Foggia, October 7-9, 2015

http://www.msfooday.darepuglia.it

SCIENTIFIC PROGRAMME

Wednesday, October 7th, 2015

11:00 – 14:00 Registration and reception

14:00 – 14:30 Opening ceremonies

Institutional addresses:

Prof. Maurizio Ricci / Rector of University of Foggia

Dr. Gianluca Nardone / President of D.A.Re.

Prof. Raffaele Riccio / President Italian Chemical Society

Prof. Gianluca Giorgi / Chair of the Scientific Committee

Dr. Antonio Logrieco / Director of ISPA-CNR

Special Guests: Luogotenente Biagio Manzella/ Antisophistication and Health Core Commander of Carabinieri-Foggia Dr. Michele Panunzio/ Director of SIAN ASL Foggia sud, Italian Society of hygienics and preventive medicine scientific commeettee, academic of nutritonal education at University of Foggia

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14:30 – 16:30 1st

Session

Chair: Michele Suman – Barilla, Parma (Italy)

14:30 PL1: LIQUID CHROMATOGRAPHY COUPLED TO HIGH RESOLUTION MASS SPECTROMETRY WITHIN PESTICIDE RESIDUE CONTROL IN FOOD

Amadeo Fernandez-Alba, EURL-FV, Almería (Spain) 15:00 OR1: MS-BASED METHODS AND PROFICIENCY TESTED MATERIALS FOR RELIABLE ANALYSIS OF FOOD CONTAMINANTS: MYCOTOXINS AND PESTICIDES IN CEREALS

A. Visconti, V. M.T. Lattanzio, A. De Girolamo, R. Anzivino, L. Bonassisa, ISPA-CNR, Bari (Italy) 15:15 OR2: DETERMINATION OF 62 ANTIBIOTICS IN MILK BY HIGH PERFORMANCE LIQUID CHROMATOGRAPHY COUPLED TO HYBRID HIGH RESOLUTION MASS SPECTROMETRY

S. Moretti, R. Rossi, G. Saluti, R. Galarini, IZS Umbria e Marche, Perugia (Italy) 15:30 OR3: MEPS EXTRACTION OF PESTICIDES IN WHEAT FOLLOWED UHPLC-MS/MS ANALYSIS

F. Di Ottavio, M. C. Simeoni, F. Della Pelle, C. Montesano, R. Curini, M. Sergi, P. Pittia, D. Compagnone University of Teramo (Italy) 15:45 OR4: LIQUID CHROMATOGRAPHY–TANDEM MASS SPECTROMETRY AND PASSIVE SAMPLING: POWERFUL TOOLS FOR THE DETERMINATION OF PHARMACEUTICALS IN WATER FOR HUMAN CONSUMPTION

M. Di Carro, C. Mirasole, E. Magi, University of Genoa (Italy) 16:00 OR5: THE QUANTITATION AND IDENTIFICATION OF APPROXIMATELY 500 PESTICIDES AND VETERINARY DRUG RESIDUES IN FOOD EXTRACTS BY LC-QTOF MASS SPECTROMETRY

Anthony Drury, Bruker Daltonik GmbH, Bremen (Germany) 16:15 OR6: GC-QqQ-MS ANALYSIS OF FIFTEEN POLYBROMINATED DIPHENYL ETHERS IN FOOD

T. Tavoloni, C. Lestingi, E. Bastari, A. Piersanti IZS Umbria e Marche, Perugia (Italy)

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16:30 – 17:00 Coffee break

17:00 – 18:30 2

nd Session

Chair: Diego Centonze – Università di Foggia (Italy)

17:00 PL2: CHEMICAL PROTEOMICS OF NATURAL COMPOUNDS USEFUL FOR THE DEVELOPMENT OF NUTRACEUTICS

M. C. Monti, A. Capolupo, F. del Gaudio, A. Casapullo, R. Riccio,Dept. of Pharmacy, University of Salerno (Italy) 17:30 OR7: STUDY OF GRAPE DRYING BY HRMS METABOLOMICS

M. De Rosso, S. Soligo, A. Dalla Vedova, R. Flamini CREA-VIT, Conegliano (Italy)

17:45 OR8: METABOLOMICS AND BIOACTIVITIES OF MULBERRY

G. D’Urso, J. J. Mes, C. Pizza, P. Montoro, R.C.H. de Vos Università degli Studi di Salerno, Fisciano (Italy) 18:00 OR9: LIPIDOME CHARACTERIZATION OF WILD SPARUS AURATA FILLETS BY LIQUID CHROMATOGRAPHY WITH ELECTROSPRAY IONIZATION AND FOURIER-TRANSFORM MASS SPECTROMETRY (LC-ESI-FTMS)

S. Granafei, A. Spinelli, P. Azzone, I. Losito, F. Palmisano, T.R.I. Cataldi Università degli Studi di Bari “Aldo Moro”, Bari (Italy)

18:15 OR10: CHEMICAL EVALUATION OF CULTIVATED ROOTS OF GENTIANA LUTEA L. AND OF BY-PRODUCT OBTAINED DURING BITTER LIQUEURS PRODUCTION BY USING MASS SPECTROMETRY

