· 37 75% c2h5oh/ 25% azdne 38 a plasticizer (tegdn) 39 ab-1 40 acetic acid 41 acetone 42 acetone...

of 20TABLE ILIST OF DOCUMENTED WASTE DISPOSED OF AT AREA I BURN PIT AIBP SWMU 4.8 RFI WORK PLANBOEING SANTA SUSANA FIELD LABORATORYVENTURA COUNTY, CALIFORNIA

1 #200 Thinner2 #-81 Blasting Caps3 (0.6 lbs solids: KClO4, Ap, ZrH2 60%; NC, NG 40%). ( 61.4 lbs liquids: Acetone, etoh, etac)4 (1.5 lbs solids: CAB, NC, CMP, CONPALT, TMETN, DEGDN, TEGDN, NG, EC PVAC, TEGDA, PEG, R-45, GAP,

GAPA, ATEC, NDPA, RDX, AP, KP, ZRH2, TAGN, K2SO4, C, CUO2O2, Al, Mg, B), (152.5 lbs liguids: acetone, toluene, ETOH, ETAC)

5 (27 lbs liquids: Acetone, ethanol, isopropanol, NG, TMETN, DANPE), (Trace amounts: Al, Mg, Cr, Si)6 (C2H4)4B2H27 (C2H5)2PH8 (C2H5)3B9 (CH3)2BrB2

10 (CH3)2NP(CH3)211 (CH3)2PH12 (CH3)2PH/CH3PH213 (CH3)2PN(CH3)214 (CH3)3P15 (CH3NBH)316 (Me2N)2BCl17 (Me2NBCL2)218 (NCH3C6H4)2PN(CH3)219 (PF2)3N20 (PF2N)n21 0BCl222 0MePH23 0PH224 1 of 13 was CC/DOT 3A480-chlorine25 1,3-Diphenphinophosphine26 1,3-Diphosphino propane27 1,4-Diphosphino butane28 10% Fluorine29 20% Nitroglycerine, 80% methylene chloride30 30% Methylene chloride solution31 4 bottles unknown liquid32 49-75 gram RDX pellets (SSME)33 5% TEAB34 5% TEAB/RP-135 50% propyl nitrate/50% isopropyl alcohol36 6 samples of FTM37 75% C2H5OH/ 25% AZDNE38 a plasticizer (TEGDN)39 AB-140 Acetic Acid41 Acetone42 Acetone (contaminated)43 Acetone, ETOH, ETAC, NC, CAB, DANPE, NG, RDX, AP, RDX, Al2O3, Cr2O3, MgO, Al, Mg, Cr, paper towels,

pastic containers44 Acetonitrile

Haley & Aldrich, Inc.G:\Projects\26472\Reports\M477 A1BP RFI Work Plan\Tables\2006-1110-HAI-SSFL.M477.T01.F.xls November 2006


45 Acetylene46 Acid-cleaning47 Acids48 Acids/misc acids49 AFN2550 Alcohol51 Alcohol (contaminated)52 Alcohols53 Alkali metals54 Alkaline Cleaner55 Alkaline powder56 Aluminium57 Aluminum58 Aluminum Chloride59 Aluminum oxide60 Aluminum powder61 Aluminum powder 54 gm + Freon TF62 Alumnium turnings 33 gm saturated with sulfur-base cutting oil + Freon TF63 Ammonia64 Ammonia (liquid)65 Ammonia perchlorate66 Ammonia, small cylinders67 Ammonium perchloate (oxidizers)68 Ammonium perchlorate69 Ammonium perchlorate, AP70 Amyl nitrate71 Anhydrous ammonia72 AP nitrate esters73 AP, GAP, TMETN, N-100, C, NMA. 74 approximately 60 cubic yards of loosely packed empty steel drums and misc. scrap metals formally hazardous

materials75 Aqua ammonia76 Aqueous ammonia77 Argon78 Argon Gas79 aromatic naptha80 Arsenic81 AZDNE/MeCl282 B5H8Et83 B5H8I84 B5H985 Barium86 Barium chloride87 Bases88 BBr389 Benzaldehyde90 Benzene



91 Benzene on sawdust92 Benzene/MBDA recovery93 Benzene-HCL94 Benzene-Hydrochloric Acid Mixture95 Benzol96 Bermite Carbides97 Beryllium98 BH Polymer99 Binders100 Bis Ethyl 2 Chloroformal101 Bis( 2,2-difluoramino-5,5,5-fluorodinitropentyl) formal (SYFO) 50# solution in 30% methylene chloride solution102 Bis(2,2-diflouroemino-5,5,5-fluorodinitropentyl) formil (SYFO)103 Bis(fluorodinitroethoxy) 2,2-bis(difluoramino) propane (SYEP)104 Bis(fluorodinitroethoxy)-2-isopropanol (SECOH)105 Bis(fluorodintitroethoxy) 2,2-bis(difluoroamino) propane (SYEP) 35# solution in 30% methylene chloride solution106 Bis(fluorodintitroethoxy)2-propanol (SECOH) 200# solution in 30% methylene chloride solution107 Black Powder108 Blasting caps109 B-methyl Borazine110 Boric oxide111 Borol112 Boron 90%113 Boron amorphous114 Boron Fuel115 Boron hydride116 Boron trifluoride117 Bottles118 Breathing air119 Bromide pentaflouride serial RS0215120 Bromine121 Bromine pentafluoride122 Bromine pentafluoride (cylinder)123 Bromine pentafluoride general chemical serial R-59124 Bromine triflouride125 Bromine trifluoride126 BTU NF compound127 Butadiene128 Butadiene polymate129 Butadiene polymer, R-45130 Butadienes131 Butanetriol trinitrate132 C2H5BCl2133 C2H5PH2134 C2H5SH135 Cadmium136 CaH2137 CAL-3



138 Calcium chloride139 Calcium hydride140 Carbon Tetrachloride141 Cartridge NA5-28088-1142 Cartridge NA5-28124143 Cartridge NA5-28124T1144 Caustic Potash145 Caustic soda146 CCl4147 Cesium148 CF2Cl2149 CF3I150 CF3SF5151 CH3HP(CH2)3PHCH3152 CH3MgBr in THF: 3-100 gm bottles153 CH3PCl2154 CH3SiCl3155 Chem Solvent156 Chemicals, unknown157 Chlorine158 Chlorine & O2 gas159 Chlorine Gas160 Chlorine pentafluoride (compound A)161 Chlorine Pentafluoride, Compound A162 Chlorine Trifluoride163 Chlorine trifluoride (cylinder)164 Chlorine trifluorine165 Chlorobutadiene166 Chloroform167 Chloropropane168 Chromic acid Solution169 Cleaning materials and swabs170 CMP, N-100, DANPE, CMP, NC, NG, PCOE, SYEP, CAB, ATEC, GAPA, R-45, DD1, DOA, PEC, CMGA, RDX,

NDPA, ZrH2, Si, HMX, B, KClO3, NaHCO3, DATH, S, yellow dye, Al, am. Iodate, dechlorane, PbV2, K2Cr2O2, hexachloroethane, acetone, toluene, ethanol, ethyl acetate.

171 CO172 CO2173 CO2 (cylinder)174 Comp A.175 Comp C-4176 Comp. A177 Composite solid propellant grain178 Compound A179 Compress gas cylinder180 Compressed air181 Conax valves182 Copper



183 Crude CH3SF5184 CTF cylinder185 CTF cylinders186 CTF-Igniter187 Cupric chloride188 Cyclonite, RDX189 Cyclo-tetramethylene-Nitramine190 Cyclotrimethylene trinitramine191 Cylinders192 Cylinders with strong oxidizers193 Cylinders with unknown material194 DATB195 Daworals sodium196 DCFO/CH3CN197 Decaborane198 Decon.199 Decon. Soln.200 DEGDN201 Dekazine202 Delta203 Desiccator with unknown contents + cap204 Detonating primers 2 Gr Long 8258-470640-3205 Deuterium, small cylinders206 DHSG ignition, TEB canisters207 Diazidylnitramino pentane, DANPE208 Dibutylphthalate209 Diesel fuel210 Diesel fuel oil211 Diethyl ether/benzene/magnesium boro hydride diammoniate (MBDA) residues. 4 ~1-L bottles212 Diethylcyclohexane213 Diethylene glycol dinitrate214 Diethylene triamine215 Dimazine216 Dimethyl mercury217 Dinitrotoluene218 Dioctylphthalate219 Dioctylphthalate, DOP220 Dioxane221 Dioxin222 Ditto fluid223 DPA-HPE-NFPA224 Dry nitrogen225 Dynamite226 Elec. Lighters227 Electric igniters228 Electric squibb229 Electric squibb ignitors



