02660 s2 puma mon8.qxp 210x279€¦ · 2 the s2 puma is an incredibly adaptable and powerful...

Innovation with IntegrityEDXRF

Spectrometry Solutions

S2 PUMA

02660_S2_PUMA_MON8.qxp_210x279 21.06.16 10:29 Seite 1

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The S2 PUMA is an incredibly adaptable and powerful spectrometer.

The Puma is an incredibly adaptable and powerful animal.


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S2 PUMA –Analyze.Everything.Faster.

S2 PUMA Single

S2 PUMA EasyLoad XY Autochanger

S2 PUMA EasyLoad Carousel

Analyze.

Accessing information about sample composition is essential for process and quality control in industrial laboratories, but also in research applications in academia. No matter if you need a quick idea of elements present, or accurate concentrations for all elements from C to Am in the range of 100 % down to a few ppm, the S2 PUMA is the optimal choice.

Everything.

Samples come in different forms, shapes and sizes,and time and cost savings for sample preparation are always a consideration. Whetheryou need to analyze solids or liquids, compactpieces or powders, large or very small samples, the S2 PUMA analyzes all your samples in manual or fully automated mode.

Faster.

Results must be obtained in the shortest possible time since time-to-result is always critical for process control. Large sets of samples are analyzed throughout the day. The S2 PUMA delivers fast, accurate results all day, every day.

The S2 PUMA is the most adaptableand powerful EDXRF solution for your analytical needs.


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S2 PUMA

with HighSense™ –

the top-performing

EDXRF

HighSense™ is the key to the unrivaled analytical performance of the S2 PUMA. The instrument's direct-excitation beam path makes full use of the 50-watt power ofthe X-ray tube. The optimal excitation of all elements in thesample is guaranteed with up to 50 kV voltage. The high-countrate, high-resolution XFlash® silicon drift detector (SDD)further enhances the instrument's performance and recordssample spectra in HD mode. But that’s not all. With the all-new instrument X-ray optics, the distances between the X-ray tube, the sample and the detector are even shorter thanbefore. This results in better detection limits, higher precision and shorter measurement times.

Top performance is the result of perfect teamwork. For the S2 PUMA, we call this HighSense™ technology!

Elemental analysis couldn’t be easier!

Energy-dispersive X-ray fluorescence (EDXRF) with the S2 PUMA offers all you need to measure and monitor elements in your samples, independent of the industry or environment in which you are working. The outstandingstrength of EDXRF is the wide range of elements covered by the technique, from very light elements like C, to heavy elements like Am.

Unmatched detection limits, precision and speed in EDXRF byHighSense™ technology:

Direct-excitation, closely coupledbeam path

X-ray tube with up to 50 W power and 50 kV excitation

XFlash® SDD with energy resolutiontypically 135 eV

HD-mode spectrum recording with4K multi-channel analyzer (MCA)

Optimal Light Element (LE) configu-ration with thin-window X-ray tubeand XFlash® X-ray detector

X-ray tube, air-cooled

Best performance at light elements: EDXRF

XFlash® X-ray detector

MgKa

> 20 %

NaKa

FKa

OKa

S2 PUMA Previous system

KeV

cps/

mA


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10-position filter wheel

for optimized peak-to-

background ratios

Collimator masks

for small samples or

small-spot analysisSample spinner and

precise sample positioning

DustShield™

detector capDuraBeryllium®

tube shield

Video camera

for viewing sample

position

X-ray tube

50 W, 50 kV

Ag or Pd target

XFlash® X-ray detector

Silicon Drift Detector (SDD)

with typ. 135 eV resolution

The S2 PUMA with HighSense™ technologyuses the 50-W end-window X-ray tube to directly excite X-ray fluorescence in a sample. By setting the high voltage for the X-ray tubeand choosing the filter material, the energyrange is selected. The XFlash® thin-window detector with multi-channel analyzer detects

the X-ray fluorescence radiation and accumu-lates counts to form an intensity versus energy spectrum of the sample. Lighter elements withlow-energy fluorescence are analyzed by eitherflushing the sample chamber with helium or by evacuating it with a vacuum pump.

