,. albuquerque, new mexico 87107 phone (505) 344-3777 fax ... alamos national labs/ta...

,.

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2

5 October 27, 2000

NMEDHWB 2044 A Galisteo Street Santa Fe, NM 87505

PL I.D. 008096

Project Name/Number: LANL PAJARITO 2-MILE HWB 8.24.00 CG

Attention: John Young

2709-D Pan American Freeway NE Albuquerque, New Mexico 87107 Phone (505) 344-3777 Fax(505)344-4413

UBRARYCOPY

On 08/25/00, Pinnacle Laboratories Inc., (ADHS License No. AZ0592 pending), received a request to analyze aqueous samples. The samples were analyzed with EPA methodology or equivalent methods. The results of these analyses and the quality control data, which follow each set of analyses, are enclosed.

This report is being issued in part to include results for Radiological data from Enviro-Test and Organic data from A TEL. One additional parameter (EPA method 8081, Pesticides and PCB's) will follow at a later date.

c;tle study was logged in for Appendix IX organics. Due to miscommunication, EPA method 8081 analysis was not run in hold-time. The sample will now be processed and data will be submitted at a later date. There will be no charge for this analysis. A credit memo has been issued. We regret this error and apologize for any inconvenience this may have caused.

Radiological chemistry analyses was performed by Envirotest, Casper, WY.

Appendix IX analyses were performed by A TEL, Melmore and Marion, OH.

EPA method 8270 SIMS analyses were performed by Environmental Services Laboratory, Inc., Portland, OR.

EPA method 8330 High Explosives, analyses were performed by Barringer Laboratories, Inc., Golden, CO.

Perchlorate analyses were performed by ATEL, Tucson, AZ.

All other analyses were performed by ATEL, Marion, OH.

If you have any questions or comments, please do not hesitate to contact us at (505) 344-3777.

JJru; rMitchell Rubenstein, Ph.D. ~neral Manager

\\\\\\\\\\\\\\\\\ '\\\\ \\\\\\\\ 306()

c

CLIENT

PROJECT#

PROJECT NAME

01

:NMEDHWB

:HWB 8.24.00 CG :LANL PAJARITO 2-MILE

PL ID: 008096 PINNACLE CLIENT ID# DESCRIPTION 008096-01 P ARAJITO@ TWO

MILE

---TOTALS---

2709-D Pan American Freeway NE Albuquerque, New Mexico 871 07 Phone (505) 344-3777 Fax(505)344-4413

DATE RECEIVED :08/25/00

REPORT DATE :09/25/00

DATE MATRIX COLLECTED

AQUEOUS 08/24/00

MATRIX AQUEOUS

#SAMPLES 1

, .•

ATEL

Aqua Tech Environmental Laboratories, Inc.

-CERTIFICATE OF ANALYSIS (REPRINT) -Client #: T0608

Pinnacle Labs, Inc. Report Date: 24-0ct-00

Original Report Date: 13-Sep-00 2709-D Pan-American Freeway, NE Albuquerque, NM 87107-

Phone: (505) 344-3777 Ext: Attn: Mitch Rubenstein

Our Lab#: MAR00-22526

Date Logged-In: 8/30/00 Matrix: Groundwater

Project#: 008096

FAX: (505) 344-4413

Your Sample ID: 008096-01 PARAJITO @TWO MILE

Sample Source: RCRA Client Project#: PO#: 008096

Date Submitted to Lab: 8/29/2000

-COLLECTION INFORMATION-

Dateffime/By: 8/24/00 9:55AM

Test Group EPA Method Test Result Units Analysis

Date Analyst

L-ICP-D 60108 Aluminum, AI, Dissolved ND (100) UGIL 8/30/00 SMM AL-ICP 60108 Aluminum, AI 12400 (100) UGIL 8/30/00 SMM BA-ICP 60108 Barium,Ba 467 (10) UG/L 8/30/00 SMM BA-ICP-D 60108 Barium, 8a, Dissolved 163 (10) UGIL 8/30/00 SMM CA-ICP-D 60108 Calcium, Ca, Dissolved 44 (0.1) MGIL 8/30/00 SMM CA-ICP 60108 Calcium, Ca 50 (0.1) MGIL 8/30/00 SMM CO-ICP-D 60108 Cobalt, Co, Dissolved ND (10) UGIL 8/30/00 SMM CR-ICP 60108 Chromium, Cr ND (20) UGIL 8/30/00 SMM CU-ICP-D 60108 Copper, Cu, Dissolved ND (10) UG/L 8/30/00 SMM

CO-ICP 60108 Cobalt, Co ND (10) UG/L 8/30/00 SMM FE-ICP-D 60108 Iron, Fe, Dissolved 175 (40) UGIL 8/30/00 SMM

CU-ICP 60108 Copper, Cu 19 (10) UGIL 8/30/00 SMM MG-ICP-D 60108 Magnesium, Mg, Dissolved 7.3 (0.1) MG/L 8/30/00 SMM FE-ICP 60108 Iron, Fe 7260 (40) UG/L 8/30/00 SMM MG-ICP 60108 Magnesium, Mg 8.5 (0.1) MGIL 8/30/00 SMM

MN-ICP-D 60108 Manganese, Mn, Dissolved 980 (10) UGIL 8/30/00 SMM MN-ICP 60108 Manganese, Mn 1600 (10) UGIL 8/30/00 SMM HG-D 7470A Mercury, Hg, Dissolved ND (0.2) UGIL 9/1/00 SMM

HG 7470A Mercury, Hg ND (0.2) UGIL 9/1100 SMM 'I-ICP-D 60108 Nickel, Ni, Dissolved ND (20) UGIL 8/30/00 SMM

'- NI-ICP 60108 Nickel, Ni ND (20) UGIL 8/30/00 SMM

WS#

22416

22416

22416

22416

22416

22416

22416

22416

22416

22416

22416

22416

22416

22416

22416

22416

22416

22452

22452

22416

22416

Lab Number MAR00-22526:Page I

1776 MARION-WALDO RD. • P.O. BOX 436 • MARION, OH 43301-0436 PHONE 740-389-5991 • 1-800-873-2835 • FAX 740-389-1481

Test Group

K-ICP-D

K-ICP

SE-GFAA-D

SE-GFAA

NA-ICP-D

V-ICP-D

NA-ICP

ZN-ICP-D

V-ICP

ZN-ICP

CR-ICP-D

AS-MS

AS-MS-D

>-MS-D

SB-MS

PB-MS-D

TL-MS

TL-MS-D

CD-MS

SB-MS-D

PB-MS

BE-MS-D

BE-MS

TAL Metals

TAL Metals-D

AG-ICP

AG-ICP-D

CN

NH3

TKN

N03+N02

BR-IC-HI

-IC


-CERTIFICATE OF ANALYSIS (REPRINT)-

EPA Method Test

60108

60108

7740

7740

60108

6010B

60108

60108

6010B

6010B

60108

6020

6020

6020

6020

6020

6020

6020

6020

6020

6020

6020

6020

6010B

6010B

335.4/9012A

350.1

351.3

353.2/9200

300.0

300.0

Potassium, K, Dissolved

Potassium, K

Selenium, Se, Dissolved

Selenium, Se

Sodium, Na, Dissolved

Vanadium, V, Dissolved

Sodium, Na

Zinc, Zn, Dissolved

Vanadium, V

Zinc, Zn

Chromium, Cr, Dissolved

Arsenic, As

Arsenic, As, Dissolved

Cadmium, Cd, Dissolved

Antimony, Sb

Lead, Pb, Dissolved

Thallium, Tl

Thallium, Tl, Dissolved

Cadmium, Cd

Antimony, Sb, Dissolved

Lead, Pb

Beryllium, Be, Dissolved

Beryllium, Be

TAL Metals List

TAL Metals-Dissolved

Silver, Ag

Silver, Ag, Dissolved

Cyanide, Total, CN

Nitrogen, Ammonia, N

Nitrogen, Total Kjeldahl, TKN

Nitrogen, Nitrate+ Nitrite (as N)

Bromide, Br

Chloride, Cl

Lab Number MAR00-22526 -Continued from Previous Page

Analysis Result Units Date Analyst WS#

10 (2.0)

12.1 (2.0)

ND (3.0)

ND (3.0)

7.4 (0.4)

ND (20)

8.06 (0.40)

ND (10)

ND (20)

47 (10)

ND (20)

6.2 (3.0)

4.8 (3.0)

ND (0.5)

ND (3.0)

ND (2.0)

ND (1.0)

ND (1.0)

ND (0.5)

ND (3.0)

21 (2.0)

ND (0.5)

0.6 (0.5)

()

()

MGIL

MGIL

UGIL

UGIL

MG/L

UG/L

MG/L

UG/L

UGIL

UG/L

UG/L

UGIL

UG/L

UG/L

UG/L

UGIL

UG/L

UG/L

UGIL

UG/L

UGIL

UGIL

UG/L

ND (10) UG/L

ND (10) UGIL

ND (0.005) MGIL

ND (0.05) MG/L

4.66 (2.00) MGIL

ND (0.05) MGIL

ND (0.5) MGIL

11 (5) MGIL

8130100

8/30/00

9/1/00

9/1/00

8/30/00

8/30/00

8/30/00

8/30/00

8130100

8/30/00

8/30/00

915100

915/00

915/00

915/00

915/00

9/5100

915/00

915/00

915100

915/00

9/5/00

9/5/00

8/30/00

8/30/00

9/6/00

917100

9/7100

9/8/00

9/5100

9/5/00

SMM

SMM

ROH

ROH

SMM

SMM

SMM

SMM

SMM

SMM

SMM

RCM

RCM

RCM

RCM

RCM

RCM

RCM

RCM

RCM

RCM

RCM

RCM

SMM

SMM

MDO

JEL

KVS

JEL

JEL

JEL

22416

22416

22455

22455

22416

22416

22416

22416

22416

22416

22416

22479

22479

22479

22479

22479

22479

22479

22479

22479

22479

22479

22479

0

0

22416

22416

22492

22505

22518

22530

22472

22472

Lab Number MAR00-22526:Page 2

PARAJITO @TWO MILE


Test Group

F

p

P04

S04-IC

ALK

TOC

U-MS

U-MS-D

TDS

TSS

SI-MS

SI-MS-D

SR-MS

\., ~-MS-D

LI-MS

LI-MS-D

B-MS

8-MS-D

MO-MS

MO-MS-D

C03

HC03

SN-GFAA

SN-GFAA-D


-CERTIFICATE OF ANALYSIS (REPRINT)-Lab Number MAR00-22526 -Continued from Previous Page

