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BMCM Manual Control Module for VTU User Manual Version 002 Innovation with Integrity NMR

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BMCM

Manual Control Module for VTU

User Manual

Version 002

Innovation with Integrity

NMR

The information in this manual may be altered without notice.

BRUKER accepts no responsibility for actions taken as a result of use of this ma-nual. BRUKER accepts no liability for any mistakes contained in the manual, lead-ing to coincidental damage, whether during installation or operation of the instru-ment. Unauthorised reproduction of manual contents, without written permission from the publishers, or translation into an other language, either the entire manual or a part of it, is forbidden.

This manual describes the units as they are at the date of printing. On request, the manufacturer shall supply circuit diagrams, lists of components, descriptions, cali-brating instructions and any other information for use by qualified personnel of the user, in charge of repairing the parts of the unit which have been stated by the manufacturer to be "repairable". Such supply shall in no event constitute permis-sion to modify or repair the units or approval of the same.

All rights reserved for the units, circuits, processes and appellations mentioned herein.

This unit is not designed for any type of use which is not specifically described in this manual. Such use may be hazardous.

This manual was written by

KRENCKER Patrick

© June 29, 2004: Bruker Biospin SA

Wissembourg, France

P/N: Z31463DWG-Nr: 1170.002

Contents

Contents .............................................................. iii

Index ..................................................................... 5

1 Introduction .......................................................... 71.1 Front panel .......................................................................... 71.2 Sub-assemblies ................................................................... 7

Probe Heater .................................................................. 7LN2 Evaporator Heater .................................................... 7Gas Flow Control ............................................................ 8

2 Requirements ........................................................ 92.1 Hardware ............................................................................ 92.2 Firmware ............................................................................. 92.3 New firmware installation ..................................................... 9

3 BMCM Module installation ................................... 11

4 BVT3000 Temperature Controller Configuration 134.1 Sensor selection ................................................................ 134.2 Eurotherm 902 configuration .............................................. 134.3 Parameter selection ........................................................... 154.4 Target Temperature Setting ................................................ 164.5 Eurotherm Self Tune .......................................................... 16

5 BVT3300 Temperature Controller Configuration 175.1 Sensor selection ................................................................ 175.2 Eurotherm 847 configuration .............................................. 175.3 Parameter selection ........................................................... 195.4 Self tune ............................................................................ 195.5 Target temperature selection ............................................. 19

6 Appendix ............................................................. 21

Figures ................................................................ 25

Tables .................................................................. 27

BMCM Version 002 iii

Contents

iv BMCM Version 002

Index

B

BTO2000 ............................................................................................... 14, 17–18

C

Cold Junction Compensation ...................................................................... 18–19Configuration mode ..................................................................................... 17, 19

D

Derivative time .................................................................................................. 15

H

Heater output limit ............................................................................................. 19

I

Integral time ...................................................................................................... 15

P

Parameter selection .......................................................................................... 19Parameters ........................................................................................................ 16Proportional band .............................................................................................. 15PT100 .................................................................................................... 14, 17–18

S

Self Tune ........................................................................................................... 16Sensor ................................................................................................... 14, 17–19Switch .......................................................................................................... 17–18

T

Thermocouple ....................................................................................... 14, 17–18

BMCM Version 002 5 (29)

Index

6 (29) BMCM Version 002

1Introduction 1

Front panel 1.1

The BMCM (W1101240) is an electronic module which allows to control manually the main functions of the temperature unit. It can be used with a BVT3000 or a BVT3300.

Figure 1.1. BMCM Front panel

Sub-assemblies 1.2

The following functions of the temperature unit can be controlled :

Probe Heater 1.2.1

The left push button turns on the main probe heater. The probe heater is on when the green led lits.

LN2 Evaporator Heater 1.2.2

The right push button turns on the LN2 evaporator heater. The LN2 evaporator heater status is indicated by a green led in the button. The status of the LN2 level sensors are indicated by two red leds on the bottom. The LN2 heater power level is set with the rightmost potentiometer.

LN2 HEATER

ON/OFF ON/OFF

HEATER

REFILL

LN2 LEVEL

EMPTY

1 15

8

POWER

FLOW LN2

BMCM Version 002 7 (29)

Introduction

Gas Flow Control 1.2.3

The knob «FLOW» selects manually stepwise the gas flow from 0 to 2000 l/h.