HighSense™ beam path of the S2 PUMA

Element range of S2 PUMA Additional elements with S2 PUMA LE


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Cement, Minerals & Mining, Geology

Metals, Slags Petrochemicals, Refinery Chemicals Food, Cosmetics, Pharmaceuticals

Add efficiency to your labwithS2 PUMA

Productivity is paramount when you are analyzing numerouslarge series of samples per day. S2 PUMA with the EasyLoad™ XY Autochanger enhances the efficiency in your lab: Add samplesat any time without interruptingcurrent measurements, add up to20 samples in one go, run mixedbatches of solids and liquids, eachsample in the optimal mode.

Quick, convenient sample loading with the S2 PUMA EasyLoad XY Autochanger


7Metal cuts,Solids

Loose powders,Rocks,

Granules

Pressedpellets

Fusedbeads

Liquids,Slurries

Filters Films, Coatings,

Foils

Small parts

Automationrings, Belt conveyor

Environmental Academia


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High sample throughput, low cost of ownership and extreme reliability count in many industries and here iswhere the S2 PUMA shines. No matter if the samples arepressed pellets, fused beads, powders, solids, or liquids,up to 20 samples can be loaded at once with the EasyLoad™ XY sample tray. New samples can be addedat any time – even while a measurement is running. EasyLoad™ maximizes the sample throughput and minimizes the cost of ownership of the instrument.

Enhancing performance! Reducing costs!

The S2 PUMA analyses each sample with the optimalmethod: Liquids are analyzed under helium atmosphere,while solids are run under vacuum. This is essential to get the best performance for lighter elements. The S2 PUMA's optional vacuum pump eliminates the needfor helium when light elements in solid samples are analyzed. There is simply no other EDXRF instrument as efficient as the S2 PUMA!

S2 PUMA EasyLoad XY Autochanger –ready to run 24/7!

S2 PUMA –

utmost efficiency

with EasyLoad™

Visual monitoring during measurements

Additional sample trays with mixed sample batches

S2 PUMA EasyLoad XY Autochanger:

Trays with 20 sample positions Pressed powders, fused beads and

liquid cups with 40 mm sample size Direct handling of 51.5 mm sample

rings from automated samplepreparation

Mixed batches of liquids and solidsfor highest sample flexibility

Prepare the next sample tray whileprevious tray is running

High sample throughput, large sample series run overnight

New samples can be loaded andadded at any time


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The S2 PUMA is an indispensable tool to enhance productivity in industrial high throughput laboratories by offering a fully integrated automation solution for the XY Autochanger configuration.

The samples are feed directly from automated samplepreparation via robot or belt to the S2 PUMA from behind.

The AXSCOM communication interface connects toprocess control software ensuring the control of samplehandling and analysis process through one integrated solution.

Buffer positions for samples within the instrument compensate for delays in the lab automation. This leavesthe EasyLoad™ sample tray available for other out-of-linesamples. These samples can be added at any time andcan be analyzed with lower priority than the automationsamples. With this setup the S2 PUMA becomes an on-line elemental analyzer and concurrently maintaining its standalone capabilities.

S2 PUMA –

no compromise

on productivity

Flexible sample feeding – at anytime – manually, via sample tray, and – around the clock – fully automated, via conveyor belt

Connectivity in an automated laboratory at its best – S2 PUMA XY Autochanger

The S2 PUMA Automation can analyze longer series ofsamples autonomously and will free up valuable stafftime. Together with an automated press and mill it requires minimum lab space and is the ideal system either as standalone solution or as a backup system forlarger automated WDX instruments.

The system in this configuration is unrivalled and the onlyEDX benchtop instrument which offers you a professional,fully integrated automation solution.

The S2 PUMA Automation is the ideal solution as inte-grated backup in larger automated labs in addition toWDXRF systems, e.g. in cement plants, with mining operations, and in commercial service labs.

As a standalone automation solution, the S2 PUMA Automation is the perfect fit for raw mill control in cementplants cement plants and grinding facilities or for slaganalysis in steel plants.


