result
Reporting Limit
Result Qualifier
LCSD Rec
RPD Limit
RPD
136777-61-2 M+P-XYLENE 20 193 1 97 25 2
95-47-6 O-XYLENE 10 983 05 98 25 2
95-49-8 2middotCHLOROTOLUENE 10 9A9 05 95 15 2
541-73-1 13middotDICHLOROBENZENE 10 997 05 100 25 2
106-46-7 14-DICHLOROBeNZENE 10 974 05 97 25 1
95-50middot1 12middotDICHLOROBENZeNE 10 101 05 101 25 2
91middot20-3 NAPHTHALENe 10 105 05 105 24 6
87-61-6 123-TRICHLOROBENZENE 10 102 05 102 33 3
Surrogate Recovery LCSLCSD
CASNO Target Analyte Spike Added
LCS Rec
LCS Flag
LCSD Rec
LCSD Flag
Control Limits
460middot00-4 4-BROMOFLUOROBeNZENE 25 100 100 82 - 121
1868-53middot7 DIBROMOFLUOROMeTHANE 25 101 100 80middot 123
2037middot26-5 TOLUENEmiddotD8 25 102 100 85middot 116
Data Package 10 VL0911214-
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- Fe Page 4 of 4
UMS Verslmt 6317A
23
GCMS Volati les Method SW8260_25B
Sample Results
Lab Name ALS Laboratory Group -- FC
Worlt Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-111809(HWB Rmiddot37 VOCs) PAR 002731703
Field 10 Rmiddot37 Scr jmiddot111809
Lab 10 0911214-2
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml Moisture NfA QCBatchID VL091125-4middot5 Final Volume 10 ml
Date Collected 18middotNov-09 Run 10 VL091125-4A Result Units UGfL Date Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Analysis ReqCode 104 Date Analyzed 25middotNov-09 Basis As Received Prep Method SW5030 Rev C File Name 028045
CASNO Target Analyte Dilution Factor
Result Reporting Limit
MOL Result Qualifier
EPA Qualifier
75-71-8 DICHLORODIFLUOROMETHANE 1 05 05 017 U
74-87-3 CHLOROMETHANE 1 05 05 017 U
75-01middot4 VINYL CHLORIDE 1 05 05 017 U
74-83-9 BROMOMETHANE 1 1 1 017 U
75middot00middot3 CHLOROETHANE j 05 05 017 U
75-69-4 TRICHLOROFLUOROMETHANE 1 05 05 017 U
107-02-8 ACROLEIN 1 100 100 17 U
i 75-35-4 11-DICHLOROETHENE 1 05 05 017 U
67-64middot1 ACETONE 1 10 10 33 U
74-8S-4 IODOMETHANE 1 5 5 017 U
75-15-0 CARBON DISULFIDE 1 10 10 017 U
75-09-2 METHYLENE CHLORIDE 1 1 1 017 U
156-60-5 TRANS-12-DICHLOROETHENE 1 05 05 017 U
1634-04-4 METHYL TERTIARY BUTYL ETHER 1 1 1 017 U
107-13-1 ACRYLONITRILE 1 10 10 17 U
75-34middot3 11-DICHLOROETHANE 05 05 017 U
i 108-05-4 VINYL ACETATE 1 10 10 067 U
115659-2 CISmiddot 2middotDICHLOROETHENE 1 05 05 017 U
178-933 2middotBUTANONE 1 5 5 17 U
74-97middot5 BROMOCHLOROMET HANE 1 1 1 017 U
67-66-3 CHLOROFORM 1 05 05 017 U
71-55middot6 111middotTRICHLOROETHANE 1 1 1 017 U
594-20-7 22middotDICHLOROPROPANE 1 05 05 017 U
56-23-5 CARBON TETRACHLORIDE 1 05 05 017 U
563-58-6 11middotDICHLOROPROPENE 1 05 05 017 U
107-06-2 12middotDICHL OROETHANE 1 05 05 017 U
Data Package ID VL0911214-1
Date Printed Wednesday December 022009 ALS Laboratory Group -- Fe Page 5 of 8
16
GCMS Volatiles Method SW8260_25B
Sample Results
Lab Name ALS Laboratory Group -- FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-111809(HW3 R-37 VOCs) PAR 002731703
Field 10 R-37 Scr 1-11 1809
Lab 10 0911214-2
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml
Moisture NIA QCBatchlO VL091125-4-5 Final Volume 10 ml
Date Collected 18-Nov-09 Run 10 VL091125-4A Result Units UGL
[late Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Analysis ReqCode 104 Date Analyzed 25-Nov-09
Prep Method SW5030 Rev C Basis As Received
File Name 028045
CASNO Target Analyte Dilution Factor
71-43-2 BENZENE 1
79-01-6 TRICHLOROETHENE 1
78-87-5 12-DICHLOROPROPANE 1
74-95-3 DIBROMOMETHANE 1
75-27-4 BROMODICHLOROMETHANE 1
10061-01-5 CIS-13-DICHLOROPROPENE 1
108-10-1 4-METHYL-2-PtNTANON 1
108-88-3 TOLUENE 1
10061-02-6 TRANS-13-DICHLOROPROPENE 1
79-00-5 112-TRICHLOROETHANE 1
591-78-6 2-HEXANONE 1
127-18-4 TETRACHLOROETHENE 1
142-28-9 13-DICHLOROPROPANt 1
124-48-1 DI3ROMOCHLOROMETHANE 1
106-93-4 12-DIBROMOETHANE 1
108-90-7 CHLOROBENZENE 1
OETHANE 1
- 1
LENE 1
ENE 1
ENE 1
OFORM 1
OPYlBENZENE 1
96-18-4 123-TRICHLOROPROPANE 1
79-34-5 1122-TETRACHLOROETHANE 1
108-86-1 BROMOBENZENE 1
Result Reporting Limit
05 05
05 05
05 05
05 05
05 05
05 05
5 5
025 05
05 05
05 05
10 10
05 05
05 05
1 1
1 1
05 05
05 05
05 05
1 1
05 05
05 05
05 05
05 05
2 2
05 05
05 05
MDL Result EPA Qualifier Qualifier
017 U
017 U
017 U
017 U
017 U
017 U
17 U
017 J
017 U
017 U
17 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
Data Package 10 VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- Fe Page 6 of 8
317A
17
GCMS Volatiles Method SW8260 _258
Sample Results
Lab Name ALS Laboratory Group -- FC
Work Order Number 0911214
Client Name New Mexico Environment Department 08
ClientProject 10 644-11S09(HWB R-37 VOCs) PAR 002731703
Field 10 Rmiddot37 Scr 1-111809
Lab 10 0911214-2
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml Moisture NA QCBatchlD VL091125-4-5 Final Volume 10 ml
Date Collected 18-Nov-09 Run 10 VL091125-4A Result Units UGL Date Extracted 25-Nol-09 Cleanup NONE Clean OF
Analysis ReqCode 104 Date Analyzed 25-Nov-09 Basis As Received Prep Method SW5030 Rev C File Name D28045
CASNO Target Analyte Dilution Factor
103-65-1 N-PROPYLBENZENE 1
95-49-8 2-CHLOROTOLUENE 1
108-67-8 135-TRIMETHYLBENZENE 1
106-43-4 4-CHLOROTOLUENE 1
98-06-6 TERT-BUTYLBENZENE 1
95-63-6 124-TRIMETHYLBENZENE 1
135-98-8 SEC-BUTYLBENZENE 1
i 541-73-1 13middotDICHLOROBENZENE 1
99-87-6 PmiddotISOPROPYL TOLUENE 1
106-46-7 I 14-DICHLOROBENZENE 1
104-51-8 I N-BUTYLBENZENE 1
95-50-1 l2-DICHLOROBENZENE 1
96-12-8 I 12-DIBROMO-3-CHLOROPROPANE 1
120-82-1 124-TRICHLOROBENZENE 1
87-68-3 HEXACHLOROBUT ADIENE 1
91-20-3 NAPHTHALENE 1
87-61-6 123-TRICHLOROBENZENE 1
75-05-S ACETONITRILE 1
107-05-1 ALLYL CH LORIDE 1
110-57-6 TRAN S-14-DICHLORO-2-BUTENE 1
64-17-5 ETHANOL 1
97-63-2 ETHYL METHACRYLATE 1
78-83-1 ISOBUTYL ALCOHOL 1
126-98-7 METHACRYLONITRILE 1
80-62-6 METHYL METHACRYLATE 1
107-12-0 I PROPIONITRILE 1
Result Reporting Limit
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
2 2
05 05
05 05
05 05
05 05
50 50
50 50 I 5 5
200 200
5 5
100 100
35 35
5 5
25 25
MDL
017
017
017
017
017
017
017
017
017
017
017
017
067
017
017
017
017
83
017
17
78
017
17
17
17
33
Result EPA Qualifier Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
Data Package 10 VL0911214-1
Date Printed Wednesday December 022009 ALS Laboratory Group -- Fe Page 7 of 8
LlMS Version 6317A
18
GCMS Volatiles Method SW8260_258
Sample Results
Lab Name ALS Laboratory Group bullbull FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644middot111B09(HWB R-37 VOCs) PAR 002731703
Sample Matrix WATER Prep Batch VL091125--4 Sample Aliquot 10 mlRmiddot37 Ser 1-111809 Moisture NA QCBatchlO VL091125--4-5 Final Volume 10 m
0911214-2 Date Collected 18-Nov-09 Run 10 VL091125--4A Result Units UGL Date Extracted 25-Nov-09 Cleanup NONE Clean OF 1 Date Analyzed 25-Nov-09 Basis As Received
10
Analysis ReqCode 104 Prep Method SW5030 Rev C File Name 028045
I
CASNO Target Analyte Dilution Factor
Result Reporting Limit
MDL Result Qualifier
EPA Qualifier
126-99-8 CHLOROPRENE 1 5 5 017 U
75-65-0 TERT-BUTANOL 1 100 100 33 U
108-20-3 ISOPROPYL ETHER 1 2 2 033 U
637-92-3 ETHYL TERT-BUTYL ETHER 1 2 2 033 U
994-05--8 TERT-AMYL MTHYL ETHER 1 2 2 033 U
67-72-1 HEXACHLOROETHANE 1 2 2 033 U
Surrogate Recovery
CASNO Surrogate Analyte Result Flag Spike Amount
Percent Control Recovery Limits
460-00-4 4middotBROMOFLUOROBENZENE 247 25 99 1
1868-53-7 DIBROMOFLUOROMETHANE 248 25 99 80 123
2037-26-5 TOLUENEmiddotDB 255 25 102 85 - 116
Data Package 10 VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- FC Page B of 8
LlMS Version 6317A
19
GCMS Volatiles Method SW8260_258