G. Caprioli, F. Maggi, A. Mustafa, M. Ricciutelli, G. Sagratini, S. Vittori University of Camerino, Camerino (Italy) 18:30 End of session

19:30 Welcome cocktail

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Thursday, October 8th, 2015

9:00 – 10:30 3rd

Session

Chair: Franco Biasioli – Fondazione Edmund Mach, S. Michele all’Adige (Itay)

9:00 PL3: HOW DO YOU SMELL? EXPLOITING ON-LINE MS AND BIOFEEDBACK TO UNDERSTAND SENSORY PERCEPTION

J. Beauchamp, A. Buettner, J. Freiherr Fraunhofer IVV, Freising (Germany)

9:30 OR11: ADDING COMPLEXTIY TO IN-VIVO MEASUREMENTS: INTERACTION BETWEEN VOLATILES IN GAS PHASE AND THE ORAL AND NASAL MUCOSA

J. A. Sánchez-López, A. Ziere, S. I.F.S. Martins, R. Zimmermann, Chahan Yeretzian, Zurich University of Applied Sciences, Wädenswil (Switzerland)

9:45 OR12: CHARACTERIZATION OF THE VOLATILE COMPOUNDS CONSTITUTING MASCARPONE CHEESE AROMA

V. Lonzarich, S. Makhoul, V. Capozzi, F. Biasioli, L. Navarini Aromalab, illycaffe s.p.a., Trieste (Italy)

10:00 OR13: PREDICTION OF ANISE FLAVOUR IN APPLE FROM GC-MS AND PTR-MS VOLATILE PROFILING

I. Khomenko, L. Cappellin, M. Charles, F. Marini, F. Gasperi, F. Biasioli Fondazione Edmund Mach, San Michele all’Adige (Italy)

10:15 OR14: INSIGHT INTO SINGLE BEAN COFFEE AROMA WITH PTR-TOF-MS

S. Yener, L. Navarini, V. Lonzarich, L. Cappellin, T. D. Märk, G. Bonn, F. Biasioli Fondazione Edmund Mach, San Michele all’Adige (Italy)

10:30 – 11:30 Coffee break

Poster session (even number posters)

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11:30 – 12:45 4th

Session

Chair: Luciano Navarini – illycaffè, Trieste (Italy)

11:30 PL4: MASS SPECTROMETRY- BASED DETECTION STRATEGIES APPLIED TO KNOWN AND UNKNOWN FUNGAL SECONDARY METABOLITES

S. De Saeger, N. Arroyo-Manzanares, L. Vanhaecke, K. Ehrlich, J. Cary, D. Bhatnagar, D. Di Mavungu J. Ghent University, Ghent (Belgium) 12:00 OR15: DIOXIN LEVELS IN LIVESTOCK AND GRAZING LAND IN THE SURROUNDINGS OF A LARGE INDUSTRIAL AREA IN TARANTO (ITALY)

V. Esposito, A. Maffei, D. Bruno, F. Montingelli, G. Battafarano, F. Basile, E. Franco, M. Conversano, G. Assennato, ARPA PUGLIA, Environmental Protection Agency of Apulia, Taranto (Italy) 12:15 OR16: REDUCING MATRIX EFFECTS, INCREASE THROUGHPUT, AND DECREASE DATA PROCESSING TIME FOR ROUTINE FOOD TESTING WITH HIGH RESOLUTION QTOF MS/MS

A. Sage, AB SCIEX, Warrington (UK) 12:30 OR17: LC-MS/MS MULTI-MYCOTOXIN ANALYSIS - A NEW APPROACH IN ROUTINE ANALYSIS

L. Kuster, G. Jaunecker, M. Kainz, G. Häubl, C. Swoboda Romer Labs, Getzersdorf (Austria)

12:45 – 14:15 Buffet lunch

14:15 – 15:45 5th

Session

Chair: Giampiero Scortichini – IZS Umbria e Marche, Perugia (Italy)

14:15 OR18: STABLE ISOTOPE ANALYSIS FOR AUTHENTICITY TESTING OF ITALIAN ORGANIC PASTA: VARIATIONS IN δ

2H, δ

13C, δ

15N, δ

18O AND δ

34S ALONG

THE PRODUCTION CHAIN

F. Camin, L. Bontempo, M. Paolini, C. Micheloni, K. H. Laursen, S. Husted Fondazione Edmund Mach, San Michele all’Adige (Italy) 14:30 OR19: AF4-spICP-MS FOR SIZING AND QUANTIFICATION OF NANOMATERIALS IN FOOD: A PROOF OF PRINCIPLE

C. Cascio, P. Nobels, R. Peters, RIKILT, Wageningen (The Netherlands)

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14:45 OR20: GEOGRAPHICAL ORIGIN AND AUTHENTICITY OF “PECORINO DI FARINDOLA” CHEESE THROUGH

