1l 1h nmr (400 mhz, cdcl3 · 1l. 13. c nmr (100 mhz, cdcl. 3) hn s o o i s. electronic...
TRANSCRIPT
1l 1H NMR (400 MHz, CDCl3)
HNS
O
O
I
S
Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013
1l 13C NMR (100 MHz, CDCl3)
HNS
O
O
I
S
Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013
Copies of 1H and 13C NMR
3a 1H NMR (400 MHz, CDCl3)
NN
I
CH3
Ts
Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013
3a 13C NMR (100 MHz, CDCl3)
NN
I
CH3
Ts
Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013
3b 1H NMR (400 MHz, CDCl3)
NN
I
F
Ms
Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013
3b 13C NMR (100 MHz, CDCl3)
NN
I
F
Ms
Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013
3c 1H NMR (400 MHz, CDCl3)
NN
I
Cl
Ms
Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013
3c 13C NMR (100 MHz, CDCl3)
NN
I
Cl
Ms
Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013
3d 1H NMR (400 MHz, CDCl3)
Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013
3d 13C NMR (100 MHz, CDCl3)
Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013
3e 1H NMR (400 MHz, CDCl3)
NN
I
F
Ts
Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013
3e 13C NMR (100 MHz, CDCl3)
Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013
3f 1H NMR (400 MHz, CDCl3)
Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013
3f 13C NMR (100 MHz, CDCl3)
Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013
3g 1H NMR (400 MHz, CDCl3)
NN
I
Cl
Ts
Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013
3g 13C NMR (100 MHz, CDCl3)
NN
I
Cl
Ts
Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013
3h 1H NMR (400 MHz, CDCl3)
Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013
3h 13C NMR (100 MHz, CDCl3)
Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013
3i 1H NMR (400 MHz, CDCl3)
NN
I
CH3
S OO
S
Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013
3i 13C NMR (100 MHz, CDCl3)
NN
I
CH3
S OO
S
Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013
3j 1H NMR (400 MHz, CDCl3)
NN
I
S OO
S
F
Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013
3j 13C NMR (100 MHz, CDCl3)
NN
I
S OO
S
F
Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013
3k 1H NMR (400 MHz, CDCl3)
NN
I
S OO
S
Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013
3k 13C NMR (100 MHz, CDCl3)
NN
I
S OO
S
Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013
3l 1H NMR (400 MHz, CDCl3)
NN
I
CH3
Ms
Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013
3l 13C NMR (100 MHz, CDCl3)
NN
I
CH3
Ms
Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013
3m 1H NMR (400 MHz, CDCl3)
Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013
3m 13C NMR (100 MHz, CDCl3)
NN
I
F
Ms
Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013
3n 1H NMR (400 MHz, CDCl3)
Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013
3n 13C NMR (100 MHz, CDCl3)
Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013
3o 1H NMR (400 MHz, CDCl3)
Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013
3o 13C NMR (100 MHz, CDCl3)
NN
I
Me
Ts
Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013
3p 1H NMR (400 MHz, CDCl3)
Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013
3p 13C NMR (100 MHz, CDCl3)
NN
I
F
Ts
Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013
3q 1H NMR (400 MHz, CDCl3)
NN
I
Cl
Ts
Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013
3q 13C NMR (100 MHz, CDCl3)
Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013
3r 1H NMR (400 MHz, CDCl3)
NN
I
Br
Ts
Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013
3r 13C NMR (100 MHz, CDCl3)
NN
I
Br
Ts
Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013
3s 1H NMR (400 MHz, CDCl3)
Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013
3s 13C NMR (100 MHz, CDCl3)
NBn
N
I
Ts
F
Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013
3t 1H NMR (400 MHz, CDCl3)
N NN
I
F
Ts
Cl
Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013
3t 13C NMR (100 MHz, CDCl3)
N NN
I
F
Ts
Cl
Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013
3u 1H NMR (400 MHz, CDCl3)
Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013
3u 13C NMR (100 MHz, CDCl3)
Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013
3v1H NMR (400 MHz, CDCl3)
NN
O2N
S OO
I
F
S
Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013