Laboratory Control Sample and Laboratory Control Sample Duplicate
Lab Name ALS Laboratory Group - FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-111809(HWB R-37 VOCs) PAR 002731703
Lab 10 VL091125-4LCS Sample Matrix WATER
Moisture NA Prep Batch VL091125-4
QCBatchlD VL091125-4-5
Sample Aliquot
Final Volume
10ml
10ml Date Collected NA Run 10 VL091125-4A Result Units UGIL Date Extracted 111252009 Cleanup NONE Clean OF 1 Date Analyzed 11252009 Basis NA
Prep Method SW5030C File Name 028040
CASNO
74-87-3
75-01-4
74-83-9
75-69-4
75-35-4
75-15-0
156-60-5
75-34-3
108-05-4
156-59-2
78-93-3
67 -66-3
71-55-6
i 56-23-5
107-06-2
71-43-2
79-01-6
78-87-5
75-27-4
108-88-3
79-00-5
591-78-6
127-18-4
106-93-4
108-90-7
63Q20-6
Target Analyte Spike Added
CHLOROMETHANE 10
VINYL CHLORIDE 10
BROMOMETHANE 10
TRICHLOROFLUOROMETHANE 10
11-DICHLOROETHENE 10
CARBON DISULFIDE 10
TRANS-12-DICHLOROETHENE 10
11-DICHLOROETHANE 10
VINYL ACETATE 10
CIS-12-DICHLOROETHENE 10
2middotBUTANONE 40
CHLOROFORM 10
111-TRICHL ORO ETHANE 10
CARBON TETRACHLORIDE 10
12-DICHLOROETHANE 10
BENZENE 10
TRICHLOROETHENE 10
12-DICHLOROPROPANE 10
BROMODICHLOROMETHANE 10
TOLUENE 10
112-TRICHLOROETHANE 10
2-HEXANONE 40
TETRACHLOROETHENE 10
12-DIBROMOETHANE 10
CHLOROBENZENE 10
1112-TETRACHLOROETHANE 10
LCS Reporting Result Result Limit Qualifier
932 05
863 05
943 1
908 05
96 05
95 10 J
996 05
992 05
10 10
102 05
412 5
993 05
974 1
943 05
106 05
983 05
962 05
10 05
988 05
974 05
989 05
409 10
956 05
991 1
984 05
101 05
LCS Control Rec Limits
93 49 -129
86 46 134
94 32-121
91 67 -152
96 61 -135
95 61 -140
100 70 -122
99 76 -119
100 62 182
102 75 126
103 61 -137
99 79 120
97 76 - 114
94 58middot135
106 75middot132
98 70 shy 125
96 74 121
100 81 -119
99 79 - 123
97 76 - 120
99 81 -126
102 45 168
96 56 -128
99 79 -123
98 75 -120
101 82 - 123
Data Package 10 VL0911214middot1
-Date Printed Wednesday December 02 2009 ALS Laboratory Group -- Fe Page 1 of 4
LiMS Version 6317A
20
GCMS Volatiles Method SW8260_25B
Laboratory Control Sample and Laboratory Control Sample Duplicate
Lab Name ALS Laboratory Group - FC
Work Order Number 0911214
Client Name New Mexico Envircnment Department OB
ClientProject 10 644-111809(HWB R-37 VOes) PAR 002731703
Lab 10 VL091125-4LCS Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml
Moisture NIA QCBatchlO VL091125-4-5 Final Volume 10 mi
Date Collected NA Run 10 VL091125-4A Result Units UGL Date Extracted 11252009 Cleanup NONE Clean OF 1 Date Analyzed 111252009 Basis NA
Prep Method SW5030e File Name 028040
CASNO Target Analyte Spike Added
LCS Result
Reporting Limit
Result Qualifier
LCS Rec
Control Limits
100-41-4 ETHYLBENZENE 10 981 05 98 79 -114
136777-61-2 M+P-XYLENE 20 197 1 98 81-115
95-47-6 O-XYLENE 10 101 05 101 81 -115
95-49-8 2-CHLOROTOLUENE 10 97 05 97 80 -128
541-73-1 13-DICHLOROBENZiNt 10 977 05 98 81-116
106-46-7 14-DICHLOROBENZENE 10 979 05 98 81 -119
95-50-1 12-DICHLOROBENZENE 10 987 05 99 79 - 116
91-20-3 NAPHTHALENE 10 993 05 99 69 -126
87-61-6 123-TRICHLOROBENZENE 10 999 05 100 60 -137
Data Package ID VL0911214-1
Date Printed Wecnesday December 02 2009 ALS Laboratory Group -- Fe Page 2 of 4
21
GCMS Volatiles Method SW8260_25B
Laboratory Control Sample and Laboratory Control Sample Duplicate
Lab Name ALS Laboratory Group bullbull FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-11 1809(HWB R-37 VOCs) PAR 002731703
Lab 10 VL091125middot4LCSD Sample Matrix WATER
Moisture NIA Prep Batch VL091125-4
QCBatchlD VL091125-4-5
Sample Aliquot
Final Volume
10 ml
10ml Date Collected NIA Run ID VL091125-4A Result Units UGIL Date Extracted 112512009 Cleanup NONE Clean DF 1 Date Analyzed 1112512009 Basis NIA
Prep Method SW5030C File Name 028041
CASNO Target Analyte Spike Added
LCSD Result
Reporting Limit
Result Qualifier
LCSD Rec
RPD Limit
RPD
74-87-3 CHLOROMETHANE 10 897 05 90 30 4
75-01-4 VINYL CHLORIDE 10 831 05 83 25 4
74-83-9 BROMO METHANE 10 945 1 94 25 0
75-69-4 TRICHLOROFLUOROMETHANE 10 873 05 87 22 4
75-35-4 11-DICHLOROETHENE 10 909 05 91 18 5
75-15-0 CARBON DISULFIDE 10 941 10 J 94 20 1
156-60middot5 TRANS-l2middotDICHLOROETHENE 10 961 05 96 25 4
75middot34middot3 11-DICHLOROETHANE 10 977 05 98 25 2
108-05-4 VINYL ACETATE 10 993 10 J 99 20 1
156middot59-2 CIS-12-DlCHLOROETHENE 10 995 05 99 25 3
i 78-93-3 2-BUTANONE 40 419 5 105 30 2
67-66-3 CHLOROFORM 10 985 05 99 25 1
71-55-6 lll-TRICHLOROETHANE 10 942 1 94 25 3
56-23-5 CARBON TETRACHLORIDE 10 922 05 92 25 2
107middot06-2 12middotDICHLOROETHANE 10 106 05 106 25 0
71-43middot2 BENZENE 10 971 05 97 10 1
79middot01middot6 TRICHLOROETHENE 10 939 05 94 10 2
78middot87middot5 l2middotDICHLOROPROPANE 10 101 05 101 25 1
i 75middot27-4 BROMODICHLOROMETHANE 10 992 05 99 25 0
1108-88-3 TOLUENE 10 962 05 96 9 1
I 79005 112middotTRICHLOROETHANE 10 986 05 99 25 0
591middot78middot6 2-HEXANONE 40 418 10 104 20 2
127middot18-4 TETRACHLOROETHENE 10 918 05 92 25 4
106-93-4 12middotDIBROMOETHANE 10 999 1 100 15 1
108middot90-7 CHLOROBENZENE 10 997 05 100 11 1
630-20middot6 1112-TETRACHLOROETHANE 10 101 05 101 15 0
100-41-4 ETHYLBENZENE 10 968 05 97 25 1
Data Package ID VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- FC Page 3 of 4
lIMS Version 6317 A
22
GCMS Volatiles Method SW8260_25B
Laboratory Control Sample and Laboratory Control Sample Duplicate
Lab Name ALS Laboratory 13roup -- FC
Work Order Number 0911214
Client Name New Mexico Environment Department OS
ClientProject 10 644-11 1809(HWB R-37 VOCs) PAR 002731703
Lab 10 VL091125-4LCSD Sample Matrix WATER
Moisture NA Prep Batch VL091125-4
QCBatchlO VL091125-4-5
Sample Aliquot
Final Volume
10 ml
10ml Date Collected NA Run 10 VL091125-4A Result Units UGL Date Extracted 11252009 Cleanup NONE Clean OF Date Analyzed 11252009 Basis NIA
Prep Method SW5030C File Name 028041
CASNO Target Analyte Spike Added
LCSD Result
Reporting Limit
Result Qualifier
LCSD Rec
RPD Limit
RPD
136777-61-2 M+P-XYLENE 20 193 1 97 25 2
95-47-6 O-XYLENE 10 983 05 98 25 2
95-49-8 2middotCHLOROTOLUENE 10 9A9 05 95 15 2
541-73-1 13middotDICHLOROBENZENE 10 997 05 100 25 2
106-46-7 14-DICHLOROBeNZENE 10 974 05 97 25 1
95-50middot1 12middotDICHLOROBENZeNE 10 101 05 101 25 2
91middot20-3 NAPHTHALENe 10 105 05 105 24 6
87-61-6 123-TRICHLOROBENZENE 10 102 05 102 33 3
Surrogate Recovery LCSLCSD
CASNO Target Analyte Spike Added
LCS Rec
LCS Flag
LCSD Rec
LCSD Flag
Control Limits
460middot00-4 4-BROMOFLUOROBeNZENE 25 100 100 82 - 121
1868-53middot7 DIBROMOFLUOROMeTHANE 25 101 100 80middot 123
2037middot26-5 TOLUENEmiddotD8 25 102 100 85middot 116
Data Package 10 VL0911214-
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- Fe Page 4 of 4
UMS Verslmt 6317A
23
GCMS Volatiles Method SW8260_25B
Sample Results
Lab Name ALS Laboratory Group -- FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-111809(HW3 R-37 VOCs) PAR 002731703
Field 10 R-37 Scr 1-11 1809
Lab 10 0911214-2
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml
Moisture NIA QCBatchlO VL091125-4-5 Final Volume 10 ml
Date Collected 18-Nov-09 Run 10 VL091125-4A Result Units UGL
[late Extracted 25-Nov-09 Cleanup NONE Clean OF 1
Analysis ReqCode 104 Date Analyzed 25-Nov-09
Prep Method SW5030 Rev C Basis As Received
File Name 028045
CASNO Target Analyte Dilution Factor
71-43-2 BENZENE 1
79-01-6 TRICHLOROETHENE 1
78-87-5 12-DICHLOROPROPANE 1
74-95-3 DIBROMOMETHANE 1
75-27-4 BROMODICHLOROMETHANE 1
10061-01-5 CIS-13-DICHLOROPROPENE 1
108-10-1 4-METHYL-2-PtNTANON 1
108-88-3 TOLUENE 1