87Sr/

86Sr ISOTOPIC RATIO,

ELEMENTAL PROFILES AND CHEMOMETRICS

F. Marchegiani, S. Milone, G. Migliorati, P.R. Trincherini, S.Nisi, M. Ferrante, M. L. Di Vacri, IZS Abruzzo e Molise “G. Caporale”, Teramo (Italy) 15:00 OR21: SINGLE PARTICLE ICP-MS: A POTENTIAL ANALYTICAL APPROACH TO DETECT SILVER NANOPARTICLES IN REAL SAMPLES

F. Gallocchio, G. Biancotto, V. Cibin, C. Losasso, S. Belluco, G. van Bemmel, R. Peters, S. Weigel, A Ricci, IZS delle Venezie, Padova (Italy)

15:15 OR22: APPLICATIONS OF ISOTOPE RATIO MASS SPECTROMETRY (IRMS) TO ORIGIN AND NATURALNESS CHARACTERIZATION OF FOOD PRODUCTS

L. Mounier, A. Hilkert, Thermo Fisher Scientific, Coutaboeuf Cedex (France) 15:30 OR23: PHENOTYPING THE PLANT X ENVIRONMENT INTERACTION ON THE IMPRINTING OF STABLE ISOTOPE COMPOSITIONS IN AGRO-FOOD PRODUCTS

M. Lauteri, S. Portarena, F. Chiocchini, M. Ciolfi, G. Russo, E. Brugnoli, CNR, Roma (Italy)

15:45 – 16:30 Coffee break

Poster session (odd number posters)

16:30 – 18:15 6th

Session

Chair: Roberta Galarini – IZS Umbria e Marche, Perugia (Italy) 16:30 OR24: ESTABLISHING THE OCCURRENCE OF MAJOR AND MINOR SOYASAPONINS IN FAGIOLI DI SARCONI BEANS (Phaseolus vulgaris L.) ECOTYPES BY LC–ESI-HYBRID LINEAR ION-TRAP AND INFRARED MULTIPHOTON DISSOCIATION FOURIER-TRANSFORM ION CYCLOTRON RESONANCE MASS SPECTROMETRY

G. Bianco, C.F. Carbone, A. Buchicchio, G. Pace, T.R.I. Cataldi Università degli Studi della Basilicata, Potenza (Italy)

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16:45 OR25: ELUCIDATION OF THE MECHANISTIC INTERACTION BETWEEN ANTIOXIDANTS USING CHEMILUMINESCENCE TECHNIQUE COUPLED WITH LC-MS

M. A. Abbas Mahmoud, V. S. Chedea, A.Abdelgawad University of Erlangen-Nuremberg, Erlangen (Germany)

17:00 OR26: TECHNICAL EVOLUTIONS ON LCMS JET STREAM SYSTEMS: SENSITIVE TARGET DETECTION BY 6470 LC-QQQ AND UNTARGET SCREENING WORKFLOW BY NEW 6545 LC-QTOF

N. Cimino, Agilent Technologies Italia

17:15 OR27: GLUCOSYL DERIVATIVES OF TYPE-A TRICHOTHECENES: MASS SPECTROMETRIC CHARACTERIZATION OF PLANT AND FUNGAL METABOLITES, AND NATURAL OCCURRENCE IN CEREALS

V. M. T. Lattanzio, B. Ciasca, A. Visconti, M. Pascale ISPA-CNR, Bari (Italy)

17:30 OR28: DETECTION BY HPLC/TOF-MS OF ISOBARIC LIGNANS FROM LAMPANTE AND REFINED OLIVE OIL AS POSSIBLE QUALITY MARKERS

L. Cecchi, M. Innocenti, M. Migliorini, C. Cherubini, N. Mulinacci Università degli Studi di Firenze, Sesto Fiorentino (Italy)

17:45 OR29: ISOFLAVONES IN ESPRESSO COFFEE: A NEW SPE-HPLC-MS/MS METHOD FOR THEIR DETERMINATION

G. Sagratini, L. Navarini, M. Ricciutelli, E. Torregiani, S. Vittori, G. Caprioli University of Camerino, Camerino (Italy)

18:00 OR30: RAPID NON-INVASIVE QUALITY CONTROL OF SEMI-FINISHED PRODUCTS FOR THE FOOD INDUSTRY BY DIRECT INJECTION MASS SPECTROMETRY HEADSPACE ANALYSIS: THE CASE OF MILK POWDER, WHEY POWDER, AND ANHYDROUS MILK FAT

S. Makhoul, S. Yener, I. Khomenko, V. Capozzi, L. Cappellin, E. Aprea, M. Scampicchio, F. Gasperi, F. Biasioli Fondazione Edmund Mach, San Michele all’Adige (Italy)

18:15 End of session

20:30 Social dinner

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Friday, October 9th, 2015

9:00 – 10:45 7th

Session

Chair: Arnaldo Dossena – University of Parma, Parma (Italy)