Analysis EPA Method Test Result Units Date Analyst WS#

SM 4500F-C Fluoride, F, Dissolved 0.19 (0.10) MG/L 8/31/00 JEL 22436 SM4500-P-E2 Phosphorus, P 1.58 (0.02) MG/L 9/1/00 RJA/BSR 22451

Calc. Phosphorus, P04 4.84 (.02) MGIL 0 300.0 Sulfate, S04 10 (5) MG/L 9/5100 JEL 22472

SM2320B Alkalinity, Total 152 (2) MGIL 8/31/00 TLC 22441 SM 531 OC/9060 Carbon, Total Organic, TOC 37 (0.7) MG/L 9/l/00 DLQ 22465

6020 Uranium, U ND (20.0) UGIL 915100 RCM 22479 6020 Uranium, U, Dissolved ND (20.0) UGIL 9/5100 RCM 22479 160.1 Residue, Total Dissolved 286 (20) MG/L 8/31/00 TLC 22444 160.2 Residue, Suspended (NonFilterable) 104 (5) MG/L 8/30/00 MDO 22415 200.8 Silicon, Si 24.1 (0.20) MGIL 915/00 RCM 22479

200.8/6020 Silicon, Si, Dissolved 12.5 (0.2) MG/L 915100 RCM 22479 200.8/6020 Strontium, Sr 290 (25) UGIL 9/5100 RCM 22479

6020 Strontium, Sr, Dissolved 240 (25) UGIL 9/5100 RCM 22479 6020 Lithium, Li ND (100) UGIL 9/5100 RCM 22479 6020 Lithium, Li, Dissolved ND (100) UG/L 9/5100 RCM 22479 6020 Boron, B 64 (50) UGIL 915100 RCM 22479 6020 Boron, B, Dissolved 80 (50) UGIL 9/5100 RCM 22479 200.8 Molybdenum, Mo ND (30) UGIL 915100 RCM 22479 200.8 Molybdenum, Mo, Dissolved ND (30) UGIL 915100 RCM 22479

SM2320B Alkalinity, Carbonate (as CaC03) ND (2) MGIL 0 SM2320B Alkalinity, Bicarbonate (as CaC03) 152 (2) MGIL 0

3113B/7871 Tin, Sn ND (50) UGIL 9/11/00 RCM 22548 31138/7871 Tin, Sn, Dissolved ND (50) UG/L 9/11/00 RCM 22548

Report Approved By: · ., '~. f).~~ This report shall not be reproduced, except in its entirety, without the written approval of the laboratory. ,}"

Lab Number MAR00-22526:Page 3

PARAJITO @TWO MILE



- CERTIFICATE OF ANALYSIS -

Client #: T0608

Attn:

Pinnacle Laboratories Inc

2709-D Panamerican PKWY NE

AJbuquerque,~ 87107-

Report Date: 18-0ct-00

Phone: (505) 344-3777 Ext:

FAX: (505) 344-4413

Your Sample ID: 008096-01 PARAllTO @TWO MILE

Sample Source: RCRA

Client Project #:

Our Lab#: MEL00-13166

Date Logged In: 8/30/00

Sample Type: Water

Project#: Date Submitted to Lab: 8/29/2000 PO#: 008096

EPA Method

8151

Analyst

DAW

-COLLECTION INFORMATION-

Date/Time/By: 8/24/00

Prep Date

8/30/00

Analysis Date

9/1/00

9:55AM

CAS Number

94-75-7

88-85-7

93-72-1

93-76-5

Analyst

Parameter Result Typical Report Limit

EPA Method

8260 MLS

CAS Number

67-64-1

107-05-1

71-43-2

75-27-4

75-25-2

74-83-9

75-15-0

56-23-5

108-90-7

75-00-3

67-66-3

74-87-3

126-99-8

124-48-1

2,4-Dichlorophenoxyacetic acid (2,4-D)

Dinoseb

Silvex

2,4,5-T

Prep Date

Parameter

Acetone

Allyl chloride

Analysis Date

9ntoo

Benzene

Bromodichloromethane

Bromoform

Bromomethane

Carbon disulfide

Carbon tetrachloride

Chlorobenzene

Chloroethane

Chloroform

Chloromethane

Chloroprene

Dibromochloromethane

< 10 ug/1

< 1.0 ug/1

<2.0 ug/1

<2.0 ug/1

10

I

2

2

Result Typical Report Limit

<20 ug/1 20

<20 ug/1 20

< 1.0 ug/1

<l.Oug/1

< 1.0 ug/1

< 1.0 ug/1

< 5.0 ug/1

< 1.0 ug/1

< 1.0 ug/1

< 1.0 ug/1

< 0.5 ug/1

< 1.0 ug/1

< 20 ug/1

< 1.0 ug/1

5

0.5

1

20

Your Sample ID: 008096-01 Lab Number MEL00-13166

6878 S. STATE ROUTE 100 • P.O. BOX 76 • MELMORE, OH 44845-9999 PHONE 419-397-2659 • 1-800-858-8869 • FAX 419-397-2229


- CERTIFICATE OF ANALYSIS -CAS Number Parameter

96-12-8 1 ,2-Dibromo-3-chloropropane

106-93-4 1,2-Dibromoethane (EDB)

74-95-3 Dibromomethane

110-57-6 Trans-1 ,4-Dichloro-2-Butene

75-71-8 Dichlorodifluoromethane

75-34-3 1, 1-Dichloroethane

107-06-2 1 ,2-Dichloroethane

75-35-4 1, 1-Dichloroethene

156-60-5 trans-1 ,2-Dichloroethene

78-87-5 1 ,2-Dichloropropane

10061-01-5 cis-1 ,3-Dichloropropene

10061-02-6 trans-1 ,3-Dichloropropene

123-91-1 1 ,4-Dioxane

100-41-4 Ethyl benzene

97-63-2 Ethylmethacrylate

591-78-6 2-Hexanone

126-98-7 Methacrylonitrile

75-09-2 Methylene chloride

78-93-3 Methyl ethyl ketone

74-88-4 Methyl Iodide

80-62-6 Methylmethacrylate

108-10-1 4-Methyl-2-pentanone (MIBK)

