additional materials available on the hei … appendix i... · additional materials available on...

ADDITIONAL MATERIALS AVAILABLE ON THE HEI WEB SITE

Research Report 184

Advanced Collaborative Emissions Study (ACES): Lifetime Cancer and Non-Cancer Assessment in Rats Exposed to New-Technology Diesel

Exhaust

Part 1. Assessment of Carcinogenicity and Biologic Responses in Rats after Lifetime Inhalation of New-Technology Diesel Exhaust in the ACES Bioassay

Appendix I.

Characterization of Exposure Atmospheres in the ACES Bioassay

McDonald et al.

Additional Materials I.D. Fuel and Oil Analyses

Additional Materials may appear in a different order from that in the original Investigators’ Report, and

some remnants of their original names may be apparent.

Additional Materials I.D was originally Appendices B and C.

The HEI Exposure Characterization Panel reviewed the draft of this appendix but not the final version. This appendix did not undergo the HEI scientific editing and production process but was proofread for spelling and

grammar only.

Correspondence may be addressed to Dr. Jacob D. McDonald, Lovelace Respiratory Research Institute, 2425

Ridgecrest Dr., SE, Albuquerque, NM 87108; e-mail: [email protected].

Although this document was produced with partial funding by the United States Department of Energy (DOE), under the terms of Contract/Award Number DE-AC26-05NT42429, and certain motor vehicle and engine

manufacturers, the opinion expressed herein are those of the authors and do not necessarily reflect the views of the DOE or motor vehicle and engine manufacturers.

© 2015 Health Effects Institute, 101 Federal Street, Suite 500, Boston, MA 02110-1817

ACES: Phase 3B: Characterization of Exposure Atmospheres

68

Appendix B

Fuel Analysis

Michael Clearwater

2425 Ridgecrest Drive, SEAlbuquerque NM 87108

03/11/10

LOVEMC

V7000244A

Description :Sample ID: 19FEB10-F409-111, Diesel Fuel

JLMAMSP.O. Number :

Test Performed Proc-Rev Result

Page 1

Client Code :

Certificate of AnalysisLab Number

Sample Date : 02/19/10

Lovelace Respiratory Research Institute

Herguth ID : LABV7000244

Oil Type : Diesel Fuel (GN_130)Serial#: 1802741 09744

Unit Type : Diesel Fuel (GN_DF001)

Distillation of Petroleum ASTM D86 . . . . . . . . . . . . . . . . . . . . . . . 0086-2.6Observed Barometric Pressure . . . . . . . . . . . . . . . . . . . . . . . . . . . . 757 mm HgAll results are corrected to 760 mm Hg . . . . . . . . . . . . . . . . . . . . . .Initial Boiling Point . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 315 Deg. F5% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 369 Deg. F10% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 388 Deg. F15% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 402 Deg. F20% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 414 Deg. F30% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 434 Deg. F40% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 458 Deg. F50% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 483 Deg. F60% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 509 Deg. F70% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 538 Deg. F80% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 571 Deg. F85% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 590 Deg. F90% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 614 Deg. F95% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 648 Deg. FEnd Point . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 660 Deg. FRecovery . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 97.0 % vol.Sulfur, X-Ray Fluorescence ASTM D4294 . . . . . . . . . . . . . . . . . . 4294-2.8 <0.0020 % WtCetane Index ASTM D976 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 0976-1.3 49.0API Gravity @ 60 Deg F ASTM D287 . . . . . . . . . . . . . . . . . . . . . 0287-2.1 38.2 Deg. APIHydrocarbon Types by FIA ASTM D1319 . . . . . . . . . . . . . . . . . . . 1319-1.0Aromatics . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 25.2 % volOlefins . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2.0 % volSaturates . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 72.8 % vol

101 Corporate Place, Vallejo, CA 94590-6968 * Toll-Free Phone 1-800-645-5227 * Fax 1-707-554-0109 * www.herguth.com

These results are submitted pursuant to our current Terms, Conditions and Limitations and Laboratory Pricing Policy. No responsibility or liability is assumed for the manner in which these results are used or interpreted.

erlabcs.frx Rev. 03/26/07ISO 9001:2000 Certified


69

Michael Clearwater


03/11/10

LOVEMC

V7000244A


JLMAMSP.O. Number :


Page 2

Client Code :




Herguth ID :



Sulfur by Microcoulometry ASTM D3120 . . . . . . . . . . . . . . . . . . . 3120-3.0 5 mg/kg

Michael Clearwater

REVISED REPORT supersedes lab # V7000244 and includes sulfur by D3120 result.Result(s) meet the specifications of ASTM D975 for S15 No. 2 Diesel Fuel for the test(s) performed.Hydrocarbon Types by FIA was subbed out.

Respectfully Submitted,Herguth Laboratories, Inc.

Bobby R Licu, Senior Evaluatorcc:





70

Michael Clearwater


03/11/10

LOVEMC

V7000244A


JLMAMSP.O. Number :


Page 1

Client Code :







Distillation of Petroleum ASTM D86 . . . . . . . . . . . . . . . . . . . . . . . 0086-2.6Observed Barometric Pressure . . . . . . . . . . . . . . . . . . . . . . . . . . . . 757 mm HgAll results are corrected to 760 mm Hg . . . . . . . . . . . . . . . . . . . . . .Initial Boiling Point . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 315 Deg. F5% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 369 Deg. F10% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 388 Deg. F15% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 402 Deg. F20% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 414 Deg. F30% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 434 Deg. F40% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 458 Deg. F50% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 483 Deg. F60% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 509 Deg. F70% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 538 Deg. F80% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 571 Deg. F85% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 590 Deg. F90% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 614 Deg. F95% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 648 Deg. FEnd Point . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 660 Deg. FRecovery . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 97.0 % vol.Sulfur, X-Ray Fluorescence ASTM D4294 . . . . . . . . . . . . . . . . . . 4294-2.8 <0.0020 % WtCetane Index ASTM D976 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 0976-1.3 49.0API Gravity @ 60 Deg F ASTM D287 . . . . . . . . . . . . . . . . . . . . . 0287-2.1 38.2 Deg. APIHydrocarbon Types by FIA ASTM D1319 . . . . . . . . . . . . . . . . . . . 1319-1.0Aromatics . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 25.2 % volOlefins . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2.0 % volSaturates . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 72.8 % vol





71

Michael Clearwater


03/11/10

LOVEMC

V7000244A


JLMAMSP.O. Number :


Page 2

Client Code :




Herguth ID :



Sulfur by Microcoulometry ASTM D3120 . . . . . . . . . . . . . . . . . . . 3120-3.0 5 mg/kg

Michael Clearwater

REVISED REPORT supersedes lab # V7000244 and includes sulfur by D3120 result.Result(s) meet the specifications of ASTM D975 for S15 No. 2 Diesel Fuel for the test(s) performed.Hydrocarbon Types by FIA was subbed out.







72

Tom Holmes


04/26/10

LOVEMC

V7000633

Description :Serial# F409-111-14APR10, Clear Diesel

JLMDEMP.O. Number :


Page 1

Client Code :





Oil Type : Diesel Fuel (GN_130)Unit Type : Diesel Fuel (GN_DF001)

Distillation of Petroleum ASTM D86 . . . . . . . . . . . . . . . . . . . . . . . 0086-2.6Observed Barometric Pressure . . . . . . . . . . . . . . . . . . . . . . . . . . . . 754 mm HgAll results are corrected to 760 mm Hg . . . . . . . . . . . . . . . . . . . . . .Initial Boiling Point . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 343 Deg. F5% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 381 Deg. F10% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 398 Deg. F15% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 413 Deg. F20% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 427 Deg. F30% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 452 Deg. F40% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 478 Deg. F50% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 504 Deg. F60% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 530 Deg. F70% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 559 Deg. F80% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 593 Deg. F85% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 614 Deg. F90% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 639 Deg. F95% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 680 Deg. FEnd Point . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 689 Deg. FRecovery . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 96.9 % vol.Cetane Index ASTM D976 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 0976-1.3 51.0API Gravity @ 60 Deg F ASTM D287 . . . . . . . . . . . . . . . . . . . . . 0287-2.1 37.0 Deg. APIHydrocarbon Types by FIA ASTM D1319 . . . . . . . . . . . . . . . . . . . 1319-1.0Aromatics . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 28.1 % volOlefins . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1.1 % volSaturates . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 70.8 % volSulfur, X-Ray Fluorescence ASTM D4294 . . . . . . . . . . . . . . . . . . 4294-2.8 <0.0020 % Wt





73

Tom Holmes


04/26/10

LOVEMC

V7000633


JLMDEMP.O. Number :


Page 2

Client Code :




Herguth ID :

Tom Holmes

Result(s) meet the specifications of ASTM D975 for No. 2 Diesel Fuel for the test(s) performed.Hydrocarbon Types by FIA was subbed out.







74

Tom Holmes


04/30/10

LOVEMC

V7000633A


JLMDEMP.O. Number :


Page 1

Client Code :






Distillation of Petroleum ASTM D86 . . . . . . . . . . . . . . . . . . . . . . . 0086-2.6Observed Barometric Pressure . . . . . . . . . . . . . . . . . . . . . . . . . . . . 754 mm HgAll results are corrected to 760 mm Hg . . . . . . . . . . . . . . . . . . . . . .Initial Boiling Point . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 343 Deg. F5% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 381 Deg. F10% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 398 Deg. F15% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 413 Deg. F20% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 427 Deg. F30% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 452 Deg. F40% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 478 Deg. F50% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 504 Deg. F60% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 530 Deg. F70% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 559 Deg. F80% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 593 Deg. F85% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 614 Deg. F90% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 639 Deg. F95% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 680 Deg. FEnd Point . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 689 Deg. FRecovery . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 96.9 % vol.Cetane Index ASTM D976 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 0976-1.3 51.0API Gravity @ 60 Deg F ASTM D287 . . . . . . . . . . . . . . . . . . . . . 0287-2.1 37.0 Deg. APIHydrocarbon Types by FIA ASTM D1319 . . . . . . . . . . . . . . . . . . . 1319-1.0Aromatics . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 28.1 % volOlefins . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1.1 % volSaturates . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 70.8 % volSulfur by Microcoulometry ASTM D3120 . . . . . . . . . . . . . . . . . . . 3120-3.0 5 ppm





75

Tom Holmes


04/30/10

LOVEMC

V7000633A


JLMDEMP.O. Number :


Page 2

Client Code :




Herguth ID :

Tom Holmes

REVISED REPORT supersedes lab # V7000633 and includes updated sulfur test.Result(s) meet the specifications of ASTM D975 for S15 No. 2 Diesel Fuel for the test(s) performed.Hydrocarbon Types by FIA was subbed out.







76

Tom Holmes


06/22/10

LOVEMC

V7001241

Description :Sample ID: FY09-111-08JUN10-Fuel, Chevron #2 Clear Diesel

JK101621P.O. Number :


Page 1

Client Code :





Oil Type : Diesel Fuel (GN_130)Label States: Total Engine Hours: 2586





erlabcs.frx Rev. 06/21/2010ISO 9001:2008 and ISO/IEC 17025:2005 Certified


77

Tom Holmes


06/22/10

LOVEMC

V7001241

Description :Sample ID: FY09-111-08JUN10-Fuel, Chevron #2 Clear Diesel



Page 2

Client Code :




Herguth ID :

Label States: Total Engine Hours: 2586

Tom Holmes

Result(s) meet the specifications of ASTM D975 for S15 No. 2 Diesel Fuel for the test(s) performed.Hydrocarbon Types by FIA was subbed out.







78

Tom Holmes


08/16/10

LOVEMC

V7001845

Description :Sample ID: FY09-111-30JUL10-Fuel, Chevron #2 Clear Diesel



Page 1

Client Code :





Oil Type : Diesel Fuel (GN_130)Project# FY09-111 ACES, Acct/Org/Project: JLMEPR







79

Tom Holmes


08/16/10

LOVEMC

V7001845

Description :Sample ID: FY09-111-30JUL10-Fuel, Chevron #2 Clear Diesel



Page 2

Client Code :




Herguth ID :

Project# FY09-111 ACES, Acct/Org/Project: JLMEPR

Tom Holmes








80

Tom Holmes


10/14/10

LOVEMC

V7002326

Description :Sample ID: FY09-111-01OCT10, Chevron #2 Clear Diesel Fuel

FY09-111 ACESP.O. Number :


Page 1

Client Code :






Distillation of Petroleum ASTM D86 . . . . . . . . . . . . . . . . . . . . . . . 0086-2.6Observed Barometric Pressure . . . . . . . . . . . . . . . . . . . . . . . . . . . . 762 mm HgAll results are corrected to 760 mm Hg . . . . . . . . . . . . . . . . . . . . . .Initial Boiling Point . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 340 Deg. F5% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 379 Deg. F10% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 398 Deg. F15% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 411 Deg. F20% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 422 Deg. F30% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 445 Deg. F40% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 468 Deg. F50% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 492 Deg. F60% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 518 Deg. F70% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 550 Deg. F80% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 588 Deg. F85% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 611 Deg. F90% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 641 Deg. F95% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . DNR Deg. FEnd Point . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 686 Deg. FRecovery . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 95.8 % vol.Cetane Index ASTM D976 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 0976-1.3 48.5API Gravity @ 60 Deg F ASTM D287 . . . . . . . . . . . . . . . . . . . . . 0287-2.1 37.3 Deg. APIHydrocarbon Types by FIA ASTM D1319 . . . . . . . . . . . . . . . . . . . 1319-1.0Aromatics . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 33.6 % volOlefins . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1.1 % volSaturates . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 65.3 % volSulfur by Microcoulometry ASTM D3120 . . . . . . . . . . . . . . . . . . . 3120-3.1 3 ppm





81

Tom Holmes


10/14/10

LOVEMC

V7002326

Description :Sample ID: FY09-111-01OCT10, Chevron #2 Clear Diesel Fuel



Page 2

Client Code :




Herguth ID :

Tom Holmes

Result does not meet the specifications of ASTM D975 for S15 No. 2 Diesel Fuel for the test(s) performed.Distillation at 90% exceeds maximum (640°F). Testing could not be completed due to sample condition.Value(s) have been rechecked and verified.Hydrocarbon Types by FIA was subbed out.







82

Tom Holmes


12/09/10

LOVEMC

V7003059

Description :Sample: FY09-111-24nov10-fuel, Chevon #2 Clear Diesel Fuel



Page 1

Client Code :












83

Tom Holmes


12/09/10

LOVEMC

V7003059

Description :Sample: FY09-111-24nov10-fuel, Chevon #2 Clear Diesel Fuel



Page 2

Client Code :




Herguth ID :


Tom Holmes








84

Tom Holmes


01/28/11

LOVEMC

V7003451

Description :Sample ID: FY09-111-17Jan11-Fuel



Page 1

Client Code :





Oil Type : Diesel Fuel (GN_130)

Total Engine Hours: 5082, Paperwork States: Sample Description: Chevron #2 Clear Diesel Fuel,Project/PO#: FY09-111 ACES


Distillation of Petroleum ASTM D86 . . . . . . . . . . . . . . . . . . . . . . . 0086-2.6Observed Barometric Pressure . . . . . . . . . . . . . . . . . . . . . . . . . . . . 764 mm HgAll results are corrected to 760 mm Hg . . . . . . . . . . . . . . . . . . . . . .Initial Boiling Point . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 331 Deg. F5% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 361 Deg. F10% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 375 Deg. F15% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 386 Deg. F20% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 399 Deg. F30% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 422 Deg. F40% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 445 Deg. F50% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 471 Deg. F60% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 500 Deg. F70% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 530 Deg. F80% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 566 Deg. F85% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 586 Deg. F90% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 610 Deg. F95% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 646 Deg. FEnd Point . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 659 Deg. FRecovery . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 97.5 % vol.Cetane Index ASTM D976 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 0976-1.3 46.5API Gravity @ 60 Deg F ASTM D287 . . . . . . . . . . . . . . . . . . . . . 0287-2.1 38.4 Deg. APIHydrocarbon Types by FIA ASTM D1319 . . . . . . . . . . . . . . . . . . . 1319-1.0Aromatics . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 28.0 % volOlefins . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2.3 % volSaturates . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 69.7 % vol





85

Tom Holmes


01/28/11

LOVEMC

V7003451




Page 2

Client Code :




Herguth ID :




Sulfur, X-Ray Fluorescence ASTM D4294 . . . . . . . . . . . . . . . . . . 4294-2.8 <0.0020 % Wt

Tom Holmes








86

Tom Holmes


02/10/11

LOVEMC

V7003451A




Page 1

Client Code :








Distillation of Petroleum ASTM D86 . . . . . . . . . . . . . . . . . . . . . . . 0086-2.6Observed Barometric Pressure . . . . . . . . . . . . . . . . . . . . . . . . . . . . 764 mm HgAll results are corrected to 760 mm Hg . . . . . . . . . . . . . . . . . . . . . .Initial Boiling Point . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 331 Deg. F5% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 361 Deg. F10% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 375 Deg. F15% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 386 Deg. F20% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 399 Deg. F30% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 422 Deg. F40% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 445 Deg. F50% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 471 Deg. F60% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 500 Deg. F70% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 530 Deg. F80% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 566 Deg. F85% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 586 Deg. F90% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 610 Deg. F95% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 646 Deg. FEnd Point . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 659 Deg. FRecovery . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 97.5 % vol.Cetane Index ASTM D976 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 0976-1.3 46.5API Gravity @ 60 Deg F ASTM D287 . . . . . . . . . . . . . . . . . . . . . 0287-2.1 38.4 Deg. APIHydrocarbon Types by FIA ASTM D1319 . . . . . . . . . . . . . . . . . . . 1319-1.0Aromatics . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 28.0 % volOlefins . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2.3 % volSaturates . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 69.7 % vol





87

Tom Holmes


02/10/11

LOVEMC

V7003451A




Page 2

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Herguth ID :




Sulfur by Microcoulometry ASTM D3120 . . . . . . . . . . . . . . . . . . . 3120-3.1 3 ppm

Tom Holmes

REVISED REPORT supersedes lab # V7003451 and includes updated sulfur result.Result(s) meet the specifications of ASTM D975 for No. 2 Diesel Fuel for the test(s) performed.Hydrocarbon Types by FIA was subbed out.







88

101 CORPORATE PLACE, VALLEJO, CA 94590-6968 (707) 554-4611 (800) 645-5227 Fax (707) 554-0109

www.herguth.com

Tom Holmes Quotation No. 204887 (LOVEMC) Lovelace Respiratory Research Institute Quotation Date: February 1, 2011 2425 Ridgecrest Drive, SE Albuquerque, NM 87108 Email: [email protected] Phone: (505) 348-9600 Fax: (505) 348-4980

QUOTATION

Item Qty Description/Analysis Methodology Fee Extend ________________________________________________________________________________

1 1 Fuels 353.85 353.85 Volume of sample required: 631 ml

Distillation of Petroleum Product (FUELS) ASTM D86 Cetane Index (Calculation Only) (FUELS) ASTM D976 Gravity, API (Hydrometer Method) (FUELS) ASTM D287 *Hydrocarbon Types by Fluorescent (FUELS) ASTM D1319 Sulfur by Microcoul. (FUELS) ASTM D3120 Turnaround time is 7-10 working day(s) from receipt of sample.

QUOTATION TOTAL 353.85 each

*Test are subcontracted to another facility and should be completed between 7-10 working days

Thank you for the opportunity to provide you with the above quotation for your samples. The above quotation is based on your requested scope of work and/or our recommended analytical methods for your sample type. However, prices are subject to change based on the actual sample type as determined upon receipt. Reference oils are required for baseline data.

Our standard turn around time is four (4) working days. Rush charges are double above prices for 48-hour turn around and triple for 24-hour. Any analysis that is subcontracted to another facility (lab) will be processed within 7-10 working days depending on the test. Samples arriving in large batches may have longer turn around times based on testing and oil types. This quotation is valid for 90 days. Please refer to quotation number when submitting samples. All ASTM methods will be performed at the latest published revision.

Reports can be transmitted via email upon completion at no additional charge. We also have Internet access-iLAMP available for an additional $300/ year that will allow you to retrieve your data, view and print reports, set up units and route list, print labels, etc. Please contact Customer Service to order iLAMP.

A credit application or payment is required with all new accounts. Please fax one to 707-554-0109. Credit will be extended based on the reference verification. The sample turn around time may be longer based on credit reference responses.

Laboratory Pricing Policy

1. Hours of Operation And Normal Availability Regular laboratory hours are 8:00 AM to 5:00 PM Monday through Friday. For condition monitoring analyses, our normal turnaround is 48 hours (two working days). For all other analyses, our normal turnaround is 96 hours (four working days). Any analysis that is subcontracted to another facility


89


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(lab) will be processed within 7-10 working days depending on the test. Please note there may be delays in turn around times based on account setup and credit references.

2. Minimum Invoice Charges, Rush Analyses and Overtime Rates A minimum fee of $25.00 may be charged for any analysis invoice. For Condition Monitoring analyses, "RUSH" samples results are available within 24 hours (or less) and are charged at three times the normal analyses rate. For other analyses there are two "RUSH" provisions for work performed during our regular laboratory hours: a) 48 hour (2 working day) analysis time is charged at twice the normal analysis fee. b) 24 hour (one working day) turnaround, or less, is charged at three times the normal analysis fee. There are some analyses that cannot be completed in less than 24 hours; however, they can be moved ahead of the scheduled samples waiting for that analysis. These analyses will be charged at the 24 hour rush rate. Laboratory work performed during other hours, including Saturday, Sunday or recognized Holidays may be charged at triple our normal analyses rates, an hourly rate with a four (4) hour minimum charge, or $1,500, whichever is greater. Nuclear Quality Assured (10 CFR 50 Appendix B) or radioactive samples analyzed during periods other than normal hours will be charged a minimum of $2,500.

3. Quality Assurance Program And Surveillance Analyses performed under the Safety Related Part 21 Program are charged at 1.35 times the applicable fee. Surveillance of work performed at Herguth Laboratories, Inc. by client representatives may be charged at three times the applicable fee. All ASTM methods are performed at the latest published revision.

4. Radioactive Materials Analyses on radioactive samples will be assessed a surcharge of 1.5 times the analysis fee or a fee of $125 per sample (Condition Monitoring Rads), as specifically quoted to the customer. Radioactive lubricant samples are properly disposed of by Herguth provided the sample meets our disposal criteria. This service is not applicable for non-liquid lubricant samples, which must be returned to the client.

5. Sample Pick-Up And Delivery Sample pick-up and delivery during normal working hours may be charged at a minimum of $25 within a 25 mile radius. The fee will be $50 within a radius of 50 miles. Sample pick-up during non-working hours may be charged a minimum of $100 plus expenses. This applies to the nine (9) San Francisco Bay Area counties. Special arrangements must be made for custody transfers and pick-ups outside of this area.

6. Sample Retention and Disposal Samples will be held for a minimum of 30 days. Long term retention services are available by special request. Non-hydrocarbon samples, "unknown" samples, and samples containing elements or constituents which cannot be accommodated by our normal waste streams will either be returned, or if requested, disposed of properly. Handling and disposal surcharges may be assessed. Samples can be returned to the client if requested.

Terms, Conditions, and Limitations

All services rendered by Herguth Laboratories, Inc. are undertaken, and all rates are based upon the following terms:

(a) Neither Herguth Laboratories, Inc., nor any of its employees, agents or sub-contractors shall be liable for any loss or damage arising out of Herguth Laboratories, Inc.'s. performance or non-performance, whether by way of negligence or breach of contract, or otherwise, in any amount greater than twice the amount billed to the customer for the work leading to the claim of the customer. Said remedy shall be the sole and exclusive remedy against Herguth Laboratories, Inc. arising out of its work.


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(b) All claims must be in writing within forty-five (45) days after delivery of the Herguth Laboratories, Inc. report regarding said work, or such claim shall be deemed as irrevocably waived.

(c) Herguth Laboratories, Inc. reports are submitted in writing and are for our customers only. Our customers are considered to be only those entities being billed for our services. Acquisition of a Herguth Laboratories, Inc. report by other than our customer does not constitute a representation of Herguth Laboratories, Inc. as to the accuracy of the contents thereof.

(d) In no event shall Herguth Laboratories, Inc., its employees, agents or sub-contractors be responsible for consequential or special damages of any kind or in any amount.

(e) No deviation from the terms set forth herein shall bind Herguth Laboratories, Inc. unless explicitly agreed upon and accepted contractually, or unless explicitly expressed in writing and signed by a Corporate Officer of Herguth Laboratories, Inc.

(f) Depending on specific customer requirements and/or changes in operations, Herguth Laboratories, Inc. reserves the right to change the pricing and availability of analyses as published in price list(s).

(g) All ASTM methods are performed at the latest published revision.

Should you have any questions regarding this quote, please contact myself at 800-645-5227 ext. 3012. We look forward to working with you on this and future projects. Please refer to this quotation number when submitting samples.

Please visit our website for additional services and capabilities www.herguth.com.