9:00 PL5:: DETECTION OF UNLABELLED MEAT IN MEAT PRODUCTS USING PROTEOMICS AND GENOMICS

A. Charlton, R. Romero, H. Hird, Fera Science Ltd, York

9:30 OR31: MS-BASED CHARACTERIZATION OF MEAT PROTEINS INVOLVED IN THE MECHANISMS OF TENDERNESS

A. della Malva, R. Marino, M. Caroprese, A. Santillo, A. Sevi, M. Albenzio, University of Foggia, Foggia (Italy)

9:45 OR32: MALDI TOF MS/MS ANALYSIS OF INTACT STEROLS AND SUGAR COMPOUNDS IN FOODSTUFFS BY USING SUPERBASIC ALKYL-SUBSTITUTED BISPHOSPHAZENE PROTON SPONGES AS MATRICES

C.D. Calvano, A. Monopoli, C. Chiapperino, J. Kogel, J. Sundermeyer, T.R.I. Cataldi, F. Palmisano Università degli Studi di Bari “Aldo Moro”, Bari (Italy)

10:00 OR33: METAL-DECORATED ARRAYS OF SILICON NANOWIRES FOR LASER DESORPTION/IONIZATION MASS SPECTROMETRY IN FOOD ANALYSIS

R.A. Picca, M.J. Lo Faro, C.D. Calvano, B. Fazio, M.C. Sportelli, S. Trusso, P.M. Ossi, F. Neri, C. D’Andrea, A. Irrera, N. Cioffi Università degli Studi di Bari “Aldo Moro”, Bari (Italy)

10:15 OR34: RAPID EVAPORATIVE IONISATION MASS SPECTROMETRY (REIMS) FOR THE DISCRIMINATION OF DIFFERENT SPECIES OF MEAT AND FISH

S. Stead, S. Hird, J. Balog, S. Pringle, Z. Takats Waters Corporation, Wilmslow (UK)

10:30 OR35: TARGET AND UNTARGET ANALYTICAL METHOD FOR ALKALOIDS ANALYSIS IN HERBAL EXTRACTS BY HIGH RESOLUTION MASS SPECTROMETRY

T. Nardin, C. Barnaba, R. Larcher Fondazione Edmund Mach, San Michele all’Adige (Italy)

10:45 – 11:15 Coffee break

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11:15 – 13:00 8th

Session

Chair: Riccardo Flamini, CREA–VIT, Conegliano (Italy)

11:15 OR36: INVESTIGATION ON ORIGIN OF VOLATILE ORGANIC COMPOUNDS IN ALGAE FOOD SUPPLEMENTS

F. Papa, G. Caprioli, A. Di Muzio, M. Nicoletti, M. Ricciutelli, G. Sagratini, S. Vittori, F. Maggi, University of Camerino (Italy)

11:30 OR37: PROFILING OF APPLE VOLATILE COMPOUNDS BY SOLID PHASE MICROEXTRACTION AND COMPREHENSIVE TWO-DIMENSIONAL GAS CHROMATOGRAPHY WITH QUADRUPOLE MASS SPECTROMETRY

E. Aprea, M. Charles, I. Endrizzi, E. Betta, F. Biasioli, F. Gasperi Fondazione Edmund Mach, San Michele all’Adige (Italy)

11:45 OR38: HYPHENATION OF NOVEL MS DEVICES WITH A POWERFUL MULTIDIMENSIONAL GC PRE-SEPARATION STEP FOR THE INVESTIGATION OF FOODS

P. Q. Tranchida, L. Mondello, University of Messina (Italy)

12:00 OR39: MULTI-RESIDUAL HPLC-MS ANALYSIS OF PLASTICIZERS USED IN PVC GASKET LIDS AND ASSESSMENT OF THEIR MIGRATION INTO FOOD SAUCES

F. Lambertini, D. Catellani, M. Vindigni, M. Suman Barilla G. e R. Fratelli S.p.A., Parma (Italy)

12:15 OR40: ON LINE PRE-ENRICHMENT COUPLED TO LC SEPARATION AND MS/MS DETECTION FOR TRACING MULTIPLE ALLERGENS IN WINE

E. De Angelis, L. Monaci, ISPA-CNR, Bari (Italy)

12:30 OR41: MIGRATION OF MELAMINE AND FORMALDEHYDE FROM TABLEWARE

S. Menotta, S. Abbaleo, S. Zerbini, A. Padovani, Q. Garofalo, G. Cuciniello, G. Fedrizzi, IZS Lombardia Emilia Romagna, Bologna (Italy)

12:45 – 13:00 Closing ceremony

Announcement of next MS Food Day

13:00 – 14:15 Farewell light buffet

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POSTER COMMUNICATIONS

P1 δ

15N OF PROLINE: THE DIRECT LINK BETWEEN SOIL AND WINE

M. Paolini, D. Bertoldi, L. Ziller, R. Larcher, G. Nicolini, F. Camin Fondazione Edmund Mach, San Michele all’Adige (Italy)

P2 STABLE ISOTOPE AND MULTIELEMENT COMPOSITION OF COCOA SEEDS FROM DIFFERENT GEOGRAPHIC ORIGIN

M. Perini, D. Bertoldi, A. Barbero, L. Bontempo, R. Larcher, F. Camin Fondazione Edmund Mach, San Michele all’Adige (Italy)

