addendum no. 7 november 01, 2017 project: city of...

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ADDENDUM NO. 7 November 01, 2017

PROJECT: CITY OF SEYMOUR WATER TREATMENT PLANT The following changes and/or additions shall be made to the Plans, Specifications, and Contract Documents for the above referenced project. Bidder shall acknowledge receipt of this Addendum by signing below and returning this Addendum with the Bid.

I. Plan Sheets – The Plan Sheets have been revised to show the following:

a. Sheet A-7 – Evap Pond Berm Details

i. Detail views of the Pond Berms have been included in the attached plan sheet.

b. Sheet 06 – Concentrator Layout i. Changes have been made to the piping from the proposed head tank to the

pump skid. ii. The 4” tee and two automated valves are to be provided by the RO vendor

as part of the pump skid. iii. This change was made to allow the concentrator to perform its pre-flush

and post-flush with raw water. iv. Pre-flush and post-flush cycles shall only utilize raw well water.

Utilization of the existing RO concentrate for pre- and/or post-flush will not be allowed.

c. Sheet 9 – Pump Skid Concentrator “A” P & ID i. The feed pump total dynamic head has been updated from 150 psi to 250

psi.

d. Sheet 10 – Concentrator “B” P & ID i. The feed pump total dynamic head has been updated from 150 psi to 250

psi.

e. Sheet 18 – Control and SCADA Plan i. The control panel for the Concentrators has been updated and moved.

ii. The automated valves shall be controlled by the Concentrators’ control panel.

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II. Contract Documents – The Contract Documents have been revised to show the following:

a. Bid Schedule – The Bid Schedule has been revised i. Bid Items 3 through 8

1. Bid Item 3 – Excavation to Finished Grade a. This item includes the provision of all necessary labor and

equipment to provide the Excavation to Finished Grade as specified and shown on the plans.

b. Item shall be paid as a Lump Sum

2. Bid Item 4 – Over Excavate Berm Area a. This item includes the provision of all necessary labor and

equipment to provide the Over Excavation of the Berm Area as specified and shown on the plans. Detail examples of this line item are shown in the attached plan sheet A-7.


3. Bid Item 5 – Excavate Borrow Area a. This item includes the provision of all necessary labor and

equipment to provide the Excavation of the Borrow Area as specified and shown on the plans. This includes the excavation of all the material from 0-6 feet deep.

b. Item shall be paid as a Lump Sum 4. Bid Item 6 – Fill to Pond Floor

a. This item includes the provision of all necessary labor and equipment to construct the pond floor to the grade as specified and shown on the plans. Contractors may use sand material to perform this line item.


5. Bid Item 7 – Placement of Excavated Borrow (Berms) a. This item includes the provision of all necessary labor and

equipment to provide the Placement of the Excavation Borrow into the berms as specified and shown on the plans.


6. Bid Item 8 – Waste Material a. This item includes the provision of all necessary labor and

equipment to provide placement of Waste Material as specified and shown on the plans.


ii. All bids must use the new Bid Schedule labeled “Revised – Addendum #7”

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III. Additional Information – The following information is intended to supplement and become part of the Contract.

a. Soil Analysis – Additional Information i. Soil analysis data from soil samples taken on site are included as an

attachment. ii. A map of the sample locations in included on Sheet A-7 attached to this

addendum.

b. Lagoon Liner Ballast Tubes – Additional Clarification i. Ballasts tubes may be constructed out of 30 mil HDPE liner.

c. RO Concentrators – Additional Clarification

i. RO vendors shall meet and match the attached pretreatment process and chemicals.

ii. The system shall use Vitec 158 anti-scalant. The system already utilizes sulfuric acid for pH adjustment. The projection data and chemical uses shown on the attached Overall Recovery projection shall be utilized. This proposal includes anti-scalant and pH adjustment on the existing RO only to carry through to the concentrator. Chemical Injection equipment shown at the concentrators will remain for future use.

iii. Raw water chemistry before it is processed by the existing RO units is attached for RO vendors review.

d. General Contractors and RO Vendors – Additional Clarification i. RO vendors must be pre-qualified per Specification 11.04.01 part 1.7.

ii. RO vendors must submit qualifying information to the Project Engineer, including but not limited to: documentation of similar projects in terms of scope, contract amount, and industry type, references, examples of products and materials, examples of product controls, etc.

iii. RO vendors must have experience in municipal water supply or public water supply projects.

iv. The City of Seymour and the Project Engineer reserve the right to deny pre-qualification. Final approval must come from the project engineer.

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Prepared by: JACOB & MARTIN, LLC. Consulting Engineers 3465 Curry Lane Abilene, Texas 79606 _________________________________ Bidder’s Acknowledgment _________________________________ Date

B-2

For all Labor, Materials, Equipment and Incidentals to Furnish and Deliver the Following:Bid Description Estimated Unit Price ExtendedItem (Price to be Written) Qty. Unit (Numbers) Amount

1 MOBILIZATION, BONDS, AND INSURANCE 1 LS

2 WTP EQUIPMENT 1 LS

3 EXCAVATION TO FINISHED GRADE 1 LS

4 OVER EXCAVATE BERM AREA 1 LS

5 EXCAVATE BORROW AREA 1 LS

6 FILL TO POND FLOOR 1 LS

7 PLACEMENT OF EXCAVATED BORROW (BERMS) 1 LS

8 WASTE MATERIAL 1 LS

9 EVAPORATION POND LEAK DETECTION PIPING 6,312 LF

10 LEAK DETECTION SAMPLING PORT 3 EA

11 60 MIL TEXTURED HDPE SYNTHETIC LINER 1 LS

12 8" CONCENTRATE LINE 2,050 LF

13 8" CONCENTRATE CONNECTION AT PLANT 1 EA

14 8" PLUG VALVES 6 EA

15 POND TRANSFER PIPES 4 EA

16 EVAPORATION POND FENCE 5,100 LF

17 PHOENIX WETLAND BIRD WAILERS or equal 3 EA

18 ELECTRICAL REROUTE THROUGH POND AREA 1 LS

19 WTP ELECTRICAL (NEW EQUIPMENT INTEGRATION) 1 LS

20 WTP CONTROL AND SCADA UPGRADES 1 LS

21 POND INLETS 3 EA

22 6" C900 DR25 PVC WATERLINE 2,430 LF

23 2 - 6" WL RECONNECTIONS 2 EA

TOTAL BASE BID (ITEMS 1-23)

CITY OF SEYMOUR

BASE BID SCHEDULEWTP IMPROVEMENTS

TWDB PROJECT # 62693

Show prices in words and numerals. Words take precedence over numerals. Round off unit prices to two decimal places only.These bid prices must include furnishing & delivering all materials, profits & incidentals to cover the items called for in the Contract Documents. In case of mathematical error in extensions, (Unit Prices) prevails.

*REVISED - ADDENDUM #7*

B-2

Deductible Alternate Bid

D-1 60 MIL TEXTURED HDPE SYNTHETIC LINER 1 LS

D-2 LEAK DETECTION SAMPLING PORT 3 EA

D-3 EVAPORATION POND LEAK DETECTION PIPING 6,312 LF

Additions Alternate Bid

A-1 3' CLAY LINER FOR EVAPORATION POND 1 LS

A-2 BACKUP GENERATOR 1 LS

A-3 EXISTING RO SKID MEMBRANES 288 EA

A-4 EXISTING RO SKID MEMBRANE REPLACEMENT 1 LS

TOTAL CONTRACT PRICE (BB-D1-D-2-D3 + A-1 + A-2 + A-3 + A-4)

Seymour WTP Improvements Soil Test Results

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Test Pit

Sample ID

Soil D

epth, Ft.

Soil

Descriptio

n

Liquid Lim

it

Plastic L

imit

Plasticit

y Index

Ret No. 4

Ret No. 4

0

Ret #200

1 1A 0.0 - 3.5 Brown Silty Sand (SM) Nonplastic Nonplastic Nonplastic 0 2 58.8

1 1B 3.5 - 4.0 Gray Fat Clay (CH) 56 19 37 0 0 11.2

1 1C 4.0 - 6.0Gray Fat Clay with Sand and white particles (CH) 52 20 32 0 3 17.6

1 1D 6.0 - 8.0 Gray Fat Clay (CH) 55 21 34 0 2 9.9

2 2A 0.0 - 3.3 Reddish Brown Silty Sand (SM) Nonplastic Nonplastic Nonplastic 0 7 87.1

2 2B 3.3 - 5.0 Gray Fat Clay with Sand (CH) 51 19 32 0 2 19.7

2 2C 5.0 - 6.0 Gray Lean Clay with white particles (CL) 46 17 29 0 3 18.9

3 3A 0.0 - 3.5 Tan Silty Sand (SM) Nonplastic Nonplastic Nonplastic 0 5 86.4

3 3B 3.5 - 4.0 Light Tan & Brown Lean Clay with Sand (CL) 42 17 25 0 1 17.6

3 3C 4.0 - 6.3 Orangish Lean Clay (CL) 37 18 19 0 1 6.7

4 4A 0.0 - 3.5 Tan Silty Sand (SM) Nonplastic Nonplastic Nonplastic 0 5 87.8

4 4B 3.5 - 4.5 Dark Gray Fat Clay (CH) 62 23 39 0 1 6.1

4 4C 4.5 - 6.3Dark Gray & Brown Fat Clay with white particles (CH) 65 22 43 0 1 6.7


5 5B 3.8 - 4.5Tan lightly cemented Silty, Clayey Sand with rust colored stains (SC-SM) 25 19 6 0 2 54.8

5 5C 4.5 - 5.8 Gray Fat Clay (CH) 71 24 47 0 0 9.3


6 6B 2.7 - 5.0 Yellow, Brown & Gray Fat Clay (CH) 66 23 43 0 0 10.5

6 6C 5.0 - 6.0 Orange Lean Clay with Sand (CL-ML) 24 17 7 1 4 18.8

7 7A 0.0 - 4.0 Reddish Silty Sand (SM) Nonplastic Nonplastic Nonplastic 0 3 87.4

Seymour WTP Improvements Soil Test Results

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Test Pit

Sample ID

Soil D

epth, Ft.