10061-02-6 TRANS-13-DICHLOROPROPENE 1
79-00-5 112-TRICHLOROETHANE 1
591-78-6 2-HEXANONE 1
127-18-4 TETRACHLOROETHENE 1
142-28-9 13-DICHLOROPROPANt 1
124-48-1 DI3ROMOCHLOROMETHANE 1
106-93-4 12-DIBROMOETHANE 1
108-90-7 CHLOROBENZENE 1
OETHANE 1
- 1
LENE 1
ENE 1
ENE 1
OFORM 1
OPYlBENZENE 1
96-18-4 123-TRICHLOROPROPANE 1
79-34-5 1122-TETRACHLOROETHANE 1
108-86-1 BROMOBENZENE 1
Result Reporting Limit
05 05
05 05
05 05
05 05
05 05
05 05
5 5
025 05
05 05
05 05
10 10
05 05
05 05
1 1
1 1
05 05
05 05
05 05
1 1
05 05
05 05
05 05
05 05
2 2
05 05
05 05
MDL Result EPA Qualifier Qualifier
017 U
017 U
017 U
017 U
017 U
017 U
17 U
017 J
017 U
017 U
17 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
017 U
Data Package 10 VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- Fe Page 6 of 8
317A
17
GCMS Volatiles Method SW8260 _258
Sample Results
Lab Name ALS Laboratory Group -- FC
Work Order Number 0911214
Client Name New Mexico Environment Department 08
ClientProject 10 644-11S09(HWB R-37 VOCs) PAR 002731703
Field 10 Rmiddot37 Scr 1-111809
Lab 10 0911214-2
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml Moisture NA QCBatchlD VL091125-4-5 Final Volume 10 ml
Date Collected 18-Nov-09 Run 10 VL091125-4A Result Units UGL Date Extracted 25-Nol-09 Cleanup NONE Clean OF
Analysis ReqCode 104 Date Analyzed 25-Nov-09 Basis As Received Prep Method SW5030 Rev C File Name D28045
CASNO Target Analyte Dilution Factor
103-65-1 N-PROPYLBENZENE 1
95-49-8 2-CHLOROTOLUENE 1
108-67-8 135-TRIMETHYLBENZENE 1
106-43-4 4-CHLOROTOLUENE 1
98-06-6 TERT-BUTYLBENZENE 1
95-63-6 124-TRIMETHYLBENZENE 1
135-98-8 SEC-BUTYLBENZENE 1
i 541-73-1 13middotDICHLOROBENZENE 1
99-87-6 PmiddotISOPROPYL TOLUENE 1
106-46-7 I 14-DICHLOROBENZENE 1
104-51-8 I N-BUTYLBENZENE 1
95-50-1 l2-DICHLOROBENZENE 1
96-12-8 I 12-DIBROMO-3-CHLOROPROPANE 1
120-82-1 124-TRICHLOROBENZENE 1
87-68-3 HEXACHLOROBUT ADIENE 1
91-20-3 NAPHTHALENE 1
87-61-6 123-TRICHLOROBENZENE 1
75-05-S ACETONITRILE 1
107-05-1 ALLYL CH LORIDE 1
110-57-6 TRAN S-14-DICHLORO-2-BUTENE 1
64-17-5 ETHANOL 1
97-63-2 ETHYL METHACRYLATE 1
78-83-1 ISOBUTYL ALCOHOL 1
126-98-7 METHACRYLONITRILE 1
80-62-6 METHYL METHACRYLATE 1
107-12-0 I PROPIONITRILE 1
Result Reporting Limit
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
2 2
05 05
05 05
05 05
05 05
50 50
50 50 I 5 5
200 200
5 5
100 100
35 35
5 5
25 25
MDL
017
017
017
017
017
017
017
017
017
017
017
017
067
017
017
017
017
83
017
17
78
017
17
17
17
33
Result EPA Qualifier Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
Data Package 10 VL0911214-1
Date Printed Wednesday December 022009 ALS Laboratory Group -- Fe Page 7 of 8
LlMS Version 6317A
18
GCMS Volatiles Method SW8260_258
Sample Results
Lab Name ALS Laboratory Group bullbull FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644middot111B09(HWB R-37 VOCs) PAR 002731703
Sample Matrix WATER Prep Batch VL091125--4 Sample Aliquot 10 mlRmiddot37 Ser 1-111809 Moisture NA QCBatchlO VL091125--4-5 Final Volume 10 m
0911214-2 Date Collected 18-Nov-09 Run 10 VL091125--4A Result Units UGL Date Extracted 25-Nov-09 Cleanup NONE Clean OF 1 Date Analyzed 25-Nov-09 Basis As Received
10
Analysis ReqCode 104 Prep Method SW5030 Rev C File Name 028045
I
CASNO Target Analyte Dilution Factor
Result Reporting Limit
MDL Result Qualifier
EPA Qualifier
126-99-8 CHLOROPRENE 1 5 5 017 U
75-65-0 TERT-BUTANOL 1 100 100 33 U
108-20-3 ISOPROPYL ETHER 1 2 2 033 U
637-92-3 ETHYL TERT-BUTYL ETHER 1 2 2 033 U
994-05--8 TERT-AMYL MTHYL ETHER 1 2 2 033 U
67-72-1 HEXACHLOROETHANE 1 2 2 033 U
Surrogate Recovery
CASNO Surrogate Analyte Result Flag Spike Amount
Percent Control Recovery Limits
460-00-4 4middotBROMOFLUOROBENZENE 247 25 99 1
1868-53-7 DIBROMOFLUOROMETHANE 248 25 99 80 123
2037-26-5 TOLUENEmiddotDB 255 25 102 85 - 116
Data Package 10 VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- FC Page B of 8
LlMS Version 6317A
19
GCMS Volatiles Method SW8260_258
Laboratory Control Sample and Laboratory Control Sample Duplicate
Lab Name ALS Laboratory Group - FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-111809(HWB R-37 VOCs) PAR 002731703
Lab 10 VL091125-4LCS Sample Matrix WATER
Moisture NA Prep Batch VL091125-4
QCBatchlD VL091125-4-5
Sample Aliquot
Final Volume
10ml
10ml Date Collected NA Run 10 VL091125-4A Result Units UGIL Date Extracted 111252009 Cleanup NONE Clean OF 1 Date Analyzed 11252009 Basis NA
Prep Method SW5030C File Name 028040
CASNO
74-87-3
75-01-4
74-83-9
75-69-4
75-35-4
75-15-0
156-60-5
75-34-3
108-05-4
156-59-2
78-93-3
67 -66-3
71-55-6
i 56-23-5
107-06-2
71-43-2
79-01-6
78-87-5
75-27-4
108-88-3
79-00-5
591-78-6
127-18-4
106-93-4
108-90-7
63Q20-6
Target Analyte Spike Added
CHLOROMETHANE 10
VINYL CHLORIDE 10
BROMOMETHANE 10
TRICHLOROFLUOROMETHANE 10
11-DICHLOROETHENE 10
CARBON DISULFIDE 10
TRANS-12-DICHLOROETHENE 10
11-DICHLOROETHANE 10
VINYL ACETATE 10
CIS-12-DICHLOROETHENE 10
2middotBUTANONE 40
CHLOROFORM 10
111-TRICHL ORO ETHANE 10
CARBON TETRACHLORIDE 10
12-DICHLOROETHANE 10
BENZENE 10
TRICHLOROETHENE 10
12-DICHLOROPROPANE 10
BROMODICHLOROMETHANE 10
TOLUENE 10
112-TRICHLOROETHANE 10
2-HEXANONE 40
TETRACHLOROETHENE 10
12-DIBROMOETHANE 10
CHLOROBENZENE 10
1112-TETRACHLOROETHANE 10
LCS Reporting Result Result Limit Qualifier
932 05
863 05
943 1
908 05
96 05
95 10 J
996 05
992 05
10 10
102 05
412 5
993 05
974 1
943 05
106 05
983 05
962 05
10 05
988 05
974 05
989 05
409 10
956 05
991 1
984 05
101 05
LCS Control Rec Limits
93 49 -129
86 46 134
94 32-121
91 67 -152
96 61 -135
95 61 -140
100 70 -122
99 76 -119
100 62 182
102 75 126
103 61 -137
99 79 120
97 76 - 114
94 58middot135
106 75middot132
98 70 shy 125
96 74 121
100 81 -119
99 79 - 123
97 76 - 120
99 81 -126
102 45 168
96 56 -128
99 79 -123
98 75 -120
101 82 - 123
Data Package 10 VL0911214middot1
-Date Printed Wednesday December 02 2009 ALS Laboratory Group -- Fe Page 1 of 4
LiMS Version 6317A
20
GCMS Volatiles Method SW8260_25B
Laboratory Control Sample and Laboratory Control Sample Duplicate
Lab Name ALS Laboratory Group - FC
Work Order Number 0911214
Client Name New Mexico Envircnment Department OB
ClientProject 10 644-111809(HWB R-37 VOes) PAR 002731703
Lab 10 VL091125-4LCS Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml
Moisture NIA QCBatchlO VL091125-4-5 Final Volume 10 mi
Date Collected NA Run 10 VL091125-4A Result Units UGL Date Extracted 11252009 Cleanup NONE Clean OF 1 Date Analyzed 111252009 Basis NA
Prep Method SW5030e File Name 028040
CASNO Target Analyte Spike Added
LCS Result
Reporting Limit
Result Qualifier
LCS Rec
Control Limits
100-41-4 ETHYLBENZENE 10 981 05 98 79 -114
136777-61-2 M+P-XYLENE 20 197 1 98 81-115
95-47-6 O-XYLENE 10 101 05 101 81 -115
95-49-8 2-CHLOROTOLUENE 10 97 05 97 80 -128
541-73-1 13-DICHLOROBENZiNt 10 977 05 98 81-116
106-46-7 14-DICHLOROBENZENE 10 979 05 98 81 -119
95-50-1 12-DICHLOROBENZENE 10 987 05 99 79 - 116
91-20-3 NAPHTHALENE 10 993 05 99 69 -126
87-61-6 123-TRICHLOROBENZENE 10 999 05 100 60 -137
Data Package ID VL0911214-1
Date Printed Wecnesday December 02 2009 ALS Laboratory Group -- Fe Page 2 of 4
21
GCMS Volatiles Method SW8260_25B
Laboratory Control Sample and Laboratory Control Sample Duplicate
Lab Name ALS Laboratory Group bullbull FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-11 1809(HWB R-37 VOCs) PAR 002731703
Lab 10 VL091125middot4LCSD Sample Matrix WATER
Moisture NIA Prep Batch VL091125-4
QCBatchlD VL091125-4-5
Sample Aliquot
Final Volume