230 Electrolyte231 Electrolyte Solutionn232 Electrolytic solution233 Empty cylinder(s)234 Empty Drums, UDMH235 Empty TEB canister236 Energetic binders in 300ml round-bottom flasks237 Enjay dicyclopentadine238 Epoxy239 Et2BCl240 Et2PH241 EtB5H8242 EtBBr2243 EtBCl2244 Ethane, Large cylinders245 Ethanol246 Ethenol247 Ether248 Ether Squibbs249 Ether/benzene/MBDA250 Ethyl alcohol251 ethyl benzene252 Ethyl deka borane253 Ethyl nitrate254 Ethylamine255 Ethylene diamine 256 Ethylene diamine (contaminated)257 Ethylene diamine (drain back)258 Ethylene oxide259 EtNH2260 EtPH261 EtPH2262 Explosive A+B263 explosive materials and paper contaminated with TEA and TEB264 Explosive wastes265 Explosives266 Explosives A&B267 Explosives bolts268 F2 gas generator pellets (NF4/BF4/KF/Al)269 F2 seial FL2540270 FDNE271 FDNE 400# Solution272 FDNE/alchohol273 FDNE/MeCl2/C2H5OH274 Ferrocene275 Fl empty cylinder



276 Flammable rags (90-98%) contaminated with nitrocellulose (0-5%), ammonia perchlorate (0-5%), cyclonite (0-3%), aluminum (2%), nitroglycerin (0-2%), polybutadiene (0-2%), acetone (5-10%), toluene (0-5%)

277 Flare mix278 Flares smoke279 Florox280 Flourine allied chem. 29-230411281 Flourine gas282 Fluoride283 Fluoride-matheson serial TH542284 Fluorine285 Fluorine (3 cylinders)286 Fluorine (5 cylinders)287 Fluorine cylinders288 Fluorine Gas289 Flushing oil290 Flushing oil (sludge)291 Formic Acid292 Freon293 Freon + acid294 Freon NTO295 Freon TF296 Fuel297 Fuel and addatives298 Fuel mixtures299 Fuel oil300 Fuel samples301 Fuel samples and chemicals302 Fuels, Cont.303 GAP 30%, Ap/C 70%. Mix 3-21-1304 GAP 30%, Ap/C 70%. Mix 3-21-1,2305 GAP 30%, Ap/C 70%. Mix 3-21-2306 GAP, N-100, DANPE, GAPA, AP, Mg, Cr, HMX, NC, CMP, DATH, TMETN, DADNH, HMDI, acetone, ethyl acetate,

ethanol307 GAP, N-100, DANPE, HMX, GAPA, TMETN, NC, CMP, DATH, DADNH, paper towels, plastic tubes and beakers,

Atlasol yellow dye.308 GAP, N-100, TMETN, DBTDL, DANPE, CMP, R-45, DD1, PS555, GAPA, NC, NG, R-18, IDP, HD1, CAB, DOA,

PEG, CMGA, AP, MNA, C, TPB, SiO2, Al, CuO2O2, Si, NOPA, KClO3, NaHCO3, S, yellow dye, BaCrO3I2, hexachloroethane, Fe, Mg, Fe2O3, Mo, B, I2O5, RDX, ZrH2, ATEC, EC, DATH, PCOZ, SYZP, HMX, TI, Am. IUDATE?,BI, DeChlorane,K2CR2O7, Papers, Plastic Containers.

309 GAP/DANPE 30%, AP/AL/Mg/Cr 70%. Paper towels, plastic containers.310 Gas cylinders311 Gas mixtures (cylinders)312 Gases, unknown313 Gasoline314 Gasoline soaked sawdust315 GDNFE316 GDNFE/alcohol



317 GDNFE/MeCl2/alcohol318 Gear oil319 Glycerine320 Glycidyl azide polymer321 Glycidyl Fluorodinitroethoxide (GDNFE) 160# solution in 30% methylene chloride solution322 Glycidylazide polymer azide, GAPA323 Glycidylazide polymer, GAP 324 GM lab cylinders325 Green CO2326 Green K bottle327 gun propellants: binder materials; plasticizers; and energetic and solid oxidizers328 Gunpowder329 HAP330 HCL331 Heavy aromatic naphta332 Heptane333 Heptane (contaminated with solid propellant)334 Heptane (contaminated)335 Hexamitro stilbene336 Hexane337 Hexanes338 Hexogen, HMX339 Hg(CH3)2340 Hi-Cal-3341 High explosives (Dynamite Comp. B. TNT)342 Hivelites343 HMX344 HMX scrap345 HMX-Nitrocellulose346 HNAH347 HNB348 HNF349 HNS350 HX310351 Hybaline352 Hybaline & RP-1353 Hybaline A and RP1354 Hybaline and RP355 Hybaline- Cal-3356 Hybrid motor grades357 Hybrid motor grains358 Hydraulic oil359 Hydraulic oil (contaminated)360 hydrazine361 hydrazine (contaminated)362 Hydrazine + cap363 Hydrazine 75%, Ethanol 21%, water 4%



364 Hydrazine 90%, EDA 10%365 Hydrazine and admixtures366 Hydrazine and admixtures samples367 Hydrazine and water368 Hydrazine and water (drain back)369 Hydrazine and water 20%370 Hydrazine and water 50%371 Hydrazine mixtures372 Hydrazine Nitrate373 Hydrazine, non-returnable drums374 Hydrazine, returnable drums375 Hydrazine, warehouse drums376 Hydrazine/ HMX Propellant Mixture377 Hydrazine-admixtures and lab chem.378 Hydrazinefluoride (N2F4) ICC3AA2265379 Hydrazines380 Hydrocarbon381 Hydrocarbon, non-returnable drums382 Hydrocarbon, warehouse drums383 Hydrocarbons384 Hydrocarbons EB-40385 Hydrochloric Acid386 Hydrofluoric Acid387 Hydrogen388 Hydrogen argon389 Hydrogen bromide390 Hydrogen chloride/helium391 Hydrogen fluoride392 Hydrogen fluoride RC4463393 Hydrogen gas394 Hydrogen sulfide395 Hydrogen, Large cylinders396 Hydrogen, small cylinders397 Hydrolic oil398 Hydrolic oil (Contaminated)399 Hydroxy terminated polybutadiene400 Hydroxy terminated polybutadiene, HTPB401 Hypergol igniters402 Hypergol TEA403 Hypergol TEA/TEB/RP-1 residue404 Hypergol TEB405 Igniter Class C406 Igniter ST4530001 RE001407 Igniters408 Inhibited-Red Fuming Nitric Acid409 Initiator NA5-26528-3410 Initiator R5950



411 IRFNA412 IRFNA (obsolete spec)413 IRFNA, NTO414 Iron carbonyls + caps. 3-1 pt. cans415 Iso octane416 Isopropyl alchohol417 Isopropyl alcohol418 Isopropyl Alcohol/NTO mixture419 Isopropyl Butane420 JP Fuel421 JP Fuel and water422 JP-4423 JP-4 (kersosene base)424 JP5 (contaminated)425 K bottle426 KAS(?)-10427 K-Bottle unkown (liq gas)428 K-bottle. (1 empty). Compound A429 K-bottle. Unknown quantity/contents cylinders430 K-bottle. Unknown quantity/contents. "Army"431 Kelite432 Kelite (sludge)433 Kerosene434 Ketones435 Lab chemicals436 Lab chemicals and fuel samples437 Lab chemicals and mixtures438 Lab Chemicals, fuel samples439 Lab chemicals, mixtures440 Lab samples (fuels)441 Lab silver cylinder442 Lab. Chemicals443 Laboratory waste444 Lachrymatory445 Lackrymatory446 Lacquer Dilute447 Lance grains448 Laquer Thinner449 Large TEB bottle450 Lead451 Leaded Paint (189 gallons)452 Licthih453 LiH454 linseed oil (contaminated)455 Liquid Rubber (contaminated)456 Liquid waste nitrate esters457 Liquified petroleum gas



458 Lithium459 Lithium chloride460 Lithium hydride461 Lithium metal462 Lithium metal powder463 Lube oil464 Lube oil (contaminated)465 Lube oil-heavy466 Lube oil-light467 Magnesium468 Magnesium powder469 Magnesium shavings470 Magnesium/telfon flare mix471 Manganese472 Mathane473 MBDA residues474 Me Allyl PH475 Me Isopropyl phosphine476 Me N-Propylphosphine477 Me2ETp478 Me2NBCl2 Et2O479 Me2NH480 Me2PH481 Me4P2482 Me-D3 Iodide483 MeEtPBH2484 MeEtPH485 MePH2486 Mercuric oxide487 Mercury488 Mercury salts489 Metal additives (aluminum)490 Metal and/or metal oxides (Al, Bacon, Zirconium, magnesium)491 Metal oxides492 Metals493 Metals Alkali494 Methane495 Methane ethane496 Methane, large cylinders497 Methanol498 Methanol-benzene curric chloride-AlO3499 Methanol-Cupric Chloride-Aluminum Chloride Mixture500 Methanol-HCL501 Methyl acetylyne propadiene502 Methyl alcohol503 methyl cyclo hexane504 Methyl-borate methanol



