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Copyright © 2020 by LUXON Co,. Ltd. ALL RIGHTS RESERVED.
1
Spherical Powders TechnologyVersion 1.1
For more information
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E-Mail: [email protected] (EN)
[email protected] (CN)
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INCI Name Product Name Particle Size(µ m)Oil Absorption
(ml/100g)
SILICA Non-coated
Silica
SILIA LX3 3
130~180SILIA LX7 7
SILIA LX13 13
SPHESTA SB606 6
50~80SPHESTA SB609 9
SPHESTA SB6013 13
SPHESTA MD7 7 90~130
SPHESTA HS10 10 230~270
SILICA coated
Silica
SILIA LX7 ASM 7 80~140
SPHESTA MD6 ASM 6 90~130
SPHESTA MD6 MSM 6 90~130
SPHESTA MD6 DSM 6 60 ~ 90
Spherical Porous Silica Powder
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Spherical Porous Silica powder
High Purity
Sebum Control
Semi-transparent
Soft focus effect
Smooth feeling
EU REACH
Ecocert
Spherical Porous Silica Powder
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User Guideline of SHPESTA
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Analysis recipe
Must proceed to Pure Water.
Part Ingredients %
AD.I-Water 76.5
Carbopol 940 1% sol. 17.0
BD.I-Water 1.0
TEA 0.5
C Powder 5.0
1. Prepare 200ml beaker
2. Carbopol 940 1% solution prepared in advance
3. Manufactured A Phase and prepared for the
first time.
4. Manufacture B Phase and put it into A Phase.
5. Manufactured at maximum rpm of stirrer
6. Understand the flowability of the final Phase.
TEST Method
TEST Results
MD7 ‘S’ co ‘A’ co
MD7 ‘S’ co ‘A’ co
Excellent Thickener Compatibility
Thickener compatibility TEST_Carbopol 940
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Analysis recipe
Must proceed to Pure Water.
Part Ingredients %
AD.I-Water 94.0
RHEOSOL AVH 1.0
B Powder 5.0
1. Manufactured A Phase
2. Put B Phase into A Phase.
3. Manufactured at maximum rpm of stirrer
4. Understand the flowability of the final Phase.
TEST Method
TEST Results
MD7 ‘S’ co ‘A’ co
MD7 ‘S’ co ‘A’ co
Excellent Thickener Compatibility
Thickener compatibility TEST_RHEOSOL AVH
Copyright © 2020 by LUXON Co,. Ltd. ALL RIGHTS RESERVED.
Our Proposal of Basic Foundation ( SPF40, PA+++ )