P3 GC-MS ANALYSIS FOR EVALUATION OF QUALITY AND OXIDATIVE STABILITY IN CHEWING GUM BASES

F. Ieri, L. Calamai P. Pinelli, A. Romani, University of Florence (Italy)

P4 FUSARIUM spp. IN WHEAT: SPME-GC-MS OF VOLATILE COMPOUNDS FOR IDENTIFICATION OF INFECTION INDICATORS

F. Lupi, C. Palermo, M. Quinto, D. Nardiello, A. Mentana, A. Moretti, S. Frisullo, D. Centonze Università degli Studi di Foggia, Foggia (Italy)

P5 COMPARATIVE ANALYSIS OF THE VOLATILE PROFILES FROM WILD, CULTIVATED, AND COMMERCIAL ROOTS OF GENTIANA LUTEA L. BY HEADSPACE SOLID PHASE MICROEXTRACTION (HS–SPME) COUPLED TO GAS CHROMATOGRAPHY MASS SPECTROMETRY (GC-MS)

G. Sagratini, G. Caprioli, F. Maggi, A. Mustafa, M. Ricciutelli, V. Sirocchi, S. Vittori University of Camerino, Camerino (Italy)

P6 VOLATILE PROFILE CHARACTERIZATION OF TRUFFLE OILS AND NATURAL AROMA PRODUCTS BY HS-SPME-GC-MS

E. Torregiani, G. Sagratini, S. Vittori, G. Caprioli, M. Cortese, F. Papa University of Camerino, Camerino (Italy)

P7 EFFECTS OF THE OAK CHIPS TREATMENT ON PHENOLIC AND VOLATILE COMPOSITION OF RED WINE: THE CASE OF AGLIANICO AND MONTEPULCIANO

A. Baiano, A. Mentana, M. Quinto, D. Centonze, A. De Gianni Università degli Studi di Foggia, Foggia (Italy)

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P8 MASS SPECTROMETRY HYPHENATED TECHNIQUES FOR THE ANALYSIS OF VOLATILES AND PEPTIDES IN SOFT CHEESE

A. Natale, A. Mentana, C. Palermo, A. Conte, D. Nardiello, M. Quinto, M.A. Del Nobile, D. Centonze Università degli Studi di Foggia, Foggia (Italy)

P9 LEMON GRASS ESSENTIAL OIL AS NATURAL FOOD PRESERVATION: INVESTIGATION ON VOLATILE COMPOUNDS, IN VITRO ANTIFUNGAL ACTIVITY AND CONTROL OF SACCHAROMYCES CEREVISIAE IN REAL FRUIT JUICES

B. M. Nadjib, F. M. Amine, K. Abdelkrim, S. Fairouz, T. K. Hadjer, T. Djamel Ecole Normale Supérieure de Kouba, Alger (Algeria)

P10 EXPLORING EXTRACTION DYNAMICS OF GREEN TEA VOLATILES BY PTR-TOF-MS

J. A. Sánchez-López, S. Yener, G. Bonn, T. Märk, R. Zimermann, F. Biasioli, C Yeretzian Zurich University of Applied Sciences-ZHAW, Wädenswil (Switzerland)

P11 CLASSIFICATION OF BLACK AND GREEN TEAS BASED ON VOLATILE COMPOUND PROFILES ANALYZED WITH PTR-TOF-MS

S. Yener, J. A. Sànchez-Lòpez, P. M. Granitto, L. Cappellin, T. D. Märk, G. Bonn, R. Zimmerman, C. Yeretzian, F. Biasioli Fondazione Edmund Mach, San Michele all’Adige (Italy)

P12 FROM GRAPE TO WINE: STUDY OF THE EVOLUTION OF PHOSPHONATE'S RESIDUE BY QUPPE METHOD

L. Tonidandel, T. Román Villegas, M. Malacarne, R. Larcher, G. Nicolini Fondazione E. Mach, San Michele all'Adige (Italy)

P13 FEASIBILITY STUDY OF INCLUSION OF MIXTURES OF PESTICIDES IN WHITE WINE MATRIX

F. Mottola, P. Fanizzi, C. M. Stefanelli, V.M.T. Lattanzio, B. Ciasca, A. Visconti Lab. Instruments S.r.l., Castellana Grotte (BA, Italy)

P14 MONITORING 16-EU-PAHs IN EDIBLE VEGETABLE OILS

C. Lestingi, V. Bardeggia, T. Tavoloni, A. Piersanti, IZS Umbria e Marche, Ancona (Italy)

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P15 MYCOTOXINS LIQUID CHROMATOGRAPHIC-TANDEM MASS SPECTROMETRIC ANALYSIS IN FOOD MATRICES: 3-YEARS OF SURVEILLANCE

G. Fedrizzi, E. Caprai, D. Accurso, M. G. Caschetto, A. Padovani, L. Calò, S. Menotta, IZS Lombardia Emilia Romagna, Bologna (Italy)