_______________________________________ Linda Perry Sales & Marketing


91

Tom Holmes


03/28/11

LOVEMC

V7004199

Description :Sample: FY09-111-15mar11-fuel, Chevron #2 Clear Diesel Fuel



Page 1

Client Code :






Distillation of Petroleum ASTM D86 . . . . . . . . . . . . . . . . . . . . . . . 0086-2.6Observed Barometric Pressure . . . . . . . . . . . . . . . . . . . . . . . . . . . . 755 mm HgAll results are corrected to 760 mm Hg . . . . . . . . . . . . . . . . . . . . . .Initial Boiling Point . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 337 Deg. F5% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 366 Deg. F10% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 382 Deg. F15% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 394 Deg. F20% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 405 Deg. F30% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 427 Deg. F40% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 452 Deg. F50% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 478 Deg. F60% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 505 Deg. F70% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 535 Deg. F80% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 570 Deg. F85% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 590 Deg. F90% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 615 Deg. F95% . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 651 Deg. FEnd Point . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 664 Deg. FRecovery . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 97.1 % vol.Cetane Index ASTM D976 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 0976-1.3 47.0API Gravity @ 60 Deg F ASTM D287 . . . . . . . . . . . . . . . . . . . . . 0287-2.1 37.6 Deg. APIHydrocarbon Types by FIA ASTM D1319 . . . . . . . . . . . . . . . . . . . 1319-1.0Aromatics . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 27.9 % volOlefins . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3.0 % volSaturates . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 69.1 % volSulfur by Microcoulometry ASTM D3120 . . . . . . . . . . . . . . . . . . . 3120-3.1 5 mg/kg





92

Tom Holmes


03/28/11

LOVEMC

V7004199

Description :Sample: FY09-111-15mar11-fuel, Chevron #2 Clear Diesel Fuel



Page 2

Client Code :




Herguth ID :

Tom Holmes








93

Tom Holmes


05/20/11

LOVEMC

V7004725

Description :Sample ID: FY09-111-10may-11fuel, Diesel Fuel



Page 1

Client Code :





Oil Type : Diesel Fuel (GN_130)Chevron #2 Clear Diesel Fuel, Label States: Total Engine Hours: 6351







94

Tom Holmes


05/20/11

LOVEMC

V7004725

Description :Sample ID: FY09-111-10may-11fuel, Diesel Fuel



Page 2

Client Code :





Chevron #2 Clear Diesel Fuel, Label States: Total Engine Hours: 6351

Tom Holmes








95

Tom Holmes


07/21/11

LOVEMC

V7005385

Description :Sample ID: FY09-111-07Jul11-Fuel, Diesel Fuel



Page 1

Client Code :





Oil Type : Diesel Fuel (GN_130)Chevron #2 Clear Diesel Fuel







96

Tom Holmes


07/21/11

LOVEMC

V7005385

Description :Sample ID: FY09-111-07Jul11-Fuel, Diesel Fuel



Page 2

Client Code :





Chevron #2 Clear Diesel Fuel

Tom Holmes








97

Tom Holmes


09/21/11

LOVEMC

V7006238

Description :Sample: FY09-111-06SEP11-Fuel, Chevron #2 Clear Diesel Fuel



Page 1

Client Code :











98

Tom Holmes


09/21/11

LOVEMC

V7006238

Description :Sample: FY09-111-06SEP11-Fuel, Chevron #2 Clear Diesel Fuel



Page 2

Client Code :





Tom Holmes

Result(s) meet the specifications of ASTM D975 for S15 No. 2 Diesel Fuel for the test(s) performed, noting visibledebris was present in sample.Hydrocarbon Types by FIA was subbed out.







99

Tom Holmes


11/22/11

LOVEMC

V7006931

Description :FY09-111-07NOV11-Fuel, Chevron #2 Clear Diesel Fuel



Page 1

Client Code :











100

Tom Holmes


11/22/11

LOVEMC

V7006931




Page 2

Client Code :





Tom Holmes








101

Tom Holmes


12/29/11

LOVEMC

V7007282

Description :FY09-111-13DEC11-FUEL, Chevron #2 Clear Diesel Fuel



Page 1

Client Code :











102

Tom Holmes


12/29/11

LOVEMC

V7007282

Description :FY09-111-13DEC11-FUEL, Chevron #2 Clear Diesel Fuel



Page 2

Client Code :





Tom Holmes








103

Tom Holmes


02/13/12

LOVEMC

V7007704

Description :FY09-111-30JAN2012-Fuel, Chevron #2 Clear Diesel Fuel



Page 1

Client Code :











104

Tom Holmes


02/13/12

LOVEMC

V7007704

Description :FY09-111-30JAN2012-Fuel, Chevron #2 Clear Diesel Fuel



Page 2

Client Code :





Tom Holmes








105

Tom Holmes


04/12/12

LOVEMC

V7008264

Description :Sample ID: FY09-111-29MAR2012, Chevron #2 Clear Diesel Fuel



Page 1

Client Code :












106

Tom Holmes


04/12/12

LOVEMC

V7008264

Description :Sample ID: FY09-111-29MAR2012, Chevron #2 Clear Diesel Fuel



Page 2

Client Code :






Tom Holmes








107

Tom Holmes


06/15/12

LOVEMC

V7008917

Description :Sample ID: FY09-111-29MAY2012, Chevron #2 Clear Diesel Fuel



Page 1

Client Code :











108

Tom Holmes


06/15/12

LOVEMC

V7008917

Description :Sample ID: FY09-111-29MAY2012, Chevron #2 Clear Diesel Fuel



Page 2

Client Code :





Tom Holmes



Mindy L. Villalba, Project Managercc:





109

Tom Holmes


08/23/12

LOVEMC

V7010055

Description :Sample ID: FY09-111-02Aug2012, Chevron #2 Clear Diesel Fuel



Page 1

Client Code :











110

Tom Holmes


08/23/12

LOVEMC

V7010055

Description :Sample ID: FY09-111-02Aug2012, Chevron #2 Clear Diesel Fuel



Page 2

Client Code :





Tom Holmes








111

Tom Holmes


10/11/12

LOVEMC

V7010749

Description :Sample ID: FY09-111-25Sep2012, Chevron #2 Clear Diesel Fuel



Page 1

Client Code :





Oil Type : Diesel Fuel (GN_130)Unit Type : Diesel Fuel (GN_DF001) UnitTime : 1262






112

Tom Holmes


10/11/12

LOVEMC

V7010749

Description :Sample ID: FY09-111-25Sep2012, Chevron #2 Clear Diesel Fuel



Page 2

Client Code :





Tom Holmes








113


114

Tom Holmes


12/05/12

LOVEMC

V7011835




Page 1

Client Code :











115

Tom Holmes


12/05/12

LOVEMC

V7011835




Page 2

Client Code :





Tom Holmes

Result(s) meet the specifications of ASTM D975 for S15 No. 2 Diesel Fuel for the test(s) performed. Noting,Aromatic level exceeds the maximum of 35 % vol. and Cetane Index is > 40.Hydrocarbon Types by FIA was subbed out.







116

Tom Holmes


12/19/12

LOVEMC

V7011835A




Page 1

Client Code :











117

Tom Holmes


12/19/12

LOVEMC

V7011835A




Page 2

Client Code :





Tom Holmes

REVISED REPORT supersedes lab # V7011835 and includes updated D1319 results.Result(s) meet the specifications of ASTM D975 for S15 No. 2 Diesel Fuel for the test(s) performed.Hydrocarbon Types by FIA was subbed out.







118


119

Appendix C.

Oil Analysis


www.herguth.com

Tom Holmes Quotation No. 204505 (LOVEMC) Lovelace Respiratory Research Institute Quotation Date: July 29, 2010 2425 Ridgecrest Drive, SE Albuquerque, NM 87108 Email: [email protected] Phone: (505) 348-9600 Fax: (505) 348-4980 QUOTATION Item Qty Description/Analysis Methodology Fee Extend ________________________________________________________________________________ 1 1 Diesel Engine Oils 21.63 21.63 Volume of sample required: 100 ml Viscosity Measurements (SBD1) ASTM D445 Neutralization Number (SBD1) HL-1118 FTIR Nicolet (SBD1) HL-1140 Metals by ICP AES (SBD1) HL-1158 Turnaround time is 2 working day(s) from receipt of sample. QUOTATION TOTAL 21.63 ea Thank you for the opportunity to provide you with the above quotation for your samples. The above quotation is based on your requested scope of work and/or our recommended analytical methods for your sample type and package pricing. Tests selected on a one-on-one basis and not tested as a package may be subject to price adjustments. Prices are also subject to change based on the actual sample type as determined upon receipt. Reference oils are required for baseline information. Our standard turn around time is two (2) working days. Rush analysis is triple for a 24 hour turn around time. Any analysis that is subcontracted to another facility (lab) will be processed within 7-10 working days depending on the test. Samples received in larger batches may have a longer turn around time depending on sample type and tests requested. This quotation is valid for 90 days. Please refer to this quotation number when submitting samples. Sampling kits will be included in this program. Kits include a bottle, label, ID Form, and mailer. Sampling pumps and tubing will be charged at list price. Postage paid labels are also available for an additional fee. Please visit our website to view a current list of supplies Reports can be transmitted via email upon completion at no additional charge. We also have Internet access-iLAMP available for an additional $300/ year that will allow you to retrieve your data, view and print reports, set up units and route list, print labels, etc. Please contact Customer Service to order iLAMP. A credit application or payment is required with all new accounts. Please fax one to 707-554-0109. Credit will be extended based on the reference verification. The sample turn around time may be longer based on credit reference responses. Laboratory Pricing Policy 1. Hours of Operation And Normal Availability Regular laboratory hours are 8:00 AM to 5:00 PM Monday through Friday. For condition monitoring analyses, our normal turnaround is 48 hours (two working days). For all other analyses, our normal turnaround is 96 hours (four working days). Any analysis that is subcontracted to another facility


120


www.herguth.com

(lab) will be processed within 7-10 working days depending on the test. Please note there may be delays in turn around times based on account setup and credit references. 2. Minimum Invoice Charges, Rush Analyses and Overtime Rates A minimum fee of $25.00 may be charged for any analysis invoice. For Condition Monitoring analyses, "RUSH" samples results are available within 24 hours (or less) and are charged at three times the normal analyses rate. For other analyses there are two "RUSH" provisions for work performed during our regular laboratory hours: a) 48 hour (2 working day) analysis time is charged at twice the normal analysis fee. b) 24 hour (one working day) turnaround, or less, is charged at three times the normal analysis fee. There are some analyses that cannot be completed in less than 24 hours; however, they can be moved ahead of the scheduled samples waiting for that analysis. These analyses will be charged at the 24 hour rush rate. Laboratory work performed during other hours, including Saturday, Sunday or recognized Holidays may be charged at triple our normal analyses rates, an hourly rate with a four (4) hour minimum charge, or $1,500, whichever is greater. Nuclear Quality Assured (10 CFR 50 Appendix B) or radioactive samples analyzed during periods other than normal hours will be charged a minimum of $2,500. 3. Quality Assurance Program And Surveillance Analyses performed under the Safety Related Part 21 Program are charged at 1.35 times the applicable fee. Surveillance of work performed at Herguth Laboratories, Inc. by client representatives may be charged at three times the applicable fee. All ASTM methods are performed at the latest published revision. 4. Radioactive Materials Analyses on radioactive samples will be assessed a surcharge of 1.5 times the analysis fee or a fee of $125 per sample (Condition Monitoring Rads), as specifically quoted to the customer. Radioactive lubricant samples are properly disposed of by Herguth provided the sample meets our disposal criteria. This service is not applicable for non-liquid lubricant samples, which must be returned to the client. 5. Sample Pick-Up And Delivery Sample pick-up and delivery during normal working hours may be charged at a minimum of $25 within a 25 mile radius. The fee will be $50 within a radius of 50 miles. Sample pick-up during non-working hours may be charged a minimum of $100 plus expenses. This applies to the nine (9) San Francisco Bay Area counties. Special arrangements must be made for custody transfers and pick-ups outside of this area. 6. Sample Retention and Disposal Samples will be held for a minimum of 30 days. Long term retention services are available by special request. Non-hydrocarbon samples, "unknown" samples, and samples containing elements or constituents which cannot be accommodated by our normal waste streams will either be returned, or if requested, disposed of properly. Handling and disposal surcharges may be assessed. Samples can be returned to the client if requested. Terms, Conditions, and Limitations All services rendered by Herguth Laboratories, Inc. are undertaken, and all rates are based upon the following terms: (a) Neither Herguth Laboratories, Inc., nor any of its employees, agents or sub-contractors shall be liable for any loss or damage arising out of Herguth Laboratories, Inc.'s. performance or non-performance, whether by way of negligence or breach of contract, or otherwise, in any amount greater than twice the amount billed to the customer for the work leading to the claim of the customer. Said remedy shall be the sole and exclusive remedy against Herguth Laboratories, Inc. arising out of its work.


121


www.herguth.com

(b) All claims must be in writing within forty-five (45) days after delivery of the Herguth Laboratories, Inc. report regarding said work, or such claim shall be deemed as irrevocably waived. (c) Herguth Laboratories, Inc. reports are submitted in writing and are for our customers only. Our customers are considered to be only those entities being billed for our services. Acquisition of a Herguth Laboratories, Inc. report by other than our customer does not constitute a representation of Herguth Laboratories, Inc. as to the accuracy of the contents thereof. (d) In no event shall Herguth Laboratories, Inc., its employees, agents or sub-contractors be responsible for consequential or special damages of any kind or in any amount. (e) No deviation from the terms set forth herein shall bind Herguth Laboratories, Inc. unless explicitly agreed upon and accepted contractually, or unless explicitly expressed in writing and signed by a Corporate Officer of Herguth Laboratories, Inc. (f) Depending on specific customer requirements and/or changes in operations, Herguth Laboratories, Inc. reserves the right to change the pricing and availability of analyses as published in price list(s). (g) All ASTM methods are performed at the latest published revision. Should you have any questions regarding this quote, please contact myself at 800-645-5227 ext. 3012. We look forward to working with you on this and future projects. Please refer to this quotation number when submitting samples. Please visit our website for additional services and capabilities www.herguth.com.

________________________________________ Linda Perry Sales & Marketing


122

Oil

Type

: SA

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(GN

_032

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P.O

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Lab

Num

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5661

9

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123

Oil

Type

: SA

E 40

(GN

_032

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P.O

. : K

U09

-111

Lab

Num

ber :

V10

6106

6

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124

Oil

Type

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40

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. : S

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0350

Lab

Num

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6628

2

09/2

0/10

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1

18:2

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NO

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Tom

Hol

mes

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h In

stitu

te24

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00 D

eg C

TBN

mg

KO

H/g

FTIR So

ot %

wt.

Oxi

datio

n Ab

s/cm

Wat

er F

TIR

% V

olSu

lfina

tion

Abs/

Fuel

% V

olG

lyco

l % V

olM

etal

sIro

n pp

mAl

umin

um p

pmC

hrom

ium

ppm

Cop

per p

pmLe

ad p

pmTi

n pp

mN

icke

l ppm

Silv

er p

pmAn

timon

y pp

mSi

licon

ppm

Sodi

um p

pmBo

ron

ppm

Zinc

ppm

Phos

phor

us p

pmC

alci

um p

pmM

agne

sium

ppm

Bariu

m p

pmM

olyb

denu

m p

pmPo

tass

ium

ppm

12.0

02.

0016

.80

3.0 30

0.20 30 5.0

0.20 76 7 4 32 8 4 44.

5 20

3617 0

15.7

34.

68__

____

____

**3.

7 8<0

.10 13

<2.0

<0.1

0__

____

____ 42 2 1 1 1 1 <1

<0.1 1 2 4 <1

1041 928

2011 5 <1 <1 <3

Cod

e :L

OVE

MC

Lov

elac

e R

espi

rato

ry R

esea

rch

Inst

itute

Pho

ne :(

505)

348

-960

0 F

ax :(

505)

348

-498

0Th

ese

resu

lts a

re s

ubm

itted

pur

suan

t to

our c

urre

nt T

erm

s, C

ondi

tions

and

Lim

itatio

ns a

nd L

abor

ator

y P

ricin

g P

olic

y. N

o re

spon

sibi

lity

or li

abili

ty is

ass

umed

for t

he m

anne

r in

whi

ch th

ese

resu

lts a

re u

sed

or in

terp

rete

d.

Eval

uate

d B

y: B

obby

R L

icu,

Sen

ior E

valu

ator

- F

or q

uest

ions

abo

ut th

is re

port

, ple

ase

call

888-

437-

4884

.er

labg

t1.fr

x R

ev. 0

6/21

/201

0


125

Oil

Type

: SA

E 40

(GN

_032

)

P.O

. : F

Y09-

111

ACES

Lab

Num

ber :

V10

7249

1

12/0

7/10

Page

1

08:5

1:20

AB

NO

RM

AL:

Abn

orm

al re

sults

for f

luid

are

pre

sent

. E

quip

men

t app

ears

sat

isfa

ctor

y.S

oot c

onte

nt is

hig

h. O

ther

test

resu

lts a

re a

ccep

tabl

e. D

rain

oil

and

chan

ge fi

lter(s

). A

dditi

onal

sam

ple

is n

eede

d to

hel

p es

tabl

ish

trend

. R

esam

ple

at h

alf n

orm

al in

terv

al.

Plea

se p

rovi

deeq

uipm

ent m

ake

and

mod

el a

s w

ell a

s th

e fu

ll na

me

and

grad

e of

the

lubr

ican

t in

serv

ice.

Tom

Hol

mes

Love

lace

Res

pira

tory

Res

earc

h In

stitu

te24

25 R

idge

cres

t Driv

e, S

E

Alb

uque

rque

, NM

871

08

09/3

0/10

10/0

6/10

10/0

7/10

10/1

1/10

Ship

ped

:R

ecei

ved:

Prin

ted:

Sam

pled

:

Uni

t Typ

e : E

ngin

e, D

iese

l (G

N_D

E001

)

ID: F

Y09-

111-

30SE

P10-

OIL

- FY

09-1

11-3

0SEP

10-O

IL, D

iese

l Eng

ine *

= ex

ceed

s C

autio

n lim

it

**

= e

xcee

ds A

larm

lim

it

101

Cor

pora

te P

lace

, Val

lejo

, CA

9459

0w

ww

.her

guth

.com

ISO

900

1:20

08 a

nd IS

O/IE

C 1

7025

:200

5 C

ertif

ied

Lab

Num

ber

Sam

ple

Dat

eM

inim

umM

axim

umV1

0724

9109

/30/

10

Com

para

tive

Gra

phic

Ana

lysi

s

Silic

onTin

Lead

Cop

per

Chr

omiu

m

Alum

inumIro

n

Sulfi

natio

n

Oxi

datio

n

Soot

TBN

Vis

@ 1

00 D

eg C

Und

er M

in

War

ning

Typ

ical

Typ

ical

War

ning

Ove

r Max

Uni

t Tim

e (H

R)

Oil

Tim

e (H

R)

Vis

@ 1

00 D

eg C

TBN

mg

KO

H/g

FTIR So

ot %

wt.

Oxi

datio

n Ab

s/cm

Wat

er F

TIR

% V

olSu

lfina

tion

Abs/

Fuel

% V

olG

lyco

l % V

olM

etal

sIro

n pp

mAl

umin

um p

pmC

hrom

ium

ppm

Cop

per p

pmLe

ad p

pmTi

n pp

mN

icke

l ppm

Silv

er p

pmAn

timon

y pp

mSi

licon

ppm

Sodi

um p

pmBo

ron

ppm

Zinc

ppm

Phos

phor

us p

pmC

alci

um p

pmM

agne

sium

ppm

Bariu

m p

pmM

olyb

denu

m p

pmPo

tass

ium

ppm

12.0

02.

0016

.80

3.0 30

0.20 30 5.0

0.20 76 7 4 32 8 4 44.

5 20

5063 0

15.5

35.

62__

____

____

**3.

3 15<0

.10 25

<2.0

<0.1

0__

____

____ 46 3 1 1 1 1 <1

<0.1 <1 5 3 3

1325

1060

2567 8 <1 3 <3

Cod

e :L

OVE

MC

Lov

elac

e R

espi

rato

ry R

esea

rch

Inst

itute

Pho

ne :(

505)

348

-960

0 F

ax :(

505)

348

-498

0Th

ese

resu

lts a

re s

ubm

itted

pur

suan

t to

our c

urre

nt T

erm

s, C

ondi

tions

and

Lim

itatio

ns a

nd L

abor

ator

y P

ricin

g P

olic

y. N

o re

spon

sibi

lity

or li

abili

ty is

ass

umed

for t

he m

anne

r in

whi

ch th

ese

resu

lts a

re u

sed

or in

terp

rete

d.

Eval

uate

d B

y: N

uno

H. M

orei

ra, E

valu

ator

- F

or q

uest

ions

abo

ut th

is re

port

, ple

ase

call

888-

437-

4884

.er

labg

t1.fr

x R

ev. 0

6/21

/201

0


126

Oil

Type

: SA

E 40

(GN

_032

)

P.O

. : F

Y09-

111

ACES

Lab

Num

ber :

V10

7757

7

11/0

1/10

Page

1

16:1

0:19

AB

NO

RM

AL:

Abn

orm

al re

sults

for f

luid

are

pre

sent

. E

quip

men

t app

ears

sat

isfa

ctor

y.So

ot c

onte

nt is

hig

h. P

leas

e pr

ovid

e eq

uipm

ent m

ake

and

mod

el a

s w

ell a

s th

e fu

ll na

me

and

grad

e of

the

lubr

ican

t in

serv

ice.

Dra

in o

il an

d ch

ange

filte

r(s).

Che

ck fo

r pro

per c

ombu

stio

npr

oper

ties

(exh

aust

bac

k pr

essu

re, o

pera

ting

tem

pera

ture

s, w

orn/

brok

en ri

ngs,

exc

essi

ve id

ling,

hung

val

ves,

impr

oper

fuel

set

tings

, air

inta

ke re

stric

tions

). R

esam

ple

at h

alf n

orm

al in

terv

al.

Tom

Hol

mes

Love

lace

Res

pira

tory

Res

earc

h In

stitu

te24

25 R

idge

cres

t Driv

e, S

E

Alb

uque

rque

, NM

871

08

10/2

5/10

10/2

5/10

10/2

8/10

11/0

1/10

Ship

ped

:R

ecei

ved:

Prin

ted:

Sam

pled

:

Uni

t Typ

e : E

ngin

e, D

iese

l (G

N_D

E001

)

ID: F

Y09-

111-

25O

CT1

0-O

IL -

FY09

-111

-25O

CT1

0-O

IL, D

iese

l Eng

ine * =

exce

eds

Cau

tion

limit

** =

exc

eeds

Ala

rm li

mit

101

Cor

pora

te P

lace

, Val

lejo

, CA

9459

0w

ww

.her

guth

.com

ISO

900

1:20

08 a

nd IS

O/IE

C 1

7025

:200

5 C

ertif

ied

Lab

Num

ber

Sam

ple

Dat

eM

inim

umM

axim

umV1

0775

7710

/25/

10

Com

para

tive

Gra

phic

Ana

lysi

s

Silic

on

Lead

Cop

per

Chr

omiu

m

Alum

inumIro

n

Sulfi

natio

n

Oxi

datio

n

Soot

TBN

Vis

@10

0 D

eg C

Und

er M

in

War

ning

Typ

ical

Typ

ical

War

ning

Ove

r Max

Uni

t Tim

e (H

R)

Oil

Tim

e (H

R)

Vis

@ 1

00 D

eg C

TBN

mg

KO

H/g

FTIR So

ot %

wt.

Oxi

datio

n Ab

s/cm

Wat

er F

TIR

% V

olSu

lfina

tion

Abs/

Fuel

% V

olG

lyco

l % V

olM

etal

sIro

n pp

mAl

umin

um p

pmC

hrom

ium

ppm

Cop

per p

pmLe

ad p

pmTi

n pp

mN

icke

l ppm

Silv

er p

pmAn

timon

y pp

mSi

licon

ppm

Sodi

um p

pmBo

ron

ppm

Zinc

ppm

Phos

phor

us p

pmC

alci

um p

pmM

agne

sium

ppm

Bariu

m p

pmM

olyb

denu

m p

pmPo

tass

ium

ppm

12.0

02.

0016

.80

3.0 30

0.20 30 5.0

0.20 74 4 4 7 4 4 44.

5 20

4136 0

15.5

14.

56__

____

____

**3.

5 14<0

.10 21

<2.0

<0.1

0__

____

____ 33 2 1 1 1 <1 <1

<0.1 <1 2 <2 1

919

815

1826 5 <1 1 <3

Cod

e :L

OVE

MC

Lov

elac

e R

espi

rato

ry R

esea

rch

Inst

itute

Pho

ne :(

505)

348

-960

0 F

ax :(

505)

348

-498

0Th

ese

resu

lts a

re s

ubm

itted

pur

suan

t to

our c

urre

nt T

erm

s, C

ondi

tions

and

Lim

itatio

ns a

nd L

abor

ator

y P

ricin

g P

olic

y. N

o re

spon

sibi

lity

or li

abili

ty is

ass

umed

for t

he m

anne

r in

whi

ch th

ese

resu

lts a

re u

sed

or in

terp

rete

d.

Eval

uate

d B

y: B

obby

R L

icu,

Sen

ior E

valu

ator

- F

or q

uest

ions

abo

ut th

is re

port

, ple

ase

call

888-

437-

4884

.er

labg

t1.fr

x R

ev. 0

6/21

/201

0


127

Oil

Type

: SA

E 15

W-4

0 (G

N_0

45)

P.

O. :

FY0

9-11

1 AC

ES

Lab

Num

ber :

V10

8488

7

12/0

6/10

Page

1

18:2

2:03

AB

NO

RM

AL:

Abn

orm

al re

sults

for f

luid

are

pre

sent

. E

quip

men

t app

ears

sat

isfa

ctor

y.So

ot c

onte

nt is

hig

h. L

evel

s m

ay b

e du

e to

oil

serv

ice

time

(not

pro

vide

d).

Dra

in o

il an

d ch

ange

filte

r(s).

Add

ition

al s

ampl

e is

nee

ded

to h

elp

esta

blis

h tre

nd.