107-12-0 Propionitrile

100-42-5 Styrene

630-20-6 1, 1, 1 ,2-Tetrachloroethane

79-34-5 1, 1 ,2,2-Tetrachloroethane

127-18-4 Tetrachloroethene

108-88-3 Toluene

71-55-6 1, 1,1-Trichloroethane

79-00-5 1,1 ,2-Trichloroethane

79-01-6 Trichloroethene

75-69-4 Trichlorofluoromethane

96-18-4 1 ,2,3-Trichloropropane

108-05-4 Vinyl acetate

75-01-4 Vinyl chloride

Xylene, Total

Your Sample ID: 008096-01

Result Typical Report Limit

< 1.0 ug/1

< 1.0 ug/1

< 1.0 ug/1 1

< 10 ug/1 10

< 1.0 ug/1 1

< 0.5 ug/1 0.5

< 0.5 ug/1 0.5

< 0.5 ug/1 0.5

< 0.5 ug/1 0.5

< 1.0 ug/1 1

< 1.0 ug/1

<l.Oug/1

<20 ug/1 20

<l.Oug/1 1

< 10 ug/1 10

<20 ug/1 20

< 10 ug/1 10

< 1.0 ug/1 1

< 10 ug/1 10

< 10 ug/1 10

<20 ug/1 20

<20 ug/1 20

<20 ug/1 20

< 1.0 ug/1

< 1.0 ug/1

< 1.0 ug/1 1

< 1.0 ug/1 I

< 1.0 ug/1

< 1.0 ug/1

< 1.0 ug/1

< 0.5 ug/1 0.5

< 1.0 ug/1 I

< 1.0 ug/1

< 10 ug/1 10

< 1.0 ug/1

<2.0 ug/1 2

Lab Number MEL00-13166

PARAJITO @TWO MILE 6878 S. STATE ROUTE 100 • P.O. BOX 76 • MELMORE, OH 44845-9999

PHONE 419-397-2659 • 1-800-858-8869 • FAX 419-397-2229

>t.,.~,



EPA Method Analyst Prep Date Analysis Date

8270BNAc JSM 8/30/00 9/6/00

CAS Number Parameter Result Typical Report Limit

83-32-9 Acenaphthene < 10 ug/1 10

208-96-8 Acenaphthy1ene < 10 ug/1 10

98-86-2 Acetophenone < 10 ug/1 10

53-96-3 2-Acety1aminofluorene (2AAF) < 10 ug/1 10

92-67-1 4-Aminobiphenyl < 10 ug/1 10

62-53-3 Aniline < 10 ug/1 10

120-12-7 Anthracene < 10 ug/1 10

140-57-8 Aramite < 10 ug/1 10

56-55-3 Benzo( a )anthracene < 10 ug/1 10

50-32-8 Benzo( a )pyrene < 10 ug/1 10

205-99-2 Benzo(b )fluoranthene < 10 ug/1 10

191-24-2 Benzo(ghi )Perylene < 10 ug/1 10

207-08-9 Benzo(k)fluoranthene < 10 ug/1 10

100-51-6 Benzyl alcohol <20 ug/1 20

101-55-3 4-Bromophenyl phenyl ether < 10 ug/1 10

85-68-7 Butyl benzyl phthalate < 10 ug/1 10

106-47-8 4-Chloroaniline < 20 ug/1 20

510-15-6 Chlorobenzilate <10ugll 10

111-91-1 Bis(2-chloroethoxy)methane < 10 ug/1 10

111-44-4 Bis(2-chloroethyl)ether < 10 ug/1 10

108-60-1 Bis(2-chloroisopropyl)ether < 10 ug/1 10

59-50-7 4-Chloro-3-methylphenol <20 ug/1 20

91-58-7 2-Chloronaphthalene <10ugll 10

95-57-8 2-Chlorophenol < 10 ug/1 10

7005-72-3 4-Chlorophenyl phenyl ether < 10 ug/1 10

218-01-9 Chrysene < 10 ug/1 10

2303-16-4 Diallate < 10 ug/1 10

53-70-3 Dibenzo( a,h)anthracene < 10 ug/1 10

132-64-9 Dibenzofuran < 10 ug/1 10

84-74-2 Di-n-butyl phthalate < 10 ug/1 10

95-50-1 1 ).-Dichlorobenzene < 10 ug/1 10

541-73-1 1 ,3-Dichlorobenzene < 10 ug/1 10

106-46-7 1 ,4-Dichlorobenzene < 10 ug/1 10

91-94-1 3,3'-Dichlorobenzidine <20 ug/1 20

120-83-2 2,4-Dichlorophenol < 10 ug/1 10



PARAJITO @TWOMILE

"""····· Aqua Tech Environmental Laboratories, Inc.


CAS Number Parameter Result Typical Report Limit

87-65-0 2,6-Dichlorophenol < 10 ug/1 10

84-66-2 Diethyl phthalate < 10 ug/1 10

60-51-5 Dimethoate < 10 ug/1 10

60-11-7 p-(Dimethylamino )azobenzene < 10 ug/1 10

57-97-6 7, 12-Dimethylbenz( a )anthracene < 10 ug/1 10

119-93-7 3 ,3'-Dimethylbenzidine < 10 ug/1 10

122-09-8 a,a-Dimethylphenethylamine < 10 ug/1 10

105-67-9 2,4,-Dimethylphenol < 10 ug/1 10

131-11-3 Dimethyl phthalate < 10 ug/1 10

99-65-0 1 ,3-Dinitrobenzene(DNB) < 10 ug/1 10

534-52-1 4,6-Dinitro-o-Creso1 <50 ug/1 50

51-28-5 2,4,-Dinitrophenol <50 ug/1 50

121-14-2 2,4-Dinitrotoluene < 10 ug/1 10

606-20-2 2,6-Dinitrotoluene < 10 ug/1 10

117-84-0 Di-n-octylphthalate < 10 ug/1 10

122-39-4 Diphenylamine < 10 ug/1 10

\. ... 298-04-4 Disu1foton < 10 ug/1 10

117-81-7 Bis(2-ethylhexyl)phthalate < 10 ug/1 10

62-50-0 Ethyl methanesulfonate < 10 ug/1 10

52-85-7 Famphur < 10 ug/1 10

206-44-0 Fluoranthene < 10 ug/1 10

86-73-7 Fluorene < 10 ug/1 10

118-74-1 IIexachlorobenzene < 10 ug/1 10

87-68-3 IIexachlorobutadiene < 10 ug/1 10

77-47-4 IIexachlorocyclopentadiene < 10 ug/1 10

67-72-1 IIexachloroethane < 10 ug/1 10

70-30-4 IIexachlorophene < 10 ug/1 10

1888-71-7 IIexachloropropene < 10 ug/1 10

193-39-5 Indeno( 1 ,2,3-cd)pyrene < 10 ug/1 10

465-73-6 Isodrin < 10 ug/1 10

78-59-1 Isophorone < 10 ug/1 10

120-58-1 lsosafrole < 10 ug/1 10

143-50-0 Kepone < 10 ug/1 10

91-80-5 Methapyrilene < 10 ug/1 10

56-49-5 3-Methy1cholanthrene < 10 ug/1 10

66-27-3 Methyl methanesulfonate < 10 ug/1 10

91-57-6 2-Methylnaphthalene < 10 ug/1 10

298-00-0 Methyl parathion < 10 ug/1 10

Your Sample ID: 008096-01 Lab Number MELOO-13166

PARAJITO @TWOMILE 6878 S. STATE ROUTE 100 • P.O. BOX 76 • MELMORE, OH 44845-9999

PHONE 419-397-2659 • 1-800-858-8869 • FAX 419-397-2229

. ,.,_, Aqua Tech Environmental Laboratories, Inc .

- CERTIFICATE OF ANALYSIS -CAS Number Parameter Result Typical Report Limit

95-48-7 2-Methylphenol < 10 ug/1 10

108-39-4 3-Methylphenol < 10 ug/1 10

106-44-5 4-Methylphenol < 10 ug/1 10

91-20-3 Naphthalene < 10 ug/1 10

130-15-4 I A-Naphthoquinone < 10 ug/1 10

134-32-7 1-Naphthylamine < 10 ug/1 10

91-59-8 2-Naphthylamine < 10 ug/1 10

88-74-4 2-Nitroaniline < 10 ug/1 10

99-09-2 3-Nitroaniline < 10 ug/1 10

100-01-6 4-Nitroaniline < 10 ug/1 10

98-95-3 Nitrobenzene < 10 ug/1 10

88-75-5 2-Nitropheno1 < 10 ug/1 10

100-02-7 4-Nitrophenol < 10 ug/1 10

56-57-5 4-Nitroquino1ine-1-oxide < 10 ug/1 10

924-16-3 N-Nitrosodi-n-butylamine < 10 ugll 10

55-18-5 N-Nitrosodiethylamine < 10 ug/1 10

62-75-9 N-Nitrosodimethylamine < 10 ug/1 10

86-30-6 N-Nitrosodiphenylamine < 10 ug/1 10

621-64-7 N-Nitrosodi-n-propylamine < 10 ug/1 10

10595-95-6 N-Nitrosomethylethylamine < 10 ug/1 10

59-89-2 N-Nitrosomorpholine < 10 ug/1 10

100-75-4 N-Nitrosopiperidine < 10 ug/1 10

930-55-2 N-Nitrosopyrrolidine < 10 ug/1 10

99-55-8 5-Nitro-o-toluidine < 10 ug/1 10

56-38-2 Parathion (Ethyl) < 10 ug/1 10

608-93-5 Pentachlorobenzene < 10 ug/1 10

76-01-7 Pentachloroethane < 10 ug/1 10

82-68-8 Pentachloronitrobenzene < 10 ug/1 10

87-86-5 Pentachlorophenol <50 ug/1 50

62-44-2 Phenacetin < 10 ug/1 10

85-01-8 Phenanthrene < 10 ug/1 10

108-95-2 Phenol < 10 ug/1 10

106-50-3 p-Phenylenediamine < 10 ug/1 10

298-02-2 Phorate < 10 ug/1 10

109-06-8 2-Picoline < 10 ug/1 10

23950-58-5 Pronamide < 10 ug/1 10

129-00-0 Pyrene < 10 ug/1 10

110-86-1 Pyridine < 10 ugll 10


PARAJITO @TWO MILE 6878 S. STATE ROUTE 100 • P.O. BOX 76 • MELMORE, OH 44845-9999

PHONE 419-397-2659 • 1-800-858-8869 • FAX 419-397-2229

QCLab#

MEL00-13166

MEL00-13166

MEL00-13166

MEL00-13166

MEL00-13166

MEL00-13166

MEL00-13166

MEL00-13166

MEL00-13166

MEL00-13166

ATEL


- CERTIFICATE OF ANALYSIS -CAS Number Parameter Result Typical Report Limit

94-59-7 Safrole < 10 ug/1 10

3689-24-5 Sulfotepp < 10 ug/1 10

95-94-3 1,2,4,5-Tetrachlorobenzene < 10 ug/1 10

58-90-2 2,3,4,6-Tetrachlorophenol < 10 ug/1 10

297-97-2 Thionazin < 10 ug/1 10

95-53-4 o-Toluidine < 10 ug/1 10

120-82-1 1 ,2,4-Trichlorobenzene < 10 ug/1 10

95-95-4 2,4 ,5-Trichloropheno1 < 10 ug/1 10

88-06-2 2,4,6-Trichlorophenol < 10 ug/1 10

126-68-1 0,0,0-Triethyl phosphorothioate < 10 ug/1 10

99-35-4 1 ,3,5-Trinitrobenzene(1NB) < 10 ug/1 10

--- Surrogate Recoveries ---Lower Upper

EPA Method Surrogate Name Percent Recovery Limit Limit

8151 DCAA(Surr) 70 %R 19 146

8260 Bromofluorobenzene (BFB) (Surr) 110 %R 86 115

8260 Dibromofluoromethane (Surr) 105 %R 86 118

8260 Toluene-d8 (Surr) 109 %R 88 110

8270BNAc 2,4,6-Tribromophenol (Surr) 43 %R 10 123

8270BNAc 2-Fluorobiphenyl (Surr) 61 %R 43 116

8270BNAc 2-Fluorophenol (Surr) 27 %R 21 100

8270BNAc dl4-Terphenyl (Surr) 37 %R 33 141

8270BNAc d5-Nitrobenzene (Surr) 86 %R 35 114

8270BNAc d6-Phenol (Surr) 24 %R 10 94

End of Report

Report Approved By: LUM! '( 'ue~ Wade T. DeLong

This report shall not be reprodllced, except in its entirety, without the wriJten approval of the laboratory.