PHASE RAW MATERIALS INCI %
A
LX SUN MCX Ethylhexyl Methoxycinnamate 6.00
LX SUN EHS Ethylhexyl Salicylate 4.00
SF 5600Z Phenyl Trimethicone 10.00
BSF 0015Z Cyclopentasiloxane (and) Cyclohexasiloxane 5.00
Bentone 38 VCG Disteardimonium Hectorite 0.50
CMicrocare e 9016 Cetyl PEG/PPG-10/1 Dimethicone 3.50
Rheodol AO-15 Sorbitan Sesquioleate 1.00
D
LX Bianco 200HDTitanium Dioxide / Aluminum / Hydrogen Dimethicone
10.00
LX IOY ASM Iron oxide yellow / Triethoxycaprylylsilan 0.50
LX IOR ASM Iron oxide red / Triethoxycaprylylsilan 0.15
LX IOB ASM Iron oxide blue / Triethoxycaprylylsilan 0.10
ZINC STEARATE Zinc Stearate 1.00
SILIA LX7 Silica 3.70
LX SS150 Zinc Oxide / Silica / Triethoxycaprylylsilane 2.00
E
WATER Water To 100
EDTA-2Na Disodium EDTA 0.05
MgSO4 Magnesium Sulfate Heptahydrate 1.00
LX MOILUB 1000 Biosaccharide Gum-1 2.00
F PRESERVATIVESCaprylhydroxamic Acid/CaprylylGlycol/Glycerin
2.00
Key Ingredients our products
1. LX Bianco 200HD2. LX IOY ASM, LX IOR ASM,
LX IOB ASM 3. SILIA LX74. LX SS150
Commend
5. LX SUN MCX, EHS
6. LX MOILUB 1000
HTT0714FD01
Standard Operating Procedures
1. Heat phase A to 85℃, then homomix at 3500rpm for 10 minutes.
2. After homo dispersing phase B at 2000rpm , 85 ℃, for 10 minutes, add to phase A
3. Homo disperse phase C at 1500 rpm for 5 minutes, and then add to phase A
4. Add phase D into phase A
5. After homo dispersing phase E at 1500rpm at 85℃, add to phase A
6. Add phase F into phase A at 60℃
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Our Proposal of Double Make-up Foundation (SPF 30 PA++)
PHASE RAW MATERIALS INCI %
A
TMS 803 50C Cyclopentasiloxane/ Trimethyl siloxysilicate 25.00
Microcare e9016 Cetyl PEG/PPG-10/1 Dimethicone 3.50
REODOL AO-15 Sorbitan Sesquioleate 1.50
BDC 245 Cyclopentasiloxane 5.00
BENTON 38V CG Disteardimonium Hectorite 1.50
C
LX MICA DSM Mica, Dimethicone 1.00
LX PMSQ P50 Polymethylsilsesquioxane 2.00
SPHESTA MD 7 Silica 2.00
D
DACHE EZH Ti70 Please refer to MSDS 18.00
DACHE EZH IOY50 Please refer to MSDS 2.60
DACHE EZH IOR55 Please refer to MSDS 0.70
DACHE EZH IOB60 Please refer to MSDS 0.15
E
Water Water To 100
Disodium EDTA Disodium EDTA 0.02
Sodium Chloride Sodium Chloride 1.50
LX MOILUB 1000 Biosaccharide Gum-1 0.50
Preservative Phenoxyethanol, Caprylyl Glycol, 1,2hexandiol 2.00
Allantoin Allantoin 0.02
D-Panthenol D-Panthenol 0.02
Key Ingredients of LUXON products
• DACHE EZH Ti70
• DACHE EZH IOY50
• DACHE EZH IOR55
• DACHE EZH IOB60
• LX MICA DSM
• LX PMSQ P50
• SPHESTA MD 7
• MD 7
Recommend use with
• LX MOILUB 1000
Standard Operating Procedures
1. Heat phase A to 80℃.
2. Heat phase B to 80℃., then Homomix at 3000rpm for 5minutes. And add to phase A.
3. Add phase C to phase A+B
4. Add phase D into phase A+B+C
5. After homo dispersing phase E at 3000rpm for 5minutes at 85℃, add to phase A+B+C+D
6. Homomix at 3500rpm for 10 minutes.
7. Cooling & Defoaming.
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Ingredient
Silica, Corn Starch modified, Dimethicone, Vinyl Dimethicone Crosspolymer, Caprylic/Capric Triglyceride, Mica, Methicone, Mineral Salts, Camellia Sinensis Leaf Extract,. Mentha Arvensis Leaf ExtractEthylhexylglycerin, Glyceryl caprylate, Ethylene/Acrylic Acid Copolymer, 1,2-Hexanediol, Fragrance
Key Ingredients
SPHESTA MD7
LX Mica DSM
LX PMSQ P50
Formulation for SEBUM control powder in use SPHESTA[SILIA] Series
Phase Trade Name INCI %
A SPHESTA MD7 Silica 56.75
HICOS GTC Caprylic/Capric Triglyceride 5.00
B Dry Flo PC Aluminum Starch Octenylsuccinate 25.00
LX PMSQ P50 Polymethylsilsesquioxane 10.00
LX Mica DSM Mica, Dimethicone 3.00
C SpectrastatCaprylhydroxamic Acid/CaprylylGlycol/Glycerin
0.15
Perfume 0.10
100.0
Our Proposal of Sebum control powder
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Is a cross linked polymethylmetaacrylate powder
Touch modifying agent
Soft feel effect
Gloss control
Concealing effect to hide defects
INCI Name Product Name Particle Size(µ m)Oil Absorption
(ml/100g)
PMMA
Poly methyl-metacrylate LX PMMA PR7 7 50 ~ 80
LX PMMA PR7
Poly MethylMethacylate Powder
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LX PMMA PR7 is organic crosslinked microsphere developed by Luxon’s original suspension polymerization. When it was used to cosmetic, it provides a rolling effect, the prevention of aggregation, an elegant silky texture, oil absorption etc. Also LX PMMA PR7 overcame the limitation of application due to high specifics surface and the introduction of functional groups. These characteristics of LX PMMA PR7 allow for the use of other application such as LCD panel filler, toner for electronic photos, as well as the super plasticizer of paints and inks.