Res

ampl

e at

hal

f nor

mal

inte

rval

.Pl

ease

pro

vide

equ

ipm

ent m

ake

and

mod

el a

s w

ell a

s th

e fu

ll na

me

and

grad

e of

the

lubr

ican

t in

serv

ice.

Tom

Hol

mes

Love

lace

Res

pira

tory

Res

earc

h In

stitu

te24

25 R

idge

cres

t Driv

e, S

E

Alb

uque

rque

, NM

871

08

11/1

5/10

12/0

1/10

12/0

2/10

12/0

6/10

Ship

ped

:R

ecei

ved:

Prin

ted:

Sam

pled

:

Uni

t Typ

e : E

ngin

e, D

iese

l (G

N_D

E001

)

ID: F

Y09-

111-

15N

OV1

0-E

- FY0

9-11

1-15

NO

V10,

Die

sel E

ngin

e

* =

exce

eds

Cau

tion

limit

** =

exc

eeds

Ala

rm li

mit

101

Cor

pora

te P

lace

, Val

lejo

, CA

9459

0w

ww

.her

guth

.com

ISO

900

1:20

08 a

nd IS

O/IE

C 1

7025

:200

5 C

ertif

ied

Lab

Num

ber

Sam

ple

Dat

eM

inim

umM

axim

umV1

0848

8711

/15/

10

Com

para

tive

Gra

phic

Ana

lysi

s

Silic

onTin

Lead

Cop

per

Chr

omiu

m

Alum

inumIro

n

Sulfi

natio

n

Oxi

datio

n

Soot

TBN

Vis

@ 1

00 D

eg C

Und

er M

in

War

ning

Typ

ical

Typ

ical

War

ning

Ove

r Max

Uni

t Tim

e (H

R)

Oil

Tim

e (H

R)

Vis

@ 1

00 D

eg C

TBN

mg

KO

H/g

FTIR So

ot %

wt.

Oxi

datio

n Ab

s/cm

Wat

er F

TIR

% V

olSu

lfina

tion

Abs/

Fuel

% V

olG

lyco

l % V

olM

etal

sIro

n pp

mAl

umin

um p

pmC

hrom

ium

ppm

Cop

per p

pmLe

ad p

pmTi

n pp

mN

icke

l ppm

Silv

er p

pmAn

timon

y pp

mSi

licon

ppm

Sodi

um p

pmBo

ron

ppm

Zinc

ppm

Phos

phor

us p

pmC

alci

um p

pmM

agne

sium

ppm

Bariu

m p

pmM

olyb

denu

m p

pmPo

tass

ium

ppm

12.0

02.

0016

.80

3.0 30

0.20 30 5.0

0.20 93 7 4 26 15 4 43.

1 20

0 015

.07

4.83

____

____

__**

3.2 14

<0.1

0 22<2

.0<0

.10

____

____

__ 35 2 1 1 1 1 <1<0

.1 <1 3 <2 394

096

220

92 8 <1 1 <3

Cod

e :L

OVE

MC

Lov

elac

e R

espi

rato

ry R

esea

rch

Inst

itute

Pho

ne :(

505)

348

-960

0 F

ax :(

505)

348

-498

0Th

ese

resu

lts a

re s

ubm

itted

pur

suan

t to

our c

urre

nt T

erm

s, C

ondi

tions

and

Lim

itatio

ns a

nd L

abor

ator

y P

ricin

g P

olic

y. N

o re

spon

sibi

lity

or li

abili

ty is

ass

umed

for t

he m

anne

r in

whi

ch th

ese

resu

lts a

re u

sed

or in

terp

rete

d.

Eval

uate

d B

y: D

avid

F. F

ryck

i, C

LS -

For

que

stio

ns a

bout

this

repo

rt, p

leas

e ca

ll 88

8-43

7-48

84.

erla

bgt1

.frx

Rev

. 06/

21/2

010


128

Oil

Type

: SA

E 40

(GN

_032

)

P.O

. : F

Y09-

111

ACES

Lab

Num

ber :

V10

8658

0

12/1

6/10

Page

1

17:3

3:16

AB

NO

RM

AL:

Abn

orm

al re

sults

for f

luid

are

pre

sent

. E

quip

men

t app

ears

sat

isfa

ctor

y.So

ot c

onte

nt is

hig

h. P

leas

e pr

ovid

e eq

uipm

ent m

ake

and

mod

el a

s w

ell a

s th

e fu

ll na

me

and

grad

e of

the

lubr

ican

t in

serv

ice.

Dra

in o

il an

d ch

ange

filte

r(s).

Che

ck fo

r pro

per c

ombu

stio

npr

oper

ties.

Add

ition

al s

ampl

e is

nee

ded

to h

elp

esta

blis

h tre

nd.

Res

ampl

e at

hal

f nor

mal

inte

rval

.To

m H

olm

esLo

vela

ce R

espi

rato

ry R

esea

rch

Inst

itute

2425

Rid

gecr

est D

rive,

SE

Alb

uque

rque

, NM

871

08

12/0

6/10

12/1

3/10

12/1

4/10

12/1

6/10

Ship

ped

:R

ecei

ved:

Prin

ted:

Sam

pled

:

Uni

t Typ

e : E

ngin

e, D

iese

l (G

N_D

E001

)

ID: F

Y09-

111-

10D

EC10

-OIL

- FY

09-1

11--1

0DEC

10-D

iese

l Eng

ine

* =

exce

eds

Cau

tion

limit

** =

exc

eeds

Ala

rm li

mit

101

Cor

pora

te P

lace

, Val

lejo

, CA

9459

0w

ww

.her

guth

.com

ISO

900

1:20

08 a

nd IS

O/IE

C 1

7025

:200

5 C

ertif

ied

Lab

Num

ber

Sam

ple

Dat

eM

inim

umM

axim

umV1

0865

8012

/06/

10

Com

para

tive

Gra

phic

Ana

lysi

s

Silic

on

Lead

Cop

per

Chr

omiu

m

Alum

inumIro

n

Sulfi

natio

n

Oxi

datio

n

Soot

TBN

Vis

@ 1

00 D

eg C

Und

er M

in

War

ning

Typ

ical

Typ

ical

War

ning

Ove

r Max

Uni

t Tim

e (H

R)

Oil

Tim

e (H

R)

Vis

@ 1

00 D

eg C

TBN

mg

KO

H/g

FTIR So

ot %

wt.

Oxi

datio

n Ab

s/cm

Wat

er F

TIR

% V

olSu

lfina

tion

Abs/

Fuel

% V

olG

lyco

l % V

olM

etal

sIro

n pp

mAl

umin

um p

pmC

hrom

ium

ppm

Cop

per p

pmLe

ad p

pmTi

n pp

mN

icke

l ppm

Silv

er p

pmAn

timon

y pp

mSi

licon

ppm

Sodi

um p

pmBo

ron

ppm

Zinc

ppm

Phos

phor

us p

pmC

alci

um p

pmM

agne

sium

ppm

Bariu

m p

pmM

olyb

denu

m p

pmPo

tass

ium

ppm

12.0

02.

0016

.80

3.0 30

0.20 30 5.0

0.20 66 4 4 7 4 4 44.

5 20

4627 0

15.0

95.

32__

____

____

**3.

2 11<0

.10 16

<2.0

<0.1

0__

____

____ 34 1 1 1 1 <1 <1

<0.1 <1 2 <2 <1 920

865

2016 10 <1 <1 <3

Cod

e :L

OVE

MC

Lov

elac

e R

espi

rato

ry R

esea

rch

Inst

itute

Pho

ne :(

505)

348

-960

0 F

ax :(

505)

348

-498

0Th

ese

resu

lts a

re s

ubm

itted

pur

suan

t to

our c

urre

nt T

erm

s, C

ondi

tions

and

Lim

itatio

ns a

nd L

abor

ator

y P

ricin

g P

olic

y. N

o re

spon

sibi

lity

or li

abili

ty is

ass

umed

for t

he m

anne

r in

whi

ch th

ese

resu

lts a

re u

sed

or in

terp

rete

d.

Eval

uate

d B

y: B

obby

R L

icu,

Sen

ior E

valu

ator

- F

or q

uest

ions

abo

ut th

is re

port

, ple

ase

call

888-

437-

4884

.er

labg

t1.fr

x R

ev. 0

6/21

/201

0


129

Oil

Type

: SA

E 40

(GN

_032

)

P.O

. : J

K110

737

Lab

Num

ber :

V10

8977

1

01/1

0/11

Page

1

15:5

2:38

AB

NO

RM

AL:

Abn

orm

al re

sults

for f

luid

are

pre

sent

. E

quip

men

t app

ears

sat

isfa

ctor

y.So

ot c

onte

nt is

hig

h. L

evel

s m

ay b

e du

e to

oil

serv

ice

time

(not

pro

vide

d).

Dra

in o

il an

d ch

ange

filte

r(s).

Add

ition

al s

ampl

e is

nee

ded

to h

elp

esta

blis

h tre

nd.

Res

ampl

e at

hal

f nor

mal

inte

rval

.Pl

ease

pro

vide

equ

ipm

ent m

ake

and

mod

el a

s w

ell a

s th

e fu

ll na

me

and

grad

e of

the

lubr

ican

t in

serv

ice.

Tom

Hol

mes

Love

lace

Res

pira

tory

Res

earc

h In

stitu

te24

25 R

idge

cres

t Driv

e, S

E

Alb

uque

rque

, NM

871

08

01/0

3/11

01/0

5/11

01/0

6/11

01/1

0/11

Ship

ped

:R

ecei

ved:

Prin

ted:

Sam

pled

:

Uni

t Typ

e : E

ngin

e, D

iese

l (G

N_D

E001

)

ID: F

Y09-

111-

03JA

N11

-OIL

- FY

09-1

11-0

3JA

N11

-OIL

, Die

sel E

ngin

e * =

exce

eds

Cau

tion

limit

** =

exc

eeds

Ala

rm li

mit

101

Cor

pora

te P

lace

, Val

lejo

, CA

9459

0w

ww

.her

guth

.com

ISO

900

1:20

08 a

nd IS

O/IE

C 1

7025

:200

5 C

ertif

ied

Lab

Num

ber

Sam

ple

Dat

eM

inim

umM

axim

umV1

0897

7101

/03/

11

Com

para

tive

Gra

phic

Ana

lysi

s

Silic

onTin

Lead

Cop

per

Chr

omiu

m

Alum

inumIro

n

Sulfi

natio

n

Oxi

datio

n

Soot

TBN

Vis

@10

0 D

eg C

Und

er M

in

War

ning

Typ

ical

Typ

ical

War

ning

Ove

r Max

Uni

t Tim

e (H

R)

Oil

Tim

e (H

R)

Vis

@ 1

00 D

eg C

TBN

mg

KO

H/g

FTIR So

ot %

wt.

Oxi

datio

n Ab

s/cm

Wat

er F

TIR

% V

olSu

lfina

tion

Abs/

Fuel

% V

olG

lyco

l % V

olM

etal

sIro

n pp

mAl

umin

um p

pmC

hrom

ium

ppm

Cop

per p

pmLe

ad p

pmTi

n pp

mN

icke

l ppm

Silv

er p

pmAn

timon

y pp

mSi

licon

ppm

Sodi

um p

pmBo

ron

ppm

Zinc

ppm

Phos

phor

us p

pmC

alci

um p

pmM

agne

sium

ppm

Bariu

m p

pmM

olyb

denu

m p

pmPo

tass

ium

ppm

12.0

02.

0016

.80

3.0 30

0.20 30 5.0

0.20 65 4 4 7 4 4 44.

5 20

4877 0

15.1

73.

63__

____

____

**3.

3 14<0

.10 23

<2.0

<0.1

0__

____

____ 34 1 1 1 1 1 <1

<0.1 <1 6 10 <1

1100 871

2117 6 <1 <1 <3

Cod

e :L

OVE

MC

Lov

elac

e R

espi

rato

ry R

esea

rch

Inst

itute

Pho

ne :(

505)

348

-960

0 F

ax :(

505)

348

-498

0Th

ese

resu

lts a

re s

ubm

itted

pur

suan

t to

our c

urre

nt T

erm

s, C

ondi

tions

and

Lim

itatio

ns a

nd L

abor

ator

y P

ricin

g P

olic

y. N

o re

spon

sibi

lity

or li

abili

ty is

ass

umed

for t

he m

anne

r in

whi

ch th

ese

resu

lts a

re u

sed

or in

terp

rete

d.

Eval

uate

d B

y: D

avid

F. F

ryck

i, C

LS -

For

que

stio

ns a

bout

this

repo

rt, p

leas

e ca

ll 88

8-43

7-48

84.

erla

bgt1

.frx

Rev

. 06/

21/2

010


130

Oil

Type

: SA

E 40

(GN

_032

)

P.O

. : J

K110

737

Lab

Num

ber :

V10

9363

5

02/0

2/11

Page

1

14:1

3:01

AB

NO

RM

AL:

Abn

orm

al re

sults

for f

luid

are

pre

sent

. E

quip

men

t app

ears

sat

isfa

ctor

y.So

ot c

onte

nt is

hig

h. P

leas

e pr

ovid

e eq

uipm

ent m

ake

and

mod

el a

s w

ell a

s th

e fu

ll na

me

and

grad

e of

the

lubr

ican

t in

serv

ice.

Dra

in o

il an

d ch

ange

filte

r(s).

Che

ck fo

r pro

per c

ombu

stio

npr

oper

ties

(exh

aust

bac

k pr

essu

re, o

pera

ting

tem

pera

ture

s, w

orn/

brok

en ri

ngs,

exc

essi

ve id

ling,

hung

val

ves,

impr

oper

fuel

set

tings

, air

inta

ke re

stric

tions

). R

esam

ple

at h

alf n

orm

al in

terv

al.

Tom

Hol

mes

Love

lace

Res

pira

tory

Res

earc

h In

stitu

te24

25 R

idge

cres

t Driv

e, S

E

Alb

uque

rque

, NM

871

08

01/2

4/11

01/2

7/11

01/2

8/11

02/0

2/11

Ship

ped

:R

ecei

ved:

Prin

ted:

Sam

pled

:

Uni

t Typ

e : E

ngin

e, D

iese

l (G

N_D

E001

)

ID: F

Y09-

111-

24JA

N11

-OIL

- FY

09-1

11-2

4JA

N11

-OIL

, Die

sel E

ngin

e * =

exce

eds

Cau

tion

limit

** =

exc

eeds

Ala

rm li

mit

101

Cor

pora

te P

lace

, Val

lejo

, CA

9459

0w

ww

.her

guth

.com

ISO

900

1:20

08 a

nd IS

O/IE

C 1

7025

:200

5 C

ertif

ied

Lab

Num

ber

Sam

ple

Dat

eM

inim

umM

axim

umV1

0936

3501

/24/

11

Com

para

tive

Gra

phic

Ana

lysi

s

Silic

onTin

Lead

Cop

per

Chr

omiu

m

Alum

inumIro

n

Sulfi

natio

n

Oxi

datio

n

Soot

TBN

Vis

@10

0 D

eg C

Und

er M

in

War

ning

Typ

ical

Typ

ical

War

ning

Ove

r Max

Uni

t Tim

e (H

R)

Flui

d Ti

me

(HR

)Vi

s @

100

Deg

CTB

N m

g K

OH

/gFT

IR Soot

% w

t.O

xida

tion

Abs/

cmW

ater

FTI

R %

Vol

Sulfi

natio

n Ab

s/Fu

el %

Vol

Gly

col %

Vol

Met

als

Iron

ppm

Alum

inum

ppm

Chr

omiu

m p

pmC

oppe

r ppm

Lead

ppm

Tin

ppm

Nic

kel p

pmSi

lver

ppm

Antim

ony

ppm

Silic

on p

pmSo

dium

ppm

Boro

n pp

mZi

nc p

pmPh

osph

orus

ppm

Cal

cium

ppm

Mag

nesi

um p

pmBa

rium

ppm

Mol

ybde

num

ppm

Pota

ssiu

m p

pm

12.0

02.

0016

.80

3.0 30

0.20 30 5.0

0.20 64 4 4 7 4 4 44.

5 20

5146 0

15.1

910

.10

____

____

__**

3.4 11

<0.1

0 25<2

.0<0

.10

____

____

__ 35 2 1 1 1 1 <1<0

.1 1 2 3 <1 983

812

2017 6 <1 <1 <3

Cod

e :L

OVE

MC

Lov

elac

e R

espi

rato

ry R

esea

rch

Inst

itute

Pho

ne :(

505)

348

-960

0 F

ax :(

505)

348

-498

0Th

ese

resu

lts a

re s

ubm

itted

pur

suan

t to

our c

urre

nt T

erm

s, C

ondi

tions

and

Lim

itatio

ns a

nd L

abor

ator

y P

ricin

g P

olic

y. N

o re

spon

sibi

lity

or li

abili

ty is

ass

umed

for t

he m

anne

r in

whi

ch th

ese

resu

lts a

re u

sed

or in

terp

rete

d.

Eval

uate

d B

y: B

obby

R L

icu,

Sen

ior E

valu

ator

- F

or q

uest

ions

abo

ut th

is re

port

, ple

ase

call

888-

437-

4884

.er

labg

t1.fr

x R

ev. 0

6/21

/201

0


131

Oil

Type

: SA

E 15

W-4

0 (G

N_0

45)

P.

O. :

JK1

1073

7

Lab

Num

ber :

V10

9912

7

03/0

1/11

Page

1

15:2

8:59

AB

NO

RM

AL:

Abn

orm

al re

sults

for f

luid

are

pre

sent

. E

quip

men

t app

ears

sat

isfa

ctor

y.S

oot c

onte

nt is

hig

h. O

ther

test

resu

lts a

re a

ccep

tabl

e. D

rain

oil

and

chan

ge fi

lter(s

). A

dditi

onal

sam

ple

is n

eede

d to

hel

p es

tabl

ish

trend

. R

esam

ple

at h

alf n

orm

al in

terv

al.

Plea

se p

rovi

deeq

uipm

ent m

ake

and

mod

el a

s w

ell a

s th

e fu

ll na

me

and

grad

e of

the

lubr

ican

t in

serv

ice.

Tom

Hol

mes

Love

lace

Res

pira

tory

Res

earc

h In

stitu

te24

25 R

idge

cres

t Driv

e, S

E

Alb

uque

rque

, NM

871

08

02/2

2/11

02/2

4/11

02/2

5/11

03/0

1/11

Ship

ped

:R

ecei

ved:

Prin

ted:

Sam

pled

:

Uni

t Typ

e : E

ngin

e, D

iese

l (G

N_D

E001

)

ID: F

Y09-

111-

22FE

B11

-OIL

- FY

09-1

11-2

2FEB

11-O

IL, D

iese

l Eng

ine *

= ex

ceed

s C

autio

n lim

it

**

= e

xcee

ds A

larm

lim

it

101

Cor

pora

te P

lace

, Val

lejo

, CA

9459

0w

ww

.her

guth

.com

ISO

900

1:20

08 a

nd IS

O/IE

C 1

7025

:200

5 C

ertif

ied

Lab

Num

ber

Sam

ple

Dat

eM

inim

umM

axim

umV1

0991

2702

/22/

11

Com

para

tive

Gra

phic

Ana

lysi

s

Silic

onTin

Lead

Cop

per

Chr

omiu

m

Alum

inumIro

n

Sulfi

natio

n

Oxi

datio

n

Soot

TBN

Vis

@ 1

00 D

eg C

Und

er M

in

War

ning

Typ

ical

Typ

ical

War

ning

Ove

r Max

Uni

t Tim

e (H

R)

Flui

d Ti

me

(HR

)Vi

s @

100

Deg

CTB

N m

g K

OH

/gFT

IR Soot

% w

t.O

xida

tion

Abs/

cmW

ater

FTI

R %

Vol

Sulfi

natio

n Ab

s/Fu

el %

Vol

Gly

col %

Vol

Met

als

Iron

ppm

Alum

inum

ppm

Chr

omiu

m p

pmC

oppe

r ppm

Lead

ppm

Tin

ppm

Nic

kel p

pmSi

lver

ppm

Antim

ony

ppm

Silic

on p

pmSo

dium

ppm

Boro

n pp

mZi

nc p

pmPh

osph

orus

ppm

Cal

cium

ppm

Mag

nesi

um p

pmBa

rium

ppm

Mol

ybde

num

ppm

Pota

ssiu

m p

pm

12.0

02.

0016

.80

3.0 30

0.20 30 5.0

0.20 89 7 4 24 15 4 43.

1 20

5437 0

15.3

43.

92__

____

____

**3.

8 13<0

.10 19

<2.0

<0.1

0__

____

____ 35 2 1 1 1 1 <1

<0.1 <1 3 5 <1

1010 902

1723 7 <1 <1 <3

Cod

e :L

OVE

MC

Lov

elac

e R

espi

rato

ry R

esea

rch

Inst

itute

Pho

ne :(

505)

348

-960

0 F

ax :(

505)

348

-498

0Th

ese

resu

lts a

re s

ubm

itted

pur

suan

t to

our c

urre

nt T

erm

s, C

ondi

tions

and

Lim

itatio

ns a

nd L

abor

ator

y P

ricin

g P

olic

y. N

o re

spon

sibi

lity

or li

abili

ty is

ass

umed

for t

he m

anne

r in

whi

ch th

ese

resu

lts a

re u

sed

or in

terp

rete

d.

Eval

uate

d B

y: N

uno

H. M

orei

ra, E

valu

ator

- F

or q

uest

ions

abo

ut th

is re

port

, ple

ase

call

888-

437-

4884

.er

labg

t1.fr

x R

ev. 0

6/21

/201

0


132

Oil

Type

: SA

E 40

(GN

_032

)

P.O

. : J

K110

737

Lab

Num

ber :

V11

0264

5

03/2

1/11

Page

1

13:3

1:46

AB

NO

RM

AL:

Abn

orm

al re

sults

for f

luid

are

pre

sent

. E

quip

men

t app

ears

sat

isfa

ctor

y.So

ot c

onte

nt is

hig

h. P

leas

e pr

ovid

e eq

uipm

ent m

ake

and

mod

el a

s w

ell a

s th

e fu

ll na

me

and

grad

e of

the

lubr

ican

t in

serv

ice.

Dra

in o

il an

d ch

ange

filte

r(s).

Che

ck fo

r pro

per c

ombu

stio

npr

oper

ties

(exh

aust

bac

k pr

essu

re, o

pera

ting

tem

pera

ture

s, w

orn/

brok

en ri

ngs,

exc

essi

ve id

ling,

hung

val

ves,

impr

oper

fuel

set

tings

, air

inta

ke re

stric

tions

). R

esam

ple

at h

alf n

orm

al in

terv

al.

Tom

Hol

mes

Love

lace

Res

pira

tory

Res

earc

h In

stitu

te24

25 R

idge

cres

t Driv

e, S

E

Alb

uque

rque

, NM

871

08

03/1

4/11

03/1

6/11

03/1

7/11

03/2

1/11

Ship

ped

:R

ecei

ved:

Prin

ted:

Sam

pled

:

Uni

t Typ

e : E

ngin

e, D

iese

l (G

N_D

E001

)

ID: F

Y09-

111-

14M

AR

11-O

IL -

FY09

-111

-14M

AR

11-O

IL, D

iese

l Eng

ine

* =

exce

eds

Cau

tion

limit

** =

exc

eeds

Ala

rm li

mit

101

Cor

pora

te P

lace

, Val

lejo

, CA

9459

0w

ww

.her

guth

.com

ISO

900

1:20

08 a

nd IS

O/IE

C 1

7025

:200

5 C

ertif

ied

Lab

Num

ber

Sam

ple

Dat

eM

inim

umM

axim

umV1

1026

4503

/14/

11

Com

para

tive

Gra

phic

Ana

lysi

s

Silic

on

Lead

Cop

per

Chr

omiu

m

Alum

inumIro

n

Sulfi

natio

n

Oxi

datio

n

Soot

TBN

Vis

@10

0 D

eg C

Und

er M

in

War

ning

Typ

ical

Typ

ical

War

ning

Ove

r Max

Uni

t Tim

e (H

R)

Flui

d Ti

me

(HR

)Vi

s @

100

Deg

CTB

N m

g K

OH

/gFT

IR Soot

% w

t.O

xida

tion

Abs/

cmW

ater

FTI

R %

Vol

Sulfi

natio

n Ab

s/Fu

el %

Vol

Gly

col %

Vol

Met

als

Iron

ppm

Alum

inum

ppm

Chr

omiu

m p

pmC

oppe

r ppm

Lead

ppm

Tin

ppm

Nic

kel p

pmSi

lver

ppm

Antim

ony

ppm

Silic

on p

pmSo

dium

ppm

Boro

n pp

mZi

nc p

pmPh

osph

orus

ppm

Cal

cium

ppm

Mag

nesi

um p

pmBa

rium

ppm

Mol

ybde

num

ppm

Pota

ssiu

m p

pm

12.0

02.

0016

.80

3.0 30

0.20 30 5.0

0.20 62 4 4 7 4 4 44.

5 20

5693 0

15.0

25.

07__

____

____

**3.

4 11<0

.10 24

<2.0

<0.1

0__

____

____ 34 2 1 1 2 <1 <1

<0.1 <1 2 2 <1

1064 931

2182 5 <1 <1 <3

Cod

e :L

OVE

MC

Lov

elac

e R

espi

rato

ry R

esea

rch

Inst

itute

Pho

ne :(

505)

348

-960

0 F

ax :(

505)

348

-498

0Th

ese

resu

lts a

re s

ubm

itted

pur

suan

t to

our c

urre

nt T

erm

s, C

ondi

tions

and

Lim

itatio

ns a

nd L

abor

ator

y P

ricin

g P

olic

y. N

o re

spon

sibi

lity

or li

abili

ty is

ass

umed

for t

he m

anne

r in

whi

ch th

ese

resu

lts a

re u

sed

or in

terp

rete

d.