10 ml
10ml Date Collected NIA Run ID VL091125-4A Result Units UGIL Date Extracted 112512009 Cleanup NONE Clean DF 1 Date Analyzed 1112512009 Basis NIA
Prep Method SW5030C File Name 028041
CASNO Target Analyte Spike Added
LCSD Result
Reporting Limit
Result Qualifier
LCSD Rec
RPD Limit
RPD
74-87-3 CHLOROMETHANE 10 897 05 90 30 4
75-01-4 VINYL CHLORIDE 10 831 05 83 25 4
74-83-9 BROMO METHANE 10 945 1 94 25 0
75-69-4 TRICHLOROFLUOROMETHANE 10 873 05 87 22 4
75-35-4 11-DICHLOROETHENE 10 909 05 91 18 5
75-15-0 CARBON DISULFIDE 10 941 10 J 94 20 1
156-60middot5 TRANS-l2middotDICHLOROETHENE 10 961 05 96 25 4
75middot34middot3 11-DICHLOROETHANE 10 977 05 98 25 2
108-05-4 VINYL ACETATE 10 993 10 J 99 20 1
156middot59-2 CIS-12-DlCHLOROETHENE 10 995 05 99 25 3
i 78-93-3 2-BUTANONE 40 419 5 105 30 2
67-66-3 CHLOROFORM 10 985 05 99 25 1
71-55-6 lll-TRICHLOROETHANE 10 942 1 94 25 3
56-23-5 CARBON TETRACHLORIDE 10 922 05 92 25 2
107middot06-2 12middotDICHLOROETHANE 10 106 05 106 25 0
71-43middot2 BENZENE 10 971 05 97 10 1
79middot01middot6 TRICHLOROETHENE 10 939 05 94 10 2
78middot87middot5 l2middotDICHLOROPROPANE 10 101 05 101 25 1
i 75middot27-4 BROMODICHLOROMETHANE 10 992 05 99 25 0
1108-88-3 TOLUENE 10 962 05 96 9 1
I 79005 112middotTRICHLOROETHANE 10 986 05 99 25 0
591middot78middot6 2-HEXANONE 40 418 10 104 20 2
127middot18-4 TETRACHLOROETHENE 10 918 05 92 25 4
106-93-4 12middotDIBROMOETHANE 10 999 1 100 15 1
108middot90-7 CHLOROBENZENE 10 997 05 100 11 1
630-20middot6 1112-TETRACHLOROETHANE 10 101 05 101 15 0
100-41-4 ETHYLBENZENE 10 968 05 97 25 1
Data Package ID VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- FC Page 3 of 4
lIMS Version 6317 A
22
GCMS Volatiles Method SW8260_25B
Laboratory Control Sample and Laboratory Control Sample Duplicate
Lab Name ALS Laboratory 13roup -- FC
Work Order Number 0911214
Client Name New Mexico Environment Department OS
ClientProject 10 644-11 1809(HWB R-37 VOCs) PAR 002731703
Lab 10 VL091125-4LCSD Sample Matrix WATER
Moisture NA Prep Batch VL091125-4
QCBatchlO VL091125-4-5
Sample Aliquot
Final Volume
10 ml
10ml Date Collected NA Run 10 VL091125-4A Result Units UGL Date Extracted 11252009 Cleanup NONE Clean OF Date Analyzed 11252009 Basis NIA
Prep Method SW5030C File Name 028041
CASNO Target Analyte Spike Added
LCSD Result
Reporting Limit
Result Qualifier
LCSD Rec
RPD Limit
RPD
136777-61-2 M+P-XYLENE 20 193 1 97 25 2
95-47-6 O-XYLENE 10 983 05 98 25 2
95-49-8 2middotCHLOROTOLUENE 10 9A9 05 95 15 2
541-73-1 13middotDICHLOROBENZENE 10 997 05 100 25 2
106-46-7 14-DICHLOROBeNZENE 10 974 05 97 25 1
95-50middot1 12middotDICHLOROBENZeNE 10 101 05 101 25 2
91middot20-3 NAPHTHALENe 10 105 05 105 24 6
87-61-6 123-TRICHLOROBENZENE 10 102 05 102 33 3
Surrogate Recovery LCSLCSD
CASNO Target Analyte Spike Added
LCS Rec
LCS Flag
LCSD Rec
LCSD Flag
Control Limits
460middot00-4 4-BROMOFLUOROBeNZENE 25 100 100 82 - 121
1868-53middot7 DIBROMOFLUOROMeTHANE 25 101 100 80middot 123
2037middot26-5 TOLUENEmiddotD8 25 102 100 85middot 116
Data Package 10 VL0911214-
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- Fe Page 4 of 4
UMS Verslmt 6317A
23
GCMS Volatiles Method SW8260 _258
Sample Results
Lab Name ALS Laboratory Group -- FC
Work Order Number 0911214
Client Name New Mexico Environment Department 08
ClientProject 10 644-11S09(HWB R-37 VOCs) PAR 002731703
Field 10 Rmiddot37 Scr 1-111809
Lab 10 0911214-2
Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml Moisture NA QCBatchlD VL091125-4-5 Final Volume 10 ml
Date Collected 18-Nov-09 Run 10 VL091125-4A Result Units UGL Date Extracted 25-Nol-09 Cleanup NONE Clean OF
Analysis ReqCode 104 Date Analyzed 25-Nov-09 Basis As Received Prep Method SW5030 Rev C File Name D28045
CASNO Target Analyte Dilution Factor
103-65-1 N-PROPYLBENZENE 1
95-49-8 2-CHLOROTOLUENE 1
108-67-8 135-TRIMETHYLBENZENE 1
106-43-4 4-CHLOROTOLUENE 1
98-06-6 TERT-BUTYLBENZENE 1
95-63-6 124-TRIMETHYLBENZENE 1
135-98-8 SEC-BUTYLBENZENE 1
i 541-73-1 13middotDICHLOROBENZENE 1
99-87-6 PmiddotISOPROPYL TOLUENE 1
106-46-7 I 14-DICHLOROBENZENE 1
104-51-8 I N-BUTYLBENZENE 1
95-50-1 l2-DICHLOROBENZENE 1
96-12-8 I 12-DIBROMO-3-CHLOROPROPANE 1
120-82-1 124-TRICHLOROBENZENE 1
87-68-3 HEXACHLOROBUT ADIENE 1
91-20-3 NAPHTHALENE 1
87-61-6 123-TRICHLOROBENZENE 1
75-05-S ACETONITRILE 1
107-05-1 ALLYL CH LORIDE 1
110-57-6 TRAN S-14-DICHLORO-2-BUTENE 1
64-17-5 ETHANOL 1
97-63-2 ETHYL METHACRYLATE 1
78-83-1 ISOBUTYL ALCOHOL 1
126-98-7 METHACRYLONITRILE 1
80-62-6 METHYL METHACRYLATE 1
107-12-0 I PROPIONITRILE 1
Result Reporting Limit
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
05 05
2 2
05 05
05 05
05 05
05 05
50 50
50 50 I 5 5
200 200
5 5
100 100
35 35
5 5
25 25
MDL
017
017
017
017
017
017
017
017
017
017
017
017
067
017
017
017
017
83
017
17
78
017
17
17
17
33
Result EPA Qualifier Qualifier
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
Data Package 10 VL0911214-1
Date Printed Wednesday December 022009 ALS Laboratory Group -- Fe Page 7 of 8
LlMS Version 6317A
18
GCMS Volatiles Method SW8260_258
Sample Results
Lab Name ALS Laboratory Group bullbull FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644middot111B09(HWB R-37 VOCs) PAR 002731703
Sample Matrix WATER Prep Batch VL091125--4 Sample Aliquot 10 mlRmiddot37 Ser 1-111809 Moisture NA QCBatchlO VL091125--4-5 Final Volume 10 m
0911214-2 Date Collected 18-Nov-09 Run 10 VL091125--4A Result Units UGL Date Extracted 25-Nov-09 Cleanup NONE Clean OF 1 Date Analyzed 25-Nov-09 Basis As Received
10
Analysis ReqCode 104 Prep Method SW5030 Rev C File Name 028045
I
CASNO Target Analyte Dilution Factor
Result Reporting Limit
MDL Result Qualifier
EPA Qualifier
126-99-8 CHLOROPRENE 1 5 5 017 U
75-65-0 TERT-BUTANOL 1 100 100 33 U
108-20-3 ISOPROPYL ETHER 1 2 2 033 U
637-92-3 ETHYL TERT-BUTYL ETHER 1 2 2 033 U
994-05--8 TERT-AMYL MTHYL ETHER 1 2 2 033 U
67-72-1 HEXACHLOROETHANE 1 2 2 033 U
Surrogate Recovery
CASNO Surrogate Analyte Result Flag Spike Amount
Percent Control Recovery Limits
460-00-4 4middotBROMOFLUOROBENZENE 247 25 99 1
1868-53-7 DIBROMOFLUOROMETHANE 248 25 99 80 123
2037-26-5 TOLUENEmiddotDB 255 25 102 85 - 116
Data Package 10 VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- FC Page B of 8
LlMS Version 6317A
19
GCMS Volatiles Method SW8260_258
Laboratory Control Sample and Laboratory Control Sample Duplicate
Lab Name ALS Laboratory Group - FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-111809(HWB R-37 VOCs) PAR 002731703
Lab 10 VL091125-4LCS Sample Matrix WATER
Moisture NA Prep Batch VL091125-4
QCBatchlD VL091125-4-5
Sample Aliquot
Final Volume
10ml
10ml Date Collected NA Run 10 VL091125-4A Result Units UGIL Date Extracted 111252009 Cleanup NONE Clean OF 1 Date Analyzed 11252009 Basis NA
Prep Method SW5030C File Name 028040
CASNO
74-87-3
75-01-4
74-83-9
75-69-4
75-35-4
75-15-0
156-60-5
75-34-3
108-05-4
156-59-2
78-93-3
67 -66-3
71-55-6
i 56-23-5
107-06-2
71-43-2
79-01-6
78-87-5
75-27-4
108-88-3
79-00-5
591-78-6
127-18-4
106-93-4
108-90-7
63Q20-6
Target Analyte Spike Added
CHLOROMETHANE 10
VINYL CHLORIDE 10
BROMOMETHANE 10
TRICHLOROFLUOROMETHANE 10
11-DICHLOROETHENE 10
CARBON DISULFIDE 10
TRANS-12-DICHLOROETHENE 10
11-DICHLOROETHANE 10
VINYL ACETATE 10
CIS-12-DICHLOROETHENE 10
2middotBUTANONE 40
CHLOROFORM 10
111-TRICHL ORO ETHANE 10
CARBON TETRACHLORIDE 10
12-DICHLOROETHANE 10
BENZENE 10
TRICHLOROETHENE 10
12-DICHLOROPROPANE 10
BROMODICHLOROMETHANE 10
TOLUENE 10