Table 1.1. Gas flow control

Knob position Liter/hour

0 0

1 135

2 270

3 400

4 535

5 670

6 800

7 935

8 1070

9 1200

10 1335

11 1470

12 1600

13 1735

14 1870

15 2000

8 (29) BMCM Version 002

2Requirements 2

Hardware 2.1

The BMCM can be used with NMR or EPR Variable Temperature Units. See the ECL level table below.

Table 2.1. VTU ECL Requirement

Firmware 2.2

The BMCM module works fully only with the firmware version 2.7 (970219 or lat-er). An older firmware works but it is not possible to change the gas flow in real time with the flow knob on front plate. To change the gas flow you must select a new flowrate and then switch off and on the temperature unit to update the flow-rate.

New firmware installation 2.3

When the variable temperature unit is equipped with an older firmware version, please follow these instructions to download the new firmware with a PC:

Connect the serial port (COM1) of a PC to the RS232 connector of the tempera-ture unit. Use the standard serial cable which is delivered with the temperature unit.

Switch on the main power of PC and temperature unit.

Copy the files LOADER.EXE and AP970219.HEX from the floppy disk to the PC hard disk.

From the hard disk, run LOADER.EXE AP970219.HEX AAAA and follow the in-structions given by the program.

Type P/N ECL

BVT3300 NMR W1100939 05

BVT3000 NMR W1101095 03

BVT3000 EPR Console W1101180 02

BVT3000 Table Top W1101181 02

BMCM Version 002 9 (29)

Requirements

10 (29) BMCM Version 002

3BMCM Module installation 3

CAUTION : Before any operation, disconnect the main power cord of the tempe-rature unit.

1. On the temperature unit, unscrew the front plate located under the inscription "Auxiliary sensors".

2. Remove the BMCM cover and disconnect the four flat cables from the printed circuit.

3. Insert the module in the front panel and fasten it with the two screws.

4. Connect the cables as follows. See appendix 1. "Manual control Board" on page 22, 2. "Evaporator / Exchanger Board" on page 23 and 3. "Main Board" on page 24.

• Connect the flat cable (W1101213) between J7 on BMCM board and J1 on evaporator or exchanger board.

• Connect the flat cable (W1101212) between J8 on BMCM board and J13 on main board.

• Connect the four wire flat cable (W1101211) between J1 on BMCM board and J7 on main board.

• Connect one of the end of the five wires flat cables (W1101210) to J9 on the BMCM board. The other end of the cable must be connected to the printed cir-cuit which is delivered with the BMCM module. Remove the JP6 to JP9 jum-pers on main board and plug the interface board on the jumpers JP6 to JP9. An arrow on the small printed circuit indicates the orientation toward the front panel of the temperature unit.

• Install the cover on the BMCM module

BMCM Version 002 11 (29)

BMCM Module installation

12 (29) BMCM Version 002

4BVT3000 Temperature Controller Configuration 4

Sensor selection 4.1

The BVT3000 can be used with different temperature sensors :

• Thermocouple T, K or E

• BTO2000 (T thermocouple with external CJC at 0 C°)

• PT100

Warning: Never connect two sensors at a same time on the BVT3000.

Eurotherm 902 configuration 4.2

The EUROTHERM 902 controller must be configured to work with the right type of sensor.

The configuration is done with the Eurotherm 902 controller keypad (or by soft-ware in the EDTE program).

Proceed as follows :

1. Switch off the main power.

2. Press the two left most buttons : together while powering on the BVT3000.

3. The messages CONF and UCONF appear on the display.

4. Press the scroll button until ICONF is displayed.

BMCM Version 002 13 (29)

BVT3000 Temperature Controller Configuration

5. Press the left button until C1 appears.

6. Now press the increment button or decrement button : The 4 digit code is displayed. This code must be changed to select the new sensor.

Table 4.1. Eurotherm 902 sensor code

7. With the left selection button , select the blinking digit to be modi- fied and change the value with the increment button or decrement button . When the correct code has been selected press the scroll button : C2 will be displayed.