505 Methyl-B-Trimethyl Borazine506 Metriol-tri-nitrate507 MHF-5508 MIPB509 Misc Acids510 Misc binders (FEFO/R-18, NG/R-18, TMETN/R-18, PGDNFE/EA-AA)511 Misc lab chemicals512 Misc samples of AB-1, QMB-3, and MBDA513 Misc small vials of TNM514 Misc solid propellant scraps515 Misc solid propellant waste516 Misc. Contaminated fuels517 Misc. flammables518 Misc. Lab Chemicals519 Misc. Lab Chemicals (Various Size & Type)520 Misc. Lab chemicals and samples521 Misc. Laboratory Chemicals522 Misc. phenols523 Misc. small cylinders524 Misc. Waste chem.525 Mix Oxides526 Mixed oxides527 Mixed TAGN/HMX (dry)528 MMH529 MMH 70 ml + Freon TF530 Mono-Methyl-Hydrazine531 Muriatic532 Muriatic acid533 Muriatic Acids534 Mydyne 535 Mydyne (drain back)536 N2 gas generator pellets (NaN3 based)537 N2H4 + cap; 538 NAK539 NAKA propellents540 NAKA solid541 NAKA waste-pyro scrap, Kim wipes542 Napalm543 Naphthalene544 Napthalene545 NC546 NC RDX etc547 NC, NG, R-18, NDPA, HO1, ZrH2, Si, AP, GAP, GAPA, N-100, KCLO3, NaHCO3, S, Yellow dye, Paper, plastic

containers.548 NC/CAB/DANPE/DINA/CMP 25%, RDX 75%. PEG/NG 50%, RDX/Al2O3/Cr2O3 50%.

GAP/TMETN/GAPA/TEGDN/DANPE 50%, Atlasol yellow dye 50%.549 N-Dimethyl-B-Trimethyl Borazine



550 Neutralized acid551 Nickel552 Nitrate Agar553 Nitric acid554 Nitric Acid (contaminated)555 Nitric acid Sol556 Nitric and Hydrofluoric Acid Mixture557 Nitric oxide558 Nitrocellulose559 nitrocellulose RDX560 Nitrocellulose, NC561 Nitroexthane562 Nitrogen tetroxide563 Nitrogen Tetroxide (contaminated)564 Nitrogen trifluoride565 Nitrogentetroxide566 Nitroglycerin567 Nitroglycerin 180# solution in 30% methylene chloride solution568 Nitroglycerin, NG569 Nitroguandine570 Nitromethane poured onto sawdust: 2-500 gram bottle571 Nitrostarch572 Nitrosyl chloride573 Nitrous oxide574 NONA575 NTO576 NTO cont. hardware577 NTO containing hardware578 NTO containing hardware and cylinders579 NTO cylinder 580 NTO cylinders581 NTO/ 30% alcohol and 70% E20.582 N-trimethly borazole583 N-trimethyl borazale584 N-Trimethyl borazine585 N-Trimethyl-B-Methyl boranzine586 oil587 Oil (contaminated)588 Oil Waste589 Oil, waste590 Oil/Oil waste591 Organic binder (HTPB)592 Oxidizers593 Oxidizers (ammonium nitrate)594 Oxygen595 Oxygen + nitrogen596 Oxygen cylinders



597 Oxygen difluoride598 Oxygen Difluoride Gas599 Oxygen difluorine600 Oxygen Gas601 Oxygen/nitrogen602 Oxygen-nitrogen603 Paint604 paint and thinner mix605 Paint sludge606 Paint thinner607 Paint, mixtures608 Paper towels609 Paper towels contaminated with binder610 Paper towels contaminated with small amounts of oxidizer611 Paper towels contaminated with small amounts of plasticizers612 Paper, plastic containers613 Para xylene614 Partially decomposed metallic materials all empty615 PEG/NG 50%, RDX/Al2O3/Cr2O3 50%, paper towels, plastic containers616 PEG/NG 50%, RDX/MgO 50%, paper towels, plastic containers617 Pentaborane618 Pentaborane + unknown619 Pentaborane and acetone620 Pentaborane and RP1621 Pentaborane. 2 ampoules622 Penteborane and acetone623 Penteborane and RP1624 Penteborane and RP-1625 Perchloric Acid626 Perchloroethylene627 Permangante Mix628 Pet. Benzene629 PGDNE630 PGDN-FEFO631 PH632 PH2(CH2)3PH2633 PH2(CH2)4PH2634 Phenols635 Phenyl methyl phosphine636 Phenyl phosphine637 Phillips Soltrol 150638 Phillips Soltrol 170639 Phosphoric Acid640 Phosphorous 641 Phosphorous oxychloride642 Phosphorus643 Phosphorus Oxychloride



644 Pipe residue645 Pipernal646 Plasticizer (triethyleneglycol dinitrate, TEGDN)647 Plasticizers648 Plastisol Nitrocellulose649 Plating solution650 PNC651 Polymer652 Polymer soap oil653 Polymer Waste654 Polymer/polymer waste655 Potassium656 Potassium Bromide657 Potassium cyanide658 Potassium Perchlorate659 Potassium perchlorate, KP660 Potassium permangante661 Potasssium Cyanide662 PPNF-Nitrocellulose663 PrBCl2664 Propane665 Propane/air666 Propellant and Pyrotechnic scraps 667 Propellant scraps, wipes668 Propellant, solid669 Propellant, solids670 Propellants671 Propyl nitrate 672 Propylnitrate poured onto sawdust: 1-500 gram bottle673 PS555, GAPA, N-100, AP, GAP, NAHCO3, S, KClO4, yellow dye, RDX, CMP, Si, R-45, DDI, CuO2O2, DANPE,

paper, plastic containers.674 Pyradine675 Pyridine676 Pyroforic liquids677 Pyrophoric Aluminum678 Pyrophoric Igniter679 Pyrophoric Ingiter680 Pyrotechnic igniter681 Pyrotechnic Ingiter682 Pyrotechnic misc. types683 pyrotechnics: organic binders; plasticizers; oxidizers; and metal or metal oxide additives684 Quarz Vool685 R-45, DD1, AP, CuO2O2, Al, si, CMP, GAP, N-100, GAPA, KClO4, ATLASOL yellow dye, KClo3, NaHCO3, S,

paper, plastic containers.686 R-45, DD1, GAP, GAPA, N-100, R-18, HMD1, NC, NG, PS555, DANPE, AP, KClO4, KClO3, RDX, NaHCO3, S,

Si, PMP, Al, CuO2O2



687 R-45, DD1, IDP, s, KClO3, ATLASOL yellow, NC, ba(NO3)2, NaHCO3, GAP, N-100, AP, TMETN, MNA, C, TPB, R-18, HMD1, Mo, B, DD1, I2O5, DANPE, RDX, CMP, ATEC, DATH.

688 R-45, DDi, AP, CuO2O2, Al, Si, GAP, N-100, yellow dye, GAPA, TMETN, CMP, DANPE, ethyl alcohol, acetone, toluene.

689 R-45, DDi, AP, CuO2O2, Al, Si, GAP, N-100, yellow dye, GAPA, TMETN, CMP, DANPE, paper towels, plastic containers

690 Ram set charges691 RDX692 RDX-Nitrocellulose693 Reactive waste694 reagent chemical bottles695 Red fume nitric acid696 Red Fuming HNO3697 red fuming nitric acid698 Redfume nitric acid699 Resin700 REX-17701 Rifle shells702 RJ-1703 RJ-1 fuel704 Rosin Flux705 RP0435706 RP1707 RP-1708 RP1 (contaminated)709 RP-1 (contaminated)710 RP-1 (kerosene base)711 RP1 and addatives712 RP1 and pentaborane713 RP1 and TCP714 RP1 and TEA715 RP1 and water Mix716 RP1, penteborane mix717 RP-1/TEA TEB718 Rubber binder (HTPB-hydroxy terminated polybutadiene) 719 Scrap gun propellant720 Scrap solid propellant721 Shell dispersol722 Shell laquer diluent723 Silicate of soda724 Silicon725 SKL-4-DXE726 Small B, GM cylinders727 Small cylinders728 Small GM cylinders729 Small green cylinder730 Small green smoke pellet