PARAJITO @TWO MILE


"'de FOR METHODS 8270/625 ~ WATER

ATEL SAMPLE# -13166 PARAJITO @TWO MILE

QC SAMPLE# 13151 13151 13151 QC SAMPLE DATE 9/6/00 9/6/00 9/6/00

LFB LFM BLK %DIEF QC LIMITS BASE-NEUTRAL COMPOUNDS

1 ,2,4-TRICHLOROBENZENE 60.5 60.2 39-98 ACENAPHTHENE 86.2 78.4 46-118 2,4-DINITROTOLUENE 83.7 81.6 24-96 PYRENE 76.8 75.2 26-127 N-NITROSO-di-n-PROPYLAMINE 88.1 85.2 41-116 1 ,4-DICHLOROBENZENE 67.0 67.5 36-97 NITROBENZENE 80.2 77.8 32-105 HEXACHLOROBENZENE 85.6 79.0 31-98 CHRYSENE 75.0 68.0 40-110 BENZO(A)PYRENE 60.7 60.9 38-102 PHENANTHRENE 81.8 77.6 29-95 HEXACHLOROETHANE 70.0 69.3 38-112

ACID COMPOUNDS

2,4-DIMETHYLPHENOL 2.6 * 20.5 * 23-93 PHENOL 32.3 13.1 12.0-89.0 2-CHLOROPHENOL 48.2 24.8 * 27-123 4-CHLOR0-3-METHYLPHENOL 59.4 36.0 23-97 4-NITROPHENOL 33.6 25.0 14-85

BASE-NEUTRAL SURROGATES

d5- NITROBENZENE 88 88 99 35-114 2-FLUOROBIPHENYL 78 83 82 43-116 d14- TERPHENYL 83 83 87 33-141

ACID SURROGATES

2-FLUOROPHENOL 30 23 10 * 21-100 d6-PHENOL 37 19 27 10.0-94.0 2,4,6-TRIBROMOPHENOL 28 40 9* 10-123

COMPOUNDS

Method 8151

Dalapon-Me Dicamba-Me MCPP-Me MCPA-Me Dichlorprop-~ 2,4-D-Me 2, 4,5TP-Me(Silvex) 2,4,5-T-Me 2,4-DB-Me Dinoseb-Me

Surrogate data

DCAA


BATCH QUALITY CONTROL SJUVUPLE(S):~L00-13166 PARAJITO @TWO MILE

DATE ANALYZED: 09/01/00

LRB

Jlg/L

< 1.00 <0.20 < 10.0 < 10.0 <0.20 <0.10 <0.20 <0.20 <0.10 <0.05

%Recovery

(19-146) 70

LFB LFB o/oRecovery Limits

64 35-122 53 52-145 47 44-149 49 43-133 53 52-128 58 44-134 53 55-138 56 54-142 70 37-159 5 0-126

52 19-146

LFM LFM %Rec. Limits

130 35-122 114 52-145 90 44-149 90 43-133

104 52-128 120 44-134 105 55-138 123 54-142 147 37-159 22 0-126

124

LRB= Laboratory Reagent Blank LFB=Laboratory Fortified Blank LFM=Laboratory Fortified Matrix

6878 S STATE ROUTE 100 • P.O. BOX 76 • MELMORE, OH 44845-9999 PHONE 419-397-2659 • 1-800-858-8869 • FAX 419-397-2229

~~ntitation Report

:a File I Time nple

D:\DX.B\DX130.D "''

3C l" : m~"·"'·ime:

:hod :le ;t Update ;ponse via

7 Sep 100 7:54 am LAB BLANK

Sep 7 8:18 19100

C:\HPCHEM\1\METHODS\8260W33.M 8260 WATERS Tue Sep 05 13:58:18 2000 Multiple Level Calibration

Operator: SLC-MLS Inst JIMBO Multiplr: 1.00

1ternal Standards R.T. Qion Response Cone Units Dev(Min) --------------------------------------------------------------------------) Pentafluorobenzene 6.66 168 1940694 10.00 ug/L 0.00 D 1,4-Difluorobenzene 7.59 114 2253592 10.00 ug/L 0.00 I) Chlorobenzene-d5 11.81 117 1488221 10.00 ug/L 0.00 i) 1,4-Dichlorobenzene-d4 15.76 152 693469 10.00 ug/L 0.00

rstem Monitoring Compounds %Recovery ~ ) DBFM 6.66 111 1117128 10.08 ug/L 100.82% I) BFB 13.75 95 1235091 1.0.69 ug/L 106.90% ) ) TOL-d8 9.61 98 1868913 10.83 ug/L 108.34%

Lrget Compounds Qvalue ~ ) acetone 4.29 43 24879 10.05 ug/L # 85 ) ) trans-1,4-dichloro-2-buten 13.75 88 40575 2.23 ug/L # 38 ) ) naphthalene 19.82 128 1366 0.73 ug/L 100

:) (_:}Ualifier out of range (m) = manual integration :13CI.D 8260W33.M Mon Oct 23 12:24:39 2000 JSM

PARAJITO @TWO MILE

,,~ pi~

Pirt·-~le Laboratories, Inc. lnte~b( '~ain of Custody "''" ~ /z8' ••• .,_1 of r ' ~~J:S Network Project Manager: Jacinta A. Tenorio I .. • :~: •• ·• .: .·.:•:.·.•.:··.··· ••· ANALYSIS REQUEST . - i

Pinnacle Laborator1es, Inc. ·,V'I

~ $ ~ V2 ~ F ~~ tu. I~ I~ r.) 2709-D Pan American Freeway, NE - I~ - ~

~~ 0

~ ~ ~ '0 ~ -Albuquerque, New Mexico 87107 ~ ~ N ro (1(1

'~ (1(1 ~ 0

~ ::l it505) 344-3777 Fax (505) 344-4413

~ I~ IdS - !~ ~ - c5 Cf) . -' en ).-1 (1(1 w ...J

-~ ::::E

J 0 - J: ~ ~

(/) ~ 1 ~ {3 ~ ....

N (i) ffi ~ I() -~ w

~ (9 co .... -attn: please invoice account T0608 and_ ~ ::E l) (1(1 .... '.;r\ ::::E (1(1 .s z ~ ~ I~ I~ ~ i?> .... I N

~ E ~ a. ("')

I~ a. N Q) PINNACLE requires the following QC for all l) w a. ·c: l.;f Ci5 .... .... !R g +

~ ::E ..\- I~ ('0 !£. <0 8 a::: a. -1

~ .!Cl ~ E' w - a. (5: N studies: BLANK, SPIKE & DUPLICATE. - a.

("') ~ ~ E Cl ~ 0 -1 ::;;: N .c u. ...J 0 \)(: ....

i~ c. e (.) .... 11 ~ ~ Q) 2 (3 "0 ("') l) ::::> ::::E <( 0 I- ~ ~ .c Q) (1(1 c -~

ffi Thank you .sa l)

~ ~

I i= :Q -

~ zN z ::::> (/) "<t .s ~ (IJ .s

w ' II c: C'iJ Cl Cf) .c

~ 0

]~ ~ i5 (/) .... CXl -Q) Q) Q) 0 0 .... "<t 0 I ::E (.) Q) w Q)

~ 0 SAMPLE ID DATE TIME MATRIX LABID :?: :?: ::?: (9 N (!) :l 0::: > co a. J: a. (1(1 ::::> 1- z

I

oog()qfo- o1 &124 ICJ165 AQ /'> X I>< I>< >< lX I>< >< >( IX X >< >< !x 1-Bit:: ~ I :> .• I'

!.:/.:-I>· h L , / !>•: ;.:··:·.: ~-: :-! i•. ::: ! ................

i· > >. : --

-

PROJECT INFORMATION .. : ·SAMPLE.RECEIPT· ·. .SAMPLES SENT TO: 1. RELINQUISED BY: 2. PROJECT#: Total Number of Containers PEN.SACOLA - STL-FL Signatue: Time: Chain of Custod Seals ESL- OR Received Intact? STL-CT

Printed Name• Date• BLANK Received Good Cond./Cold ATEL-AZ

ATEL- MARION Company A TEL - MELMORE 1. RECEIVED BY: 2

MMENT/.\5 ~ cJ lJr c BARRINGER Signatue: Time: ' ,'Sq. ' ' ' o,CJA WCAS CLIENT DISCOUNT: ~\,, Htt, N i 1 Se, ~ , 1\, ~ WOHL Printed Name: Date: SPECIAL CERTIFICATION REQUIRED: YES N v, lV\ 3°

Company

Enviro-Test Laboratories LLC.

Chemical Analysis Report

PINNACLE LABORATORIES, INC

Attn: PROJECT MANAGER

2709D PAN AMERICAN FREEWAY NE

ALBUQUERQUE NM 87107

Lab Work Order #: L 1826

Project P.O.#: PARAJITO @ TWO MILE

Project Reference:

Comments:

APPROVED BY: Dave Demorest

Project Manager

Enviro • Test

Date: 1 0 OCT 2000

Date Received: 29 AUG 2000

LABORATORIES LLC. 420 West Street Casper, Wyoming 8260"

Limit of Liability: Although care and due diligence is taken in the performance of our services, our liability in all cases is limited to re-analysis at our expense or refunding the analytical costs charged for the work performed.

Phone: (307) 235-5741 Fax:(307) 266-1676 Toll Free 1 (800)666-03()(

'-'chemical Analysis Report

weiNNACLE LABORATORIES, INC '090 PAN AMERICAN FREEWAY NE LBUQUERQUE NM 87107 ATTN: PROJECT MANAGER

Report Date: 1 0-0CT-00 Page: 2 of 4

PO No.: WO NO.: L1826

Sample 10: NMHWB-008096-01 PARAJITO @TWO MILE Date Collected: Job Name:

·. !?~mP1~~~x= ...