8. Now Press the selection button . ICONF appears. Press the scroll button until LEAVE appears. Press the left selection button again. Configuration is now complete and the temperature is displayed.

sensor code C1

T thermocouple internal CJC 0004

K thermocouple internal CJC 0003

E thermocouple internal CJC 0012

PT100 0024

BTO2000 1004

14 (29) BMCM Version 002

Parameter selection

Parameter selection 4.3

1. Depress button until OPER appears.

2. Push button until INST appears. The INST menu allows you to read and/or modify the Pb, Ti Td, cbl, cbh and Hl values.

3. Push button Pb appears. To scroll the list, push button .

Table 4.2. Mnemonics explanations

4. To read and/or modify one of these parameters, select the mnemonic to modify and push button or . The value displayed is the used value. To change it, push button to increment or to decrement. When value is correct, push button the next mnemonic of the list will be displayed. To leave this menu, push button INST appears. Push button until you leave the parameters menu.

Pb Proportional band

Ti Integral time

Td Derivative time

cbl Cutback low

cbh Cutback high

Hl Heater output limit (0-100%)

BMCM Version 002 15 (29)

BVT3000 Temperature Controller Configuration

Target Temperature Setting 4.4

1. Push button until SP or W appears, SP or W is the Set Point parame-ter.

2. Adjust the target temperature by pushing or .

Eurotherm Self Tune 4.5

Preparing the self tune

Before processing a self tune, verify that Ti, Td, cbl and cbh are not set to OFF. If one of these parameters are set to OFF it will not be modified by the self tune. Se-lect the target temperature before starting the self tune. The target temperature must be at least 10° above room temperature.

Processing the self tune

1. Depress button until OPER appears.

2. Push button SP1 or SPR appears.

3. Push button until St or A-T appears. St or A-T is the self tune mnemo-nic.

4. To process a self tune push both buttons and at the same time.

5. On the up right corner of the eurotherm front panel display, "A-T" or ’’S-T’’ ap-pears indicating that the self tune is activated. Turn on the BVT3000 heater by pushing the "heater power" button on the BMCM module.

6. The self tune process is finished when the "A-T" or ’’S-T’’ indication disap-pears. It takes a few minutes to complete the self tune process.

16 (29) BMCM Version 002

5BVT3300 Temperature Controller Configuration 5

Sensor selection 5.1

The BVT3300 can be used with different types of sensors :

• Thermocouple T (factory set)

• BTO2000

• PT100 sensor

Warning : Never connect two sensors at a same time on the BVT3300.

Eurotherm 847 configuration 5.2

The EUROTHERM 847 controller must be configured to work with the right type of sensor.

To access the configuration mode, a switch located inside the 847 controller must be closed.

The switch must be closed only during the configuration mode.

Proceed as follows :

1. Switch off the main power.

2. Unscrew the EUROTHERM controller front plate.

3. Remove the module out of its cabinet.

4. The switch WB1 is located on the left side at the rear of the module.

5. Close the switch.

6. Insert the controller module and screw the front panel.

BMCM Version 002 17 (29)

BVT3300 Temperature Controller Configuration

7. Switch on the main power.

8. Press the button until «Sn» appears. («Sn» is the mnemonic for sen- sor). Then select the sensor type, press the up or down key un-til the correct sensor appears.

Table 5.1. Eurotherm 847 sensor selection

If the sensor is a thermocouple or a BTO2000 you must select also the type of CJC (Cold Junction Compensation). Press the par key until CJC appears and select with the up and down key.

Table 5.2. CJC selection

• When the configuration is finished, switch off the main power, remove again the controller and open the switch.

• Close the controller and switch on the power supply.

Sensor type Sn

T Thermocouple internal CJC t tc

BTO2000 t tc

PT100 rtd3

Sensor type CJC

T Thermocouple int (internal)

BTO2000 0°C (external at 0°C)

PT100 X (don’t care)

PAR

PAR

18 (29) BMCM Version 002

Parameter selection

Parameter selection 5.3

To access the configuration mode, a switch located inside the 847 controller must be closed (see previous section).

We suppose that the internal switch is closed.

1. Pushing the button allows the user to scroll through parameters. Only six of them can be modified by the user. Modifying one of the other breaks the factory warranty.

2. The parameters the user is allowed to change are the following :

ProP Proportional band Int.t Integral time dEr.t Derivative time H PL Heater output limit (0 to 100%) Sn Sensor type CJC Cold junction compensation

3. Press button until the parameter to be modified appears. To chose a new type of sensor, CJC or to modify the value of the parameter press button

or . When the value is correct push button until the measured temperature appears.