731 Small unknown cylinders732 small white canister 733 Small white canister 30psi N2734 Smoke flares735 Smoke grenade mat.736 Smoke mix737 Smoke powder738 Soda ash739 Sodium740 Sodium (used)741 Sodium Arsenite742 Sodium chromate743 Sodium fluoride744 Sodium hydroxide745 Sodium nitrate746 Sodium nitrite747 Sodium phosphate748 Sodium Waste749 Sodium, waste750 Soldering Flux751 Solid gun propellant scrap752 Solid oxidizers (hexogen)753 Solid propellant754 solid propellant and heptane755 Solid propellant scrap756 Solid propellant scraps plus misc ampolues from VanOwen. 757 Solid propellants758 solid propellants: rubber binder, plasticizers, oxidizers, and metal additives759 Solids, unknown760 Solvent761 Solvent waste762 Solvent/Solvent waste763 Solvents764 Squib 101513765 Squib 19-403189766 Squib valve 19-403211, P/N 1943767 Stenciled fluorine768 Stoddard Solvent769 Sulfur dioxide770 Sulfuric Acid771 Sulfuric trioxide772 Sulfus dioxide773 Sulphuric Acid774 TAE775 TAGN776 TAGN in IPA777 TAMA



778 Tar779 TATB780 t-BuBCl2781 TCE782 TEA783 TEA (cylinder)784 TEA and RP1785 TEA and TEAB ignitors786 TEA and TEB mixtures with RP1787 TEA B788 TEA cylinders789 TEA samples790 TEA, RP-1791 TEA/TEB792 TEA/TEB/RP-1793 TEA/TEB/RP-1 + cap794 TEA/TEB/RP-1 + cap. 4-1 gallon cans795 TEAB796 TEAB igniters797 TEAB, RP-1798 TEAB+RP-1799 TEB800 TEB canister801 TEB in canister802 TEB+TEAB igniters803 Tetra isobutylene804 Tetrafluorane805 Tetrafluorohydrazine806 Tetraisobutylene807 Tetramethylene phosphine808 Thinner809 Thiophosgene Cl2CS810 Titanium811 Titanium Tetrachloride812 Titanium Trichloride813 TMETN/GAP 30 %, AP, CP, C 70%. Mix 3-22-1,2,3814 TMETN/GAP 30 %, AP, CP, C 70%. Mix 3-22-1815 TMETN/GAP 30 %, AP, CP, C 70%. Mix 3-22-2816 TMETN/GAP 30 %, AP, CP, C 70%. Mix 3-22-3817 TNN818 TNT819 Toluene820 Toluene discoyante821 Triaminoguanidine nitrate822 Triaminoguanidine nitrate, TAGN823 Tributylamine824 Tributylborane



825 Tri-chlor826 Trichlorethylene827 Trichloro828 Trichloroethene829 Trichloroethylene830 Trichlorr and polymer831 Triethyl Aluminum832 Triethyl Aluminum Borane833 Triethylaluminum834 Triethylaluminum/triethylboran cylinder (NEAT, TEA/TEB 14 lb)835 Triethylaluminum/triethylboron836 Triethylamine837 Triethylborane838 Triethylboron839 Triethylboron (PIG) cylinder (TEB volume 14lb; NEAT, TEA/TEB 14 lb)840 Triethylboron cylinder (TEB volume 69.5 lbs)841 Triethylboron-RPI Mixture842 Triethyleneglycol dinitrate, TEGDN843 Triethylene-Glycol-Dinitrate844 Trifluoroacetic anahydride845 Trigger Assembly 1617-170-01846 Trigger Assembly ST2840002 RES005847 Trigger Assembly ST2840002 RES007848 Trimethioltrinitrate, TMETN849 Trimethyl borane850 Trimethyl boron851 Trimethyl-borate-CH3OH852 Trimethyl-Borate-Methanol853 Trimethylolethane trinitrate854 Tri-o-cresyl borate855 TTTT855 Turbine spinner grains855 Turco acid (contaminated)855 Turco acid (Lithium chloride)855 TVOPA855 UDMH855 UDMH (contaminated)855 UDMH +cap855 UDMH 90%, water 10%855 UDMH and water855 UDMH and water (drain back)855 UDMH empty xR Drums855 UDMH mixtures855 Unidentified chemicals855 unidentified cylinder855 Unidentified Fuel855 Unidentified fuels



855 Unidentified liquid855 Unidentified material855 Union thinner855 Unknown855 Unknown (AA2015 propane/air)855 Unknown (F2)855 Unknown (large cylinder)855 Unknown ampoule855 Unknown cyclinder855 Unknown cylinder855 Unknown cylinders855 Unknown large cyclinder855 Unknown quantity/contents K-bottle855 Unknown RP C4-9208855 Unknown RP4-920855 Unknown substances855 Unknown type empty cylinders855 Unknown vial855 Unsymetrical-Dimethyl-Hydrazine855 US Navy MP0607855 Valve Assembly NA5-260180-1D855 Versamid 140855 VM-P Naptha855 Waste acid855 Waste Oil855 Waste Polymers855 Water purifier-polymetrics 7145631520855 Water with <5% binders855 Water, nitroglycerin, hexane, heptane855 white fuming nitric acid855 White K bottle855 Xylene855 Zero gas855 Zinc855 Zirconium Hydride powder855 Zirconium nitrocellulose855 Zirconium powder855 ZnEt2


of 5TABLE IIANALYTES TARGETED IN PREVIOUS INVESTIGATIONS AT AREA I BURN PITAIBP SWMU 4.8 RFI WORK PLANBOEING SANTA SUSANA FIELD LABORATORYVENTURA COUNTY, CALIFORNIA

ANALYSIS GROUP ANALYTE CAS NUMBERANIONS Bicarbonate (as CaCO3) 71523ANIONS Carbonate (as CaCO3) 3812326ANIONS Chloride 16887006ANIONS Fluoride 16984488ANIONS Nitrate 14797558ANIONS Sulfate 14808798GEN MIN Total Dissolved Solids NAVOC 1,1,1-Trichloroethane 71556VOC 1,1,2,2-Tetrachloroethane 79345VOC 1,1,2-Trichloroethane 79005VOC 1,1-Dichloroethane 75343VOC 1,1-Dichloroethene 75354VOC 1,2,4-Trichlorobenzene 120821VOC 1,2-Dibromo-3-chloropropane (DBCP) 96128VOC 1,2-Dibromoethane 106934VOC 1,2-Dichlorobenzene 95501VOC 1,2-Dichloroethane 107062VOC 1,2-Dichloroethene 540590VOC 1,2-Dichloropropane 78875VOC 1,3-Dichlorobenzene 541731VOC 1,4-Dichlorobenzene 106467VOC 2-Butanone 78933VOC 2-Hexanone 591786VOC 4-Methyl-2-pentanone 108101VOC Acetone 67641VOC Benzene 71432VOC Bromodichloromethane 75274VOC Bromoform 75252VOC Bromomethane 74839VOC Carbon disulfide 75150VOC Carbon tetrachloride 56235VOC Chlorobenzene 108907VOC Chloroethane 75003VOC Chloroform 67663VOC Chloromethane 74873VOC cis-1,2-Dichloroethene 156592VOC cis-1,3-Dichloropropene 10061015VOC Cyclohexane 110827VOC Dibromochloromethane 124481VOC trans-1,2-Dichloroethene 156605VOC Dichlorodifluoromethane (CFC-12) 75718VOC Dichloromethane 75092VOC Ethylbenzene 100414VOC Isopropanol 67630VOC Isopropylbenzene 98828VOC Methyl acetate 79209VOC Methyl cyclohexane 108872VOC 4-Methyl-2-pentanone (MIBK) 108101VOC Methyl tert butyl ether (MTBE) 1634044VOC Methylene chloride 75092

Haley & Aldrich, Inc. G:\Projects\26472\Reports\M477 A1BP RFI Workplan\Tables\2006-1110-HAI-SSFL.M477.T02.F.xls

November 2006


ANALYSIS GROUP ANALYTE CAS NUMBERVOC Styrene 100425VOC Tetrachloroethene 127184VOC Toluene 108883VOC trans-1,3-Dichloropropene 10061026VOC Trichloroethane NAVOC Trichloroethene 79016VOC Trichlorofluoromethane (CFC-11) 75694VOC 1,1,2-Trichlorotrifluoroethane 76131VOC Trifluorotrichloroethane (Freon 113) 76131VOC Vinyl chloride 75014VOC 1,4-Dioxane 123911VOC Xylenes, Total 1330207SVOC 2,2'-oxybis(1-Chloropropane) (bis(2-chloroisopropyl) ether) 108601SVOC 2,4,5-Trichlorophenol 95954SVOC 2,4,6-Trichlorophenol 88062SVOC 2,4-Dichlorophenol 120832SVOC 2,4-Dimethylphenol 105679SVOC 2,4-Dinitrophenol 51285SVOC 2,4-Dinitrotoluene 121142SVOC 2,6-Dinitrotoluene 606202SVOC 2-Chloronaphthalene 91587SVOC 2-Chlorophenol 95578SVOC 2-Methylnaphthalene 91576SVOC 2-Methylphenol 95487SVOC 2-Nitroaniline 88744SVOC 2-Nitrophenol 88755SVOC 4-Nitrophenol 100027SVOC 3,3'-Dichlorobenzidine 91941SVOC 3-Nitroaniline 99092SVOC 4,6-Dinitro-2-methylphenol 534521SVOC 4-Bromophenyl phenyl ether 101553SVOC 2-Bromophenol 95567SVOC 4-Chloro-3-methylphenol 59507SVOC 4-Chloroaniline 106478SVOC 4-Chlorophenyl phenyl ether 7005723SVOC 4-Methylphenol 106445SVOC 4-Nitroaniline 100016SVOC 4-Nitrophenol 100027SVOC Acenaphthene 83329SVOC Acenaphthylene 208968SVOC Acetophenone 98862SVOC Anthracene 120127SVOC Atrazine 1912249SVOC Benzaldehyde 100527SVOC Benzo(a)anthracene 56553SVOC Benzo(a)pyrene 50328SVOC Benzo(b)fluoranthene 205992SVOC Benzo(g,h,i)perylene 191242SVOC Benzo(k)fluoranthene 207089SVOC Biphenyl 92524