Eval

uate

d B

y: B

obby

R L

icu,

Sen

ior E

valu

ator

- F

or q

uest

ions

abo

ut th

is re

port

, ple

ase

call

888-

437-

4884

.er

labg

t1.fr

x R

ev. 0

6/21

/201

0


133

Oil

Type

: SA

E 40

(GN

_032

)

P.O

. : J

K110

737

Lab

Num

ber :

V11

0627

4

04/1

2/11

Page

1

17:4

1:32

AB

NO

RM

AL:

Abn

orm

al re

sults

for f

luid

are

pre

sent

. E

quip

men

t app

ears

sat

isfa

ctor

y.S

oot c

onte

nt is

hig

h. O

ther

test

resu

lts a

re a

ccep

tabl

e. D

rain

oil

and

chan

ge fi

lter(s

). A

dditi

onal

sam

ple

is n

eede

d to

hel

p es

tabl

ish

trend

. R

esam

ple

at h

alf n

orm

al in

terv

al.

Plea

se p

rovi

deeq

uipm

ent m

ake

and

mod

el a

s w

ell a

s th

e fu

ll na

me

and

grad

e of

the

lubr

ican

t in

serv

ice.

Tom

Hol

mes

Love

lace

Res

pira

tory

Res

earc

h In

stitu

te24

25 R

idge

cres

t Driv

e, S

E

Alb

uque

rque

, NM

871

08

04/0

1/11

04/0

7/11

04/0

8/11

04/1

2/11

Ship

ped

:R

ecei

ved:

Prin

ted:

Sam

pled

:

Uni

t Typ

e : E

ngin

e, D

iese

l (G

N_D

E001

)

ID: F

Y09-

111-

05A

PR11

-OIL

- FY

09-1

11-0

5APR

11-O

IL, D

iese

l Eng

ine * =

exce

eds

Cau

tion

limit

** =

exc

eeds

Ala

rm li

mit

101

Cor

pora

te P

lace

, Val

lejo

, CA

9459

0w

ww

.her

guth

.com

ISO

900

1:20

08 a

nd IS

O/IE

C 1

7025

:200

5 C

ertif

ied

Lab

Num

ber

Sam

ple

Dat

eM

inim

umM

axim

umV1

1062

7404

/01/

11

Com

para

tive

Gra

phic

Ana

lysi

s

Silic

onTin

Lead

Cop

per

Chr

omiu

m

Alum

inumIro

n

Sulfi

natio

n

Oxi

datio

n

Soot

TBN

Vis

@ 1

00 D

eg C

Und

er M

in

War

ning

Typ

ical

Typ

ical

War

ning

Ove

r Max

Uni

t Tim

e (H

R)

Flui

d Ti

me

(HR

)Vi

s @

100

Deg

CTB

N m

g K

OH

/gFT

IR Soot

% w

t.O

xida

tion

Abs/

cmW

ater

FTI

R %

Vol

Sulfi

natio

n Ab

s/Fu

el %

Vol

Gly

col %

Vol

Met

als

Iron

ppm

Alum

inum

ppm

Chr

omiu

m p

pmC

oppe

r ppm

Lead

ppm

Tin

ppm

Nic

kel p

pmSi

lver

ppm

Antim

ony

ppm

Silic

on p

pmSo

dium

ppm

Boro

n pp

mZi

nc p

pmPh

osph

orus

ppm

Cal

cium

ppm

Mag

nesi

um p

pmBa

rium

ppm

Mol

ybde

num

ppm

Pota

ssiu

m p

pm

12.0

02.

0016

.80

3.0 30

0.20 30 5.0

0.20 60 4 4 7 4 4 44.

5 20

5950 0

15.2

84.

15__

____

____

**3.

3 12<0

.10 15

<2.0

<0.1

0__

____

____ 35 2 1 1 1 1 <1

<0.1 <1 2 <2 <1 987

899

2103 7 <1 <1 <3

Cod

e :L

OVE

MC

Lov

elac

e R

espi

rato

ry R

esea

rch

Inst

itute

Pho

ne :(

505)

348

-960

0 F

ax :(

505)

348

-498

0Th

ese

resu

lts a

re s

ubm

itted

pur

suan

t to

our c

urre

nt T

erm

s, C

ondi

tions

and

Lim

itatio

ns a

nd L

abor

ator

y P

ricin

g P

olic

y. N

o re

spon

sibi

lity

or li

abili

ty is

ass

umed

for t

he m

anne

r in

whi

ch th

ese

resu

lts a

re u

sed

or in

terp

rete

d.

Eval

uate

d B

y: N

uno

H. M

orei

ra, E

valu

ator

- F

or q

uest

ions

abo

ut th

is re

port

, ple

ase

call

888-

437-

4884

.er

labg

t1.fr

x R

ev. 0

6/21

/201

0


134

Oil

Type

: SA

E 40

(GN

_032

)

P.O

. : J

K110

737

Lab

Num

ber :

V11

0934

4

05/0

2/11

Page

1

13:3

6:18

This

is a

bas

elin

e re

fere

nce

sam

ple.

Res

ult(s

) app

ear a

ccep

tabl

e, n

otin

g th

e fu

ll na

me

and

grad

e of

the

lubr

ican

t in

unav

aila

ble.

Tom

Hol

mes

Love

lace

Res

pira

tory

Res

earc

h In

stitu

te24

25 R

idge

cres

t Driv

e, S

E

Alb

uque

rque

, NM

871

08

04/2

6/11

04/2

7/11

04/2

8/11

05/0

2/11

Ship

ped

:R

ecei

ved:

Prin

ted:

Sam

pled

:

Uni

t Typ

e : N

ew O

il (G

N_N

O00

1)

ID: F

Y09-

111-

26A

PR11

-NEW

- N

ew M

otor

Oil:

FY0

9-11

1-26

APR

11-O

S222

049C

* =

exce

eds

Cau

tion

limit

** =

exc

eeds

Ala

rm li

mit

101

Cor

pora

te P

lace

, Val

lejo

, CA

9459

0w

ww

.her

guth

.com

ISO

900

1:20

08 a

nd IS

O/IE

C 1

7025

:200

5 C

ertif

ied

Lab

Num

ber

Sam

ple

Dat

eM

inim

umM

axim

umV1

1093

4404

/26/

11

Com

para

tive

Gra

phic

Ana

lysi

s

Silic

on

Alum

inumIro

n

Oxi

datio

n

TBN

Vis

@ 1

00 D

eg C

Und

er M

in

War

ning

Typ

ical

Typ

ical

War

ning

Ove

r Max

Uni

t Tim

e (H

R)

Flui

d Ti

me

(HR

)Vi

s @

100

Deg

CTB

N m

g K

OH

/gFT

IR Soot

% w

t.O

xida

tion

Abs/

cmW

ater

FTI

R %

Vol

Sulfi

natio

n Ab

s/Fu

el %

Vol

Gly

col %

Vol

Met

als

Iron

ppm

Alum

inum

ppm

Chr

omiu

m p

pmC

oppe

r ppm

Lead

ppm

Tin

ppm

Nic

kel p

pmSi

lver

ppm

Antim

ony

ppm

Silic

on p

pmSo

dium

ppm

Boro

n pp

mZi

nc p

pmPh

osph

orus

ppm

Cal

cium

ppm

Mag

nesi

um p

pmBa

rium

ppm

Mol

ybde

num

ppm

Pota

ssiu

m p

pm

12.0

02.

0016

.80

3.0 30

0.20 30 5.0

0.20 6 4 4 7 4 4 44.

5 20

0 015

.93

8.43

____

____

__<0

.1 3<0

.10 <2

<2.0

<0.1

0__

____

____ 2 1 <1 <1 <1 <1 <1

<0.1 <1 3 16 1

1339

1161

2558 8 <1 <1 <3

Cod

e :L

OVE

MC

Lov

elac

e R

espi

rato

ry R

esea

rch

Inst

itute

Pho

ne :(

505)

348

-960

0 F

ax :(

505)

348

-498

0Th

ese

resu

lts a

re s

ubm

itted

pur

suan

t to

our c

urre

nt T

erm

s, C

ondi

tions

and

Lim

itatio

ns a

nd L

abor

ator

y P

ricin

g P

olic

y. N

o re

spon

sibi

lity

or li

abili

ty is

ass

umed

for t

he m

anne

r in

whi

ch th

ese

resu

lts a

re u

sed

or in

terp

rete

d.

Eval

uate

d B

y: D

avid

F. F

ryck

i, C

LS -

For

que

stio

ns a

bout

this

repo

rt, p

leas

e ca

ll 88

8-43

7-48

84.

erla

bgt1

.frx

Rev

. 06/

21/2

010


135

Oil

Type

: SA

E 40

(GN

_032

)

P.O

. : J

K110

737

Lab

Num

ber :

V11

0934

5

05/0

2/11

Page

1

13:3

6:20

AB

NO

RM

AL:

Abn

orm

al re

sults

for f

luid

are

pre

sent

. E

quip

men

t app

ears

sat

isfa

ctor

y.So

ot c

onte

nt is

hig

h. T

he T

otal

Bas

e N

umbe

r (re

serv

e al

kalin

ity) i

s ap

proa

chin

g m

inim

umac

cept

able

leve

l. L

evel

s m

ay b

e du

e to

oil

serv

ice

time

(not

pro

vide

d).

Dra

in o

il an

d ch

ange

filte

r(s).

Addi

tiona

l sam

ple

is n

eede

d to

hel

p es

tabl

ish

trend

. R

esam

ple

at h

alf n

orm

al in

terv

al.

Plea

sepr

ovid

e eq

uipm

ent m

ake

and

mod

el a

s w

ell a

s th

e fu

ll na

me

and

grad

e of

the

lubr

ican

t in

serv

ice.

Tom

Hol

mes

Love

lace

Res

pira

tory

Res

earc

h In

stitu

te24

25 R

idge

cres

t Driv

e, S

E

Alb

uque

rque

, NM

871

08

04/2

6/11

04/2

7/11

04/2

8/11

05/0

2/11

Ship

ped

:R

ecei

ved:

Prin

ted:

Sam

pled

:

Uni

t Typ

e : E

ngin

e, D

iese

l (G

N_D

E001

)

ID: F

Y09-

111-

26A

PR11

-OIL

- FY

09-1

11-2

6APR

11-O

IL, D

iese

l Eng

ine * =

exce

eds

Cau

tion

limit

** =

exc

eeds

Ala

rm li

mit

101

Cor

pora

te P

lace

, Val

lejo

, CA

9459

0w

ww

.her

guth

.com

ISO

900

1:20

08 a

nd IS

O/IE

C 1

7025

:200

5 C

ertif

ied

Lab

Num

ber

Sam

ple

Dat

eM

inim

umM

axim

umV1

1093

4504

/26/

11

Com

para

tive

Gra

phic

Ana

lysi

s

Silic

on

Lead

Cop

per

Chr

omiu

m

Alum

inumIro

n

Sulfi

natio

n

Oxi

datio

n

Soot

TBN

Vis

@ 1

00 D

eg C

Und

er M

in

War

ning

Typ

ical

Typ

ical

War

ning

Ove

r Max

Uni

t Tim

e (H

R)

Flui

d Ti

me

(HR

)Vi

s @

100

Deg

CTB

N m

g K

OH

/gFT

IR Soot

% w

t.O

xida

tion

Abs/

cmW

ater

FTI

R %

Vol

Sulfi

natio

n Ab

s/Fu

el %

Vol

Gly

col %

Vol

Met

als

Iron

ppm

Alum

inum

ppm

Chr

omiu

m p

pmC

oppe

r ppm

Lead

ppm

Tin

ppm

Nic

kel p

pmSi

lver

ppm

Antim

ony

ppm

Silic

on p

pmSo

dium

ppm

Boro

n pp

mZi

nc p

pmPh

osph

orus

ppm

Cal

cium

ppm

Mag

nesi

um p

pmBa

rium

ppm

Mol

ybde

num

ppm

Pota

ssiu

m p

pm

12.0

02.

0016

.80

3.0 30

0.20 30 5.0

0.20 59 4 4 7 4 4 44.

5 20

6191 0

15.3

4*4

.52

____

____

__**

3.3 15

<0.1

0 19<2

.0<0

.10

____

____

__ 31 2 1 1 1 <1 <1<0

.1 <1 2 <2 <110

24 894

2082 6 <1 <1 <3

Cod

e :L

OVE

MC

Lov

elac

e R

espi

rato

ry R

esea

rch

Inst

itute

Pho

ne :(

505)

348

-960

0 F

ax :(

505)

348

-498

0Th

ese

resu

lts a

re s

ubm

itted

pur

suan

t to

our c

urre

nt T

erm

s, C

ondi

tions

and

Lim

itatio

ns a

nd L

abor

ator

y P

ricin

g P

olic

y. N

o re

spon

sibi

lity

or li

abili

ty is

ass

umed

for t

he m

anne

r in

whi

ch th

ese

resu

lts a

re u

sed

or in

terp

rete

d.

Eval

uate

d B

y: D

avid

F. F

ryck

i, C

LS -

For

que

stio

ns a

bout

this

repo

rt, p

leas

e ca

ll 88

8-43

7-48

84.

erla

bgt1

.frx

Rev

. 06/

21/2

010


136

Oil

Type

: SA

E 40

(GN

_032

)

P.O

. : J

K110

737

Lab

Num

ber :

V11

1273

9

05/2

4/11

Page

1

17:0

9:56

AB

NO

RM

AL:

Abn

orm

al re

sults

for f

luid

are

pre

sent

. E

quip

men

t app

ears

sat

isfa

ctor

y.S

oot c

onte

nt is

hig

h. D

rain

oil

and

chan

ge fi

lter(s

). C

heck

for p

rope

r com

bust

ion

prop

ertie

s(e

xhau

st b

ack

pres

sure

, ope

ratin

g te

mpe

ratu

res,

wor

n/br

oken

ring

s, e

xces

sive

idlin

g, h

ung

valv

es,

impr

oper

fuel

set

tings

, air

inta

ke re

stric

tions

). A

dditi

onal

sam

ple

is n

eede

d to

hel

p es

tabl

ish

trend

.R

esam

ple

at h

alf n

orm

al in

terv

al.

Tom

Hol

mes

Love

lace

Res

pira

tory

Res

earc

h In

stitu

te24

25 R

idge

cres

t Driv

e, S

E

Alb

uque

rque

, NM

871

08

05/1

8/11

05/1

9/11

05/2

0/11

05/2

4/11

Ship

ped

:R

ecei

ved:

Prin

ted:

Sam

pled

:

Uni

t Typ

e : E

ngin

e, D

iese

l (G

N_D

E001

)

* =

exce

eds

Cau

tion

limit

** =

exc

eeds

Ala

rm li

mit

101

Cor

pora

te P

lace

, Val

lejo

, CA

9459

0w

ww

.her

guth

.com

ISO

900

1:20

08 a

nd IS

O/IE

C 1

7025

:200

5 C

ertif

ied

ID: F

Y09-

111-

18M

AY1

1-O

IL -

FY09

-111

-18M

AR

11-O

IL, D

iese

l Eng

ine

Lab

Num

ber

Sam

ple

Dat

eM

inim

umM

axim

umV1

1127

3905

/18/

11

Com

para

tive

Gra

phic

Ana

lysi

s

Silic

on

Lead

Cop

per

Chr

omiu

m

Alum

inumIro

n

Sulfi

natio

n

Oxi

datio

n

Soot

TBN

Vis

@ 1

00 D

eg C

Und

er M

in

War

ning

Typ

ical

Typ

ical

War

ning

Ove

r Max

Uni

t Tim

e (H

R)

Flui

d Ti

me

(HR

)Vi

s @

100

Deg

CTB

N m

g K

OH

/gFT

IR Soot

% w

t.O

xida

tion

Abs/

cmW

ater

FTI

R %

Vol

Sulfi

natio

n Ab

s/Fu

el %

Vol

Gly

col %

Vol

Met

als

Iron

ppm

Alum

inum

ppm

Chr

omiu

m p

pmC

oppe

r ppm

Lead

ppm

Tin

ppm

Nic

kel p

pmSi

lver

ppm

Antim

ony

ppm

Silic

on p

pmSo

dium

ppm

Boro

n pp

mZi

nc p

pmPh

osph

orus

ppm

Cal

cium

ppm

Mag

nesi

um p

pmBa

rium

ppm

Mol

ybde

num

ppm

Pota

ssiu

m p

pm

12.0

02.

0016

.80

3.0 30

0.20 30 5.0

0.20 58 4 4 7 4 4 44.

5 20

6438 0

15.2

44.

37__

____

____

**3.

1 14<0

.10 19

<2.0

<0.1

0__

____

____ 21 1 1 1 1 <1 <1

<0.1 <1 1 5 <1 827

705

1622 4 <1 <1 <3

Cod

e :L

OVE

MC

Lov

elac

e R

espi

rato

ry R

esea

rch

Inst

itute

Pho

ne :(

505)

348

-960

0 F

ax :(

505)

348

-498

0Th

ese

resu

lts a

re s

ubm

itted

pur

suan

t to

our c

urre

nt T

erm

s, C

ondi

tions

and

Lim

itatio

ns a

nd L

abor

ator

y P

ricin

g P

olic

y. N

o re

spon

sibi

lity

or li

abili

ty is

ass

umed

for t

he m

anne

r in

whi

ch th

ese

resu

lts a

re u

sed

or in

terp

rete

d.

Eval

uate

d B

y: B

obby

R L

icu,

Sen

ior E

valu

ator

- F

or q

uest

ions

abo

ut th

is re

port

, ple

ase

call

888-

437-

4884

.er

labg

t1.fr

x R

ev. 0

5/19

/11


137

Oil

Type

: SA

E 15

W-4

0 (G

N_0

45)

P.

O. :

JK1

1073

7

Lab

Num

ber :

V11

1619

3

06/2

1/11

Page

1

09:0

8:18

AB

NO

RM

AL:

Abn

orm

al re

sults

for f

luid

are

pre

sent

. E

quip

men

t app

ears

sat

isfa

ctor

y.So

ot c

onte

nt is

hig

h. L

evel

s m

ay b

e du

e to

oil

serv

ice

time

(not

pro

vide

d).

Dra

in o

il an

d ch

ange

filte

r(s).

Add

ition

al s

ampl

e is

nee

ded

to h

elp

esta

blis

h tre

nd.

Res

ampl

e at

hal

f nor

mal

inte

rval

.Pl

ease

pro

vide

equ

ipm

ent m

ake

and

mod

el a

s w

ell a

s th

e fu

ll na

me

and

grad

e of

the

lubr

ican

t in

serv

ice.

Tom

Hol

mes

Love

lace

Res

pira

tory

Res

earc

h In

stitu

te24

25 R

idge

cres

t Driv

e, S

E

Alb

uque

rque

, NM

871

08

06/0

9/11

06/1

3/11

06/1

4/11

06/2

1/11

Ship

ped

:R

ecei

ved:

Prin

ted:

Sam

pled

:

Uni

t Typ

e : E

ngin

e, D

iese

l (G

N_D

E001

)

* =

exce

eds

Cau

tion

limit

** =

exc

eeds

Ala

rm li

mit

101

Cor

pora

te P

lace

, Val

lejo

, CA

9459

0w

ww

.her

guth

.com

ISO

900

1:20

08 a

nd IS

O/IE

C 1

7025

:200

5 C

ertif

ied

ID: F

Y09-

111-

09JU

N11

-OIL

- FY

09-1

11-0

9JU

N11

-OIL

, Die

sel E

ngin

e

Lab

Num

ber

Sam

ple

Dat

eM

inim

umM

axim

umV1

1161

9306

/09/

11

Com

para

tive

Gra

phic

Ana

lysi

s

Sodi

um

Silic

on

Lead

Cop

per

Chr

omiu

m

Alum

inumIro

n

Sulfi

natio

n

Oxi

datio

n

Soot

TBN

Vis

@ 1

00 D

eg C

Und

er M

in

War

ning

Typ

ical

Typ

ical

War

ning

Ove

r Max

Uni

t Tim

e (H

R)

Flui

d Ti

me

(HR

)Vi

s @

100

Deg

CTB

N m

g K

OH

/gFT

IR Soot

% w

t.O

xida

tion

Abs/

cmW

ater

FTI

R %

Vol

Sulfi

natio

n Ab

s/Fu

el %

Vol

Gly

col %

Vol

Met

als

Iron

ppm

Alum

inum

ppm

Chr

omiu

m p

pmC

oppe

r ppm

Lead

ppm

Tin

ppm

Nic

kel p

pmSi

lver

ppm

Antim

ony

ppm

Silic

on p

pmSo

dium

ppm

Boro

n pp

mZi

nc p

pmPh

osph

orus

ppm

Cal

cium

ppm

Mag

nesi

um p

pmBa

rium

ppm

Mol

ybde

num

ppm

Pota

ssiu

m p

pm

12.0

03.

0016

.80

3.0 30

0.20 30 5.0

0.20 89 7 4 24 15 4 43.

1 20 50 50

6694 0

15.2

05.

37__

____

____

**3.

3 16<0

.10 19

<2.0

<0.1

0__

____

____ 30 2 1 1 2 <1 <1

<0.1 <1 2 2 <1

1119

1045

2332 11 <1 <1 <3

Cod

e :L

OVE

MC

Lov

elac

e R

espi

rato

ry R

esea

rch

Inst

itute

Pho

ne :(

505)

348

-960

0 F

ax :(

505)

348

-498

0Th

ese

resu

lts a

re s

ubm

itted

pur

suan

t to

our c

urre

nt T

erm

s, C

ondi

tions

and

Lim

itatio

ns a

nd L

abor

ator

y P

ricin

g P

olic

y. N

o re

spon

sibi

lity

or li

abili

ty is

ass

umed

for t

he m

anne

r in

whi

ch th

ese

resu

lts a

re u

sed

or in

terp

rete

d.

Eval

uate

d B

y: D

avid

F. F

ryck

i, C

LS -

For

que

stio

ns a

bout

this

repo

rt, p

leas

e ca

ll 88

8-43

7-48

84.

erla

bgt1

.frx

Rev

. 05/

19/1

1


138

Oil

Type

: SA

E 15

W-4

0 (G

N_0

45)

P.

O. :

JK1

1073

7

Lab

Num

ber :

V11

2080

4

07/1

4/11

Page

1

15:0

3:16

AB

NO

RM

AL:

Abn

orm

al re

sults

for f

luid

are

pre

sent

. E

quip

men

t app

ears

sat

isfa

ctor

y.Th

e To

tal B

ase

Num

ber (

rese

rve

alka

linity

) is

appr

oach

ing

min

imum

acc

epta

ble

leve

l. S

oot c

onte

ntis

hig

h. D

rain

oil

and

chan

ge fi

lter(s

). C

heck

for p

rope

r com

bust

ion

prop

ertie

s (e

xhau

st b

ack

pres

sure

, ope

ratin

g te

mpe

ratu

res,

wor

n/br

oken

ring

s, e

xces

sive

idlin

g, h

ung

valv

es, i

mpr

oper

fuel

setti

ngs,

air

inta

ke re

stric

tions

). A

dditi

onal

sam

ple

is n

eede

d to

hel

p es

tabl

ish

trend

. R

esam

ple

atha

lf no

rmal

inte

rval

. Pl

ease

pro

vide

equ

ipm

ent m

ake

and

mod

el a

s w

ell a

s th

e fu

ll na

me

and

grad

e

Tom

Hol

mes

Love

lace

Res

pira

tory

Res

earc

h In

stitu

te24

25 R

idge

cres

t Driv

e, S

E

Alb

uque

rque

, NM

871

08

07/0

4/11

07/1

1/11

07/1

2/11

07/1

4/11

Ship

ped

:R

ecei

ved:

Prin

ted:

Sam

pled

:

Uni

t Typ

e : E

ngin

e, D

iese

l (G

N_D

E001

)

* =

exce

eds

Cau

tion

limit

** =

exc

eeds

Ala

rm li

mit

101

Cor

pora

te P

lace

, Val

lejo

, CA

9459

0w

ww

.her

guth

.com

ISO

900

1:20

08 a

nd IS

O/IE

C 1

7025

:200

5 C

ertif

ied

ID: F

Y09-

111-

04JU

L11-

OIL

- FY

09-1

11-0

4JU

L11-

OIL

, Die

sel E

ngin

e

Lab

Num

ber

Sam

ple

Dat

eM

inim

umM

axim

umV1

1208

0407

/04/

11

Com

para

tive

Gra

phic

Ana

lysi

s

Silic

on

Lead

Cop

per

Chr

omiu

m

Alum

inumIro

n

Sulfi

natio

n

Oxi

datio

n

Soot

TBN

Vis

@ 1

00 D

eg C

Und

er M

in

War

ning

Typ

ical

Typ

ical

War

ning

Ove

r Max

Uni

t Tim

e (H

R)

Flui

d Ti

me

(HR

)Vi

s @

100

Deg

CTB

N m

g K

OH

/gFT

IR Soot

% w

t.O

xida

tion

Abs/

cmW

ater

FTI

R %

Vol

Sulfi

natio

n Ab

s/Fu

el %

Vol

Gly

col %

Vol

Met

als

Iron

ppm

Alum

inum

ppm

Chr

omiu

m p

pmC

oppe

r ppm

Lead

ppm

Tin

ppm

Nic

kel p

pmSi

lver

ppm

Antim

ony

ppm

Silic

on p

pmSo

dium

ppm

Boro

n pp

mZi

nc p

pmPh

osph

orus

ppm

Cal

cium

ppm

Mag

nesi

um p

pmBa

rium

ppm

Mol

ybde

num

ppm

Pota

ssiu

m p

pm

12.0

03.