4. Open the internal switch as explained in the previous section.

Self tune 5.4

1. Before starting a self tune, please verify that parameters Prop, Int.t, and dEr.t are not equal to 0. Also verify that H PL contents the correct value.

2. Push button until «tune» appears.

3. To start a self tune, push button or and then, switch on the hea-ter power.

Target temperature selection 5.5

The lower part of the display shows the selected target temperature. Target temperature can be modified by pushing button or .

PAR

PAR

PAR

PAR

BMCM Version 002 19 (29)

BVT3300 Temperature Controller Configuration

20 (29) BMCM Version 002

6Appendix 6

BMCM Version 002 21 (29)

Figure 6.1. Manual control Board

8 7 6 5 4 3 2 1

A

B

C

D

12345678

D

C

B

A

BVT3X00

ART: W1101235 EC: DRAWN:DATE:

APPROV:DATE:

DWG:

RC30/04/97

W4L110570

RC30/04/97

VISA:

VISA:

SHEET: 1/1

S.a.d.i.s

SPECTROSPIN

MANUAL COMMAND

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TO

MA

IN B

RD

TO

EV

AP

BR

D

FL

OW

AD

PT

HE

AT

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DL

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ITC

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H

HEATERLN2LN2 POWER

REFILLEMPTYK K

FRONT

J12

J11

W4P110570

SW1

J10

TP

11

TP

12

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13

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22

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23

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51

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R6 R5R4 R3

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C1 C2

J9

J1

J7J8

LD2LD1

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J1

J7J8

CI : W4P110570

22 (29) BMCM Version 002

Figure 6.2. Evaporator / Exchanger Board

8 7 6 5 4 3 2 1

A

B

C

D

12345678

D

C

B

A

BDTC

ART: W1100957 or W1101049 EC: DRAWN:DATE:

APPROV:DATE:

DWG:

RC22/09/94

W4L10295

RC22/09/94

VISA:

VISA:

SHEET: 1/1

S.a.d.i.s

SPECTROSPIN

EVAPORATOR / EXCHANGERCI : W4P10295D

D

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W4P10295D

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U5 U2U6

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J1

BMCM Version 002 23 (29)

Figure 6.3. Main Board

87

65

43

21

ABCD

12

34

56

78

D C B AA

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:

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C31

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C36C35

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C60

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C73

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C33

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6

C22

C87

C86C85

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C53

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ZD4

D1

D4D3

D6

D5

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RP2

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5

RN4

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RN

3

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J11

J12

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J7

J4

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JP8JP9

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JP3

JP2

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C90

C89

C88

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J2

X1

X2

TR1

J1

TP1

TP2

TP3

TP4

TP5

TP6

TP7

TP8

TP9TP

10

TP11

TP12 TP13

TP14

TP15

TP16

TP17

TP18

TP19

TP20

TP21

TP22

TP23

TP24

TP25 TP

26

TP27

TP28 TP

29

TP30TP31

TP32

TP33

TP34

TP35

J7

JP6-

JP9

J13

24 (29) BMCM Version 002

Figures

1 Introduction 7Figure 1.1. BMCM Front panel ............................................................... 7

2 Requirements 9

3 BMCM Module installation 11

4 BVT3000 Temperature Controller Configuration 13

5 BVT3300 Temperature Controller Configuration 17

6 Appendix 21Figure 6.1. Manual control Board ......................................................... 22Figure 6.2. Evaporator / Exchanger Board ............................................ 23Figure 6.3. Main Board ......................................................................... 24

BMCM Version 002 25 (29)

Figures

26 (29) BMCM Version 002

Tables

1 Introduction 7Table 1.1. Gas flow control ............................................................... 8

2 Requirements 9Table 2.1. VTU ECL Requirement .................................................... 9

3 BMCM Module installation 11

4 BVT3000 Temperature Controller Configuration 13Table 4.1. Eurotherm 902 sensor code ........................................... 14Table 4.2. Mnemonics explanations ................................................ 15

5 BVT3300 Temperature Controller Configuration 17Table 5.1. Eurotherm 847 sensor selection ..................................... 18Table 5.2. CJC selection ................................................................ 18

6 Appendix 21

BMCM Version 002 27 (29)

Tables

28 (29) BMCM Version 002

Notes

BMCM Version 002 29 (29)

Lastpage

Bruker Corporation

[email protected]

Order No: Z31463