November 2006


ANALYSIS GROUP ANALYTE CAS NUMBERSVOC bis(2-Chloroethoxy)methane 111911SVOC bis(2-Chloroethyl)ether 111444SVOC bis(2-Ethylhexyl)phthalate 117817SVOC Butyl benzylphthalate 85687SVOC Butoxycellosolve 111762SVOC Caprolactam 105602SVOC Carbazole 86748SVOC 2-Chlorophenol 95578SVOC Chrysene 218019SVOC Di-n-butylphthalate 84742SVOC Di-n-octyl phthalate 117840SVOC Dibenz(a,h)anthracene 53703SVOC Dibenzofuran 132649SVOC Diethyl phthalate 84662SVOC 2,4-Dimethylphenol 105679SVOC Dimethyl phthalate 131113SVOC Fluoranthene 206440SVOC Fluorene 86737SVOC Hexachlorobenzene 118741SVOC Hexachlorobutadiene 87683SVOC Hexachlorocyclopentadiene 77474SVOC Hexachloroethane 67721SVOC Indeno(1,2,3-cd)pyrene 193395SVOC Isophorone 78591SVOC N-Nitrosodi-n-propylamine 621647SVOC N-Nitrosodiphenylamine 86306SVOC Naphthalene 91203SVOC Nitrobenzene 98953SVOC Pentachlorophenol 87865SVOC Phenanthrene 85018SVOC Phenol 108952SVOC Pyrene 129000SVOC Tetrachlorophenol 25167833SVOC 1,2,6-Tribromophenol NAPCB Aroclor-1016 (PCB-1016) 12674112PCB Aroclor-1221 (PCB-1221) 11104282PCB Aroclor-1232 (PCB-1232) 11141165PCB Aroclor-1242 (PCB-1242) 53469219PCB Aroclor-1248 (PCB-1248) 12672296PCB Aroclor-1254 (PCB-1254) 11097691PCB Aroclor-1260 (PCB-1260) 11096825METAL Aluminum 7429905METAL Antimony 7440360METAL Arsenic 7440382METAL Barium 7440393METAL Beryllium 7440417METAL Boron 7440428METAL Cadmium 7440439METAL Calcium 7440702METAL Chromium Total 7440473


November 2006


ANALYSIS GROUP ANALYTE CAS NUMBERMETAL Chromium, Hexavalent 18540299METAL Cobalt 7440484METAL Copper 7440508METAL Iron 7439896METAL Lead 7439921METAL Lithium 7439932METAL Magnesium 7439954METAL Manganese 7439965METAL Mercury 7439976METAL Molybdenum 7439987METAL Nickel 7440020METAL Phosphorus 14265442METAL Potassium 7440097METAL Selenium 7782492METAL Silica 7631869METAL Silicon (as (SiO2) 7440218METAL Silver 7440224METAL Sodium 7440235METAL Strontium 7440246METAL Thallium 7440280METAL Tin 7440315METAL Titanium 7440326METAL Vanadium 7440622METAL Zinc 7440666METAL Cyanide 57125Semiquantitative (TIC) Unknown Akipate NASemiquantitative (TIC) Molecular Sulfur 63705055Semiquantitative (TIC) Unknown Hydrocarbon NATPH C6-C12 (Gasoline) NATPH C07-C24 (Heavy Oil) NATPH C07-C28 (Diesel Range) NATPH C10-C24 (Diesel Range) NATPH C12-C28 NATPH C16-C28 NATPH Diesel NAPERCHLORATE Perchlorate 14797730pH pH 12408025HYDRAZINE Hydrazine 302012MERCAPTANS Mercaptans 109795DIOXIN 1,2,3,4,6,7,8-HpCDD 35822469DIOXIN 1,2,3,4,6,7,8-HpCDF 67562394DIOXIN 1,2,3,4,7,8,9-HpCDF 55673897DIOXIN 1,2,3,4,7,8-HxCDD 39227286DIOXIN 1,2,3,4,7,8-HxCDF 70648269DIOXIN 1,2,3,6,7,8-HxCDD 57653857DIOXIN 1,2,3,6,7,8-HxCDF 57117449DIOXIN 1,2,3,7,8,9-HxCDD 19408743DIOXIN 1,2,3,7,8,9-HxCDF 72918219DIOXIN 1,2,3,7,8-PeCDD 40321764DIOXIN 1,2,3,7,8-PeCDF 57117416


November 2006


ANALYSIS GROUP ANALYTE CAS NUMBERDIOXIN 2,3,4,6,7,8-HxCDF 60851345DIOXIN 2,3,4,7,8-PeCDF 57117314DIOXIN 2,3,7,8-TCDD 1746016DIOXIN 2,3,7,8-TCDF 51207319DIOXIN OCDD 3268879DIOXIN OCDF 39001020DIOXIN TCDD TEQ (ND = 0) NADIOXIN Total HpCDD 37871004DIOXIN Total HpCDF 38998753DIOXIN Total HxCDD 34465468DIOXIN Total HxCDF 55684941DIOXIN Total PeCDD 36088229DIOXIN Total PeCDF 30402154DIOXIN Total TCDD 41903575DIOXIN Total TCDF 55722275


November 2006

of 1TABLE IIIAREA I BURN PIT - SWMU 4.8 SUMMARY OF ANALYTICAL METHODS RATIONALEAIBP SWMU 4.8 RFI WORK PLANBOEING SANTA SUSANA FIELD LABORATORYVENTURA COUNTY, CALIFORNIA

Parameter(s) for Analysis Analytical Method RationaleTarget Compound List Volatile Organic Compounds (TCL VOCs)

EPA Method 8260B Historical detection of VOCs in groundwater and soils (i.e. Trichloroethene) and documented disposal of waste solvents at the A1BP.

1,4-dioxane EPA 8260B SIM Used as a preservative for chlorinated solvent TCE and 1,1,1-TCA.

Target Compound List Semi-Volatile Organic Compounds (TCL SVOCs)

EPA Method 8270C Historical detection of phthalates related to the disposal of plasticizers and the potential for the formation of Products of Incomplete Combustion (PICs) from the burning of wastes that could include polyaromatic hydrocarbons (PAHs) i.e. benzo (a) pyrene.

Formaldehyde EPA Method 8315A Historical detection and the documented disposal of formaldehyde in the AIBP.

Polychlorinated dibenzo–p-dioxins and Polychlorinated dibenzo–p-furans (PCDD/PCDFs)

EPA Method 8290 Historical detection of dioxins/furans in site soils and sediment and the potential for the formation of PICs from the burning of wastes that could include polychlorinated biphenyl (PCBs) compounds.

Target Analyte List (TAL) Metals plus boron, mercury, tin, titanium, strontium, and zirconium

EPA Method 6010B, 6020, 7471A

Historical detection (i.e. chromium) and the documented disposal of metal containing wastes in the AIBP.

Perchlorate EPA Method 314/8321M

Historical detection of perchlorate in soil leachate in the AIBP area Outfall.

PCBs EPA Method 8082 Documented disposal of PCBs containing wastes in the AIBP.

Nitroso-dimethyl amine (NDMA) EPA Method 1625C The documented disposal of Unsymmetrical Dimethyl Hydrazine (UDMH) in the AIBP area. UDMH rapidly decomposes to NDMA upon contact with soil pore moisture.

Hydrazines EPA Method 8315A Documented disposal and analytical detection of hydrazines, including monomethyl hydrazine, in the AIBP.

Nitroaromatics (Nitrobenzene, Trinitrotoluene (TNT), dintrotoluene, RDX and HMX)

EPA Method 8330A The documented use of energetic compounds to detonate waste materials for disposal in the AIBP area.

Total Anions (i.e. chloride, fluoride, sulfate, nitrate and nitrite)

EPA Method 300 The documented disposal of reagent grade acids including: Hydrochloric acid (HCl), Sulfuric acid (H2SO4), Hydrofluoric acid (HF), and Nitric acid (HNO3).

Total Cyanide (CN) EPA Method 9012A Historical detection of CN in soils within the AIBP.

Soil pH Levels EPA Method 150.2 The documented disposal of reagent grade acids and bases in the AIBP.