Soil

Descriptio

n

Liquid Lim

it

Plastic L

imit

Plasticit

y Index

Ret No. 4

Ret No. 4

0

Ret #200

7 7B 4.0 - 4.5Tan Sandy Lean Clay with rust colored stains (CL) 31 20 11 0 0 32.1

7 7C 4.5 - 6.1 Gray Fat Clay (CH) 61 23 38 0 1 8.4


8 8B 2.0 - 4.5 Gray Sandy Lean Clay (CL) 42 17 25 0 2 33.1

8 8C 4.5 - 6.1Brown and Yellow mottled Lean Clay with Sand (CL) 47 20 27 0 4 19.5

9 9A 0.0 - 3.5 Reddish Orange Silty Sand (SM) Nonplastic Nonplastic Nonplastic 0 4 77.4

9 9B 3.5 - 5.5 Reddish with Gray streaks Lean Clay (CL) 46 19 27 0 1 14.4

9 9C 5.5 - 5.9Reddish with Gray streaks and white particles Fat Clay (CH) 50 19 31 0 1 14.1

10 10A 0.0 - 3.5Tannish transitioning to Orangish Silty Sand (SM) Nonplastic Nonplastic Nonplastic 0 2 86.8

10 10B 3.5 - 5.8 Reddish Orange Lean Clay with sand (CL) 33 16 17 1 7 25.3

10 10C 5.8 - 7.2 Reddish Clayey Sand (SC) 28 16 12 4 37 57.2


11 11B 4.0 - 4.5 Yellow, Red & Tan mottled Clayey Sand (SC) 37 17 20 0 1 53.1

11 11C 4.5 - 7.0 Gray Lean Clay with Sand (CL) 48 20 28 0 1 25.3

12 12A 0.0 - 7.6 Reddish Tan Silty Sand (SM) Nonplastic Nonplastic Nonplastic 0 5 86.9


13 13B 3.5 - 4.5 Reddish Sandy Lean Clay (CL) 29 14 15 0 1 46.1

13 13C 4.5 - 6.0 Red and Gray Sandy Lean Clay (CL) 39 17 22 0 2 44.6

13 13D 6.0 - 6.7 Whitish Lean Clay with Sand (CL) 48 20 28 0 7 21.4

Project: City of Seymour

Recovery: 92% Date: 26-Oct-17Customer: Jacob Martin Prepared by: Tim KirkEngineer: Tim Kirk Water Analysis date: 18-Feb-15Note: Overall Recovery

CORPORATE OFFICES

Avista Technologies, Inc. Global Headquaters Avista Technologies (UK) Ltd140 Bosstick Blvd 13 Nasmyth Square, Houstoun Ind EstateSan Marcos, CA 92069 Livingston, EH54 5GG, UK

Tel: +1.760.744.0536 Tel: +44 (0) 131 449 6677

AdvisorCi Version 4.4.6 Antiscalant data file 0

Technical Summary

Water Chemistry Scaling Potential

Cations(mg/l) EnteredFeed

AdjustedFeed

CalculatedConcentrate

Sodium 169.00 178.42 2196.57Potassium 5.17 5.17 63.05Calcium 80.30 80.30 995.12Magnesium 52.10 52.10 645.65Iron 0.03 0.03 0.30Manganese 0.00 0.00 0.00Barium 0.07 0.07 0.87Strontium 1.19 1.19 14.74Aluminium 0.00 0.00 0.00Ammonium 0.00 0.00 0.00Anions(mg/l) Chloride 175.00 175.00 2159.94Sulfate 158.00 402.87 5012.26Bicarbonate 468.63 158.11 1915.83Carbonate 0.34 0.02 6.80Nitrate 13.20 13.20 152.87Fluoride 1.55 1.55 18.87Phosphate 0.11 0.11 1.29Silica 11.10 11.10 137.99Carbon Dioxide 58.70 336.27 336.27TDS 1144.87 14085.05

Saturation Level EnteredFeed

AdjustedFeed


CCPP 13.08 -269.02 865.26mg/l Calcium Sulfate CaSO4 0.03 0.07 1.72x Barium Sulfate BaSO4 2.71 6.67 216.45x Strontium Sulfate SrSO4 0.03 0.06 2.03x Calcium Phosphate 0.00 0.00 0.03x Calcium Fluoride CaF2 0.01 0.00 1.62x Silica SiO2 0.11 0.11 1.43x Magnesium Hydroxide

Mg(OH)20.00 0.00 0.00x

Saturation Indices Langelier Saturation

Index (LSI)0.41 -1.64 1.12

Stiff and Davis Index (S&DI)

0.18 -1.86 0.89

System Parameters pH 7.60 6.00 6.92 Ionic Strength 0.02 0.02 0.28 Temperature (deg.F) 65.00 65.00 65.00

System Details Antiscalant DetailsUsed in Dosage and Feed Rate Calculations

Feedwater Flowrate Product Flowrate820.0USGPM 754.4USGPM

Concentrate Flowrate65.6USGPM

Operating Conditions% Recovery 92Hours per Day 24Days per Week 7Weeks per Year 52Load Factor 100.0%

Antiscalant Selected Avista 158Dosage 4.36mg/lUsage 42.85 lb per day.Dosed Strength 100%Pump Rate 4.41USGPD

11.59ml/m

There is one dosing pump and chemical tank per membrane train.With 1 trains, each pump will deliver 4.41USGPD

pH CorrectionChemical choice Sulfuric acidDosage: 239.7mg/l 100% H2SO4Delivered Concentration: 98% H2SO4Usage 2403.41 lb per day.Site Dilution: 100%Pump Rate 157.60USGPD

414.56ml/m


Executive Summary

Membrane and Water TypeFeed Source: Well WaterMembrane Manufacturer: DefaultMembrane Type: Standard BrackishWater Analysis Date: 18-Feb-15

Antiscalant Recommendations

Recommended Product Recommended Dosage System Recovery

Avista 158 4.4mg/l 92%

Dosed Strength Usage Per Day pH Correction

100% 42.85 lb Sulfuric acid

239.7mg/l

Saturation Indicies

0% 10% 20% 30% 40% 50% 60% 70% 80% 90% 100% 110% 120%Percent of Product Limit

CaCO3

CaSO4

BaSO4

SrSO4

CaF2

CaPO4

SiO2

MgOH

Fe

Mn

Al

While every effort has been made to ensure the accuracy of this program, no warranty, expressed or implied, is given as actual application of the products is outside the control of Avista Technologies.


Recovery: 92% Date: 26-Oct-17Customer: Jacob Martin Prepared by: Tim KirkEngineer: Tim Kirk Water Analysis date: 18-Feb-15Note: Overall Recovery

CORPORATE OFFICES


Tel: +1.760.744.0536 Tel: +44 (0) 131 449 6677



Recovery: 60% Date: 26-Oct-17Customer: Jacob Martin Prepared by: Tim KirkEngineer: Tim Kirk Water Analysis date: 18-Feb-15Note: Concentrator RO

CORPORATE OFFICES


Tel: +1.760.744.0536 Tel: +44 (0) 131 449 6677


Technical Summary



AdjustedFeed




AdjustedFeed


CCPP 136.78 62.95 907.79mg/l Calcium Sulfate CaSO4 0.60 0.61 1.84x Barium Sulfate BaSO4 62.24 64.20 204.93x Strontium Sulfate SrSO4 0.69 0.71 2.27x Calcium Phosphate 0.00 0.00 0.00x Calcium Fluoride CaF2 0.24 0.24 1.70x Silica SiO2 0.65 0.65 1.63x Magnesium Hydroxide

Mg(OH)20.00 0.00 0.00x


Index (LSI)0.16 0.11 1.26


0.02 -0.03 1.01







10.51ml/m


Executive Summary

Membrane and Water TypeFeed Source: Well WaterMembrane Manufacturer: DefaultMembrane Type: High Rej BrackishWater Analysis Date: 18-Feb-15



Avista 158 20.3mg/l 60%


100% 38.86 lb -

Saturation Indicies


CaCO3

CaSO4

BaSO4

SrSO4

CaF2

CaPO4

SiO2

MgOH

Fe

Mn

Al



Recovery: 60% Date: 26-Oct-17Customer: Jacob Martin Prepared by: Tim KirkEngineer: Tim Kirk Water Analysis date: 18-Feb-15Note: Concentrator RO

CORPORATE OFFICES


Tel: +1.760.744.0536 Tel: +44 (0) 131 449 6677



Recovery: 80% Date: 26-Oct-17Customer: Jacob Martin Prepared by: Tim KirkEngineer: Tim Kirk Water Analysis date: 18-Feb-15Note: Primary RO

CORPORATE OFFICES


Tel: +1.760.744.0536 Tel: +44 (0) 131 449 6677


Technical Summary



AdjustedFeed




AdjustedFeed


CCPP 13.08 -269.02 84.91mg/l Calcium Sulfate CaSO4 0.03 0.07 0.58x Barium Sulfate BaSO4 2.71 6.67 67.42x Strontium Sulfate SrSO4 0.03 0.06 0.63x Calcium Phosphate 0.00 0.00 0.00x Calcium Fluoride CaF2 0.01 0.00 0.22x Silica SiO2 0.11 0.11 0.56x Magnesium Hydroxide

Mg(OH)20.00 0.00 0.00x


Index (LSI)0.41 -1.64 0.10


0.18 -1.86 -0.05







6.06ml/m


pH CorrectionChemical choice Sulfuric acidDosage: 239.7mg/l 100% H2SO4Delivered Concentration: 98% H2SO4Usage 2381.43 lb per day.Site Dilution: 100%Pump Rate 156.16USGPD

410.77ml/m


Executive Summary

Membrane and Water TypeFeed Source: Well WaterMembrane Manufacturer: DefaultMembrane Type: Standard BrackishWater Analysis Date: 18-Feb-15



Avista 158 2.3mg/l 80%


100% 22.40 lb Sulfuric acid

239.7mg/l

Saturation Indicies


CaCO3

CaSO4

BaSO4

SrSO4

CaF2

CaPO4

SiO2

MgOH

Fe

Mn

Al



Recovery: 80% Date: 26-Oct-17Customer: Jacob Martin Prepared by: Tim KirkEngineer: Tim Kirk Water Analysis date: 18-Feb-15Note: Primary RO

CORPORATE OFFICES


Tel: +1.760.744.0536 Tel: +44 (0) 131 449 6677


Phone 903/984-0551 FAX 903/984-5914 e-Mail [email protected]

Page 1 of 102/18/2015Printed

Ana-Lab Corp. P.O. Box 9000 Kilgore, TX 75663

LELAP-accredited #02008

Account Project

685118SEYM-N

Report To

City of Seymour

Rick Garcia

301 North Washington

Seymour, TX 76380

Report

Employee Owned Integrity Caring Continual Improvement

Table of Contents

PagesDescriptionReport Name

This report consists of this Table of Contents and the following pages:

685118_r03_03_ProjectResults Ana-Lab Project P:685118 C:SEYM Project Results 8 685118_r03_10_ProjectRLHCompliance Ana-Lab Project P:685118 C:SEYM Project Limits Compliance Results Report 6 685118_r10_05_ProjectQC Ana-Lab Project P:685118 C:SEYM Project Quality Control Groups 16 685118_r99_09_CoC__1_of_1 Ana-Lab CoC SEYM 685118_1_of_1 7

37 Total Pages:

Corporate Shipping: 2600 Dudley Rd. Kilgore, TX 75662

Form rptTOC Created 10/06/2004 v1.1LDSClient v1.6.7.992

NELAP-accredited #T104704201

Report Page 1 of 38

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Phone 903/984-0551 FAX 903/984-5914 e-Mail [email protected] Owned Integrity Caring Continual Improvement

Results02/18/2015Printed: Page 1 of 8

Report To

City of Seymour

Rick Garcia


Seymour, TX 76380

685118SEYM-NAccount Project

Results

BottleCASFlagsRLUnitsResultsParameter

1369496 Well

02/02/2015 13:30:00ClientCollected by:

02/04/2015Received:

Drinking Water Affiliation: City of Seymour

Prepared: 02/05/2015 00:00:00

02/05/2015 00:00:00 QCgroupAnalyzed

sentSkeeter's Attentionz

Prepared: 02/09/2015 10:05:18

600/2-78-054 3.2.19 02/09/2015 10:05:18CAL QCgroupCalculated

3.59 1Sodium Adsorption Ratio - Liquid

Prepared: 02/09/2015 15:06:16

Calculation 02/09/2015 15:06:16CAL QCgroupCalculated

<0.0159 mg/L 0.0159Sulfide as Hydrogen Sulfidez

Prepared: 599920 02/05/2015 09:30:00

EPA 200.7 4.4 02/05/2015 15:47:55LPS QCgroup 600043Analyzed

<0.025 mg/L 0.025 7439-89-6Total Iron 09N

80.3 mg/L P0.500 7440-70-2Calcium 09N

5.17 mg/L P0.500 7440-09-7Potassium 09N

52.1 mg/L P0.500 7439-95-4Magnesium, Total 09N


<0.500 mg/L 0.500 7440-42-8Boron 09N

11.1 mg/L 0.500 7740-21-3Silicon Recoverable 09N


169 mg/L D2.50 7440-23-5Sodium 09N

Prepared: 599920 02/05/2015 09:30:00

EPA 200.7, Rev. 4.4 02/06/2015 14:19:27LPS QCgroup 600201Analyzed

1.19 mg/L 0.250 7440-24-6Strontium 09N

Prepared: 600855 02/11/2015 10:17:59


<0.025 mg/L 0.025 7439-89-6Dissolved Iron 03N

Prepared: 599920 02/05/2015 09:30:00

EPA 200.8 5.4 02/06/2015 18:29:00WOB QCgroup 600280Analyzed

<0.0005 mg/L 0.0005 7439-92-1Lead, Total 09N

0.0078 mg/L 0.005 7440-66-6Zinc, Total 09N

0.070 mg/L 0.005 7440-39-3Barium 09N

0.00408 mg/L 0.0005 7440-38-2Arsenic, Total 09N

0.000984 mg/L 0.0005 7440-47-3Chromium, Total 09N

0.0162 mg/L 0.001 7782-49-2Selenium, Total 09N

<0.001 mg/L 0.001 7439-96-5Manganese, Total 09N


Form rptPROJRES Created 10/13/2004 v1.2LDSClient v1.6.7.992 www.ana-lab.com

North Texas Region: 11105 Shady Trl Ste. 123 Dallas TX 75229-7633


Report Page 2 of 38

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Results


1369496 Well


02/04/2015Received:



<0.005 mg/L 0.005 7429-90-5Aluminum, Total 09N

0.00428 mg/L 0.001 7440-50-8Copper, Total 09N

<0.0002 mg/L 0.0002 7440-22-4Silver, Total 09N

<0.0005 mg/L 0.0005 7440-43-9Cadmium, Total 09N

Prepared: 599792 02/04/2015 14:15:00

EPA 245.1 3 02/05/2015 12:55:00WOB QCgroup 599968Analyzed

<0.200 ug/L 0.200 7439-97-6Mercury 07N

Prepared: 599986 02/04/2015 12:02:43

EPA 300.0 02/04/2015 12:02:43WJY QCgroup 599986Analyzed

1.55 mg/L 0.500Fluoride 01N

13.2 mg/L 0.100 14797-55-8Nitrate-Nitrogen Total 01N

Prepared: 600138 02/06/2015 02:05:20


175 mg/L 15.0Chloride 01N

Prepared: 599986 02/04/2015 12:02:43

EPA 300.0 2.1 02/04/2015 12:02:43WJY QCgroup 599986Analyzed

0.704 mg/L 0.500Bromide 01N

<0.152 mg/L 0.152Nitrite-Nitrogen, Total 01N

Prepared: 600138 02/06/2015 02:05:20


158 mg/L 15.0Sulfate 01N

Prepared: 599904 02/05/2015 09:55:00

EPA 350.1 2 02/05/2015 13:30:00RSV QCgroup 600021Analyzed

0.0767 mg/L 0.020Ammonia Nitrogen 08N

Prepared: 02/03/2015 18:00:00

EPA 904 (sub) 02/03/2015 18:00:00LLB QCgroupAnalyzed

sent to Outreac EHL1Radium 228 DW Subcontractz

Prepared: 599733 02/04/2015 11:15:00

SM 2130 B-94 02/04/2015 11:15:00CRG QCgroup 599733Analyzed

<1.00 NTU 1.00Turbidity 01N

Prepared: 599795 02/04/2015 12:20:00

SM 2320 B-97 02/04/2015 12:20:00BAA QCgroup 599795Analyzed

384 mg/L 1.00Total Alkalinity (as CaCO3) 01N

Prepared: 02/06/2015 09:35:57

SM 2340 B-97 02/06/2015 09:35:57CAL QCgroupCalculated

415 mg/L 0.500Total Hardness Ca/Mg Eq. CaCO3N

Prepared: 600058 02/06/2015 11:00:00





Report Page 3 of 38

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Results


1369496 Well


02/04/2015Received:


SM 2540 C-97 02/06/2015 11:00:00MLC QCgroup 600058Analyzed

820 mg/L 100Total Dissolved Solids 01N

Prepared: 600324 02/06/2015 10:45:00

SM 2540 D-97 02/06/2015 10:45:00RAH QCgroup 600324Analyzed

10.5 mg/L 2.00Total Suspended Solids 01N

Prepared: 02/05/2015 12:35:16

SM 4500-CO2 D, 20th 02/05/2015 12:35:16CAL QCgroupCalculated

383 mg/L 0.5Bicarbonate (as CaCO3)/Calc

<0.5 mg/L 0.5Hydroxide


1.43 mg/L 0.5Carbonate (as CaCO3)/Calc

19.2 mg/L 0.5Free Carbon Dioxide (Calc)


357 mg/L 0.5Carbon Dioxide (Calc)

Prepared: 599923 02/05/2015 10:10:00

SM 4500-H+ B-96 02/05/2015 10:10:00JTF QCgroup 599923Analyzed

7.6@14C SU 2.00Laboratory pH 01N

Prepared: 600851 02/11/2015 08:40:00

SM 4500-P E-97 02/11/2015 08:40:00CRG QCgroup 600851Analyzed

0.109 mg/L 0.010 7723-14-0Total Phosphorus 05N

Prepared: 600327 02/09/2015 10:40:00

SM 4500-S2¯ D-2000 02/09/2015 10:40:00BAA QCgroup 600327Analyzed

<0.015 mg/L 0.015Sulfide 06N

Prepared: 600116 02/05/2015 11:38:55

SM 5310 C-96 02/05/2015 11:38:55ALH QCgroup 600116Analyzed

2.36 mg/L 0.500Total Organic Carbon 04N

Prepared: 02/03/2015 18:00:00

SM 7500-Ra B (SC) 19th ED (sub) 02/03/2015 18:00:00LLB QCgroupAnalyzed


Prepared: 02/03/2015 18:00:00

Subcontract 02/03/2015 18:00:00LLB QCgroupAnalyzed

sent to Spectra SPANParticle Size Distributionz

1369497 Reject


02/04/2015Received:


Prepared: 12/31/1899 00:00:00

00:00:00 QCgroupAnalyzed





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Results


1369497 Reject


02/04/2015Received:


00:00:00 QCgroupAnalyzed

sentSkeeter's Attentionz

Prepared: 02/09/2015 10:05:18

600/2-78-054 3.2.19 02/09/2015 10:05:18CAL QCgroupCalculated

8.33 1Sodium Adsorption Ratio - Liquid

Prepared: 02/09/2015 15:06:16

Calculation 02/09/2015 15:06:16CAL QCgroupCalculated

<0.0159 mg/L 0.0159Sulfide as Hydrogen Sulfidez

Prepared: 599920 02/05/2015 09:30:00


<0.025 mg/L 0.025 7439-89-6Total Iron 08N

30.9 mg/L 0.500 7440-09-7Potassium 08N


1.13 mg/L 1.00 7440-42-8Boron 08N

63.2 mg/L 1.00 7740-21-3Silicon Recoverable 08N


458 mg/L 5.00 7440-70-2Calcium 08N

302 mg/L 5.00 7439-95-4Magnesium, Total 08N

939 mg/L 5.00 7440-23-5Sodium 08N

Prepared: 599920 02/05/2015 09:30:00


7.41 mg/L 0.500 7440-24-6Strontium 08N

Prepared: 600855 02/11/2015 10:28:07


<0.025 mg/L 0.025 7439-89-6Dissolved Iron 03N

Prepared: 599920 02/05/2015 09:30:00


<0.0005 mg/L 0.0005 7439-92-1Lead, Total 08N

<0.005 mg/L 0.005 7440-66-6Zinc, Total 08N

0.372 mg/L 0.005 7440-39-3Barium 08N

0.0238 mg/L 0.0005 7440-38-2Arsenic, Total 08N

0.00418 mg/L 0.0005 7440-47-3Chromium, Total 08N

0.0906 mg/L 0.001 7782-49-2Selenium, Total 08N

<0.001 mg/L 0.001 7439-96-5Manganese, Total 08N

<0.005 mg/L 0.005 7429-90-5Aluminum, Total 08N

0.0042 mg/L 0.001 7440-50-8Copper, Total 08N

<0.0002 mg/L 0.0002 7440-22-4Silver, Total 08N

<0.0005 mg/L 0.0005 7440-43-9Cadmium, Total 08N

Prepared: 599959 02/05/2015 10:45:00

EPA 245.1 3 02/09/2015 14:37:00WOB QCgroup 600450Analyzed

<0.200 ug/L 0.200 7439-97-6Mercury 09N





Report Page 5 of 38

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Results


1369497 Reject


02/04/2015Received:


Prepared: 599986 02/04/2015 12:27:21


979 mg/L 15.0Chloride 01N

7.76 mg/L 5.00Fluoride 01N

66.9 mg/L 1.00 14797-55-8Nitrate-Nitrogen Total 01N

Prepared: 599986 02/04/2015 12:27:21


<5.00 mg/L 5.00Bromide 01N

<1.00 mg/L 1.00Nitrite-Nitrogen, Total 01N

Prepared: 600138 02/06/2015 02:29:56


1680 mg/L 150Sulfate 01N

Prepared: 599904 02/05/2015 09:55:00

EPA 350.1 2 02/05/2015 13:30:00RSV QCgroup 600021Analyzed

0.0821 mg/L 0.020Ammonia Nitrogen 07N

Prepared: 02/03/2015 18:00:00

EPA 904 (sub) 02/03/2015 18:00:00 QCgroupAnalyzed


Prepared: 599733 02/04/2015 11:15:00

SM 2130 B-94 02/04/2015 11:15:00CRG QCgroup 599733Analyzed

<1.00 NTU 1.00Turbidity 01N

Prepared: 599795 02/04/2015 12:20:00

SM 2320 B-97 02/04/2015 12:20:00BAA QCgroup 599795Analyzed

1480 mg/L 1.00Total Alkalinity (as CaCO3) 01N

Prepared: 02/09/2015 10:05:18

SM 2340 B-97 02/09/2015 10:05:18CAL QCgroupCalculated

2390 mg/L 5.00Total Hardness Ca/Mg Eq. CaCO3N

Prepared: 600058 02/06/2015 11:00:00

SM 2540 C-97 02/06/2015 11:00:00MLC QCgroup 600058Analyzed

5370 mg/L 100Total Dissolved Solids 01N

Prepared: 600324 02/06/2015 10:45:00

SM 2540 D-97 02/06/2015 10:45:00RAH QCgroup 600324Analyzed

6.50 mg/L 2.00Total Suspended Solids 01N

Prepared: 02/05/2015 12:35:16


1480 mg/L 0.5Bicarbonate (as CaCO3)/Calc

<0.5 mg/L 0.5Hydroxide






Report Page 6 of 38

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Results


1369497 Reject


02/04/2015Received:



3.49 mg/L 0.5Carbonate (as CaCO3)/Calc

118 mg/L 0.5Free Carbon Dioxide (Calc)


1420 mg/L 0.5Carbon Dioxide (Calc)