Characteristics of products
Spherical cross-linked organic particles Various sizes with low moisture content and neutral pH Excellent chemical and thermal stability Readily dispersed in numerous solvents Impart desirable physical properties Suitable for additive or perfume carrier due to its oil absorption Best spread ability, provides very soft feeling to skin Suitable for the payoff control of pressed-type product Water insoluble
LX PMMA PR7
Poly MethylMethacylate Powder
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Our Proposal of Loose Powder formulation
Phase Trade Name INCI %A SILIA LX-7 Silica 59.493
LX PMMA PR-7 Polymethylmethacrylate 20.0
LX ELASTA SP101Vinyl Dimethicone/MethiconeSilsesquioxane Crosspolymer
2.0
LX Glight-1000Boron Nitride &
Triethoxycaprylylsilane4.0
BNeossanceHemisqualane
Hemisqualane 1.0
DC556 Phenyl Trimethicone 5.0
Demosoft GMCY Glyceryl caprylate 0.3
SC-50 EthylhexylGlycerin 0.2
W-RF16011781 Fragrance 0.007
100.0
Key Ingredients our products
1. SILIA LX-7
2. LX PMMA PR-7
3. LX ELASTA SP101
4. LX Glight-1000
Standard Operating Procedures
1. Weigh A and Mix it2. Weigh B and Mix it 3. Input B into A Mixer 3,000rpm ; 15Sec, 3times4. Filter by 100 Mesh
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Spherical PMSQ is widely used in
Color cosmetics
Daily skin care porducts
Recreational sunscreen products
INCI Name Product Name Particle Size(µ m)Oil Absorption
(ml/100g)
PMSQ
Poly methyl-silsequioxane LX PMSQ P50 5 40 ~ 60
LX PMSQ P50
Poly Methylsilsequioxane Powder
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LX PMSQ is a silicone resin sphere with 3-dimensional network structure.
INCI name is polymethylsilsequioxane.
Low reflective index 1.43
Does not dissolve or swell in all sorts of solvent
Excellent water repellency
More slip an lubricity / better skin feel
Excellent elasticity
Water Insoluble
LX PMSQ P50
Poly Methylsilsequioxane Powder
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PHASE RAW MATERIALS INCI %
A
TMS 803 50C Cyclopentasiloxane/ Trimethyl siloxysilicate 20.00
Microcare e9016 Cetyl PEG/PPG-10/1 Dimethicone 3.50
REODOL AO-15 Sorbitan Sesquioleate 2.00
Parsol MCX Ethylhexyl Methoxycinnamate 5.00
BDowsil F2-3196 Caprylyl Methicone 5.00
BENTON 38V CG Disteardimonium Hectorite 0.50
C
LX MICA AM Mica, Lauroyl lysine 1.00
LX PMSQ P50 Polymethylsilsesquioxane 2.00
SPHESTA MD 7 Silica 2.00
D
DACHE EZH Ti70 Please refer to MSDS 25.00
DACHE EZH IOY50 Please refer to MSDS 5.60
DACHE EZH IOR55 Please refer to MSDS 1.60
DACHE EZH IOB60 Please refer to MSDS 0.2
E
Water Water To 100
Disodium EDTA Disodium EDTA 0.02
Sodium Chloride Sodium Chloride 1.50
LX MOILUB 1000 Biosaccharide Gum-1 0.50
Preservative Phenoxyethanol, Caprylyl Glycol, 1,2hexandiol 2.00
Allantoin Allantoin 0.02
D-Panthenol D-Panthenol 0.02
Our Proposal of Moisture fit Foundation (SPF 15 PA+)