Mise

Strontium-90

Isotopic Uranium 2331415/6/8

Uranium-23314 Uranium-235/6

Uranium-238

Isotopic Thorium 227/8/30/2

Thorium-228 Thorium-230 Thorium-232

Isotopic Plutonium 238/9/40

Plutonium-238 Plutonium-239/40

r l~otopic Americium and Curium

~ . Americium-241 ~· Curium-243/244

Gross Alpha/Beta

Gross Alpha Gross Beta

Gamma Spectroscopy

Actinium-228 Silver-110m Americium-241 Beryllium-7

Bismuth-212 Bismuth-214 Cerium-139

Cerium-144

Cobalt-56 Cobalt-57 Cobalt-58 Cobalt-60 Chromium-51 Cesium-134 Cesium-137

Europium-152 Europium-154 Europium-155 Iron-59

Enviro • Test LABORATORIES LLC.

420 West Street Casper. Wyoming 8260" Phone: (307) 235-5741 Fax:(307) 266-1676

Toll Free 1 (800)666-030€

Lab Sample 10:

3.6+/- 0.7 pCVL 1.4 06-SEP-00 KLS

1.32 +1- 0.55 pCVL 0.14 14-SEP-00 OMF <0.18 +1- 0.13 pCVL 0.18 14-SEP-00 OMF 1 .08 +1- 0.50 pCVL 0.31 14-SEP-00 OMF

0.8 +1- 0.5 pCVL 0.5 15-SEP-00 OMF 3 +/- 1.0 pCVL 0.3 15-SEP-00 OMF

<0.4 +1- 0.3 pCVL 0.4 15-SEP-00 OMF

<0.04 +1- 0.05 pCVL 0.04 20-SEP-00 PLJ 0.05 +1- 0.04 pCVL 0.05 20-SEP-00 PLJ

1.5 +1- 0.7 pCVL 0.4 22-SEP-00 OF <0.3 +1- 0.1 pCVL 0.3 22-SEP-00 OF

15.7+/- 4.2 pCVL 2.1 12-SEP-00 KLS 37.0+/- 2.9 pCi/L 2.5 12-SEP-00 KLS

20.2 +1- 14.5 pCVL 24.7 01-SEP-00 OMF -60.2 +1- 82.5 pCVL 136 01-SEP-00 OMF 12.2 +/- 8.6 pCVL 12.7 01-SEP-00 OMF i

I 4.3 +1- 33.2 pCVL 55.6 01-SEP-00 OMF: 14.9 +1- 54.6 pCVL 90.8 01-SEP-00 I OMF 81.0 +1- 14.9 pCVL 12.9 01-SEP-00 OMF -2.0 +1- 3.2 pCVL 5.2 01-SEP-00 OMF

-22.8 +1- 22.2 pCVL 33.9 01-SEP-00 OMF -0.5 +1- 4.4 pCVL 7.2 01-SEP-00 OMF -3.2 +1- 2.7 pCVL 4.3 01-SEP-00 OMF 1.0 +1- 4.0 pCVL 6.7 01-SEP-00 OMF

37.3 +1- 5.8 pCVL 6.9 01-SEP-00 OMF -40.1 +1- 36.3 pCVL 57.3 01-SEP-00 OMF

-1.6 +1- 4.4 pCVL 6.2 01-SEP-00 OMF -1.7 +1- 4.2 pCVL 6.8 01-SEP-00 OMF 3.4 +1- 19.7 pCVL 33.1 OMF -2.3 +1- 5.5 pCVL 9 OMF 15.8 +1- 7.4 pCVL 10.9 OMF 3.2 +1- 8.5 pCVL 14 OMF

Limit of Liability: Although care and due diligence is taken in the performance of our services. our liability in all cases is limited to re-analysis at our expense or refunding the analytical costs charged for the work performed.

~Chemical Analysis Report

" .qJNNACLE LABORATORIES, INC l._·ogo PAN AMERICAN FREEWAY NE ALBUQUERQUE NM 87107

ATTN: PROJECT MANAGER

Report Date: 1 0-0CT-00 Page: 3 of 4

PO No.: WO NO.: L 1826

NMHWB-008096-01 PARAJITO @ TWO MILE 24-AUG-00 L1826-1

Mise

Gamma Spectroscopy

""'·

lodine-131 Potassium-40 Manganese-54 Sodium-22 Niobium-94 Niobium-95 Protactinium-234m Lead-212 Lead-214 Ruthenium-1 06 Antimony-124 Antimony-125 Scandium-46 Strontium-85 Thorium-227 Thorium-234 Thallium-208 Uranium-235 Zinc-65

ElL : Enviro • Test LABORATORIES LLC.

420 West Street Casper, Wyoming 826o· Phone: (307) 235·5741 Fax:(307) 266·1676

Toll Free 1 (800)666·030{

-1.4+/-7.6 pCi/L 12.2 01-SEP-00 I DMF 958 +1- 94.2 pCi/L 58.5 01-SEP-00 DMF 0.3 +1- 4.2 pCi/L 6.9 01-SEP-00 DMF 0.6 +1- 4.4 pCi!L 7.1 01-SEP-00 DMF -1.6 +1- 4.0 pCi/L 6.5 01-SEP-00 DMF 4.5 +1- 4.5 pCi/L 7.6 01-SEP-00 DMF

858 +1- 650 pCi!L 1110 01-SEP-00 DMF, 32.6 +1- 8.6 pCi/L 10.4 01-SEP-00 DMF

41.7 +1-10.5 pCi!L 12.7 01-SEP-00 DMF 301 +1- 36.6 pCi/L 26.2 01-SEP-00 DMF -0.1 +1- 6.5 pCi!L 6.8 01-SEP-00 DMF 0.1 +1- 10.0 pCi/L 16.7 01-SEP-00 DMF 6.8 +1- 5.2 pCi/L 8.8 01-SEP-00 DMF

33.7 +1- 4.6 pCi/L 7.9 01-SEP-00 DMF 51.3 +1- 29.2 pCi!L 42.4 01-SEP-00 DMF 247 +1- 87.4 pCi/L 66.8 01-SEP-00 DMF 23.6 +1- 6.8 pCi!L 6.3 01-SEP-00 DMF 1

22.0 +1-7.8 pCi/L 37.1 01-SEP-00 DMF -7.2 +1- 9.6 pCi!L DMF


""-ETL Test Code

AM·CM-CA

GAMMA-ALL-CA

GROSSAB-CA

150-PU-ALPHA-CA

150-TH-ALPHA-CA

ISO-U-CA

SR90-CA

Matrix

Water

Water

Water

Water

Water

Water

Water

WONO.: L1826

Methodology Reference PAGE 4 of 4

PARAJITO @ TWO MILE

Test Description Methodology Reference

Isotopic Americium and Curium mod. HASL 300

Gamma Spectroscopy Mod.EPA.901.1

Gross Alpha/Beta Mod.EPA.900.0

Isotopic Plutonium 238/9/40 Mod.HASL 300

Isotopic Thorium 227/8/30/2 Mod.HASL 300

Isotopic Uranium 233/4/5/6/8 Mod.HASL 300

Strontium-90 Mod.EPA.905.0

Enviro • Test LABORATORIES LLC. Limit of Liability: Although care and due diligence is taken in the performance of our services, our liability in all cases is

limited to re-analysis at our expense or refunding the analytical costs charged for the work performed.

QA

LC1PU0925

L1826-001

Sample Activity

0.051

L 1815-001 Sample Activity -0.047

0.016

MBAPU0831 PU239

WORKGROUP#

RUN ID#

Standard Known Value 0.625

Spiked Sample Activity 1.048

PU238 Duplicate Activity 0.029

PU239 0.017

= -0.0104 = 0.008595

W&- 71:1-0

f( 571/

ISO-PU

LCS Sample Value 0.590

Standard Value 0.625

Sample ERROR 0.062

0.019

WORK ORDER # ___ L_18._1~5--

L1826

PARAJITO @ lWO MILE

10/2/2000 pCi/L

17:17:00

LCS Recovery

94.3%

Sample Spike SPIKE Volume Value RECOVERY 0.500 1.25 79.8%

Duplicate Duplicate ERROR RER 0.079 0.76

0.034 0.02

ElL Enviro • Test . LABORATORIES LLC. Limit of Liability: Although care and due diligence is taken in the performance of our services, our liability in all cases is

lim~ed to re-analysis at our expense or refunding the analytical costs charged for the work performed.

'*'""ENVIRO-TEST QC REPORT Page of 4

Workorder #: L1826 PARAJITO @ TWO MILE

<(:, ype: BLANK

Lab QC Number:

WG7031-2

SR90-CA

WG7063-3

GROSSAB-CA

WG7063-4

GROSSAB-CA

WG7120-2

ISO-PU-ALPHA-CA

WG7121-3

I SO-TH-ALPHA-CA

WG7131-3

ISO-U-CA

~09-1 AM-CM-CA

QCType: DUP

Lab QC Number: WG7120-1

ISO-PU-DIS-CA

WG7121-1

ISO-TH-DIS-CA

WG7131-1

ISO-U-DIS-CA

WG7209-2

ISO-AM-DIS-CA

Strontium-90





Uranium-233/4 Uranium-235/6 Uranium-238

Americium-241 Curium-243/244

Plutonium-238

Plutonium-239/40

Thorium-228

Thorium-230

Thorium-232

Uranium-235

Uranium-238

Americium-241

ElL Enviro • Test LABORATORIES LLC.