Prepared: 599923 02/05/2015 10:10:00

SM 4500-H+ B-96 02/05/2015 10:10:00JTF QCgroup 599923Analyzed

7.4@14C SU 2.00Laboratory pH 01N

Prepared: 600851 02/11/2015 08:40:00

SM 4500-P E-97 02/11/2015 08:40:00CRG QCgroup 600851Analyzed

1.07 mg/L 0.050 7723-14-0Total Phosphorus 05N

Prepared: 600327 02/09/2015 10:40:00

SM 4500-S2¯ D-2000 02/09/2015 10:40:00BAA QCgroup 600327Analyzed

<0.015 mg/L 0.015Sulfide 06N

Prepared: 600116 02/05/2015 12:06:34

SM 5310 C-96 02/05/2015 12:06:34ALH QCgroup 600116Analyzed

6.46 mg/L 0.500Total Organic Carbon 04N

Prepared: 02/03/2015 18:00:00

SM 7500-Ra B (SC) 19th ED (sub) 02/03/2015 18:00:00 QCgroupAnalyzed


Prepared: 02/03/2015 18:00:00

Subcontract 02/03/2015 18:00:00 QCgroupAnalyzed

sent to Spectra SPANParticle Size Distributionz

Sample Preparation

1369496 Well 02/04/2015Received:

Prepared: 02/02/2015 13:38:00

02/02/2015 13:38:00Cli QCgroupAnalyzed

filteredClient Field Filtration (Onsite)N


<2 SUBottle pH 02z

02/04/2015 11:05:44CAL QCgroupCalculated

VerifiedSUB Shippedz

Prepared: 600619 02/10/2015 14:57:04

02/10/2015 14:57:04LPS QCgroup 600619Analyzed

COMPLETEDTransfer to ICP/MS 03z





Report Page 7 of 38

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Sample Preparation

1369496 Well 02/04/2015Received:

Prepared: 599920 02/05/2015 09:30:00

EPA 200.2 2.8 02/05/2015 09:30:00TES QCgroup 599920Analyzed

50/50 mlLiquid Metals Digestion 02N

Prepared: 599792 02/04/2015 14:15:00

EPA 245.1 3 02/04/2015 14:15:00PJD QCgroup 599792Analyzed

50/25 mlMercury Liquid Metals Digestion 02N

Prepared: 599904 02/05/2015 09:55:00

EPA 350.2, Rev. 2.0 02/05/2015 09:55:00JJH QCgroup 599904Analyzed

50/50 mlAmmonia Distillation 06N

Prepared: 599932 02/06/2015 12:16:52

SM 2540 D, 20th Ed. 02/06/2015 12:16:52RAH QCgroup 599932Analyzed

StartedTSS Set StartedN

1369497 Reject 02/04/2015Received:

Prepared: 02/02/2015 14:10:00

02/02/2015 14:10:00CLI QCgroupAnalyzed

filteredClient Field Filtration (Onsite)N


8(<2) SUBottle pH 02z

02/05/2015 04:05:52CAL QCgroupCalculated

VerifiedSUB Shippedz

Prepared: 600619 02/10/2015 14:57:04

02/10/2015 14:57:04LPS QCgroup 600619Analyzed

COMPLETEDTransfer to ICP/MS 03z

Prepared: 599920 02/05/2015 09:30:00

EPA 200.2 2.8 02/05/2015 09:30:00TES QCgroup 599920Analyzed

50/50 mlLiquid Metals Digestion 02N

Prepared: 599959 02/05/2015 10:45:00

EPA 245.1 3 02/05/2015 10:45:00CLK QCgroup 599959Analyzed

50/25 mlMercury Liquid Metals Digestion 02N

Prepared: 599904 02/05/2015 09:55:00

EPA 350.2, Rev. 2.0 02/05/2015 09:55:00JJH QCgroup 599904Analyzed

50/50 mlAmmonia Distillation 05N

Prepared: 599932 02/06/2015 12:16:52

SM 2540 D, 20th Ed. 02/06/2015 12:16:52RAH QCgroup 599932Analyzed

StartedTSS Set StartedN





Report Page 8 of 38

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Qualifiers:

D - Duplicate RPD was higher than expected P - Spike recovery outside control limits due to possible matrix

We report results on an 'As Received' or wet basis unless marked 'Dry Weight'. Unless otherwise noted, testing was performed at Ana-lab's

corporate laboratory that holds the following Federal and State certificates: Texas Department of Health Lead Firm Certificate 2110076, US

Department of Agriculture Soil Import Permit S-37592, Texas Commisson on Environmental Quality Drinking Water Laboratory Certificate

TX219, Texas Commission on Environmental Quality NELAP T104704201, Oklahoma Department of Environmental Quality Drinking

Water Certification Lab ID# D9913, EPA Lab Number TX00063, USEPA Approved Perchlorate Testing Lab, Oklahoma Department of

Environmental Quality Laboratory Certificate 8125, Arkansas Department of Environmental Quality Certification #03-070-0, Louisiana

Department of Environmental Quality Laboratory Certification (NELAP, LELAP) #02008, Louisiana Department of Health and Hospitals

Drinking Water (NELAP) # LA030020, US Department of Energy Approved, State of Kansas Department of Health and Environment

Waste Water and Solid/Hazardous Waste Cert. E-10365. The Accredited column designates accreditation by N -- NELAC, or z -- not

covered under NELAC scope of accreditation.

These analytical results relate to the sample tested. This report may NOT be reproduced EXCEPT in FULL without written approval of

Ana-Lab Corp. Unless otherwise specified, these test results meet the requirements of NELAC.

RL is the Reporting Limit (sample specific quantitation limit) and is at or above the Method Detection Limit (MDL). CAS is Chemical

Abstract Service number.





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Report To

Results and LimitsPage 1 of 602/18/2015Printed


City of Seymour

Rick Garcia


Seymour, TX 76380



ProjectAccount

685118SEYM

OutUnitsLimitOut Results *ResultsParameter FlagAlert

1369496 Well Collection: 02/02/2015 13:30:00

Column 'Limits' from EPA Drinking Water Limits (40 CFR 141 MCls -- see http://water.epa.gov/drink/contaminants/). Gross Beta Alert Limit is from 40 CFR

141.66 and IS NOT an MCL.

00:00:002/5/15Analyzed

Skeeter's Attention sent

600/2-78-054 3.2.19 CAL10:05:182/9/15Analyzed

Sodium Adsorption Ratio - Liquid 13.59

Calculation CAL15:06:162/9/15Analyzed

Sulfide as Hydrogen Sulfide mg/L<0.0159

EPA 200.7 4.4 LPS15:47:552/5/15Analyzed 600043

Calcium mg/L80.3 P

Magnesium, Total mg/L52.1 P

Potassium mg/L5.17 P

Total Iron mg/L<0.025 MCL 0.300

EPA 200.7 4.4 LPS14:19:272/6/15Analyzed 600201

Boron mg/L<0.500

Silicon Recoverable mg/L11.1

EPA 200.7 4.4 LPS14:57:472/6/15Analyzed 600250

Sodium mg/L169 D

EPA 200.7, Rev. 4.4 LPS14:19:272/6/15Analyzed 600201

Strontium mg/L1.19


Dissolved Iron mg/L<0.025 MCL 0.300

EPA 200.8 5.4 WOB18:29:002/6/15Analyzed 600280

Aluminum, Total mg/L<0.005 MCL 0.050

Arsenic, Total mg/L0.00408 MCL 0.010

Barium mg/L0.070 MCL 2.00

Cadmium, Total mg/L<0.0005 MCL 0.005

Chromium, Total mg/L0.000984 MCL 0.100

Copper, Total mg/L0.00428 MCL 1.00

Lead, Total mg/L<0.0005 MCL 0.015

Manganese, Total mg/L<0.001 MCL 0.050

Selenium, Total mg/L0.0162 MCL 0.050

Silver, Total mg/L<0.0002 MCL 0.100

Zinc, Total mg/L0.0078 MCL 5.00

Form rptRLHCompliance Created 06/03/2006 v1.0LDSClient v1.6.7.992

Corporate Shipping: 2600 Dudley Rd. Kilgore, TX 75662 North Texas Region: 11105 Shady Trl Ste. 123 Dallas TX 75229-7633