Total Ammonia (NH3), Total Kjeldahl Nitrogen (TKN) and Total Organic Nitrogen (TON)

Std Methods 18th Edition Method 4500

The documented disposal of organic amines including Tetraethylamine (TEA) and other organic compounds containing forms of nitrogen. (amines, amides and ammonium salts).

Total Petroleum Hydrocarbons (TPH) EPA Method 8015 The documented use of petroleum distillates as accelerates for the disposal of wastes in the AIBP.

Organochlorine Compounds EPA Method 8081A Documented disposal of organo-chlorine compounds (trade name: Dechlorane) waste in the AIBP.

Haley & Aldrich, Inc.G:\Projects\26472\Reports\M477 A1BP RFI Workplan\Tables\2006-1110-HAI-SSFL.M477.T03.F.xls November 2006

of 7TABLE IVSUMMARY OF PROPOSED SAMPLING LOCATIONSAREA I BURN PIT AREA- SWMU 4.8BOEING SANTA SUSANA FIELD LABORATORYVENTURA COUNTY, CALIFORNIA

Area I Burn Pit Area Feature (SEE FIGURE 10) Sampling Rationale Basis/Key Document Number(s)* Proposed Sampling1

Approximate Number of Samples

Matrix

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Soil VaporTargeted locations across AIBP Area Source areas, operational features Historical operations Collect and analyze soil vapor samples at 3 ft bgs at

geophysical anomolies and at locations where depth to bedrock is 5 feet or less. Collect and analyze soil vapor samples at 3 feet and at top of bedrock at locations were depth to bedrock is greater than 5 feet.

76 Vapor 76

Earth Pond 1SW corner of SWMU 4.8 - one proposed exploratory trench

Source area Historical operations area and environmental analytical data

Collect samples at ground surface and at base of each exploratory trench. HOLD sample at base of trench if no field evidence of soil impacts.

4 Soil 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4

SW corner of SWMU 4.8 Source area Historical operations area and environmental analytical data

Collect samples at 0.5 ft bgs, between 3-5 ft bgs, and/or just above bedrock

10 Soil 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10

SW corner of SWMU 4.8 Operational feature Historical operations area and environmental analytical data

Collect samples at ground surface and 3.5-4.0 ft bgs on containment berm.

6 Soil 6 6 6 6 6 6 6 6 6 6

Earth Pond 2SW corner of SWMU 4.8 - one proposed exploratory trench


Collect samples at ground surface and at base of each exploratory trench. HOLD sample at base of trench if no field evidence of soil impacts.

4 Soil 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4

SW corner of SWMU 4.8 Source area Historical operations area and environmental analytical data


18 Soil 18 18 18 18 18 18 18 18 18 18 18 18 18 18 18 18 18 18 18 18

SW corner of SWMU 4.8 Operational feature Historical operations area and environmental analytical data

Collect samples at ground surface and 3.5-4.0 ft bgs on containment berm.

6 Soil 6 6 6 6 6 6 6 6 6 6

Former Explosive ShedsEast of Earth Ponds 1 and 2 Source area Photographs G-4.9 Collect samples at 0.5 ft bgs, between 3-5 ft bgs, and/or

just above bedrock4 Soil 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4

Former Fire Demonstration AreaFormer Fire Demonstration Area and Sample Location RR-8 - two proposed exploratory trenches


Collect samples at ground surface and at base of each exploratory trench. HOLD sample at base of trench if no field evidence of soil impacts there.

8 Soil 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8

Former Fire Demonstration Area and Sample Location RR-8 - along sides of proposed exploratory trenches



8 Soil 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8

1982 Excavations 1-5Former (1982) excavations 1-3, W of TTF Source area Historical operations area and environmental

analytical dataCollect samples at 0.5 ft bgs, between 3-5 ft bgs, and just above bedrock

12 Soil 12 12 12 12 12 12 12 12 12 12 12 12 12 12 12 12 12 12 12 12

Former (1982) excavation 4, W of TTF, and including geophysical anomaly

Source area Diagram P-3.3 Collect samples at 0.5 ft bgs, between 3-5 ft bgs, and just above bedrock

21 Soil 21 21 21 21 21 21 21 21 21 21 21 21 21 21 21 21 21 21 21 21

Perimeter of former (1982) excavation 4, W of TTF

Operational feature Historical operations area and environmental analytical data

Collect samples at 0.5 ft bgs, between 3-5 ft bgs, and just above bedrock

9 Soil 9 9 9 9 9 9 9 9 9 9

Former (1982) excavation 5, NE of Concrete Pad 2



2 Soil 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2

RFI Suite

See last page of Table IV for notes and abbreviations Haley & Aldrich, Inc. G:\Projects\26472\Reports\M477 A1BP RFI Workplan\Tables\2006-1110-HAI-SSFL.M477.T04.F.xls

November 2006




Matrix

VO

Cs

(soi

l vap

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VO

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(soi

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ium

(HO

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RFI Suite

Concrete Pad 1 AreaFormer Concrete Pad 1 Operational feature Historical operations area Collect samples at 0.5 ft bgs, between 3-5 ft bgs, and/or

just above bedrock2 Soil 2 2 2 2 2 2 2 2 2 2

Former structure, N side of Concrete Pad 1, within drum and/or equipment storage area

Operational area, potential source area

Photographs T-2_2 Collect samples at 0.5 ft bgs, between 3-5 ft bgs, and/or just above bedrock

2 Soil 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2

Within drum and/or equipment storage area, NW of Concrete Pond (removed)

Operational feature Photographs T-2_2 Collect samples at 0.5 ft bgs, between 3-5 ft bgs, and/or just above bedrock

2 Soil 2 2 2 2 2 2 2 2 2 2

Former structure, NW of Concrete Pad 1 Operational feature Photographs MW-40_5 Collect samples at 0.5 ft bgs, between 3-5 ft bgs, and/or just above bedrock

2 Soil 2 2 2 2 2 2 2 2 2 2

Concrete Pond (removed)Within former concrete pond, NE of Burn Pit 1



2 Soil 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2

Control Center AreaAt former Control Center Source area Photographs T-2_2, historical operations area and

environmental analytical dataCollect samples at 0.5 ft bgs, between 3-5 ft bgs, and/or just above bedrock

2 Soil 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2

N of former Control Center Operational feature Photographs T-2_2 Collect samples at 0.5 ft bgs, between 3-5 ft bgs, and/or just above bedrock

2 Soil 2 2 2 2 2 2 2 2 2 2

Former structures N of Control Center, within drum and/or equipment storage area

Operational feature, potential source area

Photographs T-2_2 Collect samples at 0.5 ft bgs, between 3-5 ft bgs, and/or just above bedrock

4 Soil 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4

N of Control Center (removed), within drum and/or equipment storage area

Operational feature Photographs T-2_2 Collect samples at 0.5 ft bgs, between 3-5 ft bgs, and/or just above bedrock

8 Soil 8 8 8 8 8 8 8 8 8 8

Former nitrogen tetroxide tank at NE corner of SWMU 4.8

Operational feature Diagram MW-44 Collect samples at 0.5 ft bgs, between 3-5 ft bgs, and/or just above bedrock

2 Soil 2 2 2 2 2 2 2 2 2 2

Burn Pit 1One proposed exploratory trench at former Burn Pit 1



4 Soil 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4

TTF Interim Status FacilityWithin Burn Pit 2 Source area Historical operations area and environmental

analytical dataCollect samples at 0.5 ft bgs, between 3-5 ft bgs, and/or just above bedrock

3 Soil 3 3 3 3 3 3 3 3 3 3 3 3 3 3 3 3 3 3 3 3

W and E perimeter of Burn Pit 2 Source area Historical operations area and environmental analytical data


6 Soil 6 6 6 6 6 6 6 6 6 6 6 6 6 6 6 6 6 6 6 6

Northern and southern containment berms of Burn Pit 2

Operational feature Historical operations area Collect samples at ground surface and 3.5-4.0 ft bgs on containment berm.

8 Soil 8 8 8 8 8 8 8 8 8 8

SW perimeter of Burn Pit 2 berm Operational feature Historical operations area Collect samples at 0.5 ft bgs, between 3-5 ft bgs, and/or just above bedrock

3 Soil 3 3 3 3 3 3 3 3 3 3

At former Concrete Pad 2 Source area Historical operations area and environmental analytical data


2 Soil 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2

Within containment berm of former Concrete Pad 2



6 Soil 6 6 6 6 6 6 6 6 6 6 6 6 6 6 6 6 6 6 6 6

Perimeter of former Concrete Pad 2 and containment berm, including 3 geophysical anomalies

Operational feature Historical operations area and environmental analytical data; Diagram P-3.3


8 Soil 8 8 8 8 8 8 8 8 8 8


November 2006




Matrix

VO

Cs

(soi

l vap

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VO

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(soi

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Cya

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(die

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(RD

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(HO

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RFI Suite

Containment berm of former Concrete Pad 2

Operational feature Historical operations area Collect samples at ground surface and 3.5-4.0 ft bgs on containment berm.