112-TRICHLOROETHANE 10
2-HEXANONE 40
TETRACHLOROETHENE 10
12-DIBROMOETHANE 10
CHLOROBENZENE 10
1112-TETRACHLOROETHANE 10
LCS Reporting Result Result Limit Qualifier
932 05
863 05
943 1
908 05
96 05
95 10 J
996 05
992 05
10 10
102 05
412 5
993 05
974 1
943 05
106 05
983 05
962 05
10 05
988 05
974 05
989 05
409 10
956 05
991 1
984 05
101 05
LCS Control Rec Limits
93 49 -129
86 46 134
94 32-121
91 67 -152
96 61 -135
95 61 -140
100 70 -122
99 76 -119
100 62 182
102 75 126
103 61 -137
99 79 120
97 76 - 114
94 58middot135
106 75middot132
98 70 shy 125
96 74 121
100 81 -119
99 79 - 123
97 76 - 120
99 81 -126
102 45 168
96 56 -128
99 79 -123
98 75 -120
101 82 - 123
Data Package 10 VL0911214middot1
-Date Printed Wednesday December 02 2009 ALS Laboratory Group -- Fe Page 1 of 4
LiMS Version 6317A
20
GCMS Volatiles Method SW8260_25B
Laboratory Control Sample and Laboratory Control Sample Duplicate
Lab Name ALS Laboratory Group - FC
Work Order Number 0911214
Client Name New Mexico Envircnment Department OB
ClientProject 10 644-111809(HWB R-37 VOes) PAR 002731703
Lab 10 VL091125-4LCS Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml
Moisture NIA QCBatchlO VL091125-4-5 Final Volume 10 mi
Date Collected NA Run 10 VL091125-4A Result Units UGL Date Extracted 11252009 Cleanup NONE Clean OF 1 Date Analyzed 111252009 Basis NA
Prep Method SW5030e File Name 028040
CASNO Target Analyte Spike Added
LCS Result
Reporting Limit
Result Qualifier
LCS Rec
Control Limits
100-41-4 ETHYLBENZENE 10 981 05 98 79 -114
136777-61-2 M+P-XYLENE 20 197 1 98 81-115
95-47-6 O-XYLENE 10 101 05 101 81 -115
95-49-8 2-CHLOROTOLUENE 10 97 05 97 80 -128
541-73-1 13-DICHLOROBENZiNt 10 977 05 98 81-116
106-46-7 14-DICHLOROBENZENE 10 979 05 98 81 -119
95-50-1 12-DICHLOROBENZENE 10 987 05 99 79 - 116
91-20-3 NAPHTHALENE 10 993 05 99 69 -126
87-61-6 123-TRICHLOROBENZENE 10 999 05 100 60 -137
Data Package ID VL0911214-1
Date Printed Wecnesday December 02 2009 ALS Laboratory Group -- Fe Page 2 of 4
21
GCMS Volatiles Method SW8260_25B
Laboratory Control Sample and Laboratory Control Sample Duplicate
Lab Name ALS Laboratory Group bullbull FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-11 1809(HWB R-37 VOCs) PAR 002731703
Lab 10 VL091125middot4LCSD Sample Matrix WATER
Moisture NIA Prep Batch VL091125-4
QCBatchlD VL091125-4-5
Sample Aliquot
Final Volume
10 ml
10ml Date Collected NIA Run ID VL091125-4A Result Units UGIL Date Extracted 112512009 Cleanup NONE Clean DF 1 Date Analyzed 1112512009 Basis NIA
Prep Method SW5030C File Name 028041
CASNO Target Analyte Spike Added
LCSD Result
Reporting Limit
Result Qualifier
LCSD Rec
RPD Limit
RPD
74-87-3 CHLOROMETHANE 10 897 05 90 30 4
75-01-4 VINYL CHLORIDE 10 831 05 83 25 4
74-83-9 BROMO METHANE 10 945 1 94 25 0
75-69-4 TRICHLOROFLUOROMETHANE 10 873 05 87 22 4
75-35-4 11-DICHLOROETHENE 10 909 05 91 18 5
75-15-0 CARBON DISULFIDE 10 941 10 J 94 20 1
156-60middot5 TRANS-l2middotDICHLOROETHENE 10 961 05 96 25 4
75middot34middot3 11-DICHLOROETHANE 10 977 05 98 25 2
108-05-4 VINYL ACETATE 10 993 10 J 99 20 1
156middot59-2 CIS-12-DlCHLOROETHENE 10 995 05 99 25 3
i 78-93-3 2-BUTANONE 40 419 5 105 30 2
67-66-3 CHLOROFORM 10 985 05 99 25 1
71-55-6 lll-TRICHLOROETHANE 10 942 1 94 25 3
56-23-5 CARBON TETRACHLORIDE 10 922 05 92 25 2
107middot06-2 12middotDICHLOROETHANE 10 106 05 106 25 0
71-43middot2 BENZENE 10 971 05 97 10 1
79middot01middot6 TRICHLOROETHENE 10 939 05 94 10 2
78middot87middot5 l2middotDICHLOROPROPANE 10 101 05 101 25 1
i 75middot27-4 BROMODICHLOROMETHANE 10 992 05 99 25 0
1108-88-3 TOLUENE 10 962 05 96 9 1
I 79005 112middotTRICHLOROETHANE 10 986 05 99 25 0
591middot78middot6 2-HEXANONE 40 418 10 104 20 2
127middot18-4 TETRACHLOROETHENE 10 918 05 92 25 4
106-93-4 12middotDIBROMOETHANE 10 999 1 100 15 1
108middot90-7 CHLOROBENZENE 10 997 05 100 11 1
630-20middot6 1112-TETRACHLOROETHANE 10 101 05 101 15 0
100-41-4 ETHYLBENZENE 10 968 05 97 25 1
Data Package ID VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- FC Page 3 of 4
lIMS Version 6317 A
22
GCMS Volatiles Method SW8260_25B
Laboratory Control Sample and Laboratory Control Sample Duplicate
Lab Name ALS Laboratory 13roup -- FC
Work Order Number 0911214
Client Name New Mexico Environment Department OS
ClientProject 10 644-11 1809(HWB R-37 VOCs) PAR 002731703
Lab 10 VL091125-4LCSD Sample Matrix WATER
Moisture NA Prep Batch VL091125-4
QCBatchlO VL091125-4-5
Sample Aliquot
Final Volume
10 ml
10ml Date Collected NA Run 10 VL091125-4A Result Units UGL Date Extracted 11252009 Cleanup NONE Clean OF Date Analyzed 11252009 Basis NIA
Prep Method SW5030C File Name 028041
CASNO Target Analyte Spike Added
LCSD Result
Reporting Limit
Result Qualifier
LCSD Rec
RPD Limit
RPD
136777-61-2 M+P-XYLENE 20 193 1 97 25 2
95-47-6 O-XYLENE 10 983 05 98 25 2
95-49-8 2middotCHLOROTOLUENE 10 9A9 05 95 15 2
541-73-1 13middotDICHLOROBENZENE 10 997 05 100 25 2
106-46-7 14-DICHLOROBeNZENE 10 974 05 97 25 1
95-50middot1 12middotDICHLOROBENZeNE 10 101 05 101 25 2
91middot20-3 NAPHTHALENe 10 105 05 105 24 6
87-61-6 123-TRICHLOROBENZENE 10 102 05 102 33 3
Surrogate Recovery LCSLCSD
CASNO Target Analyte Spike Added
LCS Rec
LCS Flag
LCSD Rec
LCSD Flag
Control Limits
460middot00-4 4-BROMOFLUOROBeNZENE 25 100 100 82 - 121
1868-53middot7 DIBROMOFLUOROMeTHANE 25 101 100 80middot 123
2037middot26-5 TOLUENEmiddotD8 25 102 100 85middot 116
Data Package 10 VL0911214-
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- Fe Page 4 of 4
UMS Verslmt 6317A
23
GCMS Volatiles Method SW8260_258
Sample Results
Lab Name ALS Laboratory Group bullbull FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644middot111B09(HWB R-37 VOCs) PAR 002731703
Sample Matrix WATER Prep Batch VL091125--4 Sample Aliquot 10 mlRmiddot37 Ser 1-111809 Moisture NA QCBatchlO VL091125--4-5 Final Volume 10 m
0911214-2 Date Collected 18-Nov-09 Run 10 VL091125--4A Result Units UGL Date Extracted 25-Nov-09 Cleanup NONE Clean OF 1 Date Analyzed 25-Nov-09 Basis As Received
10
Analysis ReqCode 104 Prep Method SW5030 Rev C File Name 028045
I
CASNO Target Analyte Dilution Factor
Result Reporting Limit
MDL Result Qualifier
EPA Qualifier
126-99-8 CHLOROPRENE 1 5 5 017 U
75-65-0 TERT-BUTANOL 1 100 100 33 U
108-20-3 ISOPROPYL ETHER 1 2 2 033 U
637-92-3 ETHYL TERT-BUTYL ETHER 1 2 2 033 U
994-05--8 TERT-AMYL MTHYL ETHER 1 2 2 033 U
67-72-1 HEXACHLOROETHANE 1 2 2 033 U
Surrogate Recovery
CASNO Surrogate Analyte Result Flag Spike Amount
Percent Control Recovery Limits
460-00-4 4middotBROMOFLUOROBENZENE 247 25 99 1
1868-53-7 DIBROMOFLUOROMETHANE 248 25 99 80 123
2037-26-5 TOLUENEmiddotDB 255 25 102 85 - 116
Data Package 10 VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- FC Page B of 8
LlMS Version 6317A
19
GCMS Volatiles Method SW8260_258
Laboratory Control Sample and Laboratory Control Sample Duplicate
Lab Name ALS Laboratory Group - FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-111809(HWB R-37 VOCs) PAR 002731703
Lab 10 VL091125-4LCS Sample Matrix WATER
Moisture NA Prep Batch VL091125-4
QCBatchlD VL091125-4-5
Sample Aliquot
Final Volume
10ml
10ml Date Collected NA Run 10 VL091125-4A Result Units UGIL Date Extracted 111252009 Cleanup NONE Clean OF 1 Date Analyzed 11252009 Basis NA
Prep Method SW5030C File Name 028040
CASNO
74-87-3
75-01-4
74-83-9
75-69-4
75-35-4
75-15-0
156-60-5
75-34-3
108-05-4
156-59-2
78-93-3
67 -66-3
71-55-6
i 56-23-5
107-06-2
71-43-2
79-01-6
78-87-5
75-27-4
108-88-3
79-00-5
591-78-6