www.ana-lab.com


Report Page 10 of 38

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Report To



City of Seymour

Rick Garcia


Seymour, TX 76380



ProjectAccount

685118SEYM


1369496 Well Collection: 02/02/2015 13:30:00



EPA 245.1 3 WOB12:55:002/5/15Analyzed 599968

Mercury ug/L<0.200 MCL 2.00

EPA 300.0 WJY12:02:432/4/15Analyzed 599986

Fluoride mg/L1.55 MCL 2.00

Nitrate-Nitrogen Total mg/L13.2 MCL 10.0

EPA 300.0 WJY02:05:202/6/15Analyzed 600138

Chloride mg/L175 MCL 250

EPA 300.0 2.1 WJY12:02:432/4/15Analyzed 599986

Bromide mg/L0.704

Nitrite-Nitrogen, Total mg/L<0.152 MCL 1.00

EPA 300.0 2.1 WJY02:05:202/6/15Analyzed 600138

Sulfate mg/L158 MCL 250

EPA 350.1 2 RSV13:30:002/5/15Analyzed 600021

Ammonia Nitrogen mg/L0.0767

EPA 904 (sub) LLB18:00:002/3/15Analyzed

Radium 228 DW Subcontract sent to Outreac MCL 5.00

SM 2130 B-94 CRG11:15:002/4/15Analyzed 599733

Turbidity NTU<1.00 MCL 1.00

SM 2320 B-97 BAA12:20:002/4/15Analyzed 599795

Total Alkalinity (as CaCO3) mg/L384

SM 2340 B-97 CAL09:35:572/6/15Analyzed

Total Hardness Ca/Mg Eq. CaCO3 mg/L415

SM 2540 C-97 MLC11:00:002/6/15Analyzed 600058

Total Dissolved Solids mg/L820 MCL 500

SM 2540 D-97 RAH10:45:002/6/15Analyzed 600324

Total Suspended Solids mg/L10.5 MCL 2.00

SM 4500-CO2 D, 20th CAL12:35:162/5/15Analyzed

Bicarbonate (as CaCO3)/Calc mg/L383

Carbon Dioxide (Calc) mg/L357



www.ana-lab.com



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City of Seymour

Rick Garcia


Seymour, TX 76380



ProjectAccount

685118SEYM


1369496 Well Collection: 02/02/2015 13:30:00




Carbonate (as CaCO3)/Calc mg/L1.43

Free Carbon Dioxide (Calc) mg/L19.2

Hydroxide mg/L<0.5

SM 4500-H+ B-96 JTF10:10:002/5/15Analyzed 599923

Laboratory pH SU7.6@14C 6.50 - 98.50

SM 4500-P E-97 CRG08:40:002/11/15Analyzed 600851

Total Phosphorus mg/L0.109

SM 4500-S2¯ D-2000 BAA10:40:002/9/15Analyzed 600327

Sulfide mg/L<0.015

SM 5310 C-96 ALH11:38:552/5/15Analyzed 600116

Total Organic Carbon mg/L2.36

SM 7500-Ra B (SC) 19th ED (sub) LLB18:00:002/3/15Analyzed


Subcontract LLB18:00:002/3/15Analyzed

Particle Size Distribution sent to Spectra

1369497 Reject Collection: 02/02/2015 14:00:00



00:00:0012/31/99Analyzed

Skeeter's Attention sent

600/2-78-054 3.2.19 CAL10:05:182/9/15Analyzed

Sodium Adsorption Ratio - Liquid 18.33

Calculation CAL15:06:162/9/15Analyzed

Sulfide as Hydrogen Sulfide mg/L<0.0159

EPA 200.7 4.4 LPS15:58:102/5/15Analyzed 600043

Potassium mg/L30.9



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City of Seymour

Rick Garcia


Seymour, TX 76380



ProjectAccount

685118SEYM





EPA 200.7 4.4 LPS15:58:102/5/15Analyzed 600043

Total Iron mg/L<0.025 MCL 0.300

EPA 200.7 4.4 LPS14:28:412/6/15Analyzed 600201

Boron mg/L1.13

Silicon Recoverable mg/L63.2

EPA 200.7 4.4 LPS15:07:552/6/15Analyzed 600250

Calcium mg/L458

Magnesium, Total mg/L302

Sodium mg/L939


Strontium mg/L7.41


Dissolved Iron mg/L<0.025 MCL 0.300

EPA 200.8 5.4 WOB18:37:002/6/15Analyzed 600280

Aluminum, Total mg/L<0.005 MCL 0.050

Arsenic, Total mg/L0.0238 MCL 0.010

Barium mg/L0.372 MCL 2.00

Cadmium, Total mg/L<0.0005 MCL 0.005

Chromium, Total mg/L0.00418 MCL 0.100

Copper, Total mg/L0.0042 MCL 1.00

Lead, Total mg/L<0.0005 MCL 0.015

Manganese, Total mg/L<0.001 MCL 0.050

Selenium, Total mg/L0.0906 MCL 0.050

Silver, Total mg/L<0.0002 MCL 0.100

Zinc, Total mg/L<0.005 MCL 5.00

EPA 245.1 3 WOB14:37:002/9/15Analyzed 600450

Mercury ug/L<0.200 MCL 2.00

EPA 300.0 WJY12:27:212/4/15Analyzed 599986

Chloride mg/L979 MCL 250

Fluoride mg/L7.76 MCL 2.00

Nitrate-Nitrogen Total mg/L66.9 MCL 10.0

EPA 300.0 2.1 WJY12:27:212/4/15Analyzed 599986

Bromide mg/L<5.00



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City of Seymour

Rick Garcia


Seymour, TX 76380



ProjectAccount

685118SEYM





EPA 300.0 2.1 WJY12:27:212/4/15Analyzed 599986

Nitrite-Nitrogen, Total mg/L<1.00 MCL 1.00

EPA 300.0 2.1 WJY02:29:562/6/15Analyzed 600138

Sulfate mg/L1680 MCL 250

EPA 350.1 2 RSV13:30:002/5/15Analyzed 600021

Ammonia Nitrogen mg/L0.0821

EPA 904 (sub) 18:00:002/3/15Analyzed


SM 2130 B-94 CRG11:15:002/4/15Analyzed 599733

Turbidity NTU<1.00 MCL 1.00

SM 2320 B-97 BAA12:20:002/4/15Analyzed 599795

Total Alkalinity (as CaCO3) mg/L1480

SM 2340 B-97 CAL10:05:182/9/15Analyzed

Total Hardness Ca/Mg Eq. CaCO3 mg/L2390

SM 2540 C-97 MLC11:00:002/6/15Analyzed 600058

Total Dissolved Solids mg/L5370 MCL 500

SM 2540 D-97 RAH10:45:002/6/15Analyzed 600324

Total Suspended Solids mg/L6.50 MCL 2.00


Bicarbonate (as CaCO3)/Calc mg/L1480

Carbon Dioxide (Calc) mg/L1420

Carbonate (as CaCO3)/Calc mg/L3.49

Free Carbon Dioxide (Calc) mg/L118

Hydroxide mg/L<0.5

SM 4500-H+ B-96 JTF10:10:002/5/15Analyzed 599923

Laboratory pH SU7.4@14C 6.50 - 98.50

SM 4500-P E-97 CRG08:40:002/11/15Analyzed 600851

Total Phosphorus mg/L1.07



www.ana-lab.com



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City of Seymour

Rick Garcia


Seymour, TX 76380



ProjectAccount

685118SEYM





SM 4500-S2¯ D-2000 BAA10:40:002/9/15Analyzed 600327

Sulfide mg/L<0.015

SM 5310 C-96 ALH12:06:342/5/15Analyzed 600116

Total Organic Carbon mg/L6.46

SM 7500-Ra B (SC) 19th ED (sub) 18:00:002/3/15Analyzed


Subcontract 18:00:002/3/15Analyzed

Particle Size Distribution sent to Spectra

* Out Results are beyond the listed limit. Please verify with your consultant or regulatory authority whether these limits apply to this project.

Qualifiers:

D - Duplicate RPD was higher than expected P - Spike recovery outside control limits due to possible matrix

We report results on an 'As Received' or wet basis unless marked 'Dry Weight'. Unless otherwise noted, testing was performed at Ana-lab's

corporate laboratory that holds the following Federal and State certificates: Texas Department of Health Lead Firm Certificate 2110076, US

Department of Agriculture Soil Import Permit S-37592, Texas Commisson on Environmental Quality Drinking Water Laboratory Certificate

TX219, Texas Commission on Environmental Quality NELAP T104704201, Oklahoma Department of Environmental Quality Drinking Water

Certification Lab ID# D9913, EPA Lab Number TX00063, USEPA Approved Perchlorate Testing Lab, Oklahoma Department of Environmental

Quality Laboratory Certificate 8125, Arkansas Department of Environmental Quality Certification #03-070-0, Louisiana Department of

Environmental Quality Laboratory Certification (NELAP, LELAP) #02008, Louisiana Department of Health and Hospitals Drinking Water

(NELAP) # LA030020, US Department of Energy Approved, State of Kansas Department of Health and Environment Waste Water and

Solid/Hazardous Waste Cert. E-10365. The Accredited column designates accreditation by N -- NELAC, or z -- not covered under NELAC

scope of accreditation.

These analytical results relate to the sample tested. This report may NOT be reproduced EXCEPT in FULL without written approval of

Ana-Lab Corp. Unless otherwise specified, these test results meet the requirements of NELAC.

! Reporting Level above the listed target.



www.ana-lab.com



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Quality Control Page 1 of 1602/18/2015Printed




SEYM-NAccount Project

City of Seymour

Rick Garcia


Seymour, TX 76380

Report ToDW

685118

EPA 350.1 2Drinking Water 600021

Blank

FileUnitsMQLMDLReadingPrepSetParameter

Ammonia Nitrogen 599904 ND 0.00974 0.020 mg/L 115191783

CCV

FileOutLimits%Recover%UnitsKnownReadingParameter

Ammonia Nitrogen 2.12 2.00 mg/L 106 90.0 - 110 115191753







Duplicate

Limit%RPDUnitUnknownResultTypeSampleParameter

Ammonia Nitrogen 1369818 Duplicate 0.191 0.182 mg/L 4.83 20.0

ICV



LCS

OutFileLimitsRecover%UnitsKnownReadingPrepSetParameter

Ammonia Nitrogen 599904 2.14 2.00 mg/L 107 90.0 - 110 115191784

LCS Dup

Limit%RPDUnitsLCSD%LCS%Limits%KnownLCSDLCSPrepSetParameter

Ammonia Nitrogen 599904 2.14 2.04 2.00 90.0 - 110 107 102 mg/L 4.78 20.0

Mat. Spike

FileLimits %Recovery %UnitsKnownUnknownSpikeSampleParameter

Ammonia Nitrogen 1369818 2.43 0.182 2.00 mg/L 112 80.0 - 120 115191789

SM 2540 C-97Drinking Water 600058

Blank


Total Dissolved Solids 600058 ND 9.24 10.0 mg/L 115192833

ControlBlk


Total Dissolved Solids 600058 0.0001 grams 115192820

Duplicate


Total Dissolved Solids 1369086 Duplicate 120 108 mg/L 10.5 20.0


Form rptPROJQCGrpt Created 01/27/2005 v1.0LDSClient v1.6.7.992 www.ana-lab.com




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LCS


Total Dissolved Solids 600058 192 200 mg/L 96.0 85.0 - 115 115192834

Standard

FileOutLimits%Recover%UnitsKnownReadingSampleParameter

Total Dissolved Solids 92.0 100 mg/L 92.0 90.0 - 110 115192821

SM 2540 D-97Drinking Water 600324

Blank


Total Suspended Solids 600324 ND 2.00 2.00 mg/L 115199089

Total Suspended Solids 600324 ND 2.00 2.00 mg/L 115199123

Duplicate


Total Suspended Solids 1369400 Duplicate 136 134 mg/L 1.48 20.0

Total Suspended Solids 1369443 Duplicate 4.00 ND mg/L 200 20.0

Total Suspended Solids 1369492 Duplicate 52.9 47.1 mg/L 11.6 20.0

LCS


Total Suspended Solids 600324 49.0 50.0 mg/L 98.0 90.0 - 110 115199122

Standard


Total Suspended Solids 573062 98.0 100 mg/L 98.0 90.0 - 110 115199090

EPA 300.0Drinking Water 599986

Blank


Bromide 599986 ND 0.0075 0.050 mg/L 115190737

Chloride 599986 0.0078 0.0053 0.300 mg/L 115190737

Fluoride 599986 ND 0.00863 0.050 mg/L 115190737

Nitrate-Nitrogen Total 599986 ND 0.00185 0.020 mg/L 115190737

Nitrite-Nitrogen, Total 599986 ND 0.00717 0.0152 mg/L 115190737

CCV


Bromide 10.1 10.0 mg/L 101 90.0 - 110 115190734

Bromide 10.1 10.0 mg/L 101 90.0 - 110 115190744

Bromide 9.99 10.0 mg/L 99.9 90.0 - 110 115190745

Bromide 9.89 10.0 mg/L 98.9 90.0 - 110 115190754

Chloride 10.5 10.0 mg/L 105 90.0 - 110 115190734

Chloride 10.4 10.0 mg/L 104 90.0 - 110 115190744

Chloride 10.0 10.0 mg/L 100 90.0 - 110 115190745

Chloride 9.96 10.0 mg/L 99.6 90.0 - 110 115190754

Fluoride 9.99 10.0 mg/L 99.9 90.0 - 110 115190734

Fluoride 9.94 10.0 mg/L 99.4 90.0 - 110 115190744

Fluoride 9.92 10.0 mg/L 99.2 90.0 - 110 115190745

Fluoride 9.88 10.0 mg/L 98.8 90.0 - 110 115190754

Nitrate-Nitrogen Total 2.31 2.26 mg/L 102 90.0 - 110 115190734








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CCV



Nitrite-Nitrogen, Total 3.13 3.04 mg/L 103 90.0 - 110 115190734




LCS


Bromide 599986 0.982 1.00 mg/L 98.2 90.0 - 110 115190735

Chloride 599986 1.06 1.00 mg/L 106 90.0 - 110 115190735

Fluoride 599986 0.959 1.00 mg/L 95.9 90.0 - 110 115190735

Nitrate-Nitrogen Total 599986 0.232 0.226 mg/L 103 90.0 - 110 115190735

Nitrite-Nitrogen, Total 599986 0.304 0.304 mg/L 99.9 90.0 - 110 115190735

LCS Dup


Bromide 599986 0.982 0.981 1.00 90.0 - 110 98.2 98.1 mg/L 0.102 20.0

Chloride 599986 1.06 1.07 1.00 90.0 - 110 106 107 mg/L 0.939 20.0

Fluoride 599986 0.959 0.943 1.00 90.0 - 110 95.9 94.3 mg/L 1.68 20.0

Nitrate-Nitrogen Total 599986 0.232 0.231 0.226 90.0 - 110 103 102 mg/L 0.432 20.0

Nitrite-Nitrogen, Total 599986 0.304 0.308 0.304 90.0 - 110 99.9 101 mg/L 1.31 20.0