P16 MULTI MYCOTOXIN ANALYSIS USING IMMUNOAFFINITY COLUMN CLEAN-UP FOR A RANGE OF SAMPLES PRIOR TO LC-MS/MS

J. Wilcox, D. Leeman, E. Marley, C. Milligan, R. Niemeijer, R-Biopharm Rhône Ltd

P17 INTERNATIONAL PROFICIENCY TESTING AS A TOOL TO EVALUATE THE STATE-OF-ART OF LC-MS METHODS FOR MULTI-MYCOTOXIN DETERMINATION

A. De Girolamo, B. Ciasca, J. Stroka, S. Bratinova, M. Pascale, A. Visconti, V. M.T. Lattanzio, CNR-ISPA. Bari (Italy)

P18 VALIDATION OF AN AUTOMATED CARTRIDGE EXCHANGE UNIT AND HIGH PRESSURE DISPENSER WITH HPLC USING IMMUNOPREP® ONLINE CARTRIDGES FOR AFLATOXIN ANALYSIS

R. Rhemrev, M. Pazdanska, E. Marley, C. Donnelly, E. Manning, R. Niemeijer, R-Biopharm Rhône Ltd

P19 A NEW FUMONISINS ISOMER: CHARACTERIZATION AND QUANTIFICATION

C. Falavigna, L. Righetti, A. Faccini, P. Battilani, P. Galaverna, C. Dall’Asta, University of Parma, Parma (Italy)

P20 IMPLEMENTATION OF THE OFFICIAL LC-MS/MS METHOD FOR EVALUATING LIPOPHILIC MARINE TOXIN CONTAMINATION IN MUSSELS OF NORTH-CENTRAL ADRIATIC SEA

M. Siracusa, S. Bacchiocchi, N. Spada, R. Orletti IZS Umbria e Marche, Ancona (Italy)

P21 VALIDATION OF A CONFIRMATORY ANALYTICAL METHOD FOR THE DETERMINATION OF POLYCYCLIC AROMATIC HYDROCARBONS IN MARINE MATRICES BY GAS CHROMATOGRAPHY/TANDEM MASS SPECTROMETRY

V. Nardelli, G. Berardi, A. Calitri, F. Casamassima, G. Gesualdo, P. Mambelli, IZS Puglia e Basilicata, Foggia (Italy)

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P22 SERUM LEVELS OF DIOXINS (PCDD/Fs) AND PCBs IN WOMEN FROM CAMPANIA REGION, ITALY

F. P. Serpe, G. Messina, F. Fiorito, M. Monda, M. Esposito IZS del Mezzogiorno, Portici (Italy)

P23 METABOLOMIC STUDY OF WILD AND CULTIVATED CAPER (CAPPARIS SPINOSA L.) FROM DIFFERENT AREAS OF SARDINIA AND THEIR COMPARATIVE EVALUATION

M. Maldini, M. Foddai, F. Natella, M. Chessa, G. L. Petretto, M. A. Fenu, C. I. Tuberoso, G. Pintore, University of Sassari, Sassari (Italy)

P24 PROTEOMIC STRATEGIES TO SUPPORT THE IDENTIFICATION OF GLUTEN AND METABOLIC PROTEINS IN DURUM WHEAT

C. Palermo, A. Mentana, M. M. Giuliani, M. A. De Santis, Z. Flagella, S. Masci, D. Centonze Università degli Studi di Foggia, Foggia (Italy)

P25 INNOVATIVE METHOD FOR THE DETECTION OF BOVINE BLOOD PROTEINS IN FEEDINGSTUFFS

M-C. Lecrenier, H. Marbaix, P. Veys, M. Dieu, M. Raes, Ph. Delahaut, O. Fumière, G. Berben, C. Saegerman, V. Baeten, CRA-W (Belgium)

P26 MILK AUTHENTICITY BY SHOTGUN PROTEOMICS WITH MULTI-ENZYME DIGESTION

D. Nardiello, A. Natale, C. Palermo, M. Quinto, D. Centonze Università degli Studi di Foggia, Foggia (Italy)

P27 PROTEOMIC APPROACHES FOR PROTEOLYSIS STUDY OF SILTER CHEESES PRODUCED IN VALLEY AND ALPINE PASTURES

B. la Gatta, A. Natale, G. Rusco, C. Palermo, S. Chessa, D. Nardiello, A Caroli, D. Centonze, A. Di Luccia, Università degli Studi di Foggia, Foggia (Italy)

P28 MASS SPECTROMETRY PEPTIDES IDENTIFICATION IN FUNCTIONAL PASTA FILATA OVINE CHEESE

M. Albenzio, A. Santillo, R. Marino, A. Della Malva, M. Caroprese, A. Sevi University of Foggia, Foggia (Italy)

P29 RAPID IDENTIFICATION OF ANTIMICROBIAL LIPOPEPTIDES IN BACILLUS SUBTILIS TR50 CELL-FREE SUPERNATANT BY HPLC-HIGH RESOLUTION-ORBITRAP™-BASED MASS SPECTOMETRY

L. Quintieri, L. Caputo, F. Baruzzi, A. Visconti, L. Monaci, ISPA-CNR, Bari (Italy)

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P30 DETECTION OF VITAMIN B12 IN FOOD PRODUCTS BY MATRIX-ASSISTED LASER DESORPTION/IONIZATION TIME-OF-FLIGHT MASS SPECTROMETRY