Key Ingredients of LUXON products
• DACHE EZH Ti70
• DACHE EZH IOY50
• DACHE EZH IOR55
• DACHE EZH IOB60
• LX MICA DSM
• LX PMSQ P50
• SPHESTA MD 7
Recommend use with
• LX MOILUB 1000
Standard Operating Procedures
1. Heat phase A to 80℃.
2. Heat phase B to 80℃., then Homomix at 3000rpm for 5minutes. And add to phase A.
3. Add phase C to phase A+B
4. Add phase D into phase A+B+C
5. After homo dispersing phase E at 3000rpm for 5minutes at 85℃, add to phase A+B+C+D
6. Homomix at 3500rpm for 10 minutes.
7. Cooling & Defoaming.
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Microbeads Issue
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EU proposes ban on 90% of microplastic pollutants
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Problem
Micro Beads Problems
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Plastic in cosmetics is a design error
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Our Proposal
SPHESTA SB606 HSM
SPHESTA ECO 3(Natural)
SPHESTA ECO 7(Natural)
SPHESTA ECO H10(Natural)
SS-2000
Type Spherical powder Spherical Powder Spherical Powder Spherical Powder Spherical Powder
INCISilica & Hydrogen
Dimethicone
Silica & Lauryl Alcohol& Cetyl Alcohol
Silica & Lauryl Alcohol& Cetyl Alcohol
Silica & Lauryl Alcohol& Cetyl Alcohol
Zinc Oxide & Triethoxycarylylsil
ane
CAS. NO7631-86-9
& 68037-59-2
7631-86-9& 112-53-8
& 36653-82-4
7631-86-9& 112-53-8
& 36653-82-4
7631-86-9& 112-53-8
& 36653-82-4
1314-13-2 & 2943-75-1
Particle Size 4.5 ~ 7.5 um 1.5 ~ 4.5 um 7.0 ~ 11 um 10.0 ~ 15.0 um 1.0 ~ 3.0 um
OilAbsorption
55 50 ~ 90 50 ~ 90 170 ~ 210 50 ~ 70
Hydrophobicity[LXTM-007] 3.5 min 3.5 min 3.5 min 3.5 min 3.5 min
Patent Pending: KR 10-2020-0075958
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Water Cyclopentasiloxane Liquid Paraffin Water Cyclopentasiloxane Liquid Paraffin
SPHESTA ECO H10SPHESTA ECO H10 SPHESTA ECO H10 PMMA Porous PMMA Porous PMMA Porous
SPHESTA ECO H10 PMMA Porous type
Water Cyclopentasiloxane Liquid Paraffin
SILICA STANDARD SILICA STANDARD SILICA STANDARD
SILICA Standard ( Non coating )
After input 3min After input 3min
After input 3min
Selective sebum control
Selective Sebum Control Test
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Standard Operating Procedures
1. Disperse A and B respectively
2. Mix A and B, disperse after adding C
3. Heating D at 60 °C and confirming
complete dissolution, then cooling to 25 °C
4. Put D in A~C to emulsify
( 7000rpm, 8 min )
5. Finish after cooling to 35 °C
Key Ingredients our products
1. LX NT95 HD (TIO2)
2. LX HPA30 HD (ZnO)
3. LX SS150 (ZnO)
4. SPHESTA ECO H10
5. SILIA LX7 ASM
Commend
6. LX MOILUB 1000
7. LX SUN MCX, EHS, HMS, TNS
Our Proposal of Sun Cream Sebum Care W/S ( SPF50+, PA++++ )
PHASE Ingredient INCI %
A
SF1202 Cyclopentasiloxane 16.00
BENTONE 38V CG Disteardimonium Hectorite 1.20
MICROCARE E9016 Cetyl PEG/PPG-10/1 Dimethicone 3.00
LX GEL A20Dimethicone / Phenyl Trimethicone / Cyclomethicone Crosspolymer
2.00
DC556 Phenyl Trimethicone 3.50
B
FINSOLV TN-O C12-15 Alkyl Benzoate 5.00
LX SUN MCX Ethylhexyl Methoxycinnamate 7.00
LX SUN EHS Ethylhexyl Salicylate 4.00
LX SUN HMS Homosalate 2.00
LX SUN TNSBis-Ethylhexyloxyphenol Methoxyphenyl Triazine
0.50
LX NT95 HDTitanium Dioxide / Aluminum Hydroxide / Stearic Acid / Dimethicone
7.00
LX HPA30 HD Zinc Oxide / Hydrogen Dimethicone 6.00
LX SS150Zinc Oxide / Silica / Triethoxycaprylylsilane
2.00
SPHESTA ECO H10 Silica / Cetyl Alcohol / Lauryl Alcohol 2.00
SILIA LX7 ASM Silica / Triethoxycaprylylsilane 2.00
C
D.I.WATER Water To 100
NACL Sodium Chloride 1.00