MS

Limit%RPDUnitsMSD%MS%LimitsKnownUNKMSDMSSampleParameter

Bromide 1369280 0.977 ND 1.00 80.0 - 120 97.7 mg/L 20.0

Chloride 1369280 0.953 ND 1.00 80.0 - 120 95.3 mg/L 20.0

Fluoride 1369280 0.908 ND 1.00 80.0 - 120 90.8 mg/L 20.0

Nitrate-Nitrogen Total 1369280 0.237 0.0102 0.226 80.0 - 120 105 mg/L 20.0

Nitrite-Nitrogen, Total 1369280 0.301 ND 0.304 80.0 - 120 99.0 mg/L 20.0

Bromide 1369281 9.68 0.124 10.0 80.0 - 120 95.6 mg/L 20.0

Chloride 1369281 15.1 5.84 10.0 80.0 - 120 92.6 mg/L 20.0

Fluoride 1369281 9.29 ND 10.0 80.0 - 120 92.9 mg/L 20.0

Nitrate-Nitrogen Total 1369281 2.16 0.0115 2.26 80.0 - 120 95.6 mg/L 20.0

Nitrite-Nitrogen, Total 1369281 2.97 ND 3.04 80.0 - 120 97.7 mg/L 20.0

MSD


Bromide 1369280 0.977 0.968 ND 1.00 80.0 - 120 97.7 96.8 mg/L 0.925 20.0

Chloride 1369280 0.953 0.950 ND 1.00 80.0 - 120 95.3 95.0 mg/L 0.315 20.0

Fluoride 1369280 0.908 0.918 ND 1.00 80.0 - 120 90.8 91.8 mg/L 1.10 20.0

Nitrate-Nitrogen Total 1369280 0.237 0.234 0.0102 0.226 80.0 - 120 105 104 mg/L 0.957 20.0

Nitrite-Nitrogen, Total 1369280 0.301 0.302 ND 0.304 80.0 - 120 99.0 99.3 mg/L 0.303 20.0

Bromide 1369281 9.68 9.75 0.124 10.0 80.0 - 120 95.6 96.3 mg/L 0.730 20.0

Chloride 1369281 15.1 15.0 5.84 10.0 80.0 - 120 92.6 91.6 mg/L 1.09 20.0

Fluoride 1369281 9.29 9.32 ND 10.0 80.0 - 120 92.9 93.2 mg/L 0.322 20.0

Nitrate-Nitrogen Total 1369281 2.16 2.19 0.0115 2.26 80.0 - 120 95.6 96.9 mg/L 1.35 20.0

Nitrite-Nitrogen, Total 1369281 2.97 2.92 ND 3.04 80.0 - 120 97.7 96.1 mg/L 1.65 20.0

EPA 300.0Drinking Water 600138

Blank


Chloride 600138 0.0081 0.0053 0.300 mg/L 115194717






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5






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Sulfate 600138 0.033 0.00775 0.300 mg/L * 115194717

CCV


Chloride 10.0 10.0 mg/L 100 90.0 - 110 115194714

Chloride 10.0 10.0 mg/L 100 90.0 - 110 115194731

Chloride 10.0 10.0 mg/L 100 90.0 - 110 115194742

Sulfate 9.99 10.0 mg/L 99.9 90.0 - 110 115194714

Sulfate 10.0 10.0 mg/L 100 90.0 - 110 115194731

Sulfate 10.0 10.0 mg/L 100 90.0 - 110 115194742

LCS


Chloride 600138 1.05 1.00 mg/L 105 90.0 - 110 115194715

Sulfate 600138 1.01 1.00 mg/L 101 90.0 - 110 115194715

LCS Dup


Chloride 600138 1.05 1.05 1.00 90.0 - 110 105 105 mg/L 0 20.0

Sulfate 600138 1.01 0.997 1.00 90.0 - 110 101 99.7 mg/L 1.30 20.0

MS


Chloride 1369936 174 132 50.0 80.0 - 120 84.0 mg/L 20.0

Sulfate 1369936 181 131 50.0 80.0 - 120 100 mg/L 20.0

Chloride 1369937 161 118 50.0 80.0 - 120 86.0 mg/L 20.0

Sulfate 1369937 161 117 50.0 80.0 - 120 88.0 mg/L 20.0

MSD


Chloride 1369936 174 172 132 50.0 80.0 - 120 84.0 80.0 mg/L 4.88 20.0

Sulfate 1369936 181 174 131 50.0 80.0 - 120 100 86.0 mg/L 15.1 20.0

Chloride 1369937 161 163 118 50.0 80.0 - 120 86.0 90.0 mg/L 4.55 20.0

Sulfate 1369937 161 161 117 50.0 80.0 - 120 88.0 88.0 mg/L 0 20.0


Blank


Mercury 599792 ND 0.072 0.100 ug/L 115190303

CCV


Mercury 5.09 5.000 ug/L 102 90.0 - 110 115190302

Mercury 5.10 5.000 ug/L 102 90.0 - 110 115190313

Mercury 5.11 5.000 ug/L 102 90.0 - 110 115190324

Mercury 4.92 5.000 ug/L 98.4 90.0 - 110 115190333

ICL


Mercury 19.8 20.00 ug/L 99.0 90.0 - 110 115190301

ICV


Mercury 5.31 5.000 ug/L 106 90.0 - 110 115190300






1

2

3

4

5






LCS


Mercury 599792 5.71 5.00 ug/L 114 85.0 - 115 115190304

LCS Dup


Mercury 599792 5.71 5.73 5.00 85.0 - 115 114 115 ug/L 0.350 20.0

MS


Mercury 1367344 11.6 0 0.118 10.0 70.0 - 130 115 ug/L 14.0

Mercury 1369521 11.4 0 ND 10.0 70.0 - 130 114 ug/L 14.0

MSD


Mercury 1367344 11.6 11.5 0.118 10.0 70.0 - 130 115 114 ug/L 0.873 14.0

Mercury 1369521 11.4 11.3 ND 10.0 70.0 - 130 114 113 ug/L 0.881 14.0

EPA 200.7 4.4Drinking Water 600043

Blank


Calcium 600043 0.0545 0.0419 0.500 mg/L 115192515

Magnesium, Total 600043 ND 0.0102 0.500 mg/L 115192515

Potassium 600043 0.104 0.0765 0.500 mg/L 115192515

Total Iron 600043 ND 0.00504 0.025 mg/L 115192515

CCV


Calcium 26.4 25.0 mg/L 106 90.0 - 110 115192512

Calcium 25.2 25.0 mg/L 101 90.0 - 110 115192514

Calcium 26.5 25.0 mg/L 106 90.0 - 110 115192525

Calcium 26.6 25.0 mg/L 106 90.0 - 110 115192536

Magnesium, Total 25.7 25.0 mg/L 103 90.0 - 110 115192514



Potassium 24.0 25.0 mg/L 96.0 90.0 - 110 115192514

Potassium 24.9 25.0 mg/L 99.6 90.0 - 110 115192525

Total Iron 2.52 2.50 mg/L 101 90.0 - 110 115192514

Total Iron 2.65 2.50 mg/L 106 90.0 - 110 115192525

Total Iron 2.67 2.50 mg/L 107 90.0 - 110 115192536

Total Iron 2.65 2.50 mg/L 106 90.0 - 110 115192546

Total Iron 2.64 2.50 mg/L 106 90.0 - 110 115192556

ICL


Calcium 49.4 50.0 mg/L 98.8 95.0 - 105 115192507

Magnesium, Total 49.5 50.0 mg/L 99.0 95.0 - 105 115192507

Potassium 50.2 50.0 mg/L 100 95.0 - 105 115192507

Total Iron 4.99 5.00 mg/L 99.8 95.0 - 105 115192507

ICV


Calcium 25.2 25.0 mg/L 101 90.0 - 110 115192511

Magnesium, Total 24.4 25.0 mg/L 97.6 90.0 - 110 115192511

Potassium 23.3 25.0 mg/L 93.2 90.0 - 110 115192511






1

2

3

4

5






ICV


Total Iron 2.45 2.50 mg/L 98.0 90.0 - 110 115192511

LCS


Calcium 600043 5.50 5.00 mg/L 110 85.0 - 115 115192516

Magnesium, Total 600043 5.48 5.00 mg/L 110 85.0 - 115 115192516

Potassium 600043 5.42 5.00 mg/L 108 85.0 - 115 115192516

Total Iron 600043 0.540 0.500 mg/L 108 85.0 - 115 115192516

LCS Dup


Calcium 600043 5.50 5.56 5.00 85.0 - 115 110 111 mg/L 1.08 25.0

Magnesium, Total 600043 5.48 5.52 5.00 85.0 - 115 110 110 mg/L 0.727 25.0

Potassium 600043 5.42 5.53 5.00 85.0 - 115 108 111 mg/L 2.01 25.0

Total Iron 600043 0.540 0.537 0.500 85.0 - 115 108 107 mg/L 0.557 25.0

LDR


Calcium 300 300 mg/L 100 90.0 - 110 115192513

Magnesium, Total 93.6 100 mg/L 93.6 90.0 - 110 115192508

Potassium 102 100 mg/L 102 90.0 - 110 115192508

Total Iron 9.61 10.0 mg/L 96.1 90.0 - 110 115192508

MS


Calcium 1369109 7.78 0 1.84 5.00 75.0 - 125 119 mg/L 25.0

Sodium 1369109 46.9 0 41.4 5.00 75.0 - 125 110 mg/L 25.0

Total Iron 1369109 0.573 0 0.0256 0.500 75.0 - 125 109 mg/L 25.0

Calcium 1369496 85.8 0 80.3 5.00 75.0 - 125 110 mg/L 25.0

Magnesium, Total 1369496 58.0 0 52.1 5.00 75.0 - 125 118 mg/L 25.0

Potassium 1369496 11.5 0 5.17 5.00 75.0 - 125 127 * mg/L 25.0

Total Iron 1369496 0.529 0 ND 0.500 75.0 - 125 106 mg/L 25.0

MSD


Calcium 1369109 7.78 7.80 1.84 5.00 75.0 - 125 119 119 mg/L 0 25.0

Sodium 1369109 46.9 46.4 41.4 5.00 75.0 - 125 110 100 mg/L 9.52 25.0

Total Iron 1369109 0.573 0.585 0.0256 0.500 75.0 - 125 109 112 mg/L 2.71 25.0

Calcium 1369496 85.8 86.7 80.3 5.00 75.0 - 125 110 128 * mg/L 15.1 25.0

Magnesium, Total 1369496 58.0 58.4 52.1 5.00 75.0 - 125 118 126 * mg/L 6.56 25.0

Potassium 1369496 11.5 11.4 5.17 5.00 75.0 - 125 127 * 125 mg/L 1.59 25.0

Total Iron 1369496 0.529 0.531 ND 0.500 75.0 - 125 106 106 mg/L 0 25.0

SM 5310 C-96Drinking Water 600116

AWRL


Total Organic Carbon 2.00 2.00 mg/L 100 75.0 - 125 115194303

Blank


Total Organic Carbon 600116 0.0979 0.0618 0.500 mg/L 115194302








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3

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5






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CCB

FileOutUnitsMQLMDLReadingPrepSetParameter








CCV


Total Organic Carbon 9.79 10.0 mg/L 97.9 90.0 - 110 115194299







ICL



ICV



LCS


Total Organic Carbon 600116 5.23 5.00 mg/L 105 100 - 114 115194301




MS


Total Organic Carbon 1369430 10.0 0 0.783 10.0 93.0 - 113 92.2 * mg/L 20.0

Total Organic Carbon 1369505 17.9 0 7.33 10.0 93.0 - 113 106 mg/L 20.0

Total Organic Carbon 1369780 14.2 0 3.26 10.0 93.0 - 113 109 mg/L 20.0

MSD


Total Organic Carbon 1369430 10.0 10.1 0.783 10.0 93.0 - 113 92.2 * 93.2 mg/L 1.08 20.0