4 Soil 4 4 4 4 4 4 4 4 4 4

Concrete Ponds 2 and 3 Area Within the former concrete ponds Source area Historical operations area and environmental

analytical dataCollect samples at 0.5 ft bgs, between 3-5 ft bgs, and/or just above bedrock

4 Soil 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4

Around and between the former concrete ponds

Operational feature Diagram P-3_8, photographs T-2_2 Collect samples at 0.5 ft bgs, between 3-5 ft bgs, and/or just above bedrock

10 Soil 10 10 10 10 10 10 10 10 10 10

Within former burn pit W of Concrete Pond 2 - one proposed exploratory trench

Source area Diagram P-3_8, photographs T-2_2 Collect samples at ground surface and at base of each exploratory trench. HOLD sample at base of trench if no field evidence of soil impacts there.

4 Soil 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4

Earth Pond 3 Within former Earth Pond 3 and former burn pit - two proposed exploratory trenches



10 Soil 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10

Perimeter of former Earth Pond 3 Operational feature Historical operations area and environmental analytical data


8 Soil 8 8 8 8 8 8 8 8 8 8

E of Earth Pond 3, near SW edge of Perimeter Pond

Operational feature Diagrams P-3.3 and P-3.8 suggest pipe and/or trench leading from Earth Pond 3 to Perimeter Pond


2 Soil 2 2 2 2 2 2 2 2 2 2

Isolated Geophysical Anomalies W of Earth Pond 2 Operational feature Diagram P-3.3 Collect samples at 0.5 ft bgs, between 3-5 ft bgs, and/or


N of Former Fire Demonstration Area Operational feature Diagram P-3.3 Collect samples at 0.5 ft bgs, between 3-5 ft bgs, and/or just above bedrock

6 Soil 6 6 6 6 6 6 6 6 6 6

SE side of Burn Pit 2, within former drum and/or equipment storage area

Operational feature, potential source area

Diagram P-3.3 Collect samples at 0.5 ft bgs, between 3-5 ft bgs, and/or just above bedrock

2 Soil 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2

S of TTF, just N of southern SWMU 4.8 boundary

Operational feature Diagram P-3.3 Collect samples at 0.5 ft bgs, between 3-5 ft bgs, and/or just above bedrock

2 Soil 2 2 2 2 2 2 2 2 2 2

NE edge of Earth Pond 3 Operational feature, potential source area

Diagrams P-3.3 and P-3.8 suggest pipe and/or trench leading from Earth Pond 3 to Perimeter Pond


2 Soil 2 2 2 2 2 2 2 2 2 2

NE of Concrete Pond 3 Operational feature, potential source area

Diagrams P-3.3 and P-3.8 suggest pipe and/or trench leading from Earth Pond 3 to Perimeter Pond


2 Soil 2 2 2 2 2 2 2 2 2 2

Between Earth Pond 3 and Perimeter Pond Operational feature Diagram P-3.3 Collect samples at 0.5 ft bgs, between 3-5 ft bgs, and/or just above bedrock

2 Soil 2 2 2 2 2 2 2 2 2 2

Three geophysical anomalies on S side of Earth Pond 3

Operational feature Diagram P-3.3 Collect samples at 0.5 ft bgs, between 3-5 ft bgs, and/or just above bedrock

6 Soil 6 6 6 6 6 6 6 6 6 6

Hummocky Area (West)Hummocky area NW of SWMU 4.8 - five proposed exploratory trenches

Operational feature Field reconnaissance Collect samples at ground surface and at base of each exploratory trench. HOLD sample at base of trench if no field evidence of soil impacts there.

20 Soil 20 20 20 20 20 20 20 20 20 20

Former structure N of the northwestern side of SWMU 4.8

Operational feature Diagram P-3.2 Collect samples at ground surface and at base of each exploratory trench. HOLD sample at base of trench if no field evidence of soil impacts there.

2 Soil 2 2 2 2 2 2 2 2 2 2


November 2006




Matrix

VO

Cs

(soi

l vap

or)

VO

Cs

(soi

l mat

rix)

SVO

Cs

Met

als

Cya

nide

Tot

al a

nion

s

For

mal

dehy

de

Nitr

ogen

Com

poun

ds3

pH

TPH

(die

sel a

nd o

il ra

nge)

PC

Bs

(HO

LD)

Nitr

oaro

mat

ics

(RD

X /H

MX)

Dio

xins

Per

chlo

rate

PA

Hs

PC

Bs4

Org

anoc

hlor

ine

Com

poun

ds

Hyd

razi

nes5

ND

MA

1,4

Dio

xane

Hex

aval

ent C

hrom

ium

(HO

LD)6

RFI Suite

Potential pipe outfall N of the northwestern side of SWMU 4.8

Operational feature Figure 10 feature Collect samples at ground surface and at base of each exploratory trench. HOLD sample at base of trench if no field evidence of soil impacts there.

2 Soil 2 2 2 2 2 2 2 2 2 2

Northern SWMU 4.8 Boundary AreaFormer structure NW of former Fire Dept. Demonstration Area

Operational feature 1964 photographs (MW-35) Collect samples at 0.5 ft bgs, between 3-5 ft bgs, and/or just above bedrock.

2 Soil 2 2 2 2 2 2 2 2 2 2

Former storage tanks along NW boundary of SWMU 4.8


1964 photographs (MW-35) Collect samples at 0.5 ft bgs, between 3-5 ft bgs, and/or just above bedrock.

4 Soil 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4

Eastern part of equipment storage area along northern boundary of SWMU 4.8


2 Soil 2 2 2 2 2 2 2 2 2 2

Hummocky Area (East) (North of Perimeter Pond)One proposed exploratory trench at hummocky area E of SMWU 4.8 and NW of Perimeter Pond

Operational feature Field reconnaissance Collect samples at ground surface and at base of each exploratory trench. HOLD sample at base of trench if no field evidence of soil impacts there.

4 Soil 4 4 4 4 4 4 4 4 4 4

Two proposed exploratory trenches at hummocky/former burn pit areas E of SMWU 4.8 and NW of Perimeter Pond


1964 photographs (MW-35), field reconnaissance Collect samples at ground surface and at base of each exploratory trench. HOLD sample at base of trench if no field evidence of soil impacts there.

8 Soil 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8

Four proposed exploratory trenches at hummocky/former structures area N of Perimeter Pond.

Operational feature Field reconnaissance Collect samples at 0.5 ft bgs, between 3-5 ft bgs, and/or just above bedrock.

16 Soil 16 16 16 16 16 16 16 16 16 16

One proposed exploratory trench at hummocky/former structures area N of Perimeter Pond.


1964 photographs (MW-35), field reconnaissance Collect samples at 0.5 ft bgs, between 3-5 ft bgs, and/or just above bedrock.

4 Soil 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4

Westernmost former structure N of Perimeter Pond, at end of feeder pipeline



2 Soil 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2

Former drum and/or equipment storage area, E of former structures N of Perimeter Pond



2 Soil 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2

Former drum and/or equipment storage areas, E of former structures N of Perimeter Pond


6 Soil 6 6 6 6 6 6 6 6 6 6

Former structures N of Perimeter Pond Operational feature 1964 photographs (MW-35) Collect samples at 0.5 ft bgs, between 3-5 ft bgs, and/or just above bedrock.

6 Soil 6 6 6 6 6 6 6 6 6 6

Former storage tank E of former structures, N of Perimeter Pond



2 Soil 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2

Western Migration PathwaysSW and S of Earth Pond 2, respectively Migration pathway Current topography Collect samples at 0.5 ft bgs, between 3-5 ft bgs, and/or


Along southwestern SWMU 4.8 boundary, east of Earth Pond 2

Migration pathway Current topography Collect samples at 0.5 ft bgs, between 3-5 ft bgs, and/or just above bedrock

2 Soil 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2


November 2006




Matrix

VO

Cs

(soi

l vap

or)

VO

Cs

(soi

l mat

rix)

SVO

Cs

Met

als

Cya

nide

Tot

al a

nion

s

For

mal

dehy

de

Nitr

ogen

Com

poun

ds3

pH

TPH

(die

sel a

nd o

il ra

nge)

PC

Bs

(HO

LD)

Nitr

oaro

mat

ics

(RD

X /H

MX)

Dio

xins

Per

chlo

rate

PA

Hs

PC

Bs4

Org

anoc

hlor

ine

Com

poun

ds

Hyd

razi

nes5

ND

MA

1,4

Dio

xane

Hex

aval

ent C

hrom

ium

(HO

LD)6

RFI Suite

Along southwestern SWMU 4.8 boundary and east of Earth Pond 2


4 Soil 4 4 4 4 4 4 4 4 4 4

Eastern Migration PathwaysAlong N to E side of former (1982) excavations 1-3

Migration pathway MW-44.1, current topography Collect samples at 0.5 ft bgs, between 3-5 ft bgs, and/or just above bedrock