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Cement, Minerals &Mining, Geology

Metals, Slags, Coatings Petrochemicals, Plastics,Refinery

Chemicals Food, Agriculture

S2 PUMA –quick resultsand best per-formance atyour fingertips

In process control every minutecounts! Whenever you receive asample, results are needed fast.The S2 PUMA Single is the perfect tool: Load the sample,touch the button and get resultswithin minutes. Best quality results as easy as 1-2-3, thanks to TouchControl™, the S2 PUMA’s intuitive user interface.

Quick start of sample for process control applications with S2 PUMA Single


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Education EnvironmentalCosmetics, Pharmaceuticals

Metal cuts,Solids


Granules

Pressedpellets

Fusedbeads

Liquids,Slurries


Foils

Small parts


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Sample rotation for accurate resultsQuick, easy sample loading Liquid sample analysis

Adjustable TouchControl™ interface

Island mode:No PC, keyboard and mouse required in routine operation

TouchControl™ for quick, failsafe ease-of-use

S2 PUMA with TouchControl™:Intuitive, failsafe ease-of-useIsland mode: Full functionality without PC, keyboard and mouseFree language selection:English, German, French, Spanish,Portuguese, Italian, Russian, Chinese, JapaneseNo training required – get resultsfrom day oneAdjustable touchscreen, glove-friendly


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EDXRF made

easy, only with

S2 PUMA and

TouchControl™

Thanks to TouchControl™, the operation of the S2 PUMA is easy and straightforward. The times of never-ending training, manualsthat weigh a ton and operation with adventuresin body contortions belong to the past.

With TouchControl, any user can performmeasurement jobs on the S2 PUMA. First, select the application and key in the sample ID. You can also add additional information, likepreparation or sample weight. Then simplystart the measurement and view the resultson-screen.

Instrument precision is the key fortight process control.

The S2 PUMA delivers excellent precision with its HighSense™ technology, the 50-Wattpower of the X-ray tube and the all-new closelycoupled beam path. This superior design guarantees process control at its best with avery narrow range for the results, minimizingwaste and maximizing yield in your process.

Easy and fast: Standardless analysis of unknown samples withSMART-QUANT FP

Together with the new standardless solutionSMART-QUANT FP you can use the analyticalperformance of the S2 PUMA without time-intensive calibration work on any unknownsample. Simply place your sample in the instrument, choose the appropriate methodand start the measurement.

The S2 PUMA can be used in "island mode" forroutine analysis which makes an external PCwith its periphery obsolete.

Highest intensity with S2 PUMA

Ultimate stability with S2 PUMA

CaKa

K

Ca

Mg

CaKb

S2 PUMA Previous system

KeV

cps/

mA

Conc

entra

tion

[%]

Measurements

02 4 6 8 10 12 14 16 18 20

0.2

0.4

0.6

0.8

1.0

1.2

1.4

Easy and fast: The Loader and SMART-QUANT FP

~ 20 %

3

2

1

Select sample position on EasyLoad™tray

Select appropriate SMART-QUANT FP method and name sample

Press “Start”

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2

3


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Geology Metals, Coatings Plastics, Polymers Pharmaceuticals Research, Academia, Material Science

Quick loading of sample batches or large samples with the S2 PUMA EasyLoad Carousel


15Large parts,Electronis,

PCBs

Toys, Consumerproducts

No limita tions in samplehandling – S2 PUMA

Sometimes you simply need flexibility: First, some large samples you cannot destroy. Then, “What is this black spot inthe plastic building block?” Next,analyze 12 geological samples aspressed pellets! Every job requestis different.

No need to worry, the S2 PUMAEasyLoad Carousel is the mostadaptable configuration. It handleslarge samples directly. Place theblock directly in the measurementposition, control it with the inte-grated video camera, and use thecollimator to analyze only the blackspot. But place the EasyLoad™tray in the chamber and it turnsinto an autosampler system forlarge batches.