Result Qualifier Units Limit Analyzed

<0.9+1- 0.4 pCi/L 0.9 06-SEP-00

<0.5+1- 0.3 pCi/L 0.5 12-SEP-00 3+1- 0.9 pCi/L 1.4 12-SEP-00

<0.6+1- 0.3 pCi/L 0.6 12-SEP-00 <2+/- 0.9 pCi/L 1.5 12-SEP-00

<0.03 +1- 0. pCi/L 0.03 20-SEP-00 <0.03 +1- 0. pCi/L 0.03 20-SEP-00

<0.1 +1- 0.1 pCi/L 0.1 15-SEP-00 0.2 +1- 0.1 pCi/L 0.1 15-SEP-00 <0.1 +1- 0.1 pCi/L 0.1 15-SEP-00

<0.050 +1- ( pCi/L 0.05 14-SEP-00 <0.050 +1- ( pCi/L 0.05 14-SEP-00 <0.020 +1- ( pCi/L 0.02 14-SEP-00

0.3 +1- 0.1 pCi/L 0.1 22-SEP-00 <0.1 +1- 0.1 pCi/L 0.1 22-SEP-00

RPD Qualifier Limit% Analyzed

N/A RPD-NA 0-20 20-SEP-00 0 0-20 20-SEP-00

N/A RPD-NA 0-20 15-SEP-00 9.5 RPD-NA 0-20 15-SEP-00 N/A RPD-NA 0-20 15-SEP-00

N/A RPD-NA 0-20 14-SEP-00 48 RPD-NA 0-20 14-SEP-00

30 0-20 22-SEP-00


··~NVIRO-TEST QC REPORT", .. , Page 2 of 4


Curium-243/244

QC Type: LCS

Lab QC Number:

WG7031-4 SR90-CA Strontium-90

WG7063-6 GROSSAB-CA Gross Alpha

Gross Beta


Gross Beta

WG7120-4 ISO-PU-ALPHA-CA Plutonium-239/40

~7121-4 ,.)-TH-ALPHA-CA Thorium-230

WG7131-4 ISO-U-CA Uranium-238

WG7209-4 AM-CM-CA Americium-241

QCType: MS

Lab QC Number:

WG7031-3 SR90-CA Strontium-90


Gross Beta

WG7120-3

ISO-PU-ALPHA-CA Plutonium-239/40

WG7121-2 ISO-TH-ALPHA-CA Thorium-230

WG7131-2

ElL . Enviro • Test LABORATORIES LLC.

67 RPD-NA 0-20 22-SEP-00

% Recovery Qualifier Limit% Analyzed

110 75-125 06-SEP-00

81 75-125 12-SEP-00 N/A 75-125 12-SEP-00

N/A 75-125 12-SEP-00 122 75-125 12-SEP-00

94.3 75-125 20-SEP-00

91 75-175 15-SEP-00

107 75-125 14-SEP-00

102 75-125 22-SEP-00


104 75-125 06-SEP-00

N/A 70-125 12-SEP-00 112 70-125 12-SEP-00

79.8 75-125 20-SEP-00

96 75-125 15-SEP-00


ISO-U-CA

WG7209-5 AM-CM-CA

.,ENVIRO-TEST QC REPORT#''*'\ Page 3 of 4


Uranium-238 94 75-125 14-SEP-00

Americium-241 95 75-125 22-SEP-00

Enviro • Test LABORATORIES LLC. Limit of liability: Although care and due diligence is taken in the performance of our services, our liability in all cases is


~~gend:

Qualifier:

RPD-NA A B

D E F G

QCType

BLANK

BS

BSD

CCB

CCC

CCV

DUP

ICB

rev INST BLK

LCS

LCSD

MS

MSD

SPCC

SRM

sss

~NVIRO-TEST QC REPORT Workorder #:

Description

Laboratory Blank

Blank Spike

Blank Spike Duplicate

Continuing Calibration Blank

Continuing Calibration Check

Cont. Cal. Verification

Duplicate

Instrument Blank

L1826

lnstument Calibration Verification

Instrument Blank

Laboratory Control Spike

Lab Control Spike Duplicate

Matrix Spike

Matrix Spike Duplicate

System Performance Check Compound

Standard Reference Material

Second source std

Relative Percent Difference Not Available due to result(s) being less than detection limit. Method blank exceeds detection limit. Blank correction applied, where appropriate. Method blank result exceeds detection limit, however, it is less that 5% of sample concentration. Blank correction not applied.

Page 4 of 4

PARAJITO @ TWO MILE

Method blank result exceeds detection limit, however, it is less than 5% of the regulatory limit for the analyte of interest. Blank correction not applied. Duplicate result exceeds limit due to increased variability for low level samples. Matrix spike limit exceeded due to high sample background. Silver recovery low, likely due to elevated choride levels in sample. Outlier - No assignable cause for nonconformity has been determined.

Enviro • Test LABORATORIES LLC. Limit of Liability: Although care and due diligence is taken in the performance of our services. our liability in all cases is


Job Number

Samples ShippeJ GlPSJ Federal Express Other: ~

Samples I lauJ Dclivcrccl Client ETL Lab Courier 01hcr:

Air Dill il: II of Packngcs Received: I ..

Yes No N\A Commct1ts I. Chain- of- Custody present? ,/ lf no, please fill one out. 2. Arc the COC ancl sample labels legible? ~ ., CustoJy Seal on shipping coutaincr'/ ............ J.

If yes, intact on shipping container? /

4. Custody seals on sample containers? .......

l [yes, i 11 tact 011 sam pic con lainer? /

5. Samples chilled? i./

Is temperature of cooler: 4 ± 2°C? / c/ A1'/f''"" Record lc.mp: rrmv tJ!.. '1. (, "C G. Samples received intact (good eoiH..liLion)7 L../"""

~ If volatiles required, any with hcadspaec7 ,__..,.-'

7. Adequate snmplc Yolumc provided? / t.---·

S. Samples preserved correctly? ...,__-· Na2S203, Zn.Ac,@6_91 JCI Circle presen·ative types in shipmcnl .l-bS04, NaOH, Other

9. Correct containers used? v 10. Samples received within holding time? v II. Agrcclllclll bctwccu COC ami ~illnplc labels?

..._/

12. Gam111a Sc1 ccu miVI·Ir@ sur f;1cc within Ul:g? ./

lZeccived anJ inspected by: -~(..:L(___=------

QO West Firs! Street Casper, Wyoming 82601 Phone: (307) 235·5741 Fo,;: (307) 2G6·1676

Lab Client SMP# Sample Number L 1815-1 NMHWB

Water s GAB-DIS-CA

Water s GAMMA-ALL-DIS-CA

Water s ISO-AM-DIS-CA

Water s ISO-PU-DIS-CA

Water s ISO-TH-DIS-CA

Water s ISO-U-DIS-CA

Water s SR90-DIS-CA

ENVIRO-TEST LABORATORIES LLC.

Login Chain of Custody Report (ln01) Aug. 31, 2000

12:03 PM

Logip Number: L 1815 Quote Number: Account: 10185 PINNACLE LABORATORIES, INC

Project: PARAJITO @ TWO MILE

Collect Receive Due Date Date PR Date Comments

24-AUG-00 09:55 29-AUG-00 18-SEP-00

Hold: 20-FEB-01

Hold: 20-FEB-01

Hold: 20-FEB-01

Hold: 20-FEB-01

Hold: 20-FEB-01

Hold: 20-FEB-01

Hold: 20-FEB-01

Signature: c2~ qo t~ Date : 8- 31- oo

of 1

tt Pif~ 'eCie Laboratories, Inc. ~ lnterlatt~ '\lain of Custody D-. ';5 ~ 2.8 poge,_J_ ot]~ ~ .... ~etwork Project Manager: Jacinta A. Tenorio --~ ANALYSIS REQUI;S1" Pinnacle Laboratories, Inc. lc ~~ I~

. I Vl 2709-D Pan American Freeway, NE ~ ~ i -~ - (/)

fS 0 U) - ~

Albuquerque, New Mexico 87107 ~ I~ ~ N N

i co co 0 ~· cf ::s: - 0 C) !(5a2l344-3777 Fax (505) 344-4413 -

r~ ~ (/) ~ \}-

~ ~ (/)

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sAMP.LE RECEfPT .SAMPLES SENT TO: 1~ RELINQUISED BY: .· 2, PROJECT#: Total Number of Containers PENSACOLA - STL-FL Signatue: Time: Chain of Custo Seals ESL- OR

STL-CT Date:

ATEL-AZ

Company

1. RECEIVED BY: 2 DUE DATE: Signatue: Time: -Printed Name: Date: SPECIAL CERTI~N

REQUIRED: YE N --- ---- -·- --· -· ---- -----· -- -- ----- ----~- Company I

Enviro-Test Laboratories LLC. Chemical Analysis Report

PINNACLE LABORATORIES, INC

Attn: PROJECT MANAGER

27090 PAN AMERICAN FREEWAY NE

ALBUQUERQUE NM 87107

Lab Work Order#: L1815

Project P.O. #: PARAJITO @TWO MILE

Project Reference:

Comments:

/(" / /ij-APPROVEDBY: ~·~___/

Dave 6emo;:est

Project Manager

Enviro • Test

Date: 1 0 OCT 2000

Date Received: 29 AUG 2000

LABORATORIES LLC. 420 West Street Casper, Wyoming 8260.