0016

.80

3.0 30

0.20 30 5.0

0.20 89 7 4 24 15 4 43.

1 20 50 50

6966 0

15.2

9*3

.75

____

____

__**

3.4 5

<0.1

0 8<2

.0<0

.10

____

____

__ 33 2 1 1 2 <1 <1<0

.1 <1 2 <2 113

1210

2925

72 6 <1 <1 <3

Cod

e :L

OVE

MC

Lov

elac

e R

espi

rato

ry R

esea

rch

Inst

itute

Pho

ne :(

505)

348

-960

0 F

ax :(

505)

348

-498

0Th

ese

resu

lts a

re s

ubm

itted

pur

suan

t to

our c

urre

nt T

erm

s, C

ondi

tions

and

Lim

itatio

ns a

nd L

abor

ator

y P

ricin

g P

olic

y. N

o re

spon

sibi

lity

or li

abili

ty is

ass

umed

for t

he m

anne

r in

whi

ch th

ese

resu

lts a

re u

sed

or in

terp

rete

d.

Eval

uate

d B

y: D

avid

F. F

ryck

i, C

LS -

For

que

stio

ns a

bout

this

repo

rt, p

leas

e ca

ll 88

8-43

7-48

84.

erla

bgt1

.frx

Rev

. 05/

19/1

1


139

Oil

Type

: SA

E 40

(GN

_032

)

P.O

. : J

K110

737

Lab

Num

ber :

V11

3289

9

10/0

4/11

Page

1

13:0

2:17

AB

NO

RM

AL:

Abn

orm

al re

sults

for f

luid

are

pre

sent

. E

quip

men

t app

ears

sat

isfa

ctor

y.So

ot c

onte

nt is

hig

h. P

leas

e pr

ovid

e eq

uipm

ent m

ake

and

mod

el a

s w

ell a

s th

e fu

ll na

me

and

grad

e of

the

lubr

ican

t in

serv

ice.

Dra

in o

il an

d ch

ange

filte

r(s).

Che

ck fo

r pro

per c

ombu

stio

npr

oper

ties

(exh

aust

bac

k pr

essu

re, o

pera

ting

tem

pera

ture

s, w

orn/

brok

en ri

ngs,

exc

essi

ve id

ling,

hung

val

ves,

impr

oper

fuel

set

tings

, air

inta

ke re

stric

tions

). R

esam

ple

at h

alf n

orm

al in

terv

al.

Tom

Hol

mes

Love

lace

Res

pira

tory

Res

earc

h In

stitu

te24

25 R

idge

cres

t Driv

e, S

E

Alb

uque

rque

, NM

871

08

07/2

1/11

09/2

9/11

09/3

0/11

10/0

4/11

Ship

ped

:R

ecei

ved:

Prin

ted:

Sam

pled

:

Uni

t Typ

e : E

ngin

e, D

iese

l (G

N_D

E001

)

* =

exce

eds

Cau

tion

limit

** =

exc

eeds

Ala

rm li

mit

101

Cor

pora

te P

lace

, Val

lejo

, CA

9459

0w

ww

.her

guth

.com

ISO

900

1:20

08 a

nd IS

O/IE

C 1

7025

:200

5 C

ertif

ied

ID: F

Y09-

111-

21JU

L11-

OIL

- FY

09-1

11-2

1Jul

11-O

il, D

iese

l Eng

ine

Lab

Num

ber

Sam

ple

Dat

eM

inim

umM

axim

umV1

1328

9907

/21/

11

Com

para

tive

Gra

phic

Ana

lysi

s

Sodi

um

Silic

on

Lead

Cop

per

Chr

omiu

m

Alum

inumIro

n

Sulfi

natio

n

Oxi

datio

n

Soot

TBN

Vis

@ 1

00 D

eg C

Und

er M

in

War

ning

Typ

ical

Typ

ical

War

ning

Ove

r Max

Uni

t Tim

e (H

R)

Flui

d Ti

me

(HR

)Vi

s @

100

Deg

CTB

N m

g K

OH

/gFT

IR Soot

% w

t.O

xida

tion

Abs/

cmW

ater

FTI

R %

Vol

Sulfi

natio

n Ab

s/Fu

el %

Vol

Gly

col %

Vol

Met

als

Iron

ppm

Alum

inum

ppm

Chr

omiu

m p

pmC

oppe

r ppm

Lead

ppm

Tin

ppm

Nic

kel p

pmSi

lver

ppm

Antim

ony

ppm

Silic

on p

pmSo

dium

ppm

Boro

n pp

mZi

nc p

pmPh

osph

orus

ppm

Cal

cium

ppm

Mag

nesi

um p

pmBa

rium

ppm

Mol

ybde

num

ppm

Pota

ssiu

m p

pm

12.0

03.

0016

.80

3.0 30

0.20 30 5.0

0.20 60 4 4 7 4 4 44.

5 20 50 50

7191 0

15.2

65.

65__

____

____

**3.

2 6<0

.10 13

<2.0

<0.1

0__

____

____ 28 2 1 1 1 <1 <1

<0.1 <1 2 3 1

1108

1001

2235 6 <1 <1 <3

Cod

e :L

OVE

MC

Lov

elac

e R

espi

rato

ry R

esea

rch

Inst

itute

Pho

ne :(

505)

348

-960

0 F

ax :(

505)

348

-498

0Th

ese

resu

lts a

re s

ubm

itted

pur

suan

t to

our c

urre

nt T

erm

s, C

ondi

tions

and

Lim

itatio

ns a

nd L

abor

ator

y P

ricin

g P

olic

y. N

o re

spon

sibi

lity

or li

abili

ty is

ass

umed

for t

he m

anne

r in

whi

ch th

ese

resu

lts a

re u

sed

or in

terp

rete

d.

Eval

uate

d B

y: B

obby

R L

icu,

Sen

ior E

valu

ator

- F

or q

uest

ions

abo

ut th

is re

port

, ple

ase

call

888-

437-

4884

.er

labg

t1.fr

x R

ev. 0

5/19

/11


140

Oil

Type

: SA

E 40

(GN

_032

)

P.O

. : J

K110

737

Lab

Num

ber :

V11

2561

8

08/1

8/11

Page

1

13:0

2:11

AB

NO

RM

AL:

Abn

orm

al re

sults

for f

luid

are

pre

sent

. E

quip

men

t app

ears

sat

isfa

ctor

y.So

ot c

onte

nt is

hig

h. F

TIR

indi

cate

s oi

l is

sulfi

nate

d. D

rain

oil

and

chan

ge fi

lter(s

). C

heck

for

prop

er c

ombu

stio

n pr

oper

ties

(exh

aust

bac

k pr

essu

re, o

pera

ting

tem

pera

ture

s, w

orn/

brok

en ri

ngs,

exce

ssiv

e id

ling,

hun

g va

lves

, im

prop

er fu

el s

ettin

gs, a

ir in

take

rest

rictio

ns).

Add

ition

al s

ampl

e is

need

ed to

hel

p es

tabl

ish

trend

. R

esam

ple

at h

alf n

orm

al in

terv

al.

Tom

Hol

mes

Love

lace

Res

pira

tory

Res

earc

h In

stitu

te24

25 R

idge

cres

t Driv

e, S

E

Alb

uque

rque

, NM

871

08

08/1

4/11

08/1

5/11

08/1

6/11

08/1

8/11

Ship

ped

:R

ecei

ved:

Prin

ted:

Sam

pled

:

Uni

t Typ

e : E

ngin

e, D

iese

l (G

N_D

E001

)

* =

exce

eds

Cau

tion

limit

** =

exc

eeds

Ala

rm li

mit

101

Cor

pora

te P

lace

, Val

lejo

, CA

9459

0w

ww

.her

guth

.com

ISO

900

1:20

08 a

nd IS

O/IE

C 1

7025

:200

5 C

ertif

ied

ID: F

Y09-

111-

14A

UG

11-O

IL -

FY09

-111

-14a

ug11

, Die

sel E

ngin

e

Lab

Num

ber

Sam

ple

Dat

eM

inim

umM

axim

umV1

1256

1808

/14/

11

Com

para

tive

Gra

phic

Ana

lysi

s

Sodi

um

Silic

on

Lead

Cop

per

Chr

omiu

m

Alum

inumIro

n

Sulfi

natio

n

Oxi

datio

n

Soot

TBN

Vis

@ 1

00 D

eg C

Und

er M

in

War

ning

Typ

ical

Typ

ical

War

ning

Ove

r Max

Uni

t Tim

e (H

R)

Flui

d Ti

me

(HR

)Vi

s @

100

Deg

CTB

N m

g K

OH

/gFT

IR Soot

% w

t.O

xida

tion

Abs/

cmW

ater

FTI

R %

Vol

Sulfi

natio

n Ab

s/Fu

el %

Vol

Gly

col %

Vol

Met

als

Iron

ppm

Alum

inum

ppm

Chr

omiu

m p

pmC

oppe

r ppm

Lead

ppm

Tin

ppm

Nic

kel p

pmSi

lver

ppm

Antim

ony

ppm

Silic

on p

pmSo

dium

ppm

Boro

n pp

mZi

nc p

pmPh

osph

orus

ppm

Cal

cium

ppm

Mag

nesi

um p

pmBa

rium

ppm

Mol

ybde

num

ppm

Pota

ssiu

m p

pm

12.0

03.

0016

.80

3.0 30

0.20 30 5.0

0.20 61 4 4 7 4 4 44.

5 20 50 50

7445 0

15.2

15.

45__

____

____

**3.

5 15<0

.10

*30

<2.0

<0.1

0__

____

____ 34 2 1 2 2 <1 <1

<0.1 <1 2 5 <1

1236

1115

2497 10 <1 <1 <3

Cod

e :L

OVE

MC

Lov

elac

e R

espi

rato

ry R

esea

rch

Inst

itute

Pho

ne :(

505)

348

-960

0 F

ax :(

505)

348

-498

0Th

ese

resu

lts a

re s

ubm

itted

pur

suan

t to

our c

urre

nt T

erm

s, C

ondi

tions

and

Lim

itatio

ns a

nd L

abor

ator

y P

ricin

g P

olic

y. N

o re

spon

sibi

lity

or li

abili

ty is

ass

umed

for t

he m

anne

r in

whi

ch th

ese

resu

lts a

re u

sed

or in

terp

rete

d.

Eval

uate

d B

y: B

obby

R L

icu,

Sen

ior E

valu

ator

- F

or q

uest

ions

abo

ut th

is re

port

, ple

ase

call

888-

437-

4884

.er

labg

t1.fr

x R

ev. 0

5/19

/11


141

Oil

Type

: SA

E 15

W-4

0 (G

N_0

45)

P.

O. :

JK1

1073

7

Lab

Num

ber :

V11

2968

2

09/1

5/11

Page

1

16:1

9:59

AB

NO

RM

AL:

Abn

orm

al re

sults

for f

luid

are

pre

sent

. E

quip

men

t app

ears

sat

isfa

ctor

y.So

ot c

onte

nt is

hig

h. L

evel

s m

ay b

e du

e to

oil

serv

ice

time

(not

pro

vide

d).

Dra

in o

il an

d ch

ange

filte

r(s).

Add

ition

al s

ampl

e is

nee

ded

to h

elp

esta

blis

h tre

nd.

Res

ampl

e at

hal

f nor

mal

inte

rval

.Pl

ease

pro

vide

equ

ipm

ent m

ake

and

mod

el a

s w

ell a

s th

e fu

ll na

me

and

grad

e of

the

lubr

ican

t in

serv

ice.

Tom

Hol

mes

Love

lace

Res

pira

tory

Res

earc

h In

stitu

te24

25 R

idge

cres

t Driv

e, S

E

Alb

uque

rque

, NM

871

08

09/0

7/11

09/1

2/11

09/1

3/11

09/1

5/11

Ship

ped

:R

ecei

ved:

Prin

ted:

Sam

pled

:

Uni

t Typ

e : E

ngin

e, D

iese

l (G

N_D

E001

)

* =

exce

eds

Cau

tion

limit

** =

exc

eeds

Ala

rm li

mit

101

Cor

pora

te P

lace

, Val

lejo

, CA

9459

0w

ww

.her

guth

.com

ISO

900

1:20

08 a

nd IS

O/IE

C 1

7025

:200

5 C

ertif

ied

ID: F

Y09-

111-

07SE

P11-

OIL

- FY

09-1

11-0

7SEP

11-O

IL, D

iese

l Eng

ine

Lab

Num

ber

Sam

ple

Dat

eM

inim

umM

axim

umV1

1296

8209

/07/

11

Com

para

tive

Gra

phic

Ana

lysi

s

Sodi

um

Silic

onTin

Lead

Cop

per

Chr

omiu

m

Alum

inumIro

n

Sulfi

natio

n

Oxi

datio

n

Soot

TBN

Und

er M

in

War

ning

Typ

ical

Typ

ical

War

ning

Ove

r Max

Uni

t Tim

e (H

R)

Flui

d Ti

me

(HR

)Vi

s @

100

Deg

CTB

N m

g K

OH

/gFT

IR Soot

% w

t.O

xida

tion

Abs/

cmW

ater

FTI

R %

Vol

Sulfi

natio

n Ab

s/Fu

el %

Vol

Gly

col %

Vol

Met

als

Iron

ppm

Alum

inum

ppm

Chr

omiu

m p

pmC

oppe

r ppm

Lead

ppm

Tin

ppm

Nic

kel p

pmSi

lver

ppm

Antim

ony

ppm

Silic

on p

pmSo

dium

ppm

Boro

n pp

mZi

nc p

pmPh

osph

orus

ppm

Cal

cium

ppm

Mag

nesi

um p

pmBa

rium

ppm

Mol

ybde

num

ppm

Pota

ssiu

m p

pm

12.0

03.

0016

.80

3.0 30

0.20 30 5.0

0.20 39 4 4 7 4 4 44.

5 20 50 50

0 015

.04

5.43

____

____

__*3

.0 7<0

.10 13

<2.0

<0.1

0__

____

____ 31 2 1 1 2 1 <1

<0.1 <1 2 3 3

1322

1122

2557 9 <1 1 <3

Cod

e :L

OVE

MC

Lov

elac

e R

espi

rato

ry R

esea

rch

Inst

itute

Pho

ne :(

505)

348

-960

0 F

ax :(

505)

348

-498

0Th

ese

resu

lts a

re s

ubm

itted

pur

suan

t to

our c

urre

nt T

erm

s, C

ondi

tions

and

Lim

itatio

ns a

nd L

abor

ator

y P

ricin

g P

olic

y. N

o re

spon

sibi

lity

or li

abili

ty is

ass

umed

for t

he m

anne

r in

whi

ch th

ese

resu

lts a

re u

sed

or in

terp

rete

d.

Eval

uate

d B

y: D

avid

F. F

ryck

i, C

LS -

For

que

stio

ns a

bout

this

repo

rt, p

leas

e ca

ll 88

8-43

7-48

84.

erla

bgt1

.frx

Rev

. 05/

19/1

1


142

Oil

Type

: SA

E 40

(GN

_032

)

P.O

. : J

K110

737

Lab

Num

ber :

V11

3289

8

10/0

4/11

Page

1

13:0

2:14

AB

NO

RM

AL:

Abn

orm

al re

sults

for f

luid

are

pre

sent

. E

quip

men

t app

ears

sat

isfa

ctor

y.So

ot c

onte

nt is

hig

h. G

lyco

l and

sod

ium

indi

cate

coo

lant

inhi

bito

rs; c

heck

for s

ourc

e. D

rain

oil

and

chan

ge fi

lter(

s).

Che

ck fo

r pro

per c

ombu

stio

n pr

oper

ties

(exh

aust

bac

k pr

essu

re, o

pera

ting

tem

pera

ture

s, w

orn/

brok

en ri

ngs,

exc

essi

ve id

ling,

hun

g va

lves

, im

prop

er fu

el s

ettin

gs, a

ir in

take

rest

rictio

ns).

Mon

itor c

oolin

g sy

stem

for l

evel

cha

nges

and

/or a

dditi

ons.

Res

ampl

e at

hal

f nor

mal

inte

rval

.

Tom

Hol

mes

Love

lace

Res

pira

tory

Res

earc

h In

stitu

te24

25 R

idge

cres

t Driv

e, S

E

Alb

uque

rque

, NM

871

08

09/2

6/11

09/2

9/11

09/3

0/11

10/0

4/11

Ship

ped

:R

ecei

ved:

Prin

ted:

Sam

pled

:

Uni

t Typ

e : E

ngin

e, D

iese

l (G

N_D

E001

)

* =

exce

eds

Cau

tion

limit

** =

exc

eeds

Ala

rm li

mit

101

Cor

pora

te P

lace

, Val

lejo

, CA

9459

0w

ww

.her

guth

.com

ISO

900

1:20

08 a

nd IS

O/IE

C 1

7025

:200

5 C

ertif

ied

ID: F

Y09-

111-

26SE

P11-

OIL

- FY

09-1

11-2

6Sep

11-O

il, D

iese

l Eng

ine

Lab

Num

ber

Sam

ple

Dat

eM

inim

umM

axim

umV1

1328

9809

/26/

11

Com

para

tive

Gra

phic

Ana

lysi

s

Sodi

um

Silic

on

Lead

Cop

per

Chr

omiu

m

Alum

inumIro

n

Gly

col

Sulfi

natio

n

Oxi

datio

n

Soot

TBN

Und

er M

in

War

ning

Typ

ical

Typ

ical

War

ning

Ove

r Max

Uni

t Tim

e (H

R)

Flui

d Ti

me

(HR

)Vi

s @

100

Deg

CTB

N m

g K

OH

/gFT

IR Soot

% w

t.O

xida

tion

Abs/

cmW

ater

FTI

R %

Vol

Sulfi

natio

n Ab

s/Fu

el %

Vol

Gly

col %

Vol

Met

als

Iron

ppm

Alum

inum

ppm

Chr

omiu

m p

pmC

oppe

r ppm

Lead

ppm

Tin

ppm

Nic

kel p

pmSi

lver

ppm

Antim

ony

ppm

Silic

on p

pmSo

dium

ppm

Boro

n pp

mZi

nc p

pmPh

osph

orus

ppm

Cal

cium

ppm

Mag

nesi

um p

pmBa

rium

ppm

Mol

ybde

num

ppm

Pota

ssiu

m p

pm

12.0

03.

0016

.80

3.0 30

0.20 30 5.0

0.20 60 4 4 7 4 4 44.

5 20 50 50

7937 0

14.9

05.

53__

____

____

**3.

2 7<0

.10 14

<2.0

**0.

42__

____

____ 33 2 1 1 2 <1 <1

<0.1 1 5

**15

0 12 969

875

1982 8 <1 <1 <3

Cod

e :L

OVE

MC

Lov

elac

e R

espi

rato

ry R

esea

rch

Inst

itute

Pho

ne :(

505)

348

-960

0 F

ax :(

505)

348

-498

0Th

ese

resu

lts a

re s

ubm

itted

pur

suan

t to

our c

urre

nt T

erm

s, C

ondi

tions

and

Lim

itatio

ns a

nd L

abor

ator

y P

ricin

g P

olic

y. N

o re

spon

sibi

lity

or li

abili

ty is

ass

umed

for t

he m

anne

r in

whi

ch th

ese

resu

lts a

re u

sed

or in

terp

rete

d.

Eval

uate

d B

y: B

obby

R L

icu,

Sen

ior E

valu

ator

- F

or q

uest

ions

abo

ut th

is re

port

, ple

ase

call

888-

437-

4884

.er

labg

t1.fr

x R

ev. 0

5/19

/11


143

Oil

Type

: SA

E 40

(GN

_032

)

P.O

. : J

K110

737

Lab

Num

ber :

V11

3770

0

11/0

1/11

Page

1

17:0

5:20

NO

RM

AL:

Sam

ple

data

is s

atis

fact

ory.

No

actio

n is

requ

ired

at th

is ti

me.

Addi

tiona

l sam

ple

is n

eede

d to

hel

p es

tabl

ish

trend

. R

esam

ple

at h

alf n

orm

al in

terv

al.

Plea

sepr

ovid

e eq

uipm

ent m

ake

and

mod

el a

s w

ell a

s th

e fu

ll na

me

and

grad

e of

the

lubr

ican

t in

serv

ice.

Tom

Hol

mes

Love

lace

Res

pira

tory

Res

earc

h In

stitu

te24

25 R

idge

cres

t Driv

e, S

E

Alb

uque

rque

, NM

871

08

10/2

0/11

10/2

7/11

10/2

8/11

11/0

1/11

Ship

ped

:R

ecei

ved:

Prin

ted:

Sam

pled

:

Uni

t Typ

e : E

ngin

e, D

iese

l (G

N_D

E001

)

* =

exce

eds

Cau

tion

limit

** =

exc

eeds

Ala

rm li

mit

101

Cor

pora

te P

lace

, Val

lejo

, CA

9459

0w

ww

.her

guth

.com

ISO

900

1:20

08 a

nd IS

O/IE

C 1

7025

:200

5 C

ertif

ied

ID: F

Y09-

111-

20O

CT1

1-O

IL -

FY09

-111

-20O

CT1

1-O

IL, D

iese

l Eng

ine

Lab

Num

ber

Sam

ple

Dat

eM

inim

umM

axim

umV1

1377

0010

/20/

11

Com

para

tive

Gra

phic

Ana

lysi

s

Silic

onTin

Lead

Cop

per

Chr

omiu

m

Alum

inumIro

n

Sulfi

natio

n

Oxi

datio

n

Soot

TBN

Vis

@10

0 D

eg C

Und

er M

in

War

ning

Typ

ical

Typ

ical

War

ning

Ove

r Max

Uni

t Tim

e (H

R)

Flui

d Ti

me

(HR

)Vi

s @

100

Deg

CTB

N m

g K

OH

/gFT

IR Soot

% w

t.O

xida

tion

Abs/

cmW

ater

FTI

R %

Vol

Sulfi

natio

n Ab

s/Fu

el %

Vol

Gly

col %

Vol

Met

als

Iron

ppm

Alum

inum

ppm

Chr

omiu

m p

pmC

oppe

r ppm

Lead

ppm

Tin

ppm

Nic

kel p

pmSi

lver

ppm

Antim

ony

ppm

Silic

on p

pmSo

dium

ppm

Boro

n pp

mZi

nc p

pmPh

osph

orus

ppm

Cal

cium

ppm

Mag

nesi

um p

pmBa

rium

ppm

Mol

ybde

num

ppm

Pota

ssiu

m p

pm

12.0

02.

0016

.80

3.0 30

0.20 30 5.0

0.20 99 16 4 36 50 4 43.

1 20

1487 0

15.4

45.

11__

____

____ 2.6 7

<0.1

0 14<2

.0<0

.10

____

____

__ 46 2 1 2 1 1 <1<0

.1 <1 5 4 111

5010

6323

92 6 <1 <1 <3

Cod

e :L

OVE

MC

Lov

elac

e R

espi

rato

ry R

esea

rch

Inst

itute

Pho

ne :(

505)

348

-960

0 F

ax :(

505)

348

-498

0Th

ese

resu

lts a

re s

ubm

itted

pur

suan

t to

our c

urre

nt T

erm

s, C

ondi

tions

and

Lim

itatio

ns a

nd L

abor

ator

y P

ricin

g P

olic

y. N

o re

spon

sibi

lity

or li

abili

ty is

ass

umed

for t

he m

anne

r in

whi

ch th

ese

resu

lts a

re u

sed

or in

terp

rete

d.

Eval

uate

d B

y: B

obby

R L

icu,

Sen

ior E

valu

ator

- F

or q

uest

ions

abo

ut th

is re

port

, ple

ase

call

888-

437-

4884

.er

labg

t1.fr

x R

ev. 0

5/19

/11


144

Oil

Type

: SA

E 40

(GN

_032

)

P.O

. : J

K120

015

Lab

Num

ber :

V11

4020

5

11/1

5/11

Page

1

12:5

7:03

NO

RM

AL:

Sam

ple

data

is s

atis

fact

ory.

No

actio

n is

requ

ired

at th

is ti

me.

Plea

se p

rovi

de e

quip

men

t mak

e an

d m

odel

as

wel

l as

the

full

nam

e an

d gr

ade

of th

e lu

bric

ant i

nse

rvic

e. A

dditi

onal

sam

ple

is n

eede

d to

hel

p es

tabl

ish

trend

. R

esam

ple

at h

alf n

orm

al in

terv

al.