127-18-4
106-93-4
108-90-7
63Q20-6
Target Analyte Spike Added
CHLOROMETHANE 10
VINYL CHLORIDE 10
BROMOMETHANE 10
TRICHLOROFLUOROMETHANE 10
11-DICHLOROETHENE 10
CARBON DISULFIDE 10
TRANS-12-DICHLOROETHENE 10
11-DICHLOROETHANE 10
VINYL ACETATE 10
CIS-12-DICHLOROETHENE 10
2middotBUTANONE 40
CHLOROFORM 10
111-TRICHL ORO ETHANE 10
CARBON TETRACHLORIDE 10
12-DICHLOROETHANE 10
BENZENE 10
TRICHLOROETHENE 10
12-DICHLOROPROPANE 10
BROMODICHLOROMETHANE 10
TOLUENE 10
112-TRICHLOROETHANE 10
2-HEXANONE 40
TETRACHLOROETHENE 10
12-DIBROMOETHANE 10
CHLOROBENZENE 10
1112-TETRACHLOROETHANE 10
LCS Reporting Result Result Limit Qualifier
932 05
863 05
943 1
908 05
96 05
95 10 J
996 05
992 05
10 10
102 05
412 5
993 05
974 1
943 05
106 05
983 05
962 05
10 05
988 05
974 05
989 05
409 10
956 05
991 1
984 05
101 05
LCS Control Rec Limits
93 49 -129
86 46 134
94 32-121
91 67 -152
96 61 -135
95 61 -140
100 70 -122
99 76 -119
100 62 182
102 75 126
103 61 -137
99 79 120
97 76 - 114
94 58middot135
106 75middot132
98 70 shy 125
96 74 121
100 81 -119
99 79 - 123
97 76 - 120
99 81 -126
102 45 168
96 56 -128
99 79 -123
98 75 -120
101 82 - 123
Data Package 10 VL0911214middot1
-Date Printed Wednesday December 02 2009 ALS Laboratory Group -- Fe Page 1 of 4
LiMS Version 6317A
20
GCMS Volatiles Method SW8260_25B
Laboratory Control Sample and Laboratory Control Sample Duplicate
Lab Name ALS Laboratory Group - FC
Work Order Number 0911214
Client Name New Mexico Envircnment Department OB
ClientProject 10 644-111809(HWB R-37 VOes) PAR 002731703
Lab 10 VL091125-4LCS Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml
Moisture NIA QCBatchlO VL091125-4-5 Final Volume 10 mi
Date Collected NA Run 10 VL091125-4A Result Units UGL Date Extracted 11252009 Cleanup NONE Clean OF 1 Date Analyzed 111252009 Basis NA
Prep Method SW5030e File Name 028040
CASNO Target Analyte Spike Added
LCS Result
Reporting Limit
Result Qualifier
LCS Rec
Control Limits
100-41-4 ETHYLBENZENE 10 981 05 98 79 -114
136777-61-2 M+P-XYLENE 20 197 1 98 81-115
95-47-6 O-XYLENE 10 101 05 101 81 -115
95-49-8 2-CHLOROTOLUENE 10 97 05 97 80 -128
541-73-1 13-DICHLOROBENZiNt 10 977 05 98 81-116
106-46-7 14-DICHLOROBENZENE 10 979 05 98 81 -119
95-50-1 12-DICHLOROBENZENE 10 987 05 99 79 - 116
91-20-3 NAPHTHALENE 10 993 05 99 69 -126
87-61-6 123-TRICHLOROBENZENE 10 999 05 100 60 -137
Data Package ID VL0911214-1
Date Printed Wecnesday December 02 2009 ALS Laboratory Group -- Fe Page 2 of 4
21
GCMS Volatiles Method SW8260_25B
Laboratory Control Sample and Laboratory Control Sample Duplicate
Lab Name ALS Laboratory Group bullbull FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-11 1809(HWB R-37 VOCs) PAR 002731703
Lab 10 VL091125middot4LCSD Sample Matrix WATER
Moisture NIA Prep Batch VL091125-4
QCBatchlD VL091125-4-5
Sample Aliquot
Final Volume
10 ml
10ml Date Collected NIA Run ID VL091125-4A Result Units UGIL Date Extracted 112512009 Cleanup NONE Clean DF 1 Date Analyzed 1112512009 Basis NIA
Prep Method SW5030C File Name 028041
CASNO Target Analyte Spike Added
LCSD Result
Reporting Limit
Result Qualifier
LCSD Rec
RPD Limit
RPD
74-87-3 CHLOROMETHANE 10 897 05 90 30 4
75-01-4 VINYL CHLORIDE 10 831 05 83 25 4
74-83-9 BROMO METHANE 10 945 1 94 25 0
75-69-4 TRICHLOROFLUOROMETHANE 10 873 05 87 22 4
75-35-4 11-DICHLOROETHENE 10 909 05 91 18 5
75-15-0 CARBON DISULFIDE 10 941 10 J 94 20 1
156-60middot5 TRANS-l2middotDICHLOROETHENE 10 961 05 96 25 4
75middot34middot3 11-DICHLOROETHANE 10 977 05 98 25 2
108-05-4 VINYL ACETATE 10 993 10 J 99 20 1
156middot59-2 CIS-12-DlCHLOROETHENE 10 995 05 99 25 3
i 78-93-3 2-BUTANONE 40 419 5 105 30 2
67-66-3 CHLOROFORM 10 985 05 99 25 1
71-55-6 lll-TRICHLOROETHANE 10 942 1 94 25 3
56-23-5 CARBON TETRACHLORIDE 10 922 05 92 25 2
107middot06-2 12middotDICHLOROETHANE 10 106 05 106 25 0
71-43middot2 BENZENE 10 971 05 97 10 1
79middot01middot6 TRICHLOROETHENE 10 939 05 94 10 2
78middot87middot5 l2middotDICHLOROPROPANE 10 101 05 101 25 1
i 75middot27-4 BROMODICHLOROMETHANE 10 992 05 99 25 0
1108-88-3 TOLUENE 10 962 05 96 9 1
I 79005 112middotTRICHLOROETHANE 10 986 05 99 25 0
591middot78middot6 2-HEXANONE 40 418 10 104 20 2
127middot18-4 TETRACHLOROETHENE 10 918 05 92 25 4
106-93-4 12middotDIBROMOETHANE 10 999 1 100 15 1
108middot90-7 CHLOROBENZENE 10 997 05 100 11 1
630-20middot6 1112-TETRACHLOROETHANE 10 101 05 101 15 0
100-41-4 ETHYLBENZENE 10 968 05 97 25 1
Data Package ID VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- FC Page 3 of 4
lIMS Version 6317 A
22
GCMS Volatiles Method SW8260_25B
Laboratory Control Sample and Laboratory Control Sample Duplicate
Lab Name ALS Laboratory 13roup -- FC
Work Order Number 0911214
Client Name New Mexico Environment Department OS
ClientProject 10 644-11 1809(HWB R-37 VOCs) PAR 002731703
Lab 10 VL091125-4LCSD Sample Matrix WATER
Moisture NA Prep Batch VL091125-4
QCBatchlO VL091125-4-5
Sample Aliquot
Final Volume
10 ml
10ml Date Collected NA Run 10 VL091125-4A Result Units UGL Date Extracted 11252009 Cleanup NONE Clean OF Date Analyzed 11252009 Basis NIA
Prep Method SW5030C File Name 028041
CASNO Target Analyte Spike Added
LCSD Result
Reporting Limit
Result Qualifier
LCSD Rec
RPD Limit
RPD
136777-61-2 M+P-XYLENE 20 193 1 97 25 2
95-47-6 O-XYLENE 10 983 05 98 25 2
95-49-8 2middotCHLOROTOLUENE 10 9A9 05 95 15 2
541-73-1 13middotDICHLOROBENZENE 10 997 05 100 25 2
106-46-7 14-DICHLOROBeNZENE 10 974 05 97 25 1
95-50middot1 12middotDICHLOROBENZeNE 10 101 05 101 25 2
91middot20-3 NAPHTHALENe 10 105 05 105 24 6
87-61-6 123-TRICHLOROBENZENE 10 102 05 102 33 3
Surrogate Recovery LCSLCSD
CASNO Target Analyte Spike Added
LCS Rec
LCS Flag
LCSD Rec
LCSD Flag
Control Limits
460middot00-4 4-BROMOFLUOROBeNZENE 25 100 100 82 - 121
1868-53middot7 DIBROMOFLUOROMeTHANE 25 101 100 80middot 123
2037middot26-5 TOLUENEmiddotD8 25 102 100 85middot 116
Data Package 10 VL0911214-
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- Fe Page 4 of 4
UMS Verslmt 6317A
23
GCMS Volatiles Method SW8260_258
Laboratory Control Sample and Laboratory Control Sample Duplicate
Lab Name ALS Laboratory Group - FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-111809(HWB R-37 VOCs) PAR 002731703
Lab 10 VL091125-4LCS Sample Matrix WATER
Moisture NA Prep Batch VL091125-4
QCBatchlD VL091125-4-5
Sample Aliquot
Final Volume
10ml
10ml Date Collected NA Run 10 VL091125-4A Result Units UGIL Date Extracted 111252009 Cleanup NONE Clean OF 1 Date Analyzed 11252009 Basis NA
Prep Method SW5030C File Name 028040
CASNO
74-87-3
75-01-4
74-83-9
75-69-4
75-35-4
75-15-0
156-60-5
75-34-3
108-05-4
156-59-2
78-93-3
67 -66-3
71-55-6
i 56-23-5
107-06-2
71-43-2
79-01-6
78-87-5
75-27-4
108-88-3
79-00-5
591-78-6
127-18-4
106-93-4
108-90-7
63Q20-6
Target Analyte Spike Added
CHLOROMETHANE 10
VINYL CHLORIDE 10
BROMOMETHANE 10
TRICHLOROFLUOROMETHANE 10
11-DICHLOROETHENE 10
CARBON DISULFIDE 10
TRANS-12-DICHLOROETHENE 10
11-DICHLOROETHANE 10
VINYL ACETATE 10
CIS-12-DICHLOROETHENE 10
2middotBUTANONE 40
CHLOROFORM 10
111-TRICHL ORO ETHANE 10
CARBON TETRACHLORIDE 10
12-DICHLOROETHANE 10
BENZENE 10
TRICHLOROETHENE 10
12-DICHLOROPROPANE 10
BROMODICHLOROMETHANE 10
TOLUENE 10
112-TRICHLOROETHANE 10
2-HEXANONE 40
TETRACHLOROETHENE 10
12-DIBROMOETHANE 10
CHLOROBENZENE 10
1112-TETRACHLOROETHANE 10
LCS Reporting Result Result Limit Qualifier
932 05
863 05
943 1
908 05
96 05
95 10 J
996 05
992 05
10 10
102 05
412 5
993 05
974 1
943 05
106 05
983 05
962 05
10 05
988 05
974 05
989 05