Total Organic Carbon 1369505 17.9 17.8 7.33 10.0 93.0 - 113 106 105 mg/L 0.948 20.0

Total Organic Carbon 1369780 14.2 14.1 3.26 10.0 93.0 - 113 109 108 mg/L 0.922 20.0

Standard









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5






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Boron 599920 ND 0.00501 0.100 mg/L 115195940

Silicon Recoverable 599920 ND 0.0069 0.100 mg/L 115195940

Strontium 599920 ND 0.00532 0.050 mg/L 115195940

CCV


Boron 5.33 5.00 mg/L 107 90.0 - 110 115195939

Boron 5.16 5.00 mg/L 103 90.0 - 110 115195947

Boron 5.07 5.00 mg/L 101 90.0 - 110 115195948

Silicon Recoverable 5.13 5.00 mg/L 103 90.0 - 110 115195939

Silicon Recoverable 4.95 5.00 mg/L 99.0 90.0 - 110 115195947

Silicon Recoverable 4.83 5.00 mg/L 96.6 90.0 - 110 115195948

Strontium 0.524 0.500 mg/L 105 90.0 - 110 115195939

Strontium 0.499 0.500 mg/L 99.8 90.0 - 110 115195947

Strontium 0.485 0.500 mg/L 97.0 90.0 - 110 115195948

ICL


Boron 10.3 10.0 mg/L 103 95.0 - 105 115195933


Strontium 1.02 1.00 mg/L 102 95.0 - 105 115195933

ICV


Boron 5.31 5.00 mg/L 106 90.0 - 110 115195934


Strontium 0.512 0.500 mg/L 102 90.0 - 110 115195934

LCS


Boron 599920 1.05 1.00 mg/L 105 85.0 - 115 115195941

Silicon Recoverable 599920 3.66 4.00 mg/L 91.4 85.0 - 115 115195941

Strontium 599920 0.532 0.500 mg/L 106 85.0 - 115 115195941

LCS Dup


Boron 599920 1.05 1.05 1.00 85.0 - 115 105 105 mg/L 0 25.0

Silicon Recoverable 599920 3.66 3.68 4.00 85.0 - 115 91.4 91.9 mg/L 0.545 25.0

Strontium 599920 0.532 0.547 0.500 85.0 - 115 106 109 mg/L 2.78 25.0

MS


Boron 1369496 1.48 0 0.437 1.00 75.0 - 125 104 mg/L 25.0

Silicon Recoverable 1369496 15.0 0 11.1 4.00 75.0 - 125 97.5 mg/L 25.0

Strontium 1369496 1.78 0 1.19 0.500 75.0 - 125 118 mg/L 25.0

MSD


Boron 1369496 1.48 1.50 0.437 1.00 75.0 - 125 104 106 mg/L 1.90 25.0

Silicon Recoverable 1369496 15.0 15.0 11.1 4.00 75.0 - 125 97.5 97.5 mg/L 0 25.0

Strontium 1369496 1.78 1.79 1.19 0.500 75.0 - 125 118 120 mg/L 1.68 25.0







1

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3

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5






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Calcium 599920 ND 0.0419 0.500 mg/L 115197394