Tom

Hol

mes

Love

lace

Res

pira

tory

Res

earc

h In

stitu

te24

25 R

idge

cres

t Driv

e, S

E

Alb

uque

rque

, NM

871

08

11/0

9/11

11/1

0/11

11/1

1/11

11/1

5/11

Ship

ped

:R

ecei

ved:

Prin

ted:

Sam

pled

:

Uni

t Typ

e : E

ngin

e, D

iese

l (G

N_D

E001

)

* =

exce

eds

Cau

tion

limit

** =

exc

eeds

Ala

rm li

mit

101

Cor

pora

te P

lace

, Val

lejo

, CA

9459

0w

ww

.her

guth

.com

ISO

900

1:20

08 a

nd IS

O/IE

C 1

7025

:200

5 C

ertif

ied

ID: F

Y09-

111-

09N

OV1

1-O

IL -

FY09

-111

-09N

OV1

1-O

IL, D

iese

l Eng

ine

Lab

Num

ber

Sam

ple

Dat

eM

inim

umM

axim

umV1

1402

0511

/09/

11

Com

para

tive

Gra

phic

Ana

lysi

s

Sodi

um

Silic

onTin

Lead

Cop

per

Chr

omiu

m

Alum

inumIro

n

Sulfi

natio

n

Oxi

datio

n

Soot

TBN

Und

er M

in

War

ning

Typ

ical

Typ

ical

War

ning

Ove

r Max

Uni

t Tim

e (H

R)

Flui

d Ti

me

(HR

)Vi

s @

100

Deg

CTB

N m

g K

OH

/gFT

IR Soot

% w

t.O

xida

tion

Abs/

cmW

ater

FTI

R %

Vol

Sulfi

natio

n Ab

s/Fu

el %

Vol

Gly

col %

Vol

Met

als

Iron

ppm

Alum

inum

ppm

Chr

omiu

m p

pmC

oppe

r ppm

Lead

ppm

Tin

ppm

Nic

kel p

pmSi

lver

ppm

Antim

ony

ppm

Silic

on p

pmSo

dium

ppm

Boro

n pp

mZi

nc p

pmPh

osph

orus

ppm

Cal

cium

ppm

Mag

nesi

um p

pmBa

rium

ppm

Mol

ybde

num

ppm

Pota

ssiu

m p

pm

12.0

03.

0016

.80

3.0 30

0.20 30 5.0

0.20 59 4 4 7 4 4 44.

5 20 50 50

1697 0

15.2

35.

32__

____

____ 2.3 6

<0.1

0 12<2

.0<0

.10

____

____

__ 40 2 1 1 2 1 <1<0

.1 <1 3 3 <113

0111

0024

76 6 <1 1 <3

Cod

e :L

OVE

MC

Lov

elac

e R

espi

rato

ry R

esea

rch

Inst

itute

Pho

ne :(

505)

348

-960

0 F

ax :(

505)

348

-498

0Th

ese

resu

lts a

re s

ubm

itted

pur

suan

t to

our c

urre

nt T

erm

s, C

ondi

tions

and

Lim

itatio

ns a

nd L

abor

ator

y P

ricin

g P

olic

y. N

o re

spon

sibi

lity

or li

abili

ty is

ass

umed

for t

he m

anne

r in

whi

ch th

ese

resu

lts a

re u

sed

or in

terp

rete

d.

Eval

uate

d B

y: B

obby

R L

icu,

Sen

ior E

valu

ator

- F

or q

uest

ions

abo

ut th

is re

port

, ple

ase

call

888-

437-

4884

.er

labg

t1.fr

x R

ev. 0

5/19

/11


145

Oil

Type

: SA

E 40

(GN

_032

)

P.O

. : J

K110

737

Lab

Num

ber :

V11

4304

1

12/0

6/11

Page

1

12:5

0:52

MO

NIT

OR

: D

ata

for m

achi

ne a

nd/o

r flu

id c

ondi

tion

shou

ld b

e no

ted

and

mon

itore

d.So

ot c

onte

nt is

hig

h. L

evel

s m

ay b

e du

e to

oil

serv

ice

time

(not

pro

vide

d).

Dra

in o

il an

d ch

ange

filte

r(s).

Add

ition

al s

ampl

e is

nee

ded

to h

elp

esta

blis

h tre

nd.

Res

ampl

e at

hal

f nor

mal

inte

rval

.Pl

ease

pro

vide

equ

ipm

ent m

ake

and

mod

el a

s w

ell a

s th

e fu

ll na

me

and

grad

e of

the

lubr

ican

t in

serv

ice.

Tom

Hol

mes

Love

lace

Res

pira

tory

Res

earc

h In

stitu

te24

25 R

idge

cres

t Driv

e, S

E

Alb

uque

rque

, NM

871

08

12/0

1/11

12/0

1/11

12/0

2/11

12/0

6/11

Ship

ped

:R

ecei

ved:

Prin

ted:

Sam

pled

:

Uni

t Typ

e : E

ngin

e, D

iese

l (G

N_D

E001

)

* =

exce

eds

Cau

tion

limit

** =

exc

eeds

Ala

rm li

mit

101

Cor

pora

te P

lace

, Val

lejo

, CA

9459

0w

ww

.her

guth

.com

ISO

900

1:20

08 a

nd IS

O/IE

C 1

7025

:200

5 C

ertif

ied

ID: F

Y09-

111-

01D

EC11

-OIL

- FY

09-1

11-0

1dec

11-o

il, D

iese

l Eng

ine

Lab

Num

ber

Sam

ple

Dat

eM

inim

umM

axim

umV1

1430

4112

/01/

11

Com

para

tive

Gra

phic

Ana

lysi

s

Sodi

um

Silic

on

Silv

erTin

Lead

Cop

per

Chr

omiu

m

Alu

min

umIron

Sulfi

natio

n

Oxi

datio

n

Soot

Typi

cal

War

ning

O

ver

Max

Uni

t Tim

e (H

R)

Flui

d Ti

me

(HR

)Vi

s @

100

Deg

CTB

N m

g K

OH

/gFT

IR Soot

% w

t.O

xida

tion

Abs/

cmW

ater

FTI

R %

Vol

Sulfi

natio

n Ab

s/Fu

el %

Vol

Gly

col %

Vol

Met

als

Iron

ppm

Alum

inum

ppm

Chr

omiu

m p

pmC

oppe

r ppm

Lead

ppm

Tin

ppm

Nic

kel p

pmSi

lver

ppm

Antim

ony

ppm

Silic

on p

pmSo

dium

ppm

Boro

n pp

mZi

nc p

pmPh

osph

orus

ppm

Cal

cium

ppm

Mag

nesi

um p

pmBa

rium

ppm

Mol

ybde

num

ppm

Pota

ssiu

m p

pm

12.0

03.

0016

.80

3.0 30

0.20 30 5.0

0.20 59 4 4 7 4 4 44.

5 20 50 50

1949 0

15.4

54.

67__

____

____

*2.6 6

<0.1

0 13<2

.0<0

.10

____

____

__ 40 2 1 1 1 1 <1 0.1 <1 3 2 1

1115

1017

2253 6 <1 1 <3

Cod

e :L

OVE

MC

Lov

elac

e R

espi

rato

ry R

esea

rch

Inst

itute

Pho

ne :(

505)

348

-960

0 F

ax :(

505)

348

-498

0Th

ese

resu

lts a

re s

ubm

itted

pur

suan

t to

our c

urre

nt T

erm

s, C

ondi

tions

and

Lim

itatio

ns a

nd L

abor

ator

y P

ricin

g P

olic

y. N

o re

spon

sibi

lity

or li

abili

ty is

ass

umed

for t

he m

anne

r in

whi

ch th

ese

resu

lts a

re u

sed

or in

terp

rete

d.

Eval

uate

d B

y: D

avid

F. F

ryck

i, C

LS -

For

que

stio

ns a

bout

this

repo

rt, p

leas

e ca

ll 88

8-43

7-48

84.

erla

bgt1

.frx

Rev

. 05/

19/1

1


146

Oil

Type

: SA

E 40

(GN

_032

)

P.O

. : J

K110

737

Lab

Num

ber :

V11

4304

1

12/0

6/11

Page

1

12:5

0:52

MO

NIT

OR

: D

ata

for m

achi

ne a

nd/o

r flu

id c

ondi

tion

shou

ld b

e no

ted

and

mon

itore

d.So

ot c

onte

nt is

hig

h. L

evel

s m

ay b

e du

e to

oil

serv

ice

time

(not

pro

vide

d).

Dra

in o

il an

d ch

ange

filte

r(s).

Add

ition

al s

ampl

e is

nee

ded

to h

elp

esta

blis

h tre

nd.

Res

ampl

e at

hal

f nor

mal

inte

rval

.Pl

ease

pro

vide

equ

ipm

ent m

ake

and

mod

el a

s w

ell a

s th

e fu

ll na

me

and

grad

e of

the

lubr

ican

t in

serv

ice.

Tom

Hol

mes

Love

lace

Res

pira

tory

Res

earc

h In

stitu

te24

25 R

idge

cres

t Driv

e, S

E

Alb

uque

rque

, NM

871

08

12/0

1/11

12/0

1/11

12/0

2/11

12/0

6/11

Ship

ped

:R

ecei

ved:

Prin

ted:

Sam

pled

:

Uni

t Typ

e : E

ngin

e, D

iese

l (G

N_D

E001

)

* =

exce

eds

Cau

tion

limit

** =

exc

eeds

Ala

rm li

mit

101

Cor

pora

te P

lace

, Val

lejo

, CA

9459

0w

ww

.her

guth

.com

ISO

900

1:20

08 a

nd IS

O/IE

C 1

7025

:200

5 C

ertif

ied

ID: F

Y09-

111-

01D

EC11

-OIL

- FY

09-1

11-0

1dec

11-o

il, D

iese

l Eng

ine

Lab

Num

ber

Sam

ple

Dat

eM

inim

umM

axim

umV1

1430

4112

/01/

11

Com

para

tive

Gra

phic

Ana

lysi

s

Sodi

um

Silic

on

Silv

erTin

Lead

Cop

per

Chr

omiu

m

Alu

min

umIron

Sulfi

natio

n

Oxi

datio

n

Soot

Typi

cal

War

ning

O

ver

Max

Uni

t Tim

e (H

R)

Flui

d Ti

me

(HR

)Vi

s @

100

Deg

CTB

N m

g K

OH

/gFT

IR Soot

% w

t.O

xida

tion

Abs/

cmW

ater

FTI

R %

Vol

Sulfi

natio

n Ab

s/Fu

el %

Vol

Gly

col %

Vol

Met

als

Iron

ppm

Alum

inum

ppm

Chr

omiu

m p

pmC

oppe

r ppm

Lead

ppm

Tin

ppm

Nic

kel p

pmSi

lver

ppm

Antim

ony

ppm

Silic

on p

pmSo

dium

ppm

Boro

n pp

mZi

nc p

pmPh

osph

orus

ppm

Cal

cium

ppm

Mag

nesi

um p

pmBa

rium

ppm

Mol

ybde

num

ppm

Pota

ssiu

m p

pm

12.0

03.

0016

.80

3.0 30

0.20 30 5.0

0.20 59 4 4 7 4 4 44.

5 20 50 50

1949 0

15.4

54.

67__

____

____

*2.6 6

<0.1

0 13<2

.0<0

.10

____

____

__ 40 2 1 1 1 1 <1 0.1 <1 3 2 1

1115

1017

2253 6 <1 1 <3

Cod

e :L

OVE

MC

Lov

elac

e R

espi

rato

ry R

esea

rch

Inst

itute

Pho

ne :(

505)

348

-960

0 F

ax :(

505)

348

-498

0Th

ese

resu

lts a

re s

ubm

itted

pur

suan

t to

our c

urre

nt T

erm

s, C

ondi

tions

and

Lim

itatio

ns a

nd L

abor

ator

y P

ricin

g P

olic

y. N

o re

spon

sibi

lity

or li

abili

ty is

ass

umed

for t

he m

anne

r in

whi

ch th

ese

resu

lts a

re u

sed

or in

terp

rete

d.

Eval

uate

d B

y: D

avid

F. F

ryck

i, C

LS -

For

que

stio

ns a

bout

this

repo

rt, p

leas

e ca

ll 88

8-43

7-48

84.

erla

bgt1

.frx

Rev

. 05/

19/1

1


147

Oil

Type

: SA

E 40

(GN

_032

)

P.O

. : J

K-11

0737

Lab

Num

ber :

V11

4593

8

12/2

7/11

Page

1

15:5

2:45

NO

RM

AL:

Sam

ple

data

is s

atis

fact

ory.

No

actio

n is

requ

ired

at th

is ti

me.

Plea

se p

rovi

de e

quip

men

t mak

e an

d m

odel

as

wel

l as

the

full

nam

e an

d gr

ade

of th

e lu

bric

ant i

nse

rvic

e. A

dditi

onal

sam

ple

is n

eede

d to

hel

p es

tabl

ish

trend

. R

esam

ple

at h

alf n

orm

al in

terv

al.

Tom

Hol

mes

Love

lace

Res

pira

tory

Res

earc

h In

stitu

te24

25 R

idge

cres

t Driv

e, S

E

Alb

uque

rque

, NM

871

08

12/1

9/11

12/2

0/11

12/2

1/11

12/2

7/11

Ship

ped

:R

ecei

ved:

Prin

ted:

Sam

pled

:

Uni

t Typ

e : E

ngin

e, D

iese

l (G

N_D

E001

)

* =

exce

eds

Cau

tion

limit

** =

exc

eeds

Ala

rm li

mit

101

Cor

pora

te P

lace

, Val

lejo

, CA

9459

0w

ww

.her

guth

.com

ISO

900

1:20

08 a

nd IS

O/IE

C 1

7025

:200

5 C

ertif

ied

ID: F

Y09-

111-

19D

EC11

-OIL

- FY

09-1

11-1

9dec

11-o

il, D

iese

l Eng

ine

Lab

Num

ber

Sam

ple

Dat

eM

inim

umM

axim

umV1

1459

3812

/19/

11

Com

para

tive

Gra

phic

Ana

lysi

s

Sodi

um

Silic

onTin

Lead

Cop

per

Chr

omiu

m

Alum

inumIro

n

Sulfi

natio

n

Oxi

datio

n

Soot

TBN

Und

er M

in

War

ning

Typ

ical

Typ

ical

War

ning

Ove

r Max

Uni

t Tim

e (H

R)

Flui

d Ti

me

(HR

)Vi

s @

100

Deg

CTB

N m

g K

OH

/gFT

IR Soot

% w

t.O

xida

tion

Abs/

cmW

ater

FTI

R %

Vol

Sulfi

natio

n Ab

s/Fu

el %

Vol

Gly

col %

Vol

Met

als

Iron

ppm

Alum

inum

ppm

Chr

omiu

m p

pmC

oppe

r ppm

Lead

ppm

Tin

ppm

Nic

kel p

pmSi

lver

ppm

Antim

ony

ppm

Silic

on p

pmSo

dium

ppm

Boro

n pp

mZi

nc p

pmPh

osph

orus

ppm

Cal

cium

ppm

Mag

nesi

um p

pmBa

rium

ppm

Mol

ybde

num

ppm

Pota

ssiu

m p

pm

12.0

03.

0016

.80

3.0 30

0.20 30 5.0

0.20 59 4 4 7 4 4 44.

5 20 50 50

2181 0

15.2

95.

84__

____

____ 2.4 6

<0.1

0 13<2

.0<0

.10

____

____

__ 45 3 1 1 1 1 <1<0

.1 1 6 4 <115

0312

7428

79 7 <1 1 <3

Cod

e :L

OVE

MC

Lov

elac

e R

espi

rato

ry R

esea

rch

Inst

itute

Pho

ne :(

505)

348

-960

0 F

ax :(

505)

348

-498

0Th

ese

resu

lts a

re s

ubm

itted

pur

suan

t to

our c

urre

nt T

erm

s, C

ondi

tions

and

Lim

itatio

ns a

nd L

abor

ator

y P

ricin

g P

olic

y. N

o re

spon

sibi

lity

or li

abili

ty is

ass

umed

for t

he m

anne

r in

whi

ch th

ese

resu

lts a

re u

sed

or in

terp

rete

d.

Eval

uate

d B

y: D

avid

F. F

ryck

i, C

LS -

For

que

stio

ns a

bout

this

repo

rt, p

leas

e ca

ll 88

8-43

7-48

84.

erla

bgt1

.frx

Rev

. 05/

19/1

1


148

Oil

Type

: SA

E 40

(GN

_032

)

P.O

. : J

K120

015

Lab

Num

ber :

V11

4954

3

01/1

8/12

Page

1

17:2

4:11

MO

NIT

OR

: D

ata

for m

achi

ne a

nd/o

r flu

id c

ondi

tion

shou

ld b

e no

ted

and

mon

itore

d.So

ot c

onte

nt is

hig

h. P

leas

e pr

ovid

e eq

uipm

ent m

ake

and

mod

el a

s w

ell a

s th

e fu

ll na

me

and

grad

e of

the

lubr

ican

t in

serv

ice.

Add

ition

al s

ampl

e is

nee

ded

to h

elp

esta

blis

h tre

nd.

Res

ampl

e at

half

norm

al in

terv

al.

Tom

Hol

mes

Love

lace

Res

pira

tory

Res

earc

h In

stitu

te24

25 R

idge

cres

t Driv

e, S

E

Alb

uque

rque

, NM

871

08

01/1

6/12

01/1

6/12

01/1

7/12

01/1

8/12

Ship

ped

:R

ecei

ved:

Prin

ted:

Sam

pled

:

Uni

t Typ

e : E

ngin

e, D

iese

l (G

N_D

E001

)

* =

exce

eds

Cau

tion

limit

** =

exc

eeds

Ala

rm li

mit

101

Cor

pora

te P

lace

, Val

lejo

, CA

9459

0w

ww

.her

guth

.com

ISO

900

1:20

08 a

nd IS

O/IE

C 1

7025

:200

5 C

ertif

ied

ID: F

Y09-

111-

16JA

N12

-OIL

- FY

09-1

11-1

6JA

N20

12-O

IL, D

iese

l Eng

ine

Lab

Num

ber

Sam

ple

Dat

eM

inim

umM

axim

umV1

1495

4301

/16/

12

Com

para

tive

Gra

phic

Ana

lysi

s

Sodi

um

Silic

onTin

Lead

Cop

per

Chr

omiu

m

Alum

inumIro

n

Sulfi

natio

n

Oxi

datio

n

Soot

TBN

Und

er M

in

War

ning

Typ

ical

Typ

ical

War

ning

Ove

r Max

Uni

t Tim

e (H

R)

Flui

d Ti

me

(HR

)Vi

s @

100

Deg

CTB

N m

g K

OH

/gFT

IR Soot

% w

t.O

xida

tion

Abs/

cmW

ater

FTI

R %

Vol

Sulfi

natio

n Ab

s/Fu

el %

Vol

Gly

col %

Vol

Met

als

Iron

ppm

Alum

inum

ppm

Chr

omiu

m p

pmC

oppe

r ppm

Lead

ppm

Tin

ppm

Nic

kel p

pmSi

lver

ppm

Antim

ony

ppm

Silic

on p

pmSo

dium

ppm

Boro

n pp

mZi

nc p

pmPh

osph

orus

ppm

Cal

cium

ppm

Mag

nesi

um p

pmBa

rium

ppm

Mol

ybde

num

ppm

Pota

ssiu

m p

pm

12.0

03.

0016

.80

3.0 30

0.20 30 5.0

0.20 59 4 4 7 4 4 44.

5 20 50 50

2411 0

15.2

56.

58__

____

____

*2.8 10

<0.1

0 16<2

.0<0

.10

____

____

__ 38 2 1 2 1 1 <1<0

.1 <1 2 4 589

785

619

82 11 <1 1 <3

Cod

e :L

OVE

MC

Lov

elac

e R

espi

rato

ry R

esea

rch

Inst

itute

Pho

ne :(

505)

348

-960

0 F

ax :(

505)

348

-498

0Th

ese

resu

lts a

re s

ubm

itted

pur

suan

t to

our c

urre

nt T

erm

s, C

ondi

tions

and

Lim

itatio

ns a

nd L

abor

ator

y P

ricin

g P

olic

y. N

o re

spon

sibi

lity

or li

abili

ty is

ass

umed

for t

he m

anne

r in

whi

ch th

ese

resu

lts a

re u

sed

or in

terp

rete

d.

Eval

uate

d B

y: B

obby

R L

icu,

Sen

ior E

valu

ator

- F

or q

uest

ions

abo

ut th

is re

port

, ple

ase

call

888-

437-

4884

.er

labg

t1.fr

x R

ev. 0

5/19

/11


149

Oil

Type

: SA

E 40

(GN

_032

)

P.O

. : J

K120

015

Lab

Num

ber :

V11

5278

0

02/1

3/12

Page

1

15:0

8:49

MO

NIT

OR

: D

ata

for m

achi

ne a

nd/o

r flu

id c

ondi

tion

shou

ld b

e no

ted

and

mon

itore

d.So

ot c

onte

nt is

hig

h. P

leas

e pr

ovid

e eq

uipm

ent m

ake

and

mod

el a

s w

ell a

s th

e fu

ll na

me

and

grad

e of

the

lubr

ican

t in

serv

ice.

Dra

in o

il an

d ch

ange

filte

r(s).

Add

ition

al s

ampl

e is

nee

ded

to h

elp

esta

blis

h tre

nd.

Res

ampl

e at

hal

f nor

mal

inte

rval

.To

m H

olm

esLo

vela

ce R

espi

rato

ry R

esea

rch

Inst

itute

2425

Rid

gecr

est D

rive,

SE

Alb

uque

rque

, NM

871

08

02/0

6/12

02/0

7/12

02/0

8/12

02/1

3/12

Ship

ped

:R

ecei

ved:

Prin

ted:

Sam

pled

:

Uni

t Typ

e : E

ngin

e, D

iese

l (G

N_D

E001

)

* =

exce

eds

Cau

tion

limit

** =

exc

eeds

Ala

rm li

mit

101

Cor

pora

te P

lace

, Val

lejo

, CA

9459

0w

ww

.her

guth

.com

ISO

900

1:20

08 a

nd IS

O/IE

C 1

7025

:200

5 C

ertif

ied

ID: F

Y09-

111-

06FE

B12

-OIL

- FY

09-1

11-0

6FEB

2012

-OIL

, Die

sel E

ngin

e

Lab

Num

ber

Sam

ple

Dat

eM

inim

umM

axim

umV1

1527

8002

/06/

12

Com

para

tive

Gra

phic

Ana

lysi

s

Sodi

um

Silic

onTin

Lead

Cop

per

Chr

omiu

m

Alum

inumIro

n

Sulfi

natio

n

Oxi

datio

n

Soot

TBN

Und

er M

in

War

ning

Typ

ical

Typ

ical

War

ning

Ove

r Max

Uni

t Tim

e (H

R)

Flui

d Ti

me

(HR

)Vi

s @

100

Deg

CTB

N m

g K

OH

/gFT

IR Soot

% w

t.O

xida

tion

Abs/

cmW

ater

FTI

R %

Vol

Sulfi

natio

n Ab

s/Fu

el %

Vol

Gly

col %

Vol

Met

als

Iron

ppm

Alum

inum

ppm

Chr

omiu

m p

pmC

oppe

r ppm

Lead

ppm

Tin

ppm

Nic

kel p

pmSi

lver

ppm

Antim

ony

ppm

Silic

on p

pmSo

dium

ppm

Boro

n pp

mZi

nc p

pmPh

osph

orus

ppm

Cal

cium

ppm

Mag

nesi

um p

pmBa

rium

ppm

Mol

ybde

num

ppm

Pota

ssiu

m p

pm

12.0

03.

0016

.80

3.0 30

0.20 30 5.0

0.20 59 4 4 7 4 4 44.

5 20 50 50

2683 0

15.5

34.

94__

____

____

*2.9 7

<0.1

0 15<2

.0<0

.10

____

____

__ 37 2 1 1 1 1 <1<0

.1 <1 2 3 <111

05 923

2190 6 <1 <1 <3

Cod

e :L

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MC

Lov

elac

e R

espi

rato

ry R

esea

rch

Inst

itute

Pho

ne :(

505)

348

-960

0 F

ax :(

505)

348

-498

0Th

ese

resu

lts a

re s

ubm

itted

pur

suan

t to

our c

urre

nt T

erm

s, C

ondi

tions

and

Lim

itatio

ns a

nd L

abor

ator

y P

ricin

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olic

y. N

o re

spon

sibi

lity

or li

abili

ty is

ass

umed

for t

he m

anne

r in

whi

ch th

ese

resu

lts a

re u

sed

or in

terp

rete

d.

Eval

uate

d B

y: B

obby

R L

icu,

Sen

ior E

valu

ator

- F

or q

uest

ions

abo

ut th

is re

port

, ple

ase

call

888-

437-

4884

.er

labg

t1.fr

x R

ev. 0

5/19

/11


150

Oil

Type

: SA

E 40

(GN

_032

)

P.O

. : J

K120

015

Lab

Num

ber :

V11

5713

6

03/0

9/12

Page

1

15:5

3:55

AB

NO

RM

AL:

Abn

orm

al re

sults

for f

luid

are

pre

sent

. E

quip

men

t app

ears

sat

isfa

ctor

y.So

ot c

onte

nt is

hig

h. F

TIR

indi

cate

s oi

l is

sulfi

nate

d. D

rain

oil

and

chan

ge fi

lter(s

). C

heck

for

prop

er c

ombu

stio

n pr

oper

ties

(exh

aust

bac

k pr

essu

re, o

pera

ting

tem

pera

ture

s, w

orn/

brok

en ri

ngs,

exce

ssiv

e id

ling,

hun

g va

lves

, im

prop

er fu

el s

ettin

gs, a

ir in

take

rest

rictio

ns).

Add

ition

al s

ampl

e is

need

ed to

hel

p es

tabl

ish

trend

. R

esam

ple

at h

alf n

orm

al in

terv

al.