Phone: (307) 235-5741 Fax:(307) 266-1676 Toll Free 1(800)666-030f


''"'"'Chemical Analysis Report

r~NNACLE LABORATORIES, INC \...."""' '090 PAN AMERICAN FREEWAY NE

ALBUQUERQUE NM 871 07 ATTN: PROJECT MANAGER

Mise

Strontium-90

Isotopic Uranium, Dissolved

Uranium-234 Uranium-235 Uranium-238

Isotopic Thorium, Dissolved


Isotopic Plutonium, Dissolved


·-otopic Americium, Curium, Dissolved

Americium-241 Curium-243/244

Gross Alpha/Beta, Dissolved


Gamma Spectroscopy, Dissolved

Actinium-228 Silver-110m Americium-241 Beryllium-7 Bismuth-212 Bismuth-214 Cerium-139 Cerium-144 Cobalt-56 Cobalt-57 Cobalt-58 Cobalt-60 Chromium-51 Cesium-134 Cesium-137 Europium-152 Europium-154 Europium-155 Iron-59

EILI ~~~lJ~~EI~~J. ~-• Phone: (307) 235-5741 Fax:(307) 266-1676

""'"""''"""'·'"""3 """""'· '""""""''""'J Toll Free 1 (800)666-030(

1.7+/- 0.6

0.87 +1- 0.45 <0.4 +1- 0.04 0.61 +1- 0.39

<0.3 +1- 0.1 1 +1- 0.5

<0.3 +1- 0.1

<0.05 +1- 0.06 0.02 +1- 0.02

1.9 +1- 0.7 <0.5 +1- 0.3

3.4+1- 1.4 18.3+/- 1.6

41.3+/-7.2 20.2 +1- 36.1

4.0 +1- 5.6 -11.2 +1- 14.6 32.0 +1- 23.1 115 +1- 30.8 -2.3 +1- 1.6

-1.2+/-10.5 -1.2 +/-1.7 -0.1 +1- 1.3 -0.8 +1- 1.6 -0.8 +1- 1.7

-0.6 +1- 17.1 -1.6 +/-1.9 -0.6 +1- 1.7 10.0 +1- 8.3 -0.6 +1- 2.8 2.0 +1- 3.9 -1.9 +1- 3.5

Report Date: 10-0CT-00

pCill

pCi/L pCi/L pCi/L

pCi/L pCill pCi/L

pCi/L pCi/L

pCi/L pCi/L

pCi/L pCi/L

pCi/L pCi/L pCi/L pCi/L pCi/L pCi/L pCi/L pCi/L pCi/L pCi/L pCi/L pCi/L pCi/L pCi/L pCi/L pCi/L pCi/L pCi/L pCi/L

Page: 2 of 4 PO No.: WO NO.: L1815

24-AUG-00 l1815-1

1.4

0.31 0.39 0.41

0.3 0.2 0.3

0.05 0.01

0.3 0.5

1.6 1.7

8.6 60.5 8.8 24

37.9 5.4 2.6 17.5 2.8 2.2 2.7 2.6 27 2.6 2.7 13.5 4.6 5.9 5.7

06-SEP-00 KLS

14-SEP-00 OMF 14-SEP-00 OMF 14-SEP-00 OMF

15-SEP-00 OMF 15-SEP-00 OMF 15-SEP-00 OMF.

20-SEP-00 PLJ 20-SEP-00 PLJ

22-SEP-00 OF 22-SEP-00 OF

12-SEP-00 KLS 12-SEP-00 KLS

01-SEP-00 OMF' 01-SEP-00 OMF I

01-SEP-00 OMF 01-SEP-00 OMF I 01-SEP-00 OMF 01-SEP-00 OMF 01-SEP-00 OMF 01-SEP-00 OMF 01-SEP-00 OMF 01-SEP-00 OMF 01-SEP-00 OMF 01-SEP-00 OMF 01-SEP-00 OMF' 01-SEP-00 OMF 01-SEP-00 OMF, 01-SEP-00 OMF 01-SEP-00 OMF' 01-SEP-00 OMF 01-SEP-00 OMF


""''""Chemical Analysis Report

,-~INNACLE LABORATORIES, INC ~· 090 PAN AMERICAN FREEWAY NE

ALBUQUERQUE NM 87107 ATTN: PROJECT MANAGER

NMHWB-008096 PARAJITO @ TWO MILE

Gamma Spectroscopy, Dissolved

lodine-131 Potassium-40 Manganese-54 Sodium-22 Niobium-94 Niobium-95 Protactinium-234m Lead-212 Lead-214 Ruthenium-106 Antimony-124 Antimony-125 Scandium-46 Strontium-85 Thorium-227 Thorium-234 Thallium-208 Uranium-235 Zinc-65

ElL.· Enviro • Test LABORATORIES LLC.

420 West Street Casper, Wyoming 8260' Phone: (307) 235·5741 Fax:(307) 266-1676

Toll Free 1(800)666-030€

Report Date: 10-0CT-00 Page: 3 of 4

PO No.: WO NO.: L1815

24-AUG-00

-0.2 +1- 3.5 pCi/L 5.9 01-SEP-00 1490 +1- 44.8 pCi/L 24.7 01-SEP-00 -1.1 +/-1.6 pCi/L 2.6 01-SEP-00 0.9+/-1.7 pCi/L 2.8 01-SEP-00 1.8 +1- 1.7 pCi/L 2.6 01-SEP-00 0.4 +1- 1.9 pCi/L 3.1 01-SEP-00

763 +1- 351 pCi/L 398 01-SEP-QO 18.2 +1- 3.6 pCi/L 3.6 01-SEP-00 49.7 +1- 4.8 pCi/L 5.6 01-SEP-00 342 +1- 17.5 pCi/L 11.1 01-SEP-00 -1.1 +/-2.2 pCi/L 2.9 01-SEP-00 3.7 +1- 4.5 pCi/L 7.5 01-SEP-00 DMF

17.3 +1- 3.1 pCi/L 3 01-SEP-00 DMF 14.2 +/-1.8 pCi/L 3 01-SEP-00 DMF -0.2 +1- 12.8 pCi/L 18.3 01-SEP-00 DMF 667 +1- 51.2 pCi/L 35.9 01-SEP-00 DMF 13.0 +1- 2.6 pCi/L 2.6 01-SEP-00 DMF 1

I 36.0 +I· 3.6 pCi/L 18.1 DMF \ 3.7 +1- 3.9 pCi/L DMF'

i ·- I


"""-" ETL Test Code

GAB-DIS-CA

GAMMA-ALL-DIS-CA

ISO-PU-DIS-CA

ISO-TH-DIS-CA

ISO-U-DIS-CA

SR90-DIS-CA

Matrix

Water

Water

Water

Water

Water

Water

WONO.: L1815

Methodology Reference PAGE 4 of 4

PARAJITO @ lWO MILE

Test Description Methodology Reference

Gross Alpha/Beta, Dissolved EPA 900.0

Gamma Spectroscopy, Dissolved EPA901.1

Isotopic Plutonium, Dissolved Maod.HASL 300

Isotopic Thorium, Dissolved Mod. HASL 300

Isotopic Uranium, Dissolved Mod. HASL 300

Strontium-90, Dissolved Mod. EPA 905.0

Enviro • Test , LABORATORIES LLC. Limit of Liability: Although care and due diligence is taken in the performance of our services, our liability in all cases is


QA

LC1PU0925

L 1826-001

Sample Activity

0.051

L 1815-001 Sample Activity -0.047

0.016

MBAPU0831 PU239

WORKGROUP#

RUN ID#

Standard Known Value 0.625

Spiked Sample Activity 1.048

PU238 Duplicate Activity 0.029

PU239 0.017

= -0.0104 = 0.008595

WG- 7!.20

!<. ~71/

ISO-PU

LCS Sample Value 0.590

Standard Value 0.625

Sample ERROR 0.062

0.019

WORK ORDER# L 1815 -------L1826

PARAJITO @ TWO MILE

10/2/2000 pCi/L

17:17:00

LCS Recovery

94.3%

Sample Spike SPIKE Volume Value RECOVERY 0.500 1.25 79.8%

Duplicate Duplicate ERROR RER 0.079 0.76

0.034 0.02

EJLI Enviro • Test f LABORATORIES LLC. Limit of Liability: Although care and due diligence is taken in the performance of our services, our liabilily in all cases is


"-ENVIRO-TEST QC REPORT"''"''•, Page 1 of 3 PARAJITO @ TWO MILE

Workorder #: L1815

{,':·ype: BLANK

Lab QC Number:

WG7031-2 SR90-CA

WG7063-3 GROSSAB-CA

WG7063-4 GROSSAB-CA

WG7120-2

Strontium-90

Gross Alpha

Gross Beta

Gross Alpha

Gross Beta

ISO-PU-ALPHA-CA Plutonium-238

Plutonium-239/40

WG7121-3 ISO-TH-ALPHA-CA Thorium-228

Thorium-230 Thorium-232

WG7131-3 ISO-U-CA Uranium-238

WG7209-1 1-CM-CA Americium-241

Curium-243/244

QCType: DUP

Lab QC Number:

WG7120-1

ISO-PU-DIS-CA Plutonium-238

Plutonium-239/40

WG7121-1

ISO-TH-DIS-CA Thorium-228

Thorium-230

Thorium-232

WG7131-1

ISO-U-DIS-CA Uranium-234

Uranium-235

Uranium-238

WG7209-2

ISO-AM-DIS-CA Americium-241

Curium-243/244

ElL- Enviro • Test LABORATORIES LLC.

Result Qualifier Units Limit Analyzed

<0.9+1- 0.4 pCi/L 0.9 06-SEP-00

<0.5+1- 0.3 pCi/L 0.5 12-SEP-00 3+/- 0.9 pCi!L 1.4 12-SEP-00

<0.6+1- 0.3 pCi/L 0.6 12-SEP-00 <2+/- 0.9 pCi!L 1.5 12-SEP·OO

<0.03 +1- 0. pCi/L 0.03 20-SEP-00 <0.03 +1- 0. pCi/L 0.03 20-SEP-00

<0.1 +1- 0.1 pCi/L 0.1 15-SEP-00 0.2 +1- 0.1 pCi/L 0.1 15-SEP-00 <0.1 +1- 0.1 pCi!L 0.1 15-SEP-00

<0.020 +1- ( pCi/L 0.02 14-SEP-00

0.3 +1- 0.1 pCi/L 0.1 22-SEP-00 <0.1 +1- 0.1 pCi/L 0.1 22-SEP-00

RPD Qualifier Limit% Analyzed

N/A RPD-NA 0-20 20-SEP-00 0 0-20 20-SEP-00

N/A RPD-NA 0-20 15-SEP-00 9.5 RPD-NA 0-20 15-SEP-00 N/A RPD-NA 0-20 15-SEP-00

25 0-20 14-SEP-00 N/A RPD-NA 0-20 14-SEP-00 48 RPD-NA 0-20 14-SEP-00

30 0-20 22-SEP-00 67 RPD-NA 0-20 22-SEP-00


... '·ENVIRO-TEST QC REPORT Page 2 of 3


~-·ype: LCS

Lab QC Number: WG7031-4

SR90-CA

WG7063-6

GROSSAB-CA

WG7063-7

GROSSAB-CA

WG7120-4

ISO-PU-ALPHA-CA

WG7121-4

ISO-TH-ALPHA-CA

WG7131-4

ISO-U-CA

WG7209-4

AM-CM-CA

QpType: MS -\

'~"" Lab QC Number: WG7031-3

SR90-CA

WG7063-5

GROSSAB-CA

WG7120-3

ISO-PU-ALPHA-CA

WG7121-2

ISO-TH-ALPHA-CA

WG7131-2

ISO-U-CA

WG7209-5

I AM-CM-CA

Strontium-90



Plutonium-239/40

Thorium-230

Uranium-238

Americium-241

Strontium-90

Gross Alpha

Gross Beta

Plutonium-239/40

Thorium-230

Uranium-238

Americium-241

ElL Enviro • Test LABORATORIES LLC.