Metal cuts,Solids


Granules

Pressedpellets

Fusedbeads

Liquids,Slurries


Foils

Small parts

Service Labs Automotive


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EasyLoad™ Carousel tray Lowering carousel tray during measurements

Raising carousel tray during transportation

Loading of large samplesSample positioning with video camera

Large-sample handling at its best

Footprint and height of the spectrometerchamber are limiting the maximum size oflarge samples which can be loaded into thespectrometer. With a sample chamberfootprint of 45 x 42 cm the S2 PUMA setsa new worldrecord.width max.

455 mm (17.9”)

depth max.

425 mm (16.7”)

height max.

106 mm (4.2”)


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Quick loading of sample batches with the S2 PUMA EasyLoad Carousel

S2 PUMA

EasyLoad Carousel –

Unlimited flexibility for

all kinds of samples

The S2 PUMA EasyLoad Carousel accommodates up to 12 different samples in one tray. Samples can bepowders, solids, pressed pellets, fused beads, or liquids, of sizes 32 mm, 40 mm or 51.5 mm in diameter. Different sample types and sizes can beeven mixed on a single carousel tray.

The S2 PUMA Carousel sets new standards – not only for small samples.

How to measure large samples if you don’t want to cut them to size? Nothing could be easier – just remove the tray and the sample chamber providesspace for large-sample non-destructive elementalanalysis. Very small to large samples of up to 45 x 42 cm can be directly analyzed in the S2 PUMA EasyLoad Carousel.

Mark the spot – and document your XRF measurements.

For exact sample positioning, a video camera is integrated in the S2 PUMA, providing a close-up view of the sample and enabling you to ensure thatjust the right spot is analyzed. A video camera imageis saved along with the EDXRF measurement dataand results for later reference.

Discover parts of your sample – with smallspot analysis.

When performing failure analysis, analyzing geologicalsamples or investigating consumer product safety, a specific small spot of the sample is of interest. TheS2 PUMA is equipped with an integrated collimator to perform analyses of small spots from a couple ofcentimeters down to a few millimeters.

Coating applications of multilayers –no problem for the S2 PUMA.

In research & development and materials science,multilayer systems are designed for specific functionality. The S2 PUMA delivers accurate resultsfor layer thickness and composition of single and multilayer samples. The analytical Multilayer softwarehandles EDXRF data from large samples, bulk samples and small spots!


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Safe sample handling with S2 PUMA SampleCare™

Grabber with uniquesample detection

DuraBeryllium®

tube shield

10-position filterwheel

DustShield™detector cap

Dust reservoir

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2

3

4

51

2

3 4

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S2 PUMA with SampleCare™:Unique contamination protection ofimportant system componentsGuarantees highest instrument uptimePrevents drawbacks from sampleleakagesFailsafe recognition of liquid cupsGrabber with automatic sample detectionDuraBeryllium® shield for tube window protectionUnique detector cap for detectorprotectionAvoids spillage of liquids and contamination with small sampleparticles on detector head

Stops dust & liquids

DustShield™ detector cap


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Built to last –

S2 PUMA with

SampleCare™

Built to analyze –

S2 PUMA with

SPECTRA.ELEMENTS

Solution Editor withtree structure to main-tain all relevant applica-tion parameters.

Selected ‘Manage Standards’ to enter all information on calibra-tion standards.

Overview about the standards for the steelapplication.

Spectrum of steel standard for evaluationof element lines.

Periodic table for convenient element selection.

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S2 PUMA with SampleCare™

Instrument uptime is crucial in every laboratory. But you canrely on the S2 PUMA with Bruker’s unique SampleCare™technology. SampleCare™ protects the instrument fromdamage by sample contamination. The integrated liquid sample detection of the EasyLoad™ XY Autochanger disables the vacuum mode whenever a liquid sample is detected. In addition, a DuraBeryllium® tube shield and thefilter wheel protects the X-ray tube. A third contaminationshield is the detector cap. The cap with an ultra-thin protec-tion foil avoids contamination by spills from liquid samplesand from particles of pressed pellet samples.

S2 PUMA with SPECTRA.ELEMENTS

To control your S2 PUMA it comes with the powerful SPECTRA.ELEMENTS software suite. It took tried and truefunctionalities, got upgraded with the latest technology andwas developed with the user in mind. The result is a high-performing combination of functionality and operator ergonomics.