Tom

Hol

mes

Love

lace

Res

pira

tory

Res

earc

h In

stitu

te24

25 R

idge

cres

t Driv

e, S

E

Alb

uque

rque

, NM

871

08

03/0

6/12

03/0

6/12

03/0

7/12

03/0

9/12

Ship

ped

:R

ecei

ved:

Prin

ted:

Sam

pled

:

Uni

t Typ

e : E

ngin

e, D

iese

l (G

N_D

E001

)

* =

exce

eds

Cau

tion

limit

** =

exc

eeds

Ala

rm li

mit

101

Cor

pora

te P

lace

, Val

lejo

, CA

9459

0w

ww

.her

guth

.com

ISO

900

1:20

08 a

nd IS

O/IE

C 1

7025

:200

5 C

ertif

ied

ID: F

Y09-

111-

01M

AR

12-O

IL -

FY09

-111

-01M

ar12

-Oil,

Die

sel E

ngin

e

Lab

Num

ber

Sam

ple

Dat

eM

inim

umM

axim

umV1

1571

3603

/06/

12

Com

para

tive

Gra

phic

Ana

lysi

s

Silic

on

Lead

Cop

per

Chr

omiu

m

Alum

inumIro

n

Sulfi

natio

n

Oxi

datio

n

Soot

TBN

Vis

@ 1

00 D

eg C

Und

er M

in

War

ning

Typ

ical

Typ

ical

War

ning

Ove

r Max

Uni

t Tim

e (H

R)

Flui

d Ti

me

(HR

)Vi

s @

100

Deg

CTB

N m

g K

OH

/gFT

IR Soot

% w

t.O

xida

tion

Abs/

cmW

ater

FTI

R %

Vol

Sulfi

natio

n Ab

s/Fu

el %

Vol

Gly

col %

Vol

Met

als

Iron

ppm

Alum

inum

ppm

Chr

omiu

m p

pmC

oppe

r ppm

Lead

ppm

Tin

ppm

Nic

kel p

pmSi

lver

ppm

Antim

ony

ppm

Silic

on p

pmSo

dium

ppm

Boro

n pp

mZi

nc p

pmPh

osph

orus

ppm

Cal

cium

ppm

Mag

nesi

um p

pmBa

rium

ppm

Mol

ybde

num

ppm

Pota

ssiu

m p

pm

12.0

03.

0016

.80

3.0 30

0.20 30 5.0

0.20 58 4 4 7 4 4 44.

5 20 50 50

2998 0

15.4

94.

18__

____

____

**3.

3 18<0

.10

*26

<2.0

<0.1

0__

____

____ 39 2 1 1 1 <1 <1

<0.1 <1 2 <2 1

955

815

1950 5 <1 <1 <3

Cod

e :L

OVE

MC

Lov

elac

e R

espi

rato

ry R

esea

rch

Inst

itute

Pho

ne :(

505)

348

-960

0 F

ax :(

505)

348

-498

0Th

ese

resu

lts a

re s

ubm

itted

pur

suan

t to

our c

urre

nt T

erm

s, C

ondi

tions

and

Lim

itatio

ns a

nd L

abor

ator

y P

ricin

g P

olic

y. N

o re

spon

sibi

lity

or li

abili

ty is

ass

umed

for t

he m

anne

r in

whi

ch th

ese

resu

lts a

re u

sed

or in

terp

rete

d.

Eval

uate

d B

y: B

obby

R L

icu,

Sen

ior E

valu

ator

- F

or q

uest

ions

abo

ut th

is re

port

, ple

ase

call

888-

437-

4884

.er

labg

t1.fr

x R

ev. 0

5/19

/11


151

Oil

Type

: SA

E 40

(GN

_032

)

P.O

. : J

K120

015

Lab

Num

ber :

V11

5900

0

03/2

3/12

Page

1

16:2

4:25

NO

RM

AL:

Sam

ple

data

is s

atis

fact

ory.

No

actio

n is

requ

ired

at th

is ti

me.

Plea

se p

rovi

de e

quip

men

t mak

e an

d m

odel

as

wel

l as

the

full

nam

e an

d gr

ade

of th

e lu

bric

ant i

nse

rvic

e. A

dditi

onal

sam

ple

is n

eede

d to

hel

p es

tabl

ish

trend

. R

esam

ple

at h

alf n

orm

al in

terv

al.

Tom

Hol

mes

Love

lace

Res

pira

tory

Res

earc

h In

stitu

te24

25 R

idge

cres

t Driv

e, S

E

Alb

uque

rque

, NM

871

08

03/2

0/12

03/2

0/12

03/2

1/12

03/2

3/12

Ship

ped

:R

ecei

ved:

Prin

ted:

Sam

pled

:

Uni

t Typ

e : E

ngin

e, D

iese

l (G

N_D

E001

)

* =

exce

eds

Cau

tion

limit

** =

exc

eeds

Ala

rm li

mit

101

Cor

pora

te P

lace

, Val

lejo

, CA

9459

0w

ww

.her

guth

.com

ISO

900

1:20

08 a

nd IS

O/IE

C 1

7025

:200

5 C

ertif

ied

ID: F

Y09-

111-

19M

AR

12-O

IL -

FY09

-111

-19M

AR

12-O

IL, D

iese

l Eng

ine

Lab

Num

ber

Sam

ple

Dat

eM

inim

umM

axim

umV1

1590

0003

/20/

12

Com

para

tive

Gra

phic

Ana

lysi

s

Sodi

um

Silic

onTin

Lead

Cop

per

Chr

omiu

m

Alum

inumIro

n

Sulfi

natio

n

Oxi

datio

n

Soot

TBN

Und

er M

in

War

ning

Typ

ical

Typ

ical

War

ning

Ove

r Max

Uni

t Tim

e (H

R)

Flui

d Ti

me

(HR

)Vi

s @

100

Deg

CTB

N m

g K

OH

/gFT

IR Soot

% w

t.O

xida

tion

Abs/

cmW

ater

FTI

R %

Vol

Sulfi

natio

n Ab

s/Fu

el %

Vol

Gly

col %

Vol

Met

als

Iron

ppm

Alum

inum

ppm

Chr

omiu

m p

pmC

oppe

r ppm

Lead

ppm

Tin

ppm

Nic

kel p

pmSi

lver

ppm

Antim

ony

ppm

Silic

on p

pmSo

dium

ppm

Boro

n pp

mZi

nc p

pmPh

osph

orus

ppm

Cal

cium

ppm

Mag

nesi

um p

pmBa

rium

ppm

Mol

ybde

num

ppm

Pota

ssiu

m p

pm

12.0

03.

0016

.80

3.0 30

0.20 30 2.5

0.20 58 4 4 7 4 4 44.

5 20 50 50

3189 0

14.7

66.

22__

____

____ 2.2 6

<0.1

0 12<2

.0<0

.10

____

____

__ 22 2 1 1 1 1 <1<0

.1 <1 3 2 197

987

921

23 6 <1 27 <3

Cod

e :L

OVE

MC

Lov

elac

e R

espi

rato

ry R

esea

rch

Inst

itute

Pho

ne :(

505)

348

-960

0 F

ax :(

505)

348

-498

0Th

ese

resu

lts a

re s

ubm

itted

pur

suan

t to

our c

urre

nt T

erm

s, C

ondi

tions

and

Lim

itatio

ns a

nd L

abor

ator

y P

ricin

g P

olic

y. N

o re

spon

sibi

lity

or li

abili

ty is

ass

umed

for t

he m

anne

r in

whi

ch th

ese

resu

lts a

re u

sed

or in

terp

rete

d.

Eval

uate

d B

y: B

obby

R L

icu,

Sen

ior E

valu

ator

- F

or q

uest

ions

abo

ut th

is re

port

, ple

ase

call

888-

437-

4884

.er

labg

t1.fr

x R

ev. 0

5/19

/11


152

Oil

Type

: SA

E 40

(GN

_032

)

P.O

. : J

K120

015

Lab

Num

ber :

V11

6193

5

04/1

6/12

Page

1

12:5

1:09

MO

NIT

OR

: D

ata

for m

achi

ne a

nd/o

r flu

id c

ondi

tion

shou

ld b

e no

ted

and

mon

itore

d.Pl

ease

pro

vide

equ

ipm

ent m

ake

and

mod

el a

s w

ell a

s th

e fu

ll na

me

and

grad

e of

the

lubr

ican

t in

serv

ice.

Oth

er te

st re

sults

are

acc

epta

ble.

Add

ition

al s

ampl

e is

nee

ded

to h

elp

esta

blis

h tre

nd.

Res

ampl

e at

hal

f nor

mal

inte

rval

.To

m H

olm

esLo

vela

ce R

espi

rato

ry R

esea

rch

Inst

itute

2425

Rid

gecr

est D

rive,

SE

Alb

uque

rque

, NM

871

08

04/1

0/12

04/1

1/12

04/1

2/12

04/1

6/12

Ship

ped

:R

ecei

ved:

Prin

ted:

Sam

pled

:

Uni

t Typ

e : E

ngin

e, D

iese

l (G

N_D

E001

)

* =

exce

eds

Cau

tion

limit

** =

exc

eeds

Ala

rm li

mit

101

Cor

pora

te P

lace

, Val

lejo

, CA

9459

0w

ww

.her

guth

.com

ISO

900

1:20

08 a

nd IS

O/IE

C 1

7025

:200

5 C

ertif

ied

ID: F

Y09-

111-

10A

PR20

12-O

- FY

09-1

11-1

0apr

2012

-oil,

Die

sel E

ngin

e

Lab

Num

ber

Sam

ple

Dat

eM

inim

umM

axim

umV1

1619

3504

/10/

12

Com

para

tive

Gra

phic

Ana

lysi

s

Sodi

um

Silic

on

Silv

er

Lead

Cop

per

Chr

omiu

m

Alum

inumIro

n

Sulfi

natio

n

Oxi

datio

n

Soot

TBN

Und

er M

in

War

ning

Typ

ical

Typ

ical

War

ning

Ove

r Max

Uni

t Tim

e (H

R)

Flui

d Ti

me

(HR

)Vi

s @

100

Deg

CTB

N m

g K

OH

/gFT

IR Soot

% w

t.O

xida

tion

Abs/

cmW

ater

FTI

R %

Vol

Sulfi

natio

n Ab

s/Fu

el %

Vol

Gly

col %

Vol

Met

als

Iron

ppm

Alum

inum

ppm

Chr

omiu

m p

pmC

oppe

r ppm

Lead

ppm

Tin

ppm

Nic

kel p

pmSi

lver

ppm

Antim

ony

ppm

Silic

on p

pmSo

dium

ppm

Boro

n pp

mZi

nc p

pmPh

osph

orus

ppm

Cal

cium

ppm

Mag

nesi

um p

pmBa

rium

ppm

Mol

ybde

num

ppm

Pota

ssiu

m p

pm

12.0

03.

0016

.80

3.0 30

0.20 30 2.5

0.20 59 4 4 7 4 4 44.

5 20 50 50

0 015

.03

4.83

____

____

__*2

.7 7<0

.10 14

<2.0

<0.1

0__

____

____ 27 2 1 1 1 <1 <1 0.1 1 2 2 <1 941

822

1877 4 <1 1 <3

Cod

e :L

OVE

MC

Lov

elac

e R

espi

rato

ry R

esea

rch

Inst

itute

Pho

ne :(

505)

348

-960

0 F

ax :(

505)

348

-498

0Th

ese

resu

lts a

re s

ubm

itted

pur

suan

t to

our c

urre

nt T

erm

s, C

ondi

tions

and

Lim

itatio

ns a

nd L

abor

ator

y P

ricin

g P

olic

y. N

o re

spon

sibi

lity

or li

abili

ty is

ass

umed

for t

he m

anne

r in

whi

ch th

ese

resu

lts a

re u

sed

or in

terp

rete

d.

Eval

uate

d B

y: B

obby

R L

icu,

Sen

ior E

valu

ator

- F

or q

uest

ions

abo

ut th

is re

port

, ple

ase

call

888-

437-

4884

.er

labg

t1.fr

x R

ev. 0

5/19

/11


153

Oil

Type

: SA

E 40

(GN

_032

)

P.O

. : J

K120

015

Lab

Num

ber :

V11

6193

5

04/1

6/12

Page

1

12:5

1:09

MO

NIT

OR

: D

ata

for m

achi

ne a

nd/o

r flu

id c

ondi

tion

shou

ld b

e no

ted

and

mon

itore

d.Pl

ease

pro

vide

equ

ipm

ent m

ake

and

mod

el a

s w

ell a

s th

e fu

ll na

me

and

grad

e of

the

lubr

ican

t in

serv

ice.

Oth

er te

st re

sults

are

acc

epta

ble.

Add

ition

al s

ampl

e is

nee

ded

to h

elp

esta

blis

h tre

nd.

Res

ampl

e at

hal

f nor

mal

inte

rval

.To

m H

olm

esLo

vela

ce R

espi

rato

ry R

esea

rch

Inst

itute

2425

Rid

gecr

est D

rive,

SE

Alb

uque

rque

, NM

871

08

04/1

0/12

04/1

1/12

04/1

2/12

04/1

6/12

Ship

ped

:R

ecei

ved:

Prin

ted:

Sam

pled

:

Uni

t Typ

e : E

ngin

e, D

iese

l (G

N_D

E001

)

* =

exce

eds

Cau

tion

limit

** =

exc

eeds

Ala

rm li

mit

101

Cor

pora

te P

lace

, Val

lejo

, CA

9459

0w

ww

.her

guth

.com

ISO

900

1:20

08 a

nd IS

O/IE

C 1

7025

:200

5 C

ertif

ied

ID: F

Y09-

111-

10A

PR20

12-O

- FY

09-1

11-1

0apr

2012

-oil,

Die

sel E

ngin

e

Lab

Num

ber

Sam

ple

Dat

eM

inim

umM

axim

umV1

1619

3504

/10/

12

Com

para

tive

Gra

phic

Ana

lysi

s

Sodi

um

Silic

on

Silv

er

Lead

Cop

per

Chr

omiu

m

Alum

inumIro

n

Sulfi

natio

n

Oxi

datio

n

Soot

TBN

Und

er M

in

War

ning

Typ

ical

Typ

ical

War

ning

Ove

r Max

Uni

t Tim

e (H

R)

Flui

d Ti

me

(HR

)Vi

s @

100

Deg

CTB

N m

g K

OH

/gFT

IR Soot

% w

t.O

xida

tion

Abs/

cmW

ater

FTI

R %

Vol

Sulfi

natio

n Ab

s/Fu

el %

Vol

Gly

col %

Vol

Met

als

Iron

ppm

Alum

inum

ppm

Chr

omiu

m p

pmC

oppe

r ppm

Lead

ppm

Tin

ppm

Nic

kel p

pmSi

lver

ppm

Antim

ony

ppm

Silic

on p

pmSo

dium

ppm

Boro

n pp

mZi

nc p

pmPh

osph

orus

ppm

Cal

cium

ppm

Mag

nesi

um p

pmBa

rium

ppm

Mol

ybde

num

ppm

Pota

ssiu

m p

pm

12.0

03.

0016

.80

3.0 30

0.20 30 2.5

0.20 59 4 4 7 4 4 44.

5 20 50 50

0 015

.03

4.83

____

____

__*2

.7 7<0

.10 14

<2.0

<0.1

0__

____

____ 27 2 1 1 1 <1 <1 0.1 1 2 2 <1 941

822

1877 4 <1 1 <3

Cod

e :L

OVE

MC

Lov

elac

e R

espi

rato

ry R

esea

rch

Inst

itute

Pho

ne :(

505)

348

-960

0 F

ax :(

505)

348

-498

0Th

ese

resu

lts a

re s

ubm

itted

pur

suan

t to

our c

urre

nt T

erm

s, C

ondi

tions

and

Lim

itatio

ns a

nd L

abor

ator

y P

ricin

g P

olic

y. N

o re

spon

sibi

lity

or li

abili

ty is

ass

umed

for t

he m

anne

r in

whi

ch th

ese

resu

lts a

re u

sed

or in

terp

rete

d.

Eval

uate

d B

y: B

obby

R L

icu,

Sen

ior E

valu

ator

- F

or q

uest

ions

abo

ut th

is re

port

, ple

ase

call

888-

437-

4884

.er

labg

t1.fr

x R

ev. 0

5/19

/11


154

Oil

Type

: SA

E 40

(GN

_032

)

P.O

. : J

K120

015

Lab

Num

ber :

V11

6516

0

05/0

9/12

Page

1

13:5

1:52

AB

NO

RM

AL:

Abn

orm

al re

sults

for f

luid

are

pre

sent

. E

quip

men

t app

ears

sat

isfa

ctor

y.S

oot c

onte

nt is

hig

h. D

rain

oil

and

chan

ge fi

lter(s

). C

heck

for p

rope

r com

bust

ion

prop

ertie

s (e

xhau

stba

ck p

ress

ure,

ope

ratin

g te

mpe

ratu

res,

wor

n/br

oken

ring

s, e

xces

sive

idlin

g, h

ung

valv

es, i

mpr

oper

fuel

set

tings

, air

inta

ke re

stric

tions

). Pl

ease

pro

vide

equ

ipm

ent m

ake

and

mod

el a

s w

ell a

s th

e fu

llna

me

and

grad

e of

the

lubr

ican

t in

serv

ice.

Res

ampl

e at

hal

f nor

mal

inte

rval

.To

m H

olm

esLo

vela

ce R

espi

rato

ry R

esea

rch

Inst

itute

2425

Rid

gecr

est D

rive,

SE

Alb

uque

rque

, NM

871

08

05/0

3/12

05/0

6/12

05/0

7/12

05/0

9/12

Ship

ped

:R

ecei

ved:

Prin

ted:

Sam

pled

:

Uni

t Typ

e : E

ngin

e, D

iese

l (G

N_D

E001

)

* =

exce

eds

Cau

tion

limit

** =

exc

eeds

Ala

rm li

mit

101

Cor

pora

te P

lace

, Val

lejo

, CA

9459

0w

ww

.her

guth

.com

ISO

900

1:20

08 a

nd IS

O/IE

C 1

7025

:200

5 C

ertif

ied

ID: F

Y09-

111-

03M

AY1

2-O

IL -

FY09

-111

-03M

AY2

012

OIL

, Die

sel E

ngin

e

Lab

Num

ber

Sam

ple

Dat

eM

inim

umM

axim

umV1

1651

6005

/03/

12

Com

para

tive

Gra

phic

Ana

lysi

s

Silic

onTin

Lead

Cop

per

Chr

omiu

m

Alum

inumIro

n

Sulfi

natio

n

Oxi

datio

n

Soot

TBN

Vis

@10

0 D

eg C

Und

er M

in

War

ning

Typ

ical

Typ

ical

War

ning

Ove

r Max

Uni

t Tim

e (H

R)

Flui

d Ti

me

(HR

)Vi

s @

100

Deg

CTB

N m

g K

OH

/gFT

IR Soot

% w

t.O

xida

tion

Abs/

cmW

ater

FTI

R %

Vol

Sulfi

natio

n Ab

s/Fu

el %

Vol

Gly

col %

Vol

Met

als

Iron

ppm

Alum

inum

ppm

Chr

omiu

m p

pmC

oppe

r ppm

Lead

ppm

Tin

ppm

Nic

kel p

pmSi

lver

ppm

Antim

ony

ppm

Silic

on p

pmSo

dium

ppm

Boro

n pp

mZi

nc p

pmPh

osph

orus

ppm

Cal

cium

ppm

Mag

nesi

um p

pmBa

rium

ppm

Mol

ybde

num

ppm

Pota

ssiu

m p

pm

12.5

02.

0016

.80

3.0 30

0.20 30 2.5

0.20 99 16 4 36 50 4 43.

1 20

3910 0

15.1

34.

94__

____

____

*2.9 7

<0.1

0 16<2

.0<0

.10

____

____

__ 31 2 1 1 1 1 <1<0

.1 <1 3 2 111

51 983

2404 5 <1 <1 <3

Cod

e :L

OVE

MC

Lov

elac

e R

espi

rato

ry R

esea

rch

Inst

itute

Pho

ne :(

505)

348

-960

0 F

ax :(

505)

348

-498

0Th

ese

resu

lts a

re s

ubm

itted

pur

suan

t to

our c

urre

nt T

erm

s, C

ondi

tions

and

Lim

itatio

ns a

nd L

abor

ator

y P

ricin

g P

olic

y. N

o re

spon

sibi

lity

or li

abili

ty is

ass

umed

for t

he m

anne

r in

whi

ch th

ese

resu

lts a

re u

sed

or in

terp

rete

d.

Eval

uate

d B

y: A

aron

D. L

arso

n, E

valu

ator

- F

or q

uest

ions

abo

ut th

is re

port

, ple

ase

call

888-

437-

4884

.er

labg

t1.fr

x R

ev. 0

5/19

/11


155

Oil

Type

: SA

E 40

(GN

_032

)

P.O

. : J

K110

737

Lab

Num

ber :

V11

7360

1

07/1

0/12

Page

1

17:2

2:05

AB

NO

RM

AL:

Abn

orm

al te

st re

sults

are

pre

sent

.So

ot c

onte

nt is

hig

h. C

hrom

ium

may

indi

cate

ring

wea

r. T

in is

an

indi

cato

r of b

earin

g/bu

shin

gal

loys

, bra

ss a

nd/o

r sol

der.

Dra

in o

il an

d ch

ange

filte

r(s).

Add

ition

al s

ampl

e is

nee

ded

to h

elp

esta

blis

h tre

nd.

Res

ampl

e at

hal

f nor

mal

inte

rval

. Pl

ease

pro

vide

equ

ipm

ent m

ake

and

mod

el a

sw

ell a

s th

e fu

ll na

me

and

grad

e of

the

lubr

ican

t in

serv

ice.

Tom

Hol

mes

Love

lace

Res

pira

tory

Res

earc

h In

stitu

te24

25 R

idge

cres

t Driv

e, S

E

Alb

uque

rque

, NM

871

08

07/0

2/12

07/0

8/12

07/0

9/12

07/1

0/12

Ship

ped

:R

ecei

ved:

Prin

ted:

Sam

pled

:

Uni

t Typ

e : E

ngin

e, D

iese

l (G

N_D

E001

)

* =

exce

eds

Cau

tion

limit

** =

exc

eeds

Ala

rm li

mit

101

Cor

pora

te P

lace

, Val

lejo

, CA

9459

0w

ww

.her

guth

.com

ISO

900

1:20

08 a

nd IS

O/IE

C 1

7025

:200

5 C

ertif

ied

ID: F

Y09-

111-

02JU

L201

2 - F

Y09-

111-

02ju

l201

2-oi

l

Lab

Num

ber

Sam

ple

Dat

eM

inim

umM

axim

umV1

1736

0107

/02/

12

Com

para

tive

Gra

phic

Ana

lysi

s

Silic

onTin

Lead

Cop

per

Chr

omiu

m

Alum

inumIro

n

Sulfi

natio

n

Oxi

datio

n

Soot

TBN

Vis

@10

0 D

eg C

Und

er M

in

War

ning

Typ

ical

Typ

ical

War

ning

Ove

r Max

Uni

t Tim

e (H

R)

Flui

d Ti

me

(HR

)Vi

s @

100

Deg

CTB

N m

g K

OH

/gFT

IR Soot

% w

t.O

xida

tion

Abs/

cmW

ater

FTI

R %

Vol

Sulfi

natio

n Ab

s/Fu

el %

Vol

Gly

col %

Vol

Met

als

Iron

ppm

Alum

inum

ppm

Chr

omiu

m p

pmC

oppe

r ppm

Lead

ppm

Tin

ppm

Nic

kel p

pmSi

lver

ppm

Antim

ony

ppm

Silic

on p

pmSo

dium

ppm

Boro

n pp

mZi

nc p

pmPh

osph

orus

ppm

Cal

cium

ppm

Mag

nesi

um p

pmBa

rium

ppm

Mol

ybde

num

ppm

Pota

ssiu

m p

pm

12.5

02.

0016

.80

3.0 30

0.20 30 2.5

0.20 99 16 4 36 50 4 43.

1 20

274 0

14.8

75.

09__

____

____

*3.0 15

<0.1

0 20<2

.0<0

.10

____

____

__ 72 2**

7 4 3**

6 <1<0

.1 <1 10 16 114

9311

5829

39 10 <1 1 <3

Cod

e :L

OVE

MC

Lov

elac

e R

espi

rato

ry R

esea

rch

Inst

itute

Pho

ne :(

505)

348

-960

0 F

ax :(

505)

348

-498

0Th

ese

resu

lts a

re s

ubm

itted

pur

suan

t to

our c

urre

nt T

erm

s, C

ondi

tions

and

Lim

itatio

ns a

nd L

abor

ator

y P

ricin

g P

olic

y. N

o re

spon

sibi

lity

or li

abili

ty is

ass

umed

for t

he m

anne

r in

whi

ch th

ese

resu

lts a

re u

sed

or in

terp

rete

d.

Eval

uate

d B

y: N

uno

H. M

orei

ra, Q

AM

- F

or q

uest

ions

abo

ut th

is re

port

, ple

ase

call

888-

437-

4884

.er

labg

t1.fr

x R

ev. 0

5/19

/11


156

Oil

Type

: SA

E 40

(GN

_032

)

P.O

. : J

K120

015

Lab

Num

ber :

V11

7793

9

08/0

9/12

Page

1

14:2

5:23

MO

NIT

OR

: D

ata

for m

achi

ne a

nd/o

r flu

id c

ondi

tion

shou

ld b

e no

ted

and

mon

itore

d.So

ot c

onte

nt is

hig

h. P

leas

e pr

ovid

e eq

uipm

ent m

ake

and

mod

el a

s w

ell a

s th

e fu

ll na

me

and

grad

e of

the

lubr

ican

t in

serv

ice.

Dra

in o

il an

d ch

ange

filte

r(s).

Add

ition

al s

ampl

e is

nee

ded

to h

elp

esta

blis

h tre

nd.