9 Soil 9 9 9 9 9 9 9 9 9 9

N of former (1982) excavation 4 Migration pathway MW-44.1, current topography Collect samples at 0.5 ft bgs, between 3-5 ft bgs, and/or just above bedrock

3 Soil 3 3 3 3 3 3 3 3 3 3 3 3 3 3 3 3 3 3 3 3

SW of former (1982) excavation 4 Migration pathway MW-44.1, current topography Collect samples at 0.5 ft bgs, between 3-5 ft bgs, and/or just above bedrock

3 Soil 3 3 3 3 3 3 3 3 3 3

Along minor drainage leading from Burn Pit 2 and Concrete Pad 2 to the SE, towards SE corner of SWMU 4.8


10 Soil 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10

Along drainage from SW of former nitrogen tetroxide tank, E of former Control Center to E side of Earth Pond 3


10 Soil 10 10 10 10 10 10 10 10 10 10

In minor drainage SE of Concrete Pond 3 that drains SE towards the Outfall 011


2 Soil 2 2 2 2 2 2 2 2 2 2

Along SE-trending drainage, NE of NE side of SMWU 4.8

Down-drainage sample Current topography Collect samples at 0.05 ft bgs, between 3-5 ft bgs and/or just above bedrock, within drainage, at drainage banks. Collect additional samples at 10 ft step-outs of bank locations and HOLD, pending drainage results.

4 Sediment, Soil

4 4 4 4 4 4 4 4 4 4

End of SE-trending drainage, NE of NE side of SMWU 4.8

Down-drainage sample Current topography Collect samples at 0.05 ft bgs, between 3-5 ft bgs and/or just above bedrock, within drainage, at drainage banks. Collect additional samples at 10 ft step-outs of bank locations and HOLD, pending drainage results.

2 Sediment, Soil

2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2

In 2 minor drainages leading SW from structures formerly located N of Perimeter Pond


4 Soil 4 4 4 4 4 4 4 4 4 4

In minor drainage leading S from structures formerly located N of Perimeter Pond


2 Soil 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2 2

In two minor drainage leading SE to the SE-trending drainage on NE side of SMWU 4.8


2 Soil 2 2 2 2 2 2 2 2 2 2

Western DrainagesWesternmost drainage, W of Northwest Hummocks

Down-drainage sample Current drainage Collect samples at 0.05 ft bgs, between 3-5 ft bgs and/or just above bedrock, within drainage

4 Sediment, Soil

4 4 4 4 4 4 4 4 4 4

South of Northwest Hummocks, North of Earth Pond 1

Down-drainage sample Current drainage Collect samples at 0.05 ft bgs, between 3-5 ft bgs and/or just above bedrock within drainage

6 Sediment, Soil

6 6 6 6 6 6 6 6 6 6

SW of Earth Pond 2 Down-drainage sample Current drainage Collect samples at 0.05 ft bgs, between 3-5 ft bgs and/or just above bedrock, within drainage, and at drainage banks. Collect additional samples at 10 ft step-outs of bank locations and HOLD, pending drainage results.

9-13 Sediment, Soil

9-13 9-13 9-13 9-13 9-13 9-13 9-13 9-13 9-13 9-13 9-13 9-13 9-13 9-13 9-13 9-13 9-13 9-13 9-13 9-13


November 2006




Matrix

VO

Cs

(soi

l vap

or)

VO

Cs

(soi

l mat

rix)

SVO

Cs

Met

als

Cya

nide

Tot

al a

nion

s

For

mal

dehy

de

Nitr

ogen

Com

poun

ds3

pH

TPH

(die

sel a

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il ra

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PC

Bs

(HO

LD)

Nitr

oaro

mat

ics

(RD

X /H

MX)

Dio

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Per

chlo

rate

PA

Hs

PC

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Org

anoc

hlor

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Com

poun

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Hyd

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ND

MA

1,4

Dio

xane

Hex

aval

ent C

hrom

ium

(HO

LD)6

RFI Suite

Eastern DrainagesConcrete-lined drainage along NW side of Perimeter Pond

Down-drainage sample Current concrete-lined drainage Collect samples at 0.05 ft bgs 3 Sediment 3 3 3 3 3 3 3 3 3 3

South of Outfall 011 at SE corner of SWMU 4.8

Down-drainage sample Current drainage Collect samples at 0.05 ft bgs, between 3-5 ft bgs and/or just above bedrock, within drainage, and at drainage banks. Collect additional samples at 10 ft step-outs of bank locations and HOLD, pending drainage results.

9-13 Sediment, Soil

9-13 9-13 9-13 9-13 9-13 9-13 9-13 9-13 9-13 9-13 9-13 9-13 9-13 9-13 9-13 9-13 9-13 9-13 9-13 9-13

Southern Drainages (Figure 7)South of south-central SWMU 4.8 boundary

Down-drainage sample Current drainage Collect samples at 0.05 ft bgs, between 3-5 ft bgs and/or just above bedrock

2 Sediment, Soil

2 2 2 2 2 2 2 2 2 2

SW of SWMU 4.8, in western drainage Down-drainage sample Current drainage Collect samples at 0.05 ft bgs, between 3-5 ft bgs and/or just above bedrock, within drainage, and at drainage banks. Collect additional samples at 10 ft step-outs of bank locations and HOLD, pending drainage results.

9-13 Sediment, Soil

9-13 9-13 9-13 9-13 9-13 9-13 9-13 9-13 9-13 9-13

Along eastern drainage, S of SWMU 4.8 Down-drainage sample Current drainage At single sample locations, collect samples at 0.05 ft bgs, between 3-5 ft bgs and/or just above bedrock. At the multiple sample location, collect samples at 0.05 ft bgs, between 3-5 ft bgs and/or just above bedrock, within drainage, and at drainage banks. Collect additional samples at 10 ft step-outs of bank locations and HOLD, pending drainage results.

13-17 Sediment, Soil

13-17 13-17 13-17 13-17 13-17 13-17 13-17 13-17 13-17 13-17

Along drainage S of confluence of E and W drainages near SWMU 4.8

Down-drainage sample Current drainage Collect samples at 0.05 ft bgs, between 3-5 ft bgs and/or just above bedrock

4 Sediment, Soil

4 4 4 4 4 4 4 4 4 4

Approximately 900 ft NE of Outfall 001 (Sample location BCBS07S01)

Down-drainage sample Current drainage Collect samples at 0.05 ft bgs, between 3-5 ft bgs and/or just above bedrock, within drainage, and at drainage banks. Collect additional samples at 10 ft step-outs of bank locations and HOLD, pending drainage results.

9-13 Sediment, Soil

9-13 9-13 9-13 9-13 9-13 9-13 9-13 9-13 9-13 9-13

Approximately 350 ft E of Outfall 001 Down-drainage sample Current drainage Collect samples at 0.05 ft bgs, between 3-5 ft bgs and/or just above bedrock

4 Sediment, Soil

4 4 4 4 4 4 4 4 4 4

Approximate number of samples: 539 - 559 76 463 - 483 each 201 - 209 each


November 2006

of 7TABLE IVNOTES AND ABBREVIATIONS

* This is not an inclusive list of documents that are pertinent to the described Area I Burn Pit Area features. Only key representative documents are listed.

1. The proposed sampling locations listed on this table are shown on Figures 7 and 10.

2. EPA Method Numbers: VOCs (8260B), SVOCs (8270C), formaldehyde (8315A), nitrogen compounds (SM4500), metals (6010B, 6020, 7471A), cyanide (9012A), TPH (8015), perchlorate (314.0, 8321M), total anions (300.0), pH (150.2), PCBs (8082), nitroaromatics (8330A), dioxins (8290), organochlorine compounds (8081A), PAHs (8270C), NDMA (1625C), hydrazines (8315A), and 1,4-dioxane (8260B SIM).

3. Nitrogen forms including Nitrates and Nitrites, Total Organic Nitrogen and Total Kjeldahl Nitrogen SM4500 (Standard Methods 18th ed. Method 4500).

4. PCBs will be held and analyzed in samples containing elevated oil-range TPH (>1000 mg/kg).

5. Potential hydrazine impacts will be evaluated by analyzing for hydrazines and n-nitrosodimethylamine (NDMA).

6. Samples collected for hexavalent chromium will be held pending the total chromium results. Samples containing elevated total chromium above the background concentration will be analyzed for hexavalent chromium.

Haley & Aldrich, Inc. G:\Projects\26472\Reports\M477 A1BP RFI Workplan\Tables\2006-1110-HAI-SSFL.M477.T04.F.xls November 2006

· 37 75% c2h5oh/ 25% azdne 38 a plasticizer (tegdn) 39 ab-1 40 acetic acid 41 acetone 42 acetone...

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