Set up your applications with the Solution Wizard, start themeasurement with the Loader, and with the Results Man-ager evaluate scans, report results, and export your data -the tab-based organization easily lets you control all of these functions. The S2 PUMA's standardless solutionSMART-QUANT FP is seamlessly integrated into SPECTRA.ELEMENTS and lets you have analysis results available at your fingertips.

Setting up applications, maintaining methods, and obtaining excellent results has never been so easy.


Bruker AXS GmbH

Karlsruhe . GermanyPhone +49 (0)721-50997-0Fax +49 (0)[email protected]

www.bruker.com

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Technical Data

S2 PUMA Single S2 PUMA XY Autochanger S2 PUMA Carousel

Elemental range Sodium to americium (Na – Am) with standard XFlash®

Carbon to americium (C – Am) with XFlash® Light Element (LE)

Concentration range From ppm to 100 %

X-ray tube Pd or Ag anode; max. power 50 W; max. voltage 50 kV (low kV version: 30 kV max.)

Primary beam filters 10-position automatic filter changer; for wide range elemental analysis pre-installed filters: 5 µm Ag, 20 and 500 µm Al, 100 and 250 µm Cu

Detector XFlash® Silicon Drift Detector: Peltier cooled (no need for liquid nitrogen)

Collimator masks For small spot analysis: 1, 3, 8, 12, 18, 23 and 28 mm (optional)

Sample observation Integrated HD video camera, for exact sample positioning and documenting the measurement position of a sample (optional)

Mode Air modeGas flushing (optional): Helium for liquids and loose powdersVacuum pump (optional): Enhanced light element performance, low cost of operation

TouchControl™ Integrated 12.1” TFT touchscreen, multilingual user interface

Connectivity Built-in Ethernet port RJ45, 4x USB ports for mouse, keyboard, printer

Power requirements 100-240 V, 50/60 Hz, max. power consumption 600 VA

Automation Connectivity to conveyor belt or robot (optional)

Sample types Loose powders, granules, solids, pressed pellets, fused beads and liquids up to 20 mL

Sample rotation (optional)

S2 PUMA Single S2 PUMA XY Autochanger S2 PUMA Carousel

Sample sizes Up to 51.5 mm (2.03“) Øsamples. Liquids, loosepowders and smaller samples in liquid cups: up to 20 mL

Up to 40 mm (1.56“) Ø and 38 mm (1.49“) height insample holders, max. weight200 g or 51.5 mm (2.03“) Ø as sample ring.

32, 40 or 51.5 mm (1.26, 1.56or 2.03“) Ø samples. Large samples: width max. 455 mm (17.9“)depth max. 425 mm (16.7“)height max. 106 mm (4.2“)

Sample loader Single position,manual

EasyLoad XY™ sample tray, 20-position, removable; Grabber with automatic sample detection

EasyLoad™ Carousel sampletray, 12-position, removable

Dimensions

width x depth x height; weight67 x 71 x 37 cm; 87 kg26.2 x 27.8 x 14.6“; 192 lbs

67 x 71 x 61 cm; 108 kg26.2 x 27.8 x 23.8“; 238 lbs

67 x 71 x 57 cm; 130 kg26.2 x 27.8 x 22.2“; 287 lbs

Quality & safety DIN EN ISO 9001:2008; CE-certified Machinery directive 2006/42/EC; Electrical equipment 2006/95/EC; Electromagnetic Compatibility 2004/108/EC; Fully radiation-protected system; radiation < 1 µSv/h (H*); German type approval (BfS) for X-ray safety; Conform to ICRP, IAEA, EURATOM

TouchControl™, SampleCare™, EasyLoad™, HighSense™and DustShield™ are trademarks of Bruker AXS Inc.;XFlash® is a registered trademark of Bruker Nano AnalyticsDuraBeryllium® is a trademark of Moxtek® Inc.


02660 s2 puma mon8.qxp 210x279€¦ · 2 the s2 puma is an incredibly adaptable and powerful...

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