3v 13C NMR (100 MHz, CDCl3)
NN
O2N
S OO
I
F
S
Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013
3w 1H NMR (400 MHz, CDCl3)
NN
S OO
Br
Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013
3w 13C NMR (100 MHz, CDCl3)
NN
S OO
Br
Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013
4a 1H NMR (400 MHz, CDCl3)
Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013
4a 13C NMR (100 MHz, CDCl3)
Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013
4b 1H NMR (400 MHz, CDCl3)
Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013
4b 13C NMR (100 MHz, CDCl3)
Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013
4c 1H NMR (400 MHz, CDCl3)
NN
Ms
Cl
Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013
4c 1H NMR (400 MHz, CDCl3)
NN
Ms
Cl
Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013
4d 1H NMR (400 MHz, CDCl3)
NN
Ms
Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013
4d 13C NMR (100 MHz, CDCl3)
NN
Ms
Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013
4e 1H NMR (400 MHz, CDCl3)
NN
Ts
F
Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013
4e 13C NMR (100 MHz, CDCl3)
NN
Ts
F
Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013
4f 1H NMR (400 MHz, CDCl3)
NN
Ts
Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013
4f 13C NMR (100 MHz, CDCl3)
NN
Ts
Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013
4g 1H NMR (400 MHz, CDCl3)
Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013
4g 13C NMR (100 MHz, CDCl3)
Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013
4h 1H NMR (400 MHz, CDCl3)
NN
Ts
Br
Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013
4h 13C NMR (100 MHz, CDCl3)
NN
Ts
Br
Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013
4i 1H NMR (400 MHz, CDCl3)
Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013
4i 13C NMR (100 MHz, CDCl3)
Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013
4j 1H NMR (400 MHz, CDCl3)
NN
S OO
S
F
Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013
4j 13C NMR (100 MHz, CDCl3)
NN
S OO
S
F
Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013
4k 1H NMR (400 MHz, CDCl3)
NN
S OO
S
Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013
4k 13C NMR (100 MHz, CDCl3)
Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013
4l 1H NMR (400 MHz, CDCl3)
N NMs
CH3
Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013
4l 13C NMR (100 MHz, CDCl3)
N NMs
CH3
Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013
4m 1H NMR (400 MHz, CDCl3)
Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013
4m 13C NMR (100 MHz, CDCl3)
Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013
4n 1H NMR (400 MHz, CDCl3)
Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013
4n 13C NMR (100 MHz, CDCl3)
Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013
4o 1H NMR (400 MHz, CDCl3)
Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013
4o 13C NMR (100 MHz, CDCl3)
N NTs
Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013
4p 1H NMR (400 MHz, CDCl3)
Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013
4p 13C NMR (100 MHz, CDCl3)
Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013
4q 1H NMR (400 MHz, CDCl3)
Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013
4q 13C NMR (100 MHz, CDCl3)
N NTs
Cl
Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013
4r 1H NMR (400 MHz, CDCl3)
Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013
4r 13C NMR (100 MHz, CDCl3)
Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013
4s 1H NMR (400 MHz, CDCl3)
Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013
4s 13C NMR (100 MHz, CDCl3)
NN
Ts
F
Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013
4t 1H NMR (400 MHz, CDCl3)
N NN
Ts
F
Cl
Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013
4t 13C NMR (100 MHz, CDCl3)
N NN
Ts
F
Cl
Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013
4u 1H NMR (400 MHz, CDCl3)
N
MeO
NS O
O
S
Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013
4u 13C NMR (100 MHz, CDCl3)
N
MeO
NS O
O
S
Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013
4v 1H NMR (400 MHz, CDCl3)
N
O2N
N
F
S OO
S
Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013
4v 13C NMR (100 MHz, CDCl3)
Electronic Supplementary Material (ESI) for Chemical CommunicationsThis journal is © The Royal Society of Chemistry 2013