C.D. Calvano, G. Ventura, L. Donzella, T.R.I. Cataldi, F. Palmisano Università degli Studi di Bari “Aldo Moro”, Bari (Italy)

P31 PHOSPHOLIPIDS FROM FARMED DICENTRARCHUS LABRAX BRAIN: VALUABLE WASTE

S. Granafei, R. Carlucci, A. Lionetti, T. R. I. Cataldi, F. Palmisano, G Liebisch University of Bari “Aldo Moro”, Bari (Italy)

P32 IMPROVED RESOURCE EFFICIENCY THROUGHOUT THE POST-HARVEST CHAIN OF FRESH-CUT FRUITS AND VEGETABLES

M. D. Hernando, J.L. Tadeo, A.R. Férnandez-Alba, M.J. Martinez Bueno, R. Rosal, C. Silvestre, A. Mathew, P. Muranyi, M. Mänttäri, S. Yüce National Institute for Agricultural and Food Research and Technology (INIA), Madrid (Spain)

P33 ERGOT ALKALOIDS IN ROUTINE ANALYSIS

L. Kuster, G. Jaunecker, C. Zahradnik, G. Häubl Romer Labs Division Holding GmbH, Getzersdorf (Austria)

P34 DIET EFFECTS ON INDIVIDUAL AND SEASONAL VARIABILITY OF ESSENTIAL AND TOXIC ELEMENTS IN URINE

A.R. Lovino, O. Miedico, M. Tarallo, G. Astarita, E. Chiaravalle, G. Corso, G. Paglia Università degli Studi di Foggia, Foggia (Italy)

P35 HIGH-THROUGHPUT ASSAY OF CAFFEINE IN BEVERAGES BY PAPER SPRAY TANDEM MASS SPECTROMETRY

F. Mazzotti, D. Taverna, L. Di Donna, A. Napoli, G. Sindona University of Calabria, Rende (Italy)

P36 RAPID DETEMINATION OF FUROCOUMARINS IN CITRUS FRUITS PEEL EXTRACTS BY PAPER SPRAY MASS SPECTROMETRY

D. Taverna, L. Di Donna, F. Mazzotti, G. Sindona University of Calabria, Rende (Italy)

P37 RAPID QUALITY ASSESSMENT OF FOOD BY PAPER SPRAY MASS SPECTROMETRY AND ISOTOPE DILUTION METHODS

L. Bartella, D. Taverna, F. Mazzotti, A. Napoli, G. Sindona, L. Di Donna University of Calabria, Rende (Italy)

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P38 THE EFFECT OF IN-AMPHORAE AGING ON QUALITY OF MINUTOLO WHITE WINE MADE FROM CRYOMACERATED GRAPES UNDER REDUCTIVE CONDITIONS

A. Baiano, A. Mentana, M. Quinto, D. Centonze, G. Varva Università degli Studi di Foggia, Foggia (Italy)

P39 TARGETED AND UNTARGETED DISCRIMINATION BETWEEN MYRTUS COMMUNIS CULTIVARS FROM SARDINIA REGION

G. Sarais, G. D’Urso, C. Lai, F.M. Pirisi, C. Pizza, P. Montoro University of Cagliari, Cagliari (Italy)

P40 DEVELOPMENT OF SEMI-AUTOMATED MASS SPECTROMETRY IMMUNOASSAY WORKFLOW FOR HIGH-THROUGHPUT DETECTION OF EGG ALLERGENS IN WINES

R. Pilolli, A. Di Palo, R. Chaudari, L. Monaci, ISPA-CNR, Bari (Italy)

P41 HPLC/DAD/MS-TOF STUDY OF THE BIOPHENOLS IN “PÂTÉ” OBTAINED AS BY PRODUCT OF A MILLING PROCESS

M. Bellumori, M. Innocenti, L. Sansone, N. Mulinacci, University of Florence (Italy)

P42 MALDI–TOF MASS SPECTROMETRY ANALYSIS OF ESCHERICHIA COLI EXPOSED TO NANOANTIMICROBIALS

C.D. Calvano, R.A. Picca, E. Bonerba, N. Ditaranto, T. Pellegrini, G. Tantillo, N. Cioffi, F. Palmisano, Università degli Studi di Bari, Bari (Italy)

P43 CHARACTERIZATION OF POLYPHENOLS IN APRICOT AND PEACH PUREES BY UPLC COUPLED TO HRMS Q-EXACTIVE MASS SPECTROMETER : AN APPROACH IN THE IDENTIFICATION OF ADULTERATIONS

E. Cocconi, C. Stingone, A. Zanotti, A. Trifirò Stazione Sperimentale per l’Industria delle Conserve Alimentari (SSICA), Parma Italy)

P44 SHELF-LIFE PREDICTION OF FRESH SAUSAGES BY MASS SPECTROMETRY-BASED ELECTRONIC NOSE

A. Damascelli, V. Lippolis, Salvatore Cervellieri, L. Caputo, Federico Baruzzi, Michelangelo Pascale, ISPA-CNR, Bari (Italy)

P45 DEVELOPMENT OF AN LC-MS/MS METHOD FOR THE SIMULTANEOUS DETERMINATION OF BEAUVERICIN, ENNIATINS (A, A1, B, B1) AND CEREULIDE

M. Decleer, A. Rajkovic, B. Sas, A. Madder, S. De Saeger Ghent University, Ghent (Belgium)

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P46 CHARACTERIZATION OF FREE FATTY ACIDS IN MUSSELS BY LIQUID CHROMATOGRAPHY-ELECTROSPRAY IONIZATION MASS SPECTROMETRY

L. Facchini, I. Losito, A. Valentini, T.R.I. Cataldi, F. Palmisano Università degli Studi di Bari “Aldo Moro”, Bari (Italy)

P47 ON COMMUTABILITY OF REFERENCE STANDARD MATERIALS EVALUATED BY MS SPECTROMETRY AND NMR SPECTROSCOPY

P. Fanizzi, V. Gallo, N. Intini, M. Latronico, P. Mastrorilli, F. Mottola, P. Scapicchio, C. M. Stefanelli, Lab.Instruments S.r.l., Castellana Grotte (BA, Italy)

P48 DETERMINATION BY MS OF VINEATROL® METABOLISM BY GUT MICROBIAL COMMUNITY IN IN VITRO SIMULATOR M-SHIME

C. Giuliani, A. Ghiori, M. Innocenti, M. Marzorati, T. Van de Wiele, N. Mulinacci, University of Florence (Italy)

P49 DETERMINATION OF ESSENTIAL AND TOXIC ELEMENT IN SOUTH AND CENTRAL ITALIAN HONEY SAMPLES BY INDUCTIVELY COUPLED PLASMA MASS SPECTROMETRY

M. Quinto, E. Chiaravalle, G. Spadaccino, G. Anselmi, O. Miedico, G. Paglia, D. Centonze University of Foggia and CSRA, Foggia (Italy)

P50 EXTRACTION OF FREE FATTY ACIDS IN DAIRY PRODUCTS BY MEANS OF MATRIX SOLID PHASE DISPERSION FOLLOWED HPLC MS/MS ANALYSIS

M. C. Simeoni, E. Mattocci, F. Di Ottavio, G. Martino, M. Sergi, R. Curini, D. Compagnone University of Teramo, Teramo (Italy)

P51 PREPARATION OF HMG FLAVONOIDS EXTRACTS FROM BERGAMOT FRUIT AND THEIR IDENTIFICATION BY MASS SPECTROMETRY

L. Di Donna, L. Bartella, F. Mazzotti, D. Taverna, G. Sindona Università della Calabria, Rende (Italy)

P52 CHARACTERIZATION OF SIMPLE PHENOLIC COMPOUNDS IN COCOA PRODUCTS USING HIGH-PERFORMANCE LIQUID CHROMATOGRAPHY COUPLED TO HIGH RESOLUTION MASS SPECTROMETRY (Q-ORBITRAP)

C. Barnaba, T. Nardin., A. Pierotti., F. Camin, R. Larcher Fondazione E. Mach, San Michele all'Adige (Italy)

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P53 DETERMINATION OF POLYPHENOLS IN PLANT FOODS BY MSPD EXTRACTION AND HPLC-MS/MS

M. C. Simeoni, M. Pellegrini, M. Sergi, P. Pittia, D. Compagnone University of Teramo, Teramo (Italy)

P54 MYCOTOXIN MULTIPLE-ANALYSIS BY LC MS/MS ON ITALIAN FEEDSTUFF

M. Scarpari, V. Nanni, V. Scala, M. Reverberi, C. Fanelli University of Rome “Sapienza”, Rome (Italy)

P55 MASS SPECTROMETRY BASED ANALYSIS OF LIPIDS FROM WHOLE-GRAIN SEMOLINA (Triticum turgidum var. durum) G. Picariello, L. Di Stasio, I. Stillitano, P. Ferranti, S. D’Auria, G. Mamone, Istituto di Scienze dell’Alimentazione, CNR, Avellino (Italy)

P56 PROTEOME ANALYSIS OF GLUTEN SYNTHESIS AND ACCUMULATION DURING DEVELOPMENT OF DURUM WHEAT GRAIN: THE INTEROMICS PROJECT F. Mazzeo, L. Di Stasio, G. Picariello, R. Siciliano, P. Ferranti, S. D’Auria, G. Mamone, Istituto di Scienze dell’Alimentazione, CNR, Avellino (Italy)

P57 DETERMINATION OF PHENOLS IN OILS FROM OLEA EUROPAEA VAR. SYLVESTRIS AND IN MILK FROM SHEEP FED WITH FOOD CONTAINING THE CORRISPONDENT POMACE BY TANDEM MASS SPECTROMETRY C. Benincasa, M. Pellegrino, A. Parise, S. Zelasco, G. Gatti, D. Britti, A. Poerio, E. Perri, CREA-OLI, Rende, Cosenza (Italy)