409 10
956 05
991 1
984 05
101 05
LCS Control Rec Limits
93 49 -129
86 46 134
94 32-121
91 67 -152
96 61 -135
95 61 -140
100 70 -122
99 76 -119
100 62 182
102 75 126
103 61 -137
99 79 120
97 76 - 114
94 58middot135
106 75middot132
98 70 shy 125
96 74 121
100 81 -119
99 79 - 123
97 76 - 120
99 81 -126
102 45 168
96 56 -128
99 79 -123
98 75 -120
101 82 - 123
Data Package 10 VL0911214middot1
-Date Printed Wednesday December 02 2009 ALS Laboratory Group -- Fe Page 1 of 4
LiMS Version 6317A
20
GCMS Volatiles Method SW8260_25B
Laboratory Control Sample and Laboratory Control Sample Duplicate
Lab Name ALS Laboratory Group - FC
Work Order Number 0911214
Client Name New Mexico Envircnment Department OB
ClientProject 10 644-111809(HWB R-37 VOes) PAR 002731703
Lab 10 VL091125-4LCS Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml
Moisture NIA QCBatchlO VL091125-4-5 Final Volume 10 mi
Date Collected NA Run 10 VL091125-4A Result Units UGL Date Extracted 11252009 Cleanup NONE Clean OF 1 Date Analyzed 111252009 Basis NA
Prep Method SW5030e File Name 028040
CASNO Target Analyte Spike Added
LCS Result
Reporting Limit
Result Qualifier
LCS Rec
Control Limits
100-41-4 ETHYLBENZENE 10 981 05 98 79 -114
136777-61-2 M+P-XYLENE 20 197 1 98 81-115
95-47-6 O-XYLENE 10 101 05 101 81 -115
95-49-8 2-CHLOROTOLUENE 10 97 05 97 80 -128
541-73-1 13-DICHLOROBENZiNt 10 977 05 98 81-116
106-46-7 14-DICHLOROBENZENE 10 979 05 98 81 -119
95-50-1 12-DICHLOROBENZENE 10 987 05 99 79 - 116
91-20-3 NAPHTHALENE 10 993 05 99 69 -126
87-61-6 123-TRICHLOROBENZENE 10 999 05 100 60 -137
Data Package ID VL0911214-1
Date Printed Wecnesday December 02 2009 ALS Laboratory Group -- Fe Page 2 of 4
21
GCMS Volatiles Method SW8260_25B
Laboratory Control Sample and Laboratory Control Sample Duplicate
Lab Name ALS Laboratory Group bullbull FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-11 1809(HWB R-37 VOCs) PAR 002731703
Lab 10 VL091125middot4LCSD Sample Matrix WATER
Moisture NIA Prep Batch VL091125-4
QCBatchlD VL091125-4-5
Sample Aliquot
Final Volume
10 ml
10ml Date Collected NIA Run ID VL091125-4A Result Units UGIL Date Extracted 112512009 Cleanup NONE Clean DF 1 Date Analyzed 1112512009 Basis NIA
Prep Method SW5030C File Name 028041
CASNO Target Analyte Spike Added
LCSD Result
Reporting Limit
Result Qualifier
LCSD Rec
RPD Limit
RPD
74-87-3 CHLOROMETHANE 10 897 05 90 30 4
75-01-4 VINYL CHLORIDE 10 831 05 83 25 4
74-83-9 BROMO METHANE 10 945 1 94 25 0
75-69-4 TRICHLOROFLUOROMETHANE 10 873 05 87 22 4
75-35-4 11-DICHLOROETHENE 10 909 05 91 18 5
75-15-0 CARBON DISULFIDE 10 941 10 J 94 20 1
156-60middot5 TRANS-l2middotDICHLOROETHENE 10 961 05 96 25 4
75middot34middot3 11-DICHLOROETHANE 10 977 05 98 25 2
108-05-4 VINYL ACETATE 10 993 10 J 99 20 1
156middot59-2 CIS-12-DlCHLOROETHENE 10 995 05 99 25 3
i 78-93-3 2-BUTANONE 40 419 5 105 30 2
67-66-3 CHLOROFORM 10 985 05 99 25 1
71-55-6 lll-TRICHLOROETHANE 10 942 1 94 25 3
56-23-5 CARBON TETRACHLORIDE 10 922 05 92 25 2
107middot06-2 12middotDICHLOROETHANE 10 106 05 106 25 0
71-43middot2 BENZENE 10 971 05 97 10 1
79middot01middot6 TRICHLOROETHENE 10 939 05 94 10 2
78middot87middot5 l2middotDICHLOROPROPANE 10 101 05 101 25 1
i 75middot27-4 BROMODICHLOROMETHANE 10 992 05 99 25 0
1108-88-3 TOLUENE 10 962 05 96 9 1
I 79005 112middotTRICHLOROETHANE 10 986 05 99 25 0
591middot78middot6 2-HEXANONE 40 418 10 104 20 2
127middot18-4 TETRACHLOROETHENE 10 918 05 92 25 4
106-93-4 12middotDIBROMOETHANE 10 999 1 100 15 1
108middot90-7 CHLOROBENZENE 10 997 05 100 11 1
630-20middot6 1112-TETRACHLOROETHANE 10 101 05 101 15 0
100-41-4 ETHYLBENZENE 10 968 05 97 25 1
Data Package ID VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- FC Page 3 of 4
lIMS Version 6317 A
22
GCMS Volatiles Method SW8260_25B
Laboratory Control Sample and Laboratory Control Sample Duplicate
Lab Name ALS Laboratory 13roup -- FC
Work Order Number 0911214
Client Name New Mexico Environment Department OS
ClientProject 10 644-11 1809(HWB R-37 VOCs) PAR 002731703
Lab 10 VL091125-4LCSD Sample Matrix WATER
Moisture NA Prep Batch VL091125-4
QCBatchlO VL091125-4-5
Sample Aliquot
Final Volume
10 ml
10ml Date Collected NA Run 10 VL091125-4A Result Units UGL Date Extracted 11252009 Cleanup NONE Clean OF Date Analyzed 11252009 Basis NIA
Prep Method SW5030C File Name 028041
CASNO Target Analyte Spike Added
LCSD Result
Reporting Limit
Result Qualifier
LCSD Rec
RPD Limit
RPD
136777-61-2 M+P-XYLENE 20 193 1 97 25 2
95-47-6 O-XYLENE 10 983 05 98 25 2
95-49-8 2middotCHLOROTOLUENE 10 9A9 05 95 15 2
541-73-1 13middotDICHLOROBENZENE 10 997 05 100 25 2
106-46-7 14-DICHLOROBeNZENE 10 974 05 97 25 1
95-50middot1 12middotDICHLOROBENZeNE 10 101 05 101 25 2
91middot20-3 NAPHTHALENe 10 105 05 105 24 6
87-61-6 123-TRICHLOROBENZENE 10 102 05 102 33 3
Surrogate Recovery LCSLCSD
CASNO Target Analyte Spike Added
LCS Rec
LCS Flag
LCSD Rec
LCSD Flag
Control Limits
460middot00-4 4-BROMOFLUOROBeNZENE 25 100 100 82 - 121
1868-53middot7 DIBROMOFLUOROMeTHANE 25 101 100 80middot 123
2037middot26-5 TOLUENEmiddotD8 25 102 100 85middot 116
Data Package 10 VL0911214-
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- Fe Page 4 of 4
UMS Verslmt 6317A
23
GCMS Volatiles Method SW8260_25B
Laboratory Control Sample and Laboratory Control Sample Duplicate
Lab Name ALS Laboratory Group - FC
Work Order Number 0911214
Client Name New Mexico Envircnment Department OB
ClientProject 10 644-111809(HWB R-37 VOes) PAR 002731703
Lab 10 VL091125-4LCS Sample Matrix WATER Prep Batch VL091125-4 Sample Aliquot 10 ml
Moisture NIA QCBatchlO VL091125-4-5 Final Volume 10 mi
Date Collected NA Run 10 VL091125-4A Result Units UGL Date Extracted 11252009 Cleanup NONE Clean OF 1 Date Analyzed 111252009 Basis NA
Prep Method SW5030e File Name 028040
CASNO Target Analyte Spike Added
LCS Result
Reporting Limit
Result Qualifier
LCS Rec
Control Limits
100-41-4 ETHYLBENZENE 10 981 05 98 79 -114
136777-61-2 M+P-XYLENE 20 197 1 98 81-115
95-47-6 O-XYLENE 10 101 05 101 81 -115
95-49-8 2-CHLOROTOLUENE 10 97 05 97 80 -128
541-73-1 13-DICHLOROBENZiNt 10 977 05 98 81-116
106-46-7 14-DICHLOROBENZENE 10 979 05 98 81 -119
95-50-1 12-DICHLOROBENZENE 10 987 05 99 79 - 116
91-20-3 NAPHTHALENE 10 993 05 99 69 -126
87-61-6 123-TRICHLOROBENZENE 10 999 05 100 60 -137
Data Package ID VL0911214-1
Date Printed Wecnesday December 02 2009 ALS Laboratory Group -- Fe Page 2 of 4
21
GCMS Volatiles Method SW8260_25B
Laboratory Control Sample and Laboratory Control Sample Duplicate
Lab Name ALS Laboratory Group bullbull FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-11 1809(HWB R-37 VOCs) PAR 002731703
Lab 10 VL091125middot4LCSD Sample Matrix WATER
Moisture NIA Prep Batch VL091125-4
QCBatchlD VL091125-4-5
Sample Aliquot
Final Volume
10 ml
10ml Date Collected NIA Run ID VL091125-4A Result Units UGIL Date Extracted 112512009 Cleanup NONE Clean DF 1 Date Analyzed 1112512009 Basis NIA
Prep Method SW5030C File Name 028041
CASNO Target Analyte Spike Added
LCSD Result
Reporting Limit
Result Qualifier
LCSD Rec
RPD Limit
RPD
74-87-3 CHLOROMETHANE 10 897 05 90 30 4
75-01-4 VINYL CHLORIDE 10 831 05 83 25 4
74-83-9 BROMO METHANE 10 945 1 94 25 0
75-69-4 TRICHLOROFLUOROMETHANE 10 873 05 87 22 4
75-35-4 11-DICHLOROETHENE 10 909 05 91 18 5
75-15-0 CARBON DISULFIDE 10 941 10 J 94 20 1
156-60middot5 TRANS-l2middotDICHLOROETHENE 10 961 05 96 25 4
75middot34middot3 11-DICHLOROETHANE 10 977 05 98 25 2
108-05-4 VINYL ACETATE 10 993 10 J 99 20 1