110 75-125 06-SEP-00

81 75-125 12-SEP-00 N/A 75-125 12-SEP-00

N/A 75-125 12-SEP-00 122 75-125 12-SEP-00

94.3 75-125 20-SEP-00

91 75-175 15-SEP-00

107 75-125 14-SEP-00

102 75-125 22-SEP-00


104 75-125 06-SEP-00

N/A 70-125 12-SEP-00 112 70-125 12-SEP-00

79.8 75-125 20-SEP-00

96 75-125 15-SEP-00

94 75-125 14-SEP-00

95 75-125 22-SEP-00


~end:

Qualifier:

RPD-NA A B

D E F G

QCType

BLANK

BS

BSD

CCB

CCC

CCV

DUP

ICB

ICV

INST BLK

LCS

LCSD

MS

MSD

SPCC

SRM

sss

"ENVIRO-TEST QC REPORT Workorder #:

Description

Laboratory Blank

Blank Spike

Blank Spike Duplicate

Continuing Calibration Blank

Continuing Calibration Check

Cont. Cal. Verification

Duplicate

Instrument Blank

L1815

lnstument Calibration Verification

Instrument Blank

Laboratory Control Spike

Lab Control Spike Duplicate

Matrix Spike

Matrix Spike Duplicate

System Performance Check Compound

Standard Reference Material

Second source std

Relative Percent Difference Not Available due to result(s) being less than detection limit. Method blank exceeds detection limit. Blank correction applied, where appropriate. Method blank result exceeds detection limit, however, it is less that 5% of sample concentration. Blank correction not applied.

Page 3 of 3

PARAJITO @ lWO MILE

Method blank result exceeds detection limit, however, it is less than 5% of the regulatory limit for the analyte of interest. Blank correction not applied. Duplicate result exceeds limit due to increased variability for low level samples. Matrix spike limit exceeded due to high sample background. Silver recovery low, likely due to elevated choride levels in sample. Outlier - No assignable cause for nonconformity has been determined.

ElL , Enviro • Test • LABORATORIES LLC. Limit of Liability: Although care and due diligence is taken in the performance of our services, our liability in all cases is


Job Number

Sa111pk lZcccipt Cllccldi~t

Lf~IS

Samples ShippcJ - Federal Express Other:

Samples I lanJ Delivered Client ETL Lao Courier Other:

AirDillfl: {2-'t7& 11P~D\Cf3 II of Packages Received: f ..

Yes No N\A Comments I. Chain- of- Custody present? t/ If no, please fill one oul. 2. Arc the COC and sample labels legible? I._../'

.., Custody Seal on shipping container? <./

.).

If yes, intact on shipping container? /

4. Custody seals on sample containers? v

If yes, intact on sample container? /

5. Samples chilled? ./

Is temperature of cooler: 4 ± 2°C ? / c/ ~111'/ji/=~ Record temp: rrr -v t l./. & coL G. Samples received intact (good condition)? t_../'"

~ If volatiles required, any with hcadspace? ~

Adequate sample \'Olumc provided? / v-7.

s. Samples preserved correctly? ..__.....- Na2S203, Zn.Ac,@Oj)llCI Circle prcscrYative types in shipmenl l-I2SO.:, NaOH, Other

9. Correct containers used? v I 10. Samples received within holding time? (/ I 11. Agreement betwecu COC a!lll sample labels?

. ._/ _j 12. Gamma ScJcenrnR/Hr@ sut face within !3kg7 / I AclditionaiCommenls: NottJ ~vv--;Aj i ~.~ f.dnJQ 3

SanlplcCoillaiilcr(size/nlalcriai):.~~~~-~~~L~~~· ~~~~~b~;~~~;~~~~~~~~~~~~~~~~~ Received and inspected by: (L · Datcn·imc: 1/.g.c;~ /4o tJ --;+~~~~--~~~---

QO Wesl Firs! Slreel Casper, Wyoming B2601 Phone: {307) 235·5741 Fax: (307) 266-1676

Toll Free 1 (000)6fi6·0306

Lab Client SMP# Sample Number L 1826-1 NMHWB

Water S AM-CM-CA

Water s GAMMA-ALL-CA

Water s GROSSAB-CA

Water s ISO-PU-ALPHA-CA

Water s ISO-TH-ALPHA-CA

Water s ISO-U-CA

Water s SR90-CA

ENVIRO-TEST LABORATORIES LLC.

Login Chain of Custody Report (ln01) Aug. 31, 2000

01:20PM

Login Number: L 1826 Quote Number: Account: 10185 PINNACLE LABORATORIES, INC

Project: PARAJITO @TWO MILE

Collect Receive Due Date Date PR Date Comments

24-AUG-00 00:00 29-AUG-00 18-SEP-00

Hold: 20-FEB-01

Hold: 20-FEB-01

Hold: 20-FEB-01

Hold: 20-FEB-01

Hold: 20-FEB-01

Hold: 20-FEB-01

Hold: 20-FEB-01

Signature: Q~qs f'~ Date : '8- 3.1 • co

~ Pi( ~cle Laboratories, Inc. lnterlatf !lain of Custody oat., r;)zg I /

Page: __ of 7 • ~ ... -. - ..._, Network Project Manager: Jacinta A. Tenorio .. ~ ANALYSIS REQUEST

I

Pinnacle Laboratories, Inc. I~ I~ ~ .

V'\ 2709-D Pan American Freeway, NE ~~ - ~

I~ 0 C/)

iES <0 - ~ N Albuquerque, New Mexico 87107 ~

N co 0 (.) co 0 C>

... t5CJ5) 344-3777 Fax (505) 344-4413 ct :::s:: - ~ \)-- ~..s: ~ C/)

~ ~ C/)

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SAMPLE ID DATE TIME MATRIX LAB ID ::E 0:: ::E ::E Q: (!) CD (.) a.. J: a.. CIO ~-=- ::::> (!) 1- z i aJJtJCffd -o1 8/24 ~ )fGj i I~ ~ ~X IX X I I ..

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QC LEVEL: ("""S'''iD IV Received Intact? STL-CT ~~N;;u Tf¥trv/f;gjoo Printed Name: Date: c m- REQUIREQ;:)_ MS MSD BLANK Received Good Cond./Cold ATEL-AZ. TAT(""' S_TANDAR[D RUSH!! LAB NUMBER: ATEL- MARION Pinnacle Laboratories, Inc. I

. Company , ATEL- MELMORE RECEIVED BY: ·· 1. RECEIVED BY: 2 DUE DATE: ~IlK COMMENTS: BARRINGEI~ signatuZ .J/J T1me: Signatue: Time: I

RUSH SURCHARGE: -- WCAS AI. · , 1/JDO I CLIENT DISCOUNT: - WOHL Printed Name: ~ Date:tj/~ i It Printed Name: Date: SPECIAL CERTI~N f11vt'ro 7e.sr ~ LIJ..{O,t; ;-sh ~qtfj REQUIRED: YE N Company . C:Ompany

-- --------

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' ~ ()l...(l.• ~ ~ Ll)?~~

I

i Pinnacle Labo111tories. Inc. lnter1ab Chain of Custody Date: 8/25/2000 Page: 1 of 1

r'!r A Network Project Manager: Kimberly D. McNeill ANALYSIS REQUEST

;:~·v P.li!~~rlzeCibviAttn: .lo11ir~otn9 ·. -_-.:rom Pinnacle Laboratories, Inc. CUENT: NMED HWB

2709-D Pan American Freeway, NE .. ADDRESS: %04CA Gallstoo St. Albuquerque, New Mexico 87107 ~ t

CITY, STATE, ZIP: Sant. Fe NM, 87505 505) 344-3777 Fax 505) 344-4413 {505) 827-1518 ext.,: 038 Fox {505)127-1544 I

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PROJECT INFORMA liON

PROJECT#: HWB 8.24.00 CG ( Relenqulshed bv:

Signature:

PROJ. NAME: LANL Paiarito 2-mile Printed Name:

OC LEVEL: STD. Company:

MSD BLANK Time: Date:

Signature: SlgnabJre:

RUSH SURCHARGE: •2 COOLERS •Total and Dissolved for Rad Samples •svocs and Dioxins/Furans only if enough sample is available tor proper I Printed Name: I Printed Name:tl, f\4 1 :I 1 A-"tt' 1 \ {' 1 '1.-v"'.-- b

cuENT DISCOUNT: lab QA/QC •No filtered CN- sample, reflect on invoice Company: Company;

SPECIAL CERliFICAliON Time: Date:

REQUIRED: YES NO

,. albuquerque, new mexico 87107 phone (505) 344-3777 fax ... alamos national labs/ta...

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