Res

ampl

e at

hal

f nor

mal

inte

rval

.To

m H

olm

esLo

vela

ce R

espi

rato

ry R

esea

rch

Inst

itute

2425

Rid

gecr

est D

rive,

SE

Alb

uque

rque

, NM

871

08

07/3

0/12

08/0

6/12

08/0

7/12

08/0

9/12

Ship

ped

:R

ecei

ved:

Prin

ted:

Sam

pled

:

Uni

t Typ

e : E

ngin

e, D

iese

l (G

N_D

E001

)

* =

exce

eds

Cau

tion

limit

** =

exc

eeds

Ala

rm li

mit

101

Cor

pora

te P

lace

, Val

lejo

, CA

9459

0w

ww

.her

guth

.com

ISO

900

1:20

08 a

nd IS

O/IE

C 1

7025

:200

5 C

ertif

ied

ID: F

Y09-

111-

30JU

L12-

OI -

FY0

9-11

1-30

JUL2

012

OIL

, Die

sel E

ngin

e

Lab

Num

ber

Sam

ple

Dat

eM

inim

umM

axim

umV1

1779

3907

/30/

12

Com

para

tive

Gra

phic

Ana

lysi

s

Sodi

um

Silic

onTin

Lead

Cop

per

Chr

omiu

m

Alum

inumIro

n

Sulfi

natio

n

Oxi

datio

n

Soot

TBN

Und

er M

in

War

ning

Typ

ical

Typ

ical

War

ning

Ove

r Max

Uni

t Tim

e (H

R)

Flui

d Ti

me

(HR

)Vi

s @

100

Deg

CTB

N m

g K

OH

/gFT

IR Soot

% w

t.O

xida

tion

Abs/

cmW

ater

FTI

R %

Vol

Sulfi

natio

n Ab

s/Fu

el %

Vol

Gly

col %

Vol

Met

als

Iron

ppm

Alum

inum

ppm

Chr

omiu

m p

pmC

oppe

r ppm

Lead

ppm

Tin

ppm

Nic

kel p

pmSi

lver

ppm

Antim

ony

ppm

Silic

on p

pmSo

dium

ppm

Boro

n pp

mZi

nc p

pmPh

osph

orus

ppm

Cal

cium

ppm

Mag

nesi

um p

pmBa

rium

ppm

Mol

ybde

num

ppm

Pota

ssiu

m p

pm

12.5

03.

0016

.80

3.0 30

0.20 30 2.5

0.20 67 4 4 6 4 4 44.

5 20 50 50

540 0

14.4

44.

55__

____

____

*2.9 8

<0.1

0 19<2

.0<0

.10

____

____

__ 44 2 3 2 2 3 <1<0

.1 <1 4 5 111

96 979

2255 6 <1 1 <3

Cod

e :L

OVE

MC

Lov

elac

e R

espi

rato

ry R

esea

rch

Inst

itute

Pho

ne :(

505)

348

-960

0 F

ax :(

505)

348

-498

0Th

ese

resu

lts a

re s

ubm

itted

pur

suan

t to

our c

urre

nt T

erm

s, C

ondi

tions

and

Lim

itatio

ns a

nd L

abor

ator

y P

ricin

g P

olic

y. N

o re

spon

sibi

lity

or li

abili

ty is

ass

umed

for t

he m

anne

r in

whi

ch th

ese

resu

lts a

re u

sed

or in

terp

rete

d.

Eval

uate

d B

y: B

obby

R L

icu,

Sen

ior E

valu

ator

- F

or q

uest

ions

abo

ut th

is re

port

, ple

ase

call

888-

437-

4884

.er

labg

t1.fr

x R

ev. 0

5/19

/11


157

Oil

Type

: SA

E 40

(GN

_032

)

P.O

. : J

K110

737

Lab

Num

ber :

V11

8005

6

08/2

7/12

Page

1

18:1

2:18

AB

NO

RM

AL:

Abn

orm

al re

sults

for f

luid

are

pre

sent

. E

quip

men

t app

ears

sat

isfa

ctor

y.So

ot c

onte

nt is

hig

h. P

leas

e pr

ovid

e eq

uipm

ent m

ake

and

mod

el a

s w

ell a

s th

e fu

ll na

me

and

grad

e of

the

lubr

ican

t in

serv

ice.

Dra

in o

il an

d ch

ange

filte

r(s).

Che

ck fo

r pro

per c

ombu

stio

npr

oper

ties

(exh

aust

bac

k pr

essu

re, o

pera

ting

tem

pera

ture

s, w

orn/

brok

en ri

ngs,

exc

essi

ve id

ling,

hung

val

ves,

impr

oper

fuel

set

tings

, air

inta

ke re

stric

tions

). R

esam

ple

at h

alf n

orm

al in

terv

al.

Tom

Hol

mes

Love

lace

Res

pira

tory

Res

earc

h In

stitu

te24

25 R

idge

cres

t Driv

e, S

E

Alb

uque

rque

, NM

871

08

08/2

1/12

08/2

2/12

08/2

3/12

08/2

7/12

Ship

ped

:R

ecei

ved:

Prin

ted:

Sam

pled

:

Uni

t Typ

e : E

ngin

e, D

iese

l (G

N_D

E001

)

* =

exce

eds

Cau

tion

limit

** =

exc

eeds

Ala

rm li

mit

101

Cor

pora

te P

lace

, Val

lejo

, CA

9459

0w

ww

.her

guth

.com

ISO

900

1:20

08 a

nd IS

O/IE

C 1

7025

:200

5 C

ertif

ied

ID: F

Y09-

111-

21A

UG

2012

- FY

09-1

11-2

1aug

2012

-oil

Lab

Num

ber

Sam

ple

Dat

eM

inim

umM

axim

umV1

1800

5608

/21/

12

Com

para

tive

Gra

phic

Ana

lysi

s

Sodi

um

Silic

onTin

Lead

Cop

per

Chr

omiu

m

Alum

inumIro

n

Sulfi

natio

n

Oxi

datio

n

Soot

TBN

Und

er M

in

War

ning

Typ

ical

Typ

ical

War

ning

Ove

r Max

Uni

t Tim

e (H

R)

Flui

d Ti

me

(HR

)Vi

s @

100

Deg

CTB

N m

g K

OH

/gFT

IR Soot

% w

t.O

xida

tion

Abs/

cmW

ater

FTI

R %

Vol

Sulfi

natio

n Ab

s/Fu

el %

Vol

Gly

col %

Vol

Met

als

Iron

ppm

Alum

inum

ppm

Chr

omiu

m p

pmC

oppe

r ppm

Lead

ppm

Tin

ppm

Nic

kel p

pmSi

lver

ppm

Antim

ony

ppm

Silic

on p

pmSo

dium

ppm

Boro

n pp

mZi

nc p

pmPh

osph

orus

ppm

Cal

cium

ppm

Mag

nesi

um p

pmBa

rium

ppm

Mol

ybde

num

ppm

Pota

ssiu

m p

pm

12.5

03.

0016

.80

3.0 30

0.20 30 2.5

0.20 67 4 4 6 4 4 44.

5 20 50 50

780 0

14.7

84.

81__

____

____

**3.

1 17<0

.10 25

<2.0

<0.1

0__

____

____ 42 2 2 1 2 2 <1

<0.1 <1 4 5 1

1248

1056

2543 8 <1 <1 <3

Cod

e :L

OVE

MC

Lov

elac

e R

espi

rato

ry R

esea

rch

Inst

itute

Pho

ne :(

505)

348

-960

0 F

ax :(

505)

348

-498

0Th

ese

resu

lts a

re s

ubm

itted

pur

suan

t to

our c

urre

nt T

erm

s, C

ondi

tions

and

Lim

itatio

ns a

nd L

abor

ator

y P

ricin

g P

olic

y. N

o re

spon

sibi

lity

or li

abili

ty is

ass

umed

for t

he m

anne

r in

whi

ch th

ese

resu

lts a

re u

sed

or in

terp

rete

d.

Eval

uate

d B

y: B

obby

R L

icu,

Sen

ior E

valu

ator

- F

or q

uest

ions

abo

ut th

is re

port

, ple

ase

call

888-

437-

4884

.er

labg

t1.fr

x R

ev. 0

5/19

/11


158

Oil

Type

: SA

E 40

(GN

_032

)

P.O

. : J

K110

737

Lab

Num

ber :

V11

8363

4

09/2

0/12

Page

1

13:3

3:52

AB

NO

RM

AL:

Abn

orm

al re

sults

for f

luid

are

pre

sent

. E

quip

men

t app

ears

sat

isfa

ctor

y.So

dium

may

indi

cate

coo

lant

inhi

bito

rs; c

heck

for s

ourc

e. D

rain

oil

and

chan

ge fi

lter(s

). C

heck

for

prop

er c

ombu

stio

n pr

oper

ties

(exh

aust

bac

k pr

essu

re, o

pera

ting

tem

pera

ture

s, w

orn/

brok

en ri

ngs,

exce

ssiv

e id

ling,

hun

g va

lves

, im

prop

er fu

el s

ettin

gs, a

ir in

take

rest

rictio

ns).

Add

ition

al s

ampl

e is

need

ed to

hel

p es

tabl

ish

trend

. R

esam

ple

at h

alf n

orm

al in

terv

al.

Plea

se p

rovi

de e

quip

men

t mak

ean

d m

odel

as

wel

l as

the

full

nam

e an

d gr

ade

of th

e lu

bric

ant i

n se

rvic

e.

Tom

Hol

mes

Love

lace

Res

pira

tory

Res

earc

h In

stitu

te24

25 R

idge

cres

t Driv

e, S

E

Alb

uque

rque

, NM

871

08

09/1

1/12

09/1

7/12

09/1

8/12

09/2

0/12

Ship

ped

:R

ecei

ved:

Prin

ted:

Sam

pled

:

Uni

t Typ

e : E

ngin

e, D

iese

l (G

N_D

E001

)

* =

exce

eds

Cau

tion

limit

** =

exc

eeds

Ala

rm li

mit

101

Cor

pora

te P

lace

, Val

lejo

, CA

9459

0w

ww

.her

guth

.com

ISO

900

1:20

08 a

nd IS

O/IE

C 1

7025

:200

5 C

ertif

ied

ID: F

Y09-

111-

11SE

P201

2 - F

Y09-

111-

11se

p201

2-oi

l, D

iese

l Eng

ine

Lab

Num

ber

Sam

ple

Dat

eM

inim

umM

axim

umV1

1836

3409

/11/

12

Com

para

tive

Gra

phic

Ana

lysi

s

Sodi

um

Silic

onTin

Lead

Cop

per

Chr

omiu

m

Alum

inumIro

n

Sulfi

natio

n

Oxi

datio

n

Soot

TBN

Und

er M

in

War

ning

Typ

ical

Typ

ical

War

ning

Ove

r Max

Uni

t Tim

e (H

R)

Flui

d Ti

me

(HR

)Vi

s @

100

Deg

CTB

N m

g K

OH

/gFT

IR Soot

% w

t.O

xida

tion

Abs/

cmW

ater

FTI

R %

Vol

Sulfi

natio

n Ab

s/Fu

el %

Vol

Gly

col %

Vol

Met

als

Iron

ppm

Alum

inum

ppm

Chr

omiu

m p

pmC

oppe

r ppm

Lead

ppm

Tin

ppm

Nic

kel p

pmSi

lver

ppm

Antim

ony

ppm

Silic

on p

pmSo

dium

ppm

Boro

n pp

mZi

nc p

pmPh

osph

orus

ppm

Cal

cium

ppm

Mag

nesi

um p

pmBa

rium

ppm

Mol

ybde

num

ppm

Pota

ssiu

m p

pm

12.5

03.

0016

.80

3.0 30

0.20 30 2.5

0.20 67 4 4 6 4 4 44.

5 20 50 50

1069 0

15.0

15.

02__

____

____

**3.

6 16<0

.10 23

<2.0

<0.1

0__

____

____ 42 2 2 2 1 2 <1

<0.1 <1 3 5 2

1222

1059

2291 61 <1 3 <3

Cod

e :L

OVE

MC

Lov

elac

e R

espi

rato

ry R

esea

rch

Inst

itute

Pho

ne :(

505)

348

-960

0 F

ax :(

505)

348

-498

0Th

ese

resu

lts a

re s

ubm

itted

pur

suan

t to

our c

urre

nt T

erm

s, C

ondi

tions

and

Lim

itatio

ns a

nd L

abor

ator

y P

ricin

g P

olic

y. N

o re

spon

sibi

lity

or li

abili

ty is

ass

umed

for t

he m

anne

r in

whi

ch th

ese

resu

lts a

re u

sed

or in

terp

rete

d.

Eval

uate

d B

y: D

avid

F. F

ryck

i, C

LS -

For

que

stio

ns a

bout

this

repo

rt, p

leas

e ca

ll 88

8-43

7-48

84.

erla

bgt1

.frx

Rev

. 05/

19/1

1


159

Oil

Type

: SA

E 40

(GN

_032

)

P.O

. : J

K110

737

Lab

Num

ber :

V11

9041

8

11/0

2/12

Page

1

11:0

1:43

MO

NIT

OR

: D

ata

for m

achi

ne a

nd/o

r flu

id c

ondi

tion

shou

ld b

e no

ted

and

mon

itore

d.So

ot c

onte

nt is

hig

h. P

leas

e pr

ovid

e eq

uipm

ent m

ake

and

mod

el a

s w

ell a

s th

e fu

ll na

me

and

grad

e of

the

lubr

ican

t in

serv

ice.

Add

ition

al s

ampl

e is

nee

ded

to h

elp

esta

blis

h tre

nd.

Res

ampl

e at

half

norm

al in

terv

al.

Tom

Hol

mes

Love

lace

Res

pira

tory

Res

earc

h In

stitu

te24

25 R

idge

cres

t Driv

e, S

E

Alb

uque

rque

, NM

871

08

10/2

2/12

10/2

9/12

10/3

0/12

11/0

2/12

Ship

ped

:R

ecei

ved:

Prin

ted:

Sam

pled

:

Uni

t Typ

e : E

ngin

e, D

iese

l (G

N_D

E001

)

* =

exce

eds

Cau

tion

limit

** =

exc

eeds

Ala

rm li

mit

101

Cor

pora

te P

lace

, Val

lejo

, CA

9459

0w

ww

.her

guth

.com

ISO

900

1:20

08 a

nd IS

O/IE

C 1

7025

:200

5 C

ertif

ied

ID: F

Y09-

111-

22O

CT2

012

- FY0

9-11

1-22

oct2

012-

oil,

Die

sel E

ngin

e

Lab

Num

ber

Sam

ple

Dat

eM

inim

umM

axim

umV1

1904

1810

/22/

12

Com

para

tive

Gra

phic

Ana

lysi

s

Sodi

um

Silic

on

Nic

kel

Tin

Lead

Cop

per

Chr

omiu

m

Alu

min

umIron

Sulfi

natio

n

Oxi

datio

n

Soot

Typi

cal

War

ning

O

ver

Max

Uni

t Tim

e (H

R)

Flui

d Ti

me

(HR

)Vi

s @

100

Deg

CTB

N m

g K

OH

/gFT

IR Soot

% w

t.O

xida

tion

Abs/

cmW

ater

FTI

R %

Vol

Sulfi

natio

n Ab

s/Fu

el %

Vol

Gly

col %

Vol

Met

als

Iron

ppm

Alum

inum

ppm

Chr

omiu

m p

pmC

oppe

r ppm

Lead

ppm

Tin

ppm

Nic

kel p

pmSi

lver

ppm

Antim

ony

ppm

Silic

on p

pmSo

dium

ppm

Boro

n pp

mZi

nc p

pmPh

osph

orus

ppm

Cal

cium

ppm

Mag

nesi

um p

pmBa

rium

ppm

Mol

ybde

num

ppm

Pota

ssiu

m p

pm

12.5

03.

0016

.80

3.0 30

0.20 30 2.5

0.20 66 4 4 6 4 4 44.

5 20 50 50

1625 0

14.4

34.

67__

____

____

*2.8 10

<0.1

0 16<2

.0<0

.10

____

____

__ 29 2 1 1 1 2 1<0

.1 <1 3 4 211

9910

0822

96 7 <1 <1 <3

Cod

e :L

OVE

MC

Lov

elac

e R

espi

rato

ry R

esea

rch

Inst

itute

Pho

ne :(

505)

348

-960

0 F

ax :(

505)

348

-498

0Th

ese

resu

lts a

re s

ubm

itted

pur

suan

t to

our c

urre

nt T

erm

s, C

ondi

tions

and

Lim

itatio

ns a

nd L

abor

ator

y P

ricin

g P

olic

y. N

o re

spon

sibi

lity

or li

abili

ty is

ass

umed

for t

he m

anne

r in

whi

ch th

ese

resu

lts a

re u

sed

or in

terp

rete

d.

Eval

uate

d B

y: B

obby

R L

icu,

Sen

ior E

valu

ator

- F

or q

uest

ions

abo

ut th

is re

port

, ple

ase

call

888-

437-

4884

.er

labg

t1.fr

x R

ev. 0

5/19

/11


160

Oil

Type

: SA

E 40

(GN

_032

)

P.O

. : J

K120

015

Lab

Num

ber :

V11

8675

2

10/0

9/12

Page

1

12:1

8:10

AB

NO

RM

AL:

Abn

orm

al re

sults

for f

luid

are

pre

sent

. E

quip

men

t app

ears

sat

isfa

ctor

y.So

ot c

onte

nt is

hig

h. F

TIR

indi

cate

s oi

l is

sulfi

nate

d. D

rain

oil

and

chan

ge fi

lter(s

). C

heck

for p

rope

rco

mbu

stio

n pr

oper

ties

(exh

aust

bac

k pr

essu

re, o

pera

ting

tem

pera

ture

s, w

orn/

brok

en ri

ngs,

exce

ssiv

e id

ling,

hun

g va

lves

, im

prop

er fu

el s

ettin

gs, a

ir in

take

rest

rictio

ns).

Add

ition

al s

ampl

e is

need

ed to

hel

p es

tabl

ish

trend

. R

esam

ple

at h

alf n

orm

al in

terv

al.

Tom

Hol

mes

Love

lace

Res

pira

tory

Res

earc

h In

stitu

te24

25 R

idge

cres

t Driv

e, S

E

Alb

uque

rque

, NM

871

08

10/0

3/12

10/0

4/12

10/0

5/12

10/0

9/12

Ship

ped

:R

ecei

ved:

Prin

ted:

Sam

pled

:

Uni

t Typ

e : E

ngin

e, D

iese

l (G

N_D

E001

)

* =

exce

eds

Cau

tion

limit

** =

exc

eeds

Ala

rm li

mit

101

Cor

pora

te P

lace

, Val

lejo

, CA

9459

0w

ww

.her

guth

.com

ISO

900

1:20

08 a

nd IS

O/IE

C 1

7025

:200

5 C

ertif

ied

ID: F

Y09-

111-

03O

CT1

2-O

IL -

FY09

-111

-03O

CT2

012-

OIL

, Die

sel E

ngin

e

Lab

Num

ber

Sam

ple

Dat

eM

inim

umM

axim

umV1

1867

5210

/03/

12

Com

para

tive

Gra

phic

Ana

lysi

s

Sodi

um

Silic

onTin

Lead

Cop

per

Chr

omiu

m

Alum

inumIro

n

Sulfi

natio

n

Oxi

datio

n

Soot

TBN

Und

er M

in

War

ning

Typ

ical

Typ

ical

War

ning

Ove

r Max

Uni

t Tim

e (H

R)

Flui

d Ti

me

(HR

)Vi

s @

100

Deg

CTB

N m

g K

OH

/gFT

IR Soot

% w

t.O

xida

tion

Abs/

cmW

ater

FTI

R %

Vol

Sulfi

natio

n Ab

s/Fu

el %

Vol

Gly

col %

Vol

Met

als

Iron

ppm

Alum

inum

ppm

Chr

omiu

m p

pmC

oppe

r ppm

Lead

ppm

Tin

ppm

Nic

kel p

pmSi

lver

ppm

Antim

ony

ppm

Silic

on p

pmSo

dium

ppm

Boro

n pp

mZi

nc p

pmPh

osph

orus

ppm

Cal

cium

ppm

Mag

nesi

um p

pmBa

rium

ppm

Mol

ybde

num

ppm

Pota

ssiu

m p

pm

12.5

03.

0016

.80

3.0 30

0.20 30 2.5

0.20 67 4 4 6 4 4 44.

5 20 50 50

1376 0

14.9

55.

08__

____

____

**3.

7 19<0

.10

**33

<2.0

<0.1

0__

____

____ 40 2 2 2 1 2 <1

<0.1 1 2 2 1

1155 995

2407 7 <1 1 <3

Cod

e :L

OVE

MC

Lov

elac

e R

espi

rato

ry R

esea

rch

Inst

itute

Pho

ne :(

505)

348

-960

0 F

ax :(

505)

348

-498

0Th

ese

resu

lts a

re s

ubm

itted

pur

suan

t to

our c

urre

nt T

erm

s, C

ondi

tions

and

Lim

itatio

ns a

nd L

abor

ator

y P

ricin

g P

olic

y. N

o re

spon

sibi

lity

or li

abili

ty is

ass

umed

for t

he m

anne

r in

whi

ch th

ese

resu

lts a

re u

sed

or in

terp

rete

d.

Eval

uate

d B

y: B

obby

R L

icu,

Sen

ior E

valu

ator

- F

or q

uest

ions

abo

ut th

is re

port

, ple

ase

call

888-

437-

4884

.er

labg

t1.fr

x R

ev. 0

5/19

/11


161

Oil

Type

: SA

E 40

(GN

_032

)

P.O

. : J

K120

015

Lab

Num

ber :

V11

9270

3

11/1

6/12

Page

1

10:4

6:39

AB

NO

RM

AL:

Abn

orm

al re

sults

for f

luid

are

pre

sent

. E

quip

men

t app

ears

sat

isfa

ctor

y.So

ot c

onte

nt is

hig

h. L

evel

s m

ay b

e du

e to

oil

serv

ice

time

(not

pro

vide

d).

Dra

in o

il an

d ch

ange

filte

r(s).

Add

ition

al s

ampl

e is

nee

ded

to h

elp

esta

blis

h tre

nd.

Res

ampl

e at

hal

f nor

mal

inte

rval

.Pl

ease

pro

vide

equ

ipm

ent m

ake

and

mod

el a

s w

ell a

s th

e fu

ll na

me

and

grad

e of

the

lubr

ican

t in

serv

ice.

Tom

Hol

mes

Love

lace

Res

pira

tory

Res

earc

h In

stitu

te24

25 R

idge

cres

t Driv

e, S

E

Alb

uque

rque

, NM

871

08

11/1

2/12

11/1

3/12

11/1

4/12

11/1

6/12

Ship

ped

:R

ecei

ved:

Prin

ted:

Sam

pled

:

Uni

t Typ

e : E

ngin

e, D

iese

l (G

N_D

E001

)

* =

exce

eds

Cau

tion

limit

** =

exc

eeds

Ala

rm li

mit

101

Cor

pora

te P

lace

, Val

lejo

, CA

9459

0w

ww

.her

guth

.com

ISO

900

1:20

08 a

nd IS

O/IE

C 1

7025

:200

5 C

ertif

ied

ID: F

Y09-

111-

12N

OV1

2-O

IL -

FY09

-111

-12N

ov20

12-O

il, D

iese

l Eng

ine

Lab

Num

ber

Sam

ple

Dat

eM

inim

umM

axim

umV1

1927

0311

/12/

12

Com

para

tive

Gra

phic

Ana

lysi

s

Sodi

um

Silic

onTin

Lead

Cop

per

Chr

omiu

m

Alum

inumIro

n

Sulfi

natio

n

Oxi

datio

n

Soot

TBN

Und

er M

in

War

ning

Typ

ical

Typ

ical

War

ning

Ove

r Max

Uni

t Tim

e (H

R)

Flui

d Ti

me

(HR

)Vi

s @

100

Deg

CTB

N m

g K

OH

/gFT

IR Soot

% w

t.O

xida

tion

Abs/

cmW

ater

FTI

R %

Vol

Sulfi

natio

n Ab

s/Fu

el %

Vol

Gly

col %

Vol

Met

als

Iron

ppm

Alum

inum

ppm

Chr

omiu

m p

pmC

oppe

r ppm

Lead

ppm

Tin

ppm

Nic

kel p

pmSi

lver

ppm

Antim

ony

ppm

Silic

on p

pmSo

dium

ppm

Boro

n pp

mZi

nc p

pmPh

osph

orus

ppm

Cal

cium

ppm

Mag

nesi

um p

pmBa

rium

ppm

Mol

ybde

num

ppm

Pota

ssiu

m p

pm

12.5

03.

0016

.80

3.0 30

0.20 30 2.5

0.20 66 4 4 6 4 4 44.

5 20 50 50

1889 0

14.4

04.

83__

____

____

*3.0 11

<0.1

0 18<2

.0<0

.10

____

____

__ 26 2 1 1 1 1 <1<0

.1 <1 2 4 <111

85 923

2264 6 <1 <1 <3

Cod

e :L

OVE

MC

Lov

elac

e R

espi

rato

ry R

esea

rch

Inst

itute

Pho

ne :(

505)

348

-960

0 F

ax :(

505)

348

-498

0Th

ese

resu

lts a

re s

ubm

itted

pur

suan

t to

our c

urre

nt T

erm

s, C

ondi

tions

and

Lim

itatio

ns a

nd L

abor

ator

y P

ricin

g P

olic

y. N

o re

spon

sibi

lity

or li

abili

ty is

ass

umed

for t

he m

anne

r in

whi

ch th

ese

resu

lts a

re u

sed

or in

terp

rete

d.

Eval

uate

d B

y: D

avid

F. F

ryck

i, C

LS -

For

que

stio

ns a

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