156middot59-2 CIS-12-DlCHLOROETHENE 10 995 05 99 25 3
i 78-93-3 2-BUTANONE 40 419 5 105 30 2
67-66-3 CHLOROFORM 10 985 05 99 25 1
71-55-6 lll-TRICHLOROETHANE 10 942 1 94 25 3
56-23-5 CARBON TETRACHLORIDE 10 922 05 92 25 2
107middot06-2 12middotDICHLOROETHANE 10 106 05 106 25 0
71-43middot2 BENZENE 10 971 05 97 10 1
79middot01middot6 TRICHLOROETHENE 10 939 05 94 10 2
78middot87middot5 l2middotDICHLOROPROPANE 10 101 05 101 25 1
i 75middot27-4 BROMODICHLOROMETHANE 10 992 05 99 25 0
1108-88-3 TOLUENE 10 962 05 96 9 1
I 79005 112middotTRICHLOROETHANE 10 986 05 99 25 0
591middot78middot6 2-HEXANONE 40 418 10 104 20 2
127middot18-4 TETRACHLOROETHENE 10 918 05 92 25 4
106-93-4 12middotDIBROMOETHANE 10 999 1 100 15 1
108middot90-7 CHLOROBENZENE 10 997 05 100 11 1
630-20middot6 1112-TETRACHLOROETHANE 10 101 05 101 15 0
100-41-4 ETHYLBENZENE 10 968 05 97 25 1
Data Package ID VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- FC Page 3 of 4
lIMS Version 6317 A
22
GCMS Volatiles Method SW8260_25B
Laboratory Control Sample and Laboratory Control Sample Duplicate
Lab Name ALS Laboratory 13roup -- FC
Work Order Number 0911214
Client Name New Mexico Environment Department OS
ClientProject 10 644-11 1809(HWB R-37 VOCs) PAR 002731703
Lab 10 VL091125-4LCSD Sample Matrix WATER
Moisture NA Prep Batch VL091125-4
QCBatchlO VL091125-4-5
Sample Aliquot
Final Volume
10 ml
10ml Date Collected NA Run 10 VL091125-4A Result Units UGL Date Extracted 11252009 Cleanup NONE Clean OF Date Analyzed 11252009 Basis NIA
Prep Method SW5030C File Name 028041
CASNO Target Analyte Spike Added
LCSD Result
Reporting Limit
Result Qualifier
LCSD Rec
RPD Limit
RPD
136777-61-2 M+P-XYLENE 20 193 1 97 25 2
95-47-6 O-XYLENE 10 983 05 98 25 2
95-49-8 2middotCHLOROTOLUENE 10 9A9 05 95 15 2
541-73-1 13middotDICHLOROBENZENE 10 997 05 100 25 2
106-46-7 14-DICHLOROBeNZENE 10 974 05 97 25 1
95-50middot1 12middotDICHLOROBENZeNE 10 101 05 101 25 2
91middot20-3 NAPHTHALENe 10 105 05 105 24 6
87-61-6 123-TRICHLOROBENZENE 10 102 05 102 33 3
Surrogate Recovery LCSLCSD
CASNO Target Analyte Spike Added
LCS Rec
LCS Flag
LCSD Rec
LCSD Flag
Control Limits
460middot00-4 4-BROMOFLUOROBeNZENE 25 100 100 82 - 121
1868-53middot7 DIBROMOFLUOROMeTHANE 25 101 100 80middot 123
2037middot26-5 TOLUENEmiddotD8 25 102 100 85middot 116
Data Package 10 VL0911214-
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- Fe Page 4 of 4
UMS Verslmt 6317A
23
GCMS Volatiles Method SW8260_25B
Laboratory Control Sample and Laboratory Control Sample Duplicate
Lab Name ALS Laboratory Group bullbull FC
Work Order Number 0911214
Client Name New Mexico Environment Department OB
ClientProject 10 644-11 1809(HWB R-37 VOCs) PAR 002731703
Lab 10 VL091125middot4LCSD Sample Matrix WATER
Moisture NIA Prep Batch VL091125-4
QCBatchlD VL091125-4-5
Sample Aliquot
Final Volume
10 ml
10ml Date Collected NIA Run ID VL091125-4A Result Units UGIL Date Extracted 112512009 Cleanup NONE Clean DF 1 Date Analyzed 1112512009 Basis NIA
Prep Method SW5030C File Name 028041
CASNO Target Analyte Spike Added
LCSD Result
Reporting Limit
Result Qualifier
LCSD Rec
RPD Limit
RPD
74-87-3 CHLOROMETHANE 10 897 05 90 30 4
75-01-4 VINYL CHLORIDE 10 831 05 83 25 4
74-83-9 BROMO METHANE 10 945 1 94 25 0
75-69-4 TRICHLOROFLUOROMETHANE 10 873 05 87 22 4
75-35-4 11-DICHLOROETHENE 10 909 05 91 18 5
75-15-0 CARBON DISULFIDE 10 941 10 J 94 20 1
156-60middot5 TRANS-l2middotDICHLOROETHENE 10 961 05 96 25 4
75middot34middot3 11-DICHLOROETHANE 10 977 05 98 25 2
108-05-4 VINYL ACETATE 10 993 10 J 99 20 1
156middot59-2 CIS-12-DlCHLOROETHENE 10 995 05 99 25 3
i 78-93-3 2-BUTANONE 40 419 5 105 30 2
67-66-3 CHLOROFORM 10 985 05 99 25 1
71-55-6 lll-TRICHLOROETHANE 10 942 1 94 25 3
56-23-5 CARBON TETRACHLORIDE 10 922 05 92 25 2
107middot06-2 12middotDICHLOROETHANE 10 106 05 106 25 0
71-43middot2 BENZENE 10 971 05 97 10 1
79middot01middot6 TRICHLOROETHENE 10 939 05 94 10 2
78middot87middot5 l2middotDICHLOROPROPANE 10 101 05 101 25 1
i 75middot27-4 BROMODICHLOROMETHANE 10 992 05 99 25 0
1108-88-3 TOLUENE 10 962 05 96 9 1
I 79005 112middotTRICHLOROETHANE 10 986 05 99 25 0
591middot78middot6 2-HEXANONE 40 418 10 104 20 2
127middot18-4 TETRACHLOROETHENE 10 918 05 92 25 4
106-93-4 12middotDIBROMOETHANE 10 999 1 100 15 1
108middot90-7 CHLOROBENZENE 10 997 05 100 11 1
630-20middot6 1112-TETRACHLOROETHANE 10 101 05 101 15 0
100-41-4 ETHYLBENZENE 10 968 05 97 25 1
Data Package ID VL0911214-1
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- FC Page 3 of 4
lIMS Version 6317 A
22
GCMS Volatiles Method SW8260_25B
Laboratory Control Sample and Laboratory Control Sample Duplicate
Lab Name ALS Laboratory 13roup -- FC
Work Order Number 0911214
Client Name New Mexico Environment Department OS
ClientProject 10 644-11 1809(HWB R-37 VOCs) PAR 002731703
Lab 10 VL091125-4LCSD Sample Matrix WATER
Moisture NA Prep Batch VL091125-4
QCBatchlO VL091125-4-5
Sample Aliquot
Final Volume
10 ml
10ml Date Collected NA Run 10 VL091125-4A Result Units UGL Date Extracted 11252009 Cleanup NONE Clean OF Date Analyzed 11252009 Basis NIA
Prep Method SW5030C File Name 028041
CASNO Target Analyte Spike Added
LCSD Result
Reporting Limit
Result Qualifier
LCSD Rec
RPD Limit
RPD
136777-61-2 M+P-XYLENE 20 193 1 97 25 2
95-47-6 O-XYLENE 10 983 05 98 25 2
95-49-8 2middotCHLOROTOLUENE 10 9A9 05 95 15 2
541-73-1 13middotDICHLOROBENZENE 10 997 05 100 25 2
106-46-7 14-DICHLOROBeNZENE 10 974 05 97 25 1
95-50middot1 12middotDICHLOROBENZeNE 10 101 05 101 25 2
91middot20-3 NAPHTHALENe 10 105 05 105 24 6
87-61-6 123-TRICHLOROBENZENE 10 102 05 102 33 3
Surrogate Recovery LCSLCSD
CASNO Target Analyte Spike Added
LCS Rec
LCS Flag
LCSD Rec
LCSD Flag
Control Limits
460middot00-4 4-BROMOFLUOROBeNZENE 25 100 100 82 - 121
1868-53middot7 DIBROMOFLUOROMeTHANE 25 101 100 80middot 123
2037middot26-5 TOLUENEmiddotD8 25 102 100 85middot 116
Data Package 10 VL0911214-
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- Fe Page 4 of 4
UMS Verslmt 6317A
23
GCMS Volatiles Method SW8260_25B
Laboratory Control Sample and Laboratory Control Sample Duplicate
Lab Name ALS Laboratory 13roup -- FC
Work Order Number 0911214
Client Name New Mexico Environment Department OS
ClientProject 10 644-11 1809(HWB R-37 VOCs) PAR 002731703
Lab 10 VL091125-4LCSD Sample Matrix WATER
Moisture NA Prep Batch VL091125-4
QCBatchlO VL091125-4-5
Sample Aliquot
Final Volume
10 ml
10ml Date Collected NA Run 10 VL091125-4A Result Units UGL Date Extracted 11252009 Cleanup NONE Clean OF Date Analyzed 11252009 Basis NIA
Prep Method SW5030C File Name 028041
CASNO Target Analyte Spike Added
LCSD Result
Reporting Limit
Result Qualifier
LCSD Rec
RPD Limit
RPD
136777-61-2 M+P-XYLENE 20 193 1 97 25 2
95-47-6 O-XYLENE 10 983 05 98 25 2
95-49-8 2middotCHLOROTOLUENE 10 9A9 05 95 15 2
541-73-1 13middotDICHLOROBENZENE 10 997 05 100 25 2
106-46-7 14-DICHLOROBeNZENE 10 974 05 97 25 1
95-50middot1 12middotDICHLOROBENZeNE 10 101 05 101 25 2
91middot20-3 NAPHTHALENe 10 105 05 105 24 6
87-61-6 123-TRICHLOROBENZENE 10 102 05 102 33 3
Surrogate Recovery LCSLCSD
CASNO Target Analyte Spike Added
LCS Rec
LCS Flag
LCSD Rec
LCSD Flag
Control Limits
460middot00-4 4-BROMOFLUOROBeNZENE 25 100 100 82 - 121
1868-53middot7 DIBROMOFLUOROMeTHANE 25 101 100 80middot 123
2037middot26-5 TOLUENEmiddotD8 25 102 100 85middot 116
Data Package 10 VL0911214-
Date Printed Wednesday December 02 2009 ALS Laboratory Group -- Fe Page 4 of 4
UMS Verslmt 6317A
23