LX MOILUB 1000Biosaccharide Gum-1PEG/PPG17/6 Copolymer
3.50
D PreservativesPentylene Glycol,Ethylhexylglycerin,Phenoxyethanol
2.00
SB606 HSM & Nylon-12
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SPHESTA SB606 HSM Nylon-12(T co,Ltd)
Type Spherical powder Spherical powder
INCI Silica & Hydrogen Dimethicone Nylon-12
CAS. NO7631-86-9
& 68037-59-225038-74-8
Particle Size 4.5 ~ 7.5 um 5.0 ~7.0um
Oil Absorption 50 ~ 90 50 ~ 90
Hydrophobicity[LXTM-007]
3.5 5.0
SB606 HSM & Nylon-12
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① : SPHESTA SB606 HSM ② : Nylone-12
Manufacturer LUXON ‘S’ company
Loss on Drying 0.65% 0.76%
Hydrophobicity 5 5
Median Size (㎛) 6.90 7.88
PH 7.30 7.50
Oil Absorption 53 57
SEM
Heat Resistance(130℃ 30min)
Yellow Index 3.01 Yellow Index 6.12
SPHESTA SB606 HSM & ‘S’co Nylone-12
SPHESTA SB606HSM_comparison analysis
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Analysis equipment : Malvern Instruments
① : SPHESTA SB606 HSM (LUXON)
Results
D50 6.90 ㎛
D90 11.00 ㎛
② : Nylone-12 (‘S’ company)
Results
D50 7.88 ㎛
D90 17.60 ㎛
Side Effect
# Side Effect : particle aggregation, rough feeling
Comparison Analysis
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Philicsta MD7
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No Sebum Toner
IOPEPore ResetMattifying Toner
Water, Ethanol, Propanediol, Glyserine, 1,2 hexanediol,
Green tea extract, Silica, Bis-peg 18 methylethyldimethylsilane,
PG-60 Hydrogenated Castor Oil, Butylene Glycol, SmallIndium
magnesium silicate, ethylhexyl glycerin, calcium chloride,
2Na EDTA, fragrance
All ingredients
No Sebum Toner with Silica
Silica function
Easy daily sebum care withpowder toner
Sensory additive Enhanced stability in O/W
Silica layer
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No Sebum Toner
Pong DangDaily ClarifyingFacial Toner
All ingredients Silica
Silica layer
No Sebum Toner with Silica
Silica function
Easy daily sebum care withpowder toner
Sensory additive Enhanced stability in O/W
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SPHESTA MD 7( Standard Silica )
PHILICSTA MD7( Special Silica )
Type Spherical Powder Spherical Powder
INCI Silica Silica
& Phytic Acid
CAS. NO 7631-86-97631-86-9 &
83-86-3
Particle Size 5.0 ~ 9.0 um 5.0 ~ 9.0 um
Oil Absorption 50 ~ 90 70 ~ 110
Hydrophobicity
[LXTM-007]1.0 max 1.0 max
Our Proposal
OP
HO
OHO
O
P OH
OH
OOP
OHHO
OOP
OH
HO
O
OP
HO
HO
O
OP
OH
OHO
Coating Agent
Phytic Acid
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Dispersion Test Method
1. Water : 60g + 3g ; vial 100ml2. Mixer ( 500rpm; 3min )3. Precipitation for 24hr4. Shaking 10times5. Turn vial over6. Check the redispersibility
Sample A
Water 50g Powder 2g
Powder Input
Mixer ; 500rpm 3min
Sample B
Precipitation for 24hr Hand Shaking 10times
Sample B
Turn Vial Over
Sample A Sample B
Sample A
ExcellentRedispersibility
1 2 3
4 5 6
Redispersibility test of Water
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Standard Silica HYDROPHILICSTASilica
Precipitation for 24hr After Shaking 10times, Turn over
Sample A Sample B
Sample B Sample A
ExcellentRedispersibility
Standard Silica HYDROPHILICSTASilica
Test Result of redispersibility Water
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China HuZhou Factory : No.328 Guangyuan Road,Wuxing District,Huzhou City, ZheJiang Province, China Tel:+86-572-2607665 Fax:+86-572-2607-675
Shanghai Branch : Rm 2116,Block A,East International Building,No.85 Loushanguan Rd,Changning District,Shanghai City,China Tel:+86-21-6278-2288~216 Fax:+86-21-6278-3723
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