Magnesium, Total 599920 ND 0.0102 0.500 mg/L 115197394

Sodium 599920 ND 0.0315 0.500 mg/L 115197394

CCV


Calcium 25.6 25.0 mg/L 102 90.0 - 110 115197392

Calcium 25.7 25.0 mg/L 103 90.0 - 110 115197403

Calcium 25.8 25.0 mg/L 103 90.0 - 110 115197411



Sodium 25.1 25.0 mg/L 100 90.0 - 110 115197392

Sodium 25.4 25.0 mg/L 102 90.0 - 110 115197403

Sodium 25.4 25.0 mg/L 102 90.0 - 110 115197411

Sodium 25.3 25.0 mg/L 101 90.0 - 110 115197418

ICL


Calcium 50.4 50.0 mg/L 101 95.0 - 105 115197387


Sodium 50.7 50.0 mg/L 101 95.0 - 105 115197387

ICV


Calcium 25.8 25.0 mg/L 103 90.0 - 110 115197391


Sodium 25.0 25.0 mg/L 100 90.0 - 110 115197391

LCS


Calcium 599920 5.44 5.00 mg/L 109 85.0 - 115 115197395

Magnesium, Total 599920 5.42 5.00 mg/L 108 85.0 - 115 115197395

Sodium 599920 5.21 5.00 mg/L 104 85.0 - 115 115197395

LCS Dup


Calcium 599920 5.44 5.43 5.00 85.0 - 115 109 109 mg/L 0.184 25.0

Magnesium, Total 599920 5.42 5.42 5.00 85.0 - 115 108 108 mg/L 0 25.0

Sodium 599920 5.21 5.23 5.00 85.0 - 115 104 105 mg/L 0.383 25.0

LDR


Calcium 102 100 mg/L 102 90.0 - 110 115197388

Magnesium, Total 99.1 100 mg/L 99.1 90.0 - 110 115197388

Sodium 195 200 mg/L 97.5 90.0 - 110 115197393

Total Iron 10.2 10.0 mg/L 102 90.0 - 110 115197388

MS


Calcium 1369496 85.9 0 80.3 5.00 75.0 - 125 112 mg/L 25.0

Magnesium, Total 1369496 58.3 0 51.9 5.00 75.0 - 125 128 * mg/L 25.0

Sodium 1369496 175 0 169 5.00 75.0 - 125 120 mg/L 25.0






1

2

3

4

5






MSD


Calcium 1369496 85.9 85.0 80.3 5.00 75.0 - 125 112 94.0 mg/L 17.5 25.0

Magnesium, Total 1369496 58.3 57.1 51.9 5.00 75.0 - 125 128 * 104 mg/L 20.7 25.0

Sodium 1369496 175 173 169 5.00 75.0 - 125 120 80.0 mg/L 40.0 * 25.0


Blank


Aluminum, Total 600280 ND 0.00199 0.005 mg/L 115198445

Arsenic, Total 600280 ND 0.000193 0.0005 mg/L 115198445

Barium 600280 0.000909 0.000574 0.005 mg/L 115198445

Cadmium, Total 600280 ND 0.000209 0.0005 mg/L 115198445

Chromium, Total 600280 ND 0.000282 0.0005 mg/L 115198445

Copper, Total 600280 ND 0.000425 0.001 mg/L 115198445

Lead, Total 600280 ND 0.000227 0.0005 mg/L 115198445

Manganese, Total 600280 ND 0.00033 0.001 mg/L 115198445

Selenium, Total 600280 ND 0.000728 0.001 mg/L 115198445

Silver, Total 600280 ND 0.00006280.0002 mg/L 115198445

Zinc, Total 600280 ND 0.00123 0.005 mg/L 115198445

CCV


Aluminum, Total 0.0492 0.05 mg/L 98.4 90.0 - 110 115198444


Aluminum, Total 0.0502 0.05 mg/L 100 90.0 - 110 115198464





Arsenic, Total 0.0526 0.05 mg/L 105 90.0 - 110 115198444

Arsenic, Total 0.0499 0.05 mg/L 99.8 90.0 - 110 115198453






Barium 0.0502 0.05 mg/L 100 90.0 - 110 115198444

Barium 0.0499 0.05 mg/L 99.8 90.0 - 110 115198453

Barium 0.0508 0.05 mg/L 102 90.0 - 110 115198464

Barium 0.0502 0.05 mg/L 100 90.0 - 110 115198473

Barium 0.0508 0.05 mg/L 102 90.0 - 110 115198480

Barium 0.0512 0.05 mg/L 102 90.0 - 110 115198491

Barium 0.0516 0.05 mg/L 103 90.0 - 110 115198501

Cadmium, Total 0.0497 0.05 mg/L 99.4 90.0 - 110 115198444


Cadmium, Total 0.0503 0.05 mg/L 101 90.0 - 110 115198464





Chromium, Total 0.053 0.05 mg/L 106 90.0 - 110 115198444







1

2

3

4

5






CCV







Copper, Total 0.0522 0.05 mg/L 104 90.0 - 110 115198444

Copper, Total 0.0507 0.05 mg/L 101 90.0 - 110 115198453

Copper, Total 0.0525 0.05 mg/L 105 90.0 - 110 115198464

Copper, Total 0.0523 0.05 mg/L 105 90.0 - 110 115198473

Copper, Total 0.0532 0.05 mg/L 106 90.0 - 110 115198480

Copper, Total 0.0518 0.05 mg/L 104 90.0 - 110 115198491

Copper, Total 0.054 0.05 mg/L 108 90.0 - 110 115198501

Lead, Total 0.0492 0.05 mg/L 98.4 90.0 - 110 115198444

Lead, Total 0.050 0.05 mg/L 100 90.0 - 110 115198453

Lead, Total 0.0492 0.05 mg/L 98.4 90.0 - 110 115198464

Lead, Total 0.0494 0.05 mg/L 98.8 90.0 - 110 115198473

Lead, Total 0.0489 0.05 mg/L 97.8 90.0 - 110 115198480

Lead, Total 0.0492 0.05 mg/L 98.4 90.0 - 110 115198491

Lead, Total 0.0489 0.05 mg/L 97.8 90.0 - 110 115198501

Manganese, Total 0.0505 0.05 mg/L 101 90.0 - 110 115198444






Manganese, Total 0.0498 0.05 mg/L 99.6 90.0 - 110 115198501

Selenium, Total 0.0534 0.05 mg/L 107 90.0 - 110 115198444

Selenium, Total 0.049 0.05 mg/L 98.0 90.0 - 110 115198453




Selenium, Total 0.0495 0.05 mg/L 99.0 90.0 - 110 115198491


Silver, Total 0.0508 0.05 mg/L 102 90.0 - 110 115198444

Silver, Total 0.0499 0.05 mg/L 99.8 90.0 - 110 115198453

Silver, Total 0.0506 0.05 mg/L 101 90.0 - 110 115198464

Silver, Total 0.051 0.05 mg/L 102 90.0 - 110 115198473

Silver, Total 0.0507 0.05 mg/L 101 90.0 - 110 115198480

Silver, Total 0.0509 0.05 mg/L 102 90.0 - 110 115198491

Silver, Total 0.0509 0.05 mg/L 102 90.0 - 110 115198501

Zinc, Total 0.0509 0.05 mg/L 102 90.0 - 110 115198444

Zinc, Total 0.0505 0.05 mg/L 101 90.0 - 110 115198453

Zinc, Total 0.052 0.05 mg/L 104 90.0 - 110 115198464

Zinc, Total 0.0529 0.05 mg/L 106 90.0 - 110 115198473

Zinc, Total 0.0514 0.05 mg/L 103 90.0 - 110 115198480

Zinc, Total 0.0508 0.05 mg/L 102 90.0 - 110 115198491

Zinc, Total 0.0522 0.05 mg/L 104 90.0 - 110 115198501

ICV








1

2

3

4

5






ICV



Barium 0.0512 0.05 mg/L 102 90.0 - 110 115198422



Copper, Total 0.0516 0.05 mg/L 103 90.0 - 110 115198422

Lead, Total 0.0502 0.05 mg/L 100 90.0 - 110 115198422

Manganese, Total 0.0489 0.05 mg/L 97.8 90.0 - 110 115198422


Silver, Total 0.0503 0.05 mg/L 101 90.0 - 110 115198422

Zinc, Total 0.0519 0.05 mg/L 104 90.0 - 110 115198422

LCS


Aluminum, Total 600280 0.565 0.500 mg/L 113 85.0 - 115 115198446

Arsenic, Total 600280 0.537 0.500 mg/L 107 85.0 - 115 115198446

Barium 600280 0.521 0.500 mg/L 104 85.0 - 115 115198446

Cadmium, Total 600280 0.264 0.250 mg/L 106 85.0 - 115 115198446

Chromium, Total 600280 0.539 0.500 mg/L 108 85.0 - 115 115198446

Copper, Total 600280 0.539 0.500 mg/L 108 85.0 - 115 115198446

Lead, Total 600280 0.534 0.500 mg/L 107 85.0 - 115 115198446

Manganese, Total 600280 0.527 0.500 mg/L 105 85.0 - 115 115198446

Selenium, Total 600280 0.527 0.500 mg/L 105 85.0 - 115 115198446

Silver, Total 600280 0.106 0.100 mg/L 106 85.0 - 115 115198446

Zinc, Total 600280 0.522 0.500 mg/L 104 85.0 - 115 115198446

LCS Dup


Aluminum, Total 600280 0.565 0.563 0.500 85.0 - 115 113 113 mg/L 0.355 20.0

Arsenic, Total 600280 0.537 0.530 0.500 85.0 - 115 107 106 mg/L 1.31 20.0

Barium 600280 0.521 0.515 0.500 85.0 - 115 104 103 mg/L 1.16 20.0

Cadmium, Total 600280 0.264 0.261 0.250 85.0 - 115 106 104 mg/L 1.14 20.0

Chromium, Total 600280 0.539 0.538 0.500 85.0 - 115 108 108 mg/L 0.186 20.0

Copper, Total 600280 0.539 0.534 0.500 85.0 - 115 108 107 mg/L 0.932 20.0

Lead, Total 600280 0.534 0.531 0.500 85.0 - 115 107 106 mg/L 0.563 20.0

Manganese, Total 600280 0.527 0.530 0.500 85.0 - 115 105 106 mg/L 0.568 20.0

Selenium, Total 600280 0.527 0.529 0.500 85.0 - 115 105 106 mg/L 0.379 20.0

Silver, Total 600280 0.106 0.104 0.100 85.0 - 115 106 104 mg/L 1.90 20.0

Zinc, Total 600280 0.522 0.515 0.500 85.0 - 115 104 103 mg/L 1.35 20.0

MS


Aluminum, Total 1369496 0.559 0 ND 0.500 70.0 - 130 112 mg/L 20.0

Arsenic, Total 1369496 0.539 0 0.00408 0.500 70.0 - 130 107 mg/L 20.0

Barium 1369496 0.583 0 0.070 0.500 70.0 - 130 103 mg/L 20.0

Cadmium, Total 1369496 0.255 0 ND 0.250 70.0 - 130 102 mg/L 20.0

Chromium, Total 1369496 0.522 0 0.000984 0.500 70.0 - 130 104 mg/L 20.0

Copper, Total 1369496 0.515 0 0.00428 0.500 70.0 - 130 102 mg/L 20.0

Lead, Total 1369496 0.508 0 ND 0.500 70.0 - 130 102 mg/L 20.0

Manganese, Total 1369496 0.507 0 ND 0.500 70.0 - 130 101 mg/L 20.0

Selenium, Total 1369496 0.522 0 0.0162 0.500 70.0 - 130 101 mg/L 20.0

Silver, Total 1369496 0.102 0 ND 0.100 70.0 - 130 102 mg/L 20.0

Zinc, Total 1369496 0.483 0 0.0078 0.500 70.0 - 130 95.0 mg/L 20.0






1

2

3

4

5






MSD


Aluminum, Total 1369496 0.559 0.555 ND 0.500 70.0 - 130 112 111 mg/L 0.897 20.0

Arsenic, Total 1369496 0.539 0.531 0.00408 0.500 70.0 - 130 107 105 mg/L 1.89 20.0

Barium 1369496 0.583 0.579 0.070 0.500 70.0 - 130 103 102 mg/L 0.976 20.0

Cadmium, Total 1369496 0.255 0.254 ND 0.250 70.0 - 130 102 102 mg/L 0 20.0

Chromium, Total 1369496 0.522 0.517 0.000984 0.500 70.0 - 130 104 103 mg/L 0.966 20.0

Copper, Total 1369496 0.515 0.509 0.00428 0.500 70.0 - 130 102 101 mg/L 0.985 20.0

Lead, Total 1369496 0.508 0.504 ND 0.500 70.0 - 130 102 101 mg/L 0.985 20.0

Manganese, Total 1369496 0.507 0.502 ND 0.500 70.0 - 130 101 100 mg/L 0.995 20.0

Selenium, Total 1369496 0.522 0.517 0.0162 0.500 70.0 - 130 101 100 mg/L 0.995 20.0

Silver, Total 1369496 0.102 0.102 ND 0.100 70.0 - 130 102 102 mg/L 0 20.0

Zinc, Total 1369496 0.483 0.478 0.0078 0.500 70.0 - 130 95.0 94.0 mg/L 1.06 20.0


Blank


Mercury 599959 ND 0.072 0.100 ug/L 115202347

CCV


Mercury 4.91 5.000 ug/L 98.2 90.0 - 110 115202346

Mercury 4.98 5.000 ug/L 99.6 90.0 - 110 115202350

Mercury 4.93 5.000 ug/L 98.6 90.0 - 110 115202361

ICL


Mercury 19.6 20.00 ug/L 98.0 90.0 - 110 115202327

ICV


Mercury 5.11 5.000 ug/L 102 90.0 - 110 115202326

LCS


Mercury 599959 5.18 5.00 ug/L 104 85.0 - 115 115202348

LCS Dup


Mercury 599959 5.18 5.06 5.00 85.0 - 115 104 101 ug/L 2.34 20.0

MS


Mercury 1368631 10.4 0 ND 10.0 70.0 - 130 104 ug/L 14.0

MSD


Mercury 1368631 10.4 10.4 ND 10.0 70.0 - 130 104 104 ug/L 0 14.0


CCV


Dissolved Iron 2.49 2.50 mg/L 99.6 90.0 - 110 115210842







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Dir. SPKD

Limit%RPDUnitsDSPKD%DSPK%Limits%KnownUNKDSPKDDSPKSampleParameter

Dissolved Iron 1369496 0.465 0.519 ND 0.500 75.0 - 125 93.0 104 mg/L 11.2 20.0

Direct SPK

UnitsDSPK%Limits%KnownUNKDSPKSampleParameter

Dissolved Iron 1369496 0.465 ND 0.500 75.0 - 125 93.0 mg/L 20.0

ICL


Dissolved Iron 5.13 5.00 mg/L 103 95.0 - 105 115210835

ICV


Dissolved Iron 2.55 2.50 mg/L 102 90.0 - 110 115210839

LDR



SM 2130 B-94Drinking Water 599733

Blank


Turbidity 599733 ND 1.00 1.00 NTU 115186285

Duplicate


Turbidity 1369325 Duplicate ND ND NTU 20.0

Turbidity 1369497 Duplicate ND ND NTU 20.0

Mat. Spike


Turbidity 1369325 41.9 ND 40.0 NTU 105 70.0 - 130 115186290

Turbidity 1369497 43.6 ND 40.0 NTU 109 70.0 - 130 115186303

Standard


Turbidity 599733 9.96 10.0 NTU 99.6 90.0 - 110 115186286

Turbidity 599733 99.8 100 NTU 99.8 90.0 - 110 115186287

Turbidity 599733 9.97 10.0 NTU 99.7 90.0 - 110 115186300

Turbidity 599733 9.98 10.0 NTU 99.8 90.0 - 110 115186304

SM 2320 B-97Drinking Water 599795

Blank


Total Alkalinity (as CaCO3) 599795 ND 1.00 1.00 mg/L 115186307

CCV


Total Alkalinity (as CaCO3) 25.7 25.0 mg/L 103 90.0 - 110 115186306

Total Alkalinity (as CaCO3) 24.7 25.0 mg/L 98.8 90.0 - 110 115186320


Duplicate


Total Alkalinity (as CaCO3) 1368654 Duplicate 49.8 51.3 mg/L 2.97 20.0






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Duplicate


Total Alkalinity (as CaCO3) 1369298 Duplicate 98.2 108 mg/L 9.51 20.0

ICV



Mat. Spike


Total Alkalinity (as CaCO3) 1368654 77.0 51.3 25.0 mg/L 103 70.0 - 130 115186310

Total Alkalinity (as CaCO3) 1369298 129 108 25.0 mg/L 84.0 70.0 - 130 115186323

SM 4500-H+ B-96Drinking Water 599923

Duplicate


Laboratory pH 1369061 Duplicate 8.2 8.2 SU 0 20.0

Laboratory pH 1369494 Duplicate 7.9 7.9 SU 0 20.0

Standard


Laboratory pH 599923 7.01 7.00 SU 100 90.0 - 110 115189526

Laboratory pH 599923 4.01 4.00 SU 100 90.0 - 110 115189527

Laboratory pH 599923 10.05 10.00 SU 100 90.0 - 110 115189528

Laboratory pH 599923 6.01 6.00 SU 100 90.0 - 110 115189529

Laboratory pH 599923 8.03 8.00 SU 100 90.0 - 110 115189530

Laboratory pH 599923 6.05 6.00 SU 101 90.0 - 110 115189542

Laboratory pH 599923 8.05 8.00 SU 101 90.0 - 110 115189543

Laboratory pH 599923 6.05 6.00 SU 101 90.0 - 110 115189555

Laboratory pH 599923 8.05 8.00 SU 101 90.0 - 110 115189556

SM 4500-S2¯ D-2000Drinking Water 600327

Blank


Sulfide 600327 ND 0.0091 0.015 mg/L 115199183

Duplicate


Sulfide 1369496 Duplicate ND ND mg/L 20.0

LCS


Sulfide 600327 0.0768 0.075 mg/L 102 90.0 - 110 115199184

LCS Dup


Sulfide 600327 0.0768 0.0753 0.075 90.0 - 110 102 100 mg/L 1.97 10.0

SM 4500-P E-97Drinking Water 600851

Blank


Total Phosphorus 600851 0.00336 0.00285 0.010 mg/L 115210730

CCV







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CCV


Total Phosphorus 0.316 0.300 mg/L 105 90.0 - 110 115210731



LCS


Total Phosphorus 600851 0.296 0.300 mg/L 98.8 80.0 - 120 115210732

LCS Dup


Total Phosphorus 600851 0.296 0.287 0.300 80.0 - 120 98.8 95.5 mg/L 3.09 20.0

MS


Total Phosphorus 1369496 0.430 0 0.109 0.300 70.0 - 130 107 mg/L 20.0

Total Phosphorus 1369592 0.401 0 0.0829 0.300 70.0 - 130 106 mg/L 20.0

MSD


Total Phosphorus 1369496 0.430 0.410 0.109 0.300 70.0 - 130 107 100 mg/L 6.76 20.0

Total Phosphorus 1369592 0.401 0.381 0.0829 0.300 70.0 - 130 106 99.4 mg/L 6.43 20.0

RPD is Relative Percent Difference: abs(r1-r2) / mean(r1,r2) * 100% Recover% is Recovery Percent: result / known * 100%

Blank - Method Blank; CCV - Continuing Calibration Verification; ICV - Initial Calibration Verification; LCS - Laboratory Control Sample; MS - Matrix

Spike; LDR - Linear Dynamic Range Standard; CCB - Continuing Calibration Blank; AWRL - Ambient Water